RI 8103 Nitride Intermediates in the Preparation of Columbium, Vanadium, and Tantalum Metals (In Two Parts) 2. Thermal Decomposition of the Nitrides

The National Institute for Occupational Safety and Health (NIOSH)
R. A. Guidotti
Organization:
The National Institute for Occupational Safety and Health (NIOSH)
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18
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4321 KB
Publication Date:
Jan 1, 1976

Abstract

The Federal Bureau of Mines studied the thermal decomposition of the nitrides of the Group V A metals (CbN, Ta3N5, and VN) with the goal of preparing high-purity metals. Solid-state purification and arc and electron-beam melting were examined. Electron-beam melting proved to be the most efficient means of nitrogen and oxygen removal. Columbium and tantalum of 99.9-pct purity were prepared by this technique; in the case of vanadium, however, nitrogen could not be reduced below the solid-solution level.
Citation

APA: R. A. Guidotti  (1976)  RI 8103 Nitride Intermediates in the Preparation of Columbium, Vanadium, and Tantalum Metals (In Two Parts) 2. Thermal Decomposition of the Nitrides

MLA: R. A. Guidotti RI 8103 Nitride Intermediates in the Preparation of Columbium, Vanadium, and Tantalum Metals (In Two Parts) 2. Thermal Decomposition of the Nitrides. The National Institute for Occupational Safety and Health (NIOSH), 1976.

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