Power And Operating Behavior In Stirred Media Mills

While applications of stirred media mills for fine particle production have continued to increase, there is a lack of understanding of operating behavior and power requirement. Investigations in laboratory stirred media mills have been carried out with grinding media, limestone and yttria stabilized zirconia. The torque required to rotate impellers immersed in dense particulate media with supernatant versus impeller rotational speed displays four regions marked by sharp transitions: transition from static to dynamic friction; channel- ling; dispersing; and centrifuging. Equations, including dimension- less group correlations of power and modified Reynolds number, for relating power, speed, impeller and tank dimensions and design, media size and density, solid concentration, and other relevant variables have been established. Scale-up guidelines with respect to power consumption are also proposed. The best operating conditions for grinding limestone in the laboratory stirred media mill have been identified. Complexation by the polymer during ultrafine grinding of zirconia has been found to cause extraction of yttrium into solution with possibly significant changes in the surface chemical composition of the product.