A Field Test for Gold

THE prospecter and geologist in the field, in the search for gold, are very often faced with a real difficulty. The: mineralized rock _frequently contains gold which is so finely divided or associated with sulphides that it is not recognizable in the gold pan. In recent years, the practice has been to take samples, send them to an assay office, and sit down and wait for results. This paper describes a method of solving the difficulty of proving the presence of this fine gold. The investigation is still in an experimental stage; but certain results have been obtained which would seem to justify publication. We do not consider that the method outlined is quantitative, but we believe that qualitative results are assured. The procedure has the great merit of simplicity. A sample of approximately two pounds of the mineralized rock should be taken and powdered as fine as is practicable. This powder is theo panned and the heavy minerals concentrated. Approximately two grams of these concentrates are taken for the test (one gram can be roughly gauged in the field by heaping up the powder on a Canadian twenty-five cent piece). The material is placed in a test-tube and 6 c.c. of a 10 per cent solution of iodine in alcohol are added (one-third of a test-tube full is approximately equal to 6 c.c.). Heat gently for about ten minutes over a spirit lamp, but without actual boiling. Allow to stand undisturbed until the sediment has settled to the bottom. Remove the clear iodine solution with an eye dropper. Allow it to fall, drop after drop, on a warmed pyrex watch-glass (the drops should be of equal size), taking care that the successive drops fall in the same place and that each drop evaporates before the next drop falls. Heat is applied to the lower side of the watch-glass by means of a spirit lamp. If gold is present in amounts of $2.00 or more per ton, a gold mirror will be formed on the watch-glass. This process of dropping and evaporating should be continued until no clear solution remains. If no mirror has appeared when all the solution has been used, another 6 c.c. of the iodine solution should be added to the powder and the process repeated. The absence of a mirror after the double treatment denotes an amount of gold less than two dollars per ton at the present price, or that the ore contains no gold. The mirror obtained must be washed with nitric acid ( 1: 1) to remove any copper, silver, lead, zinc, and iron. The yellow mirror remaining is pure gold.