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By Rudolf Lesch

Till date, coke has been produced mainly from coals with a content of volatile matters in the range of 20% to 28% and good coking properties. If such so-called "selfcoking" coals are available, blast furnace coke or foundry coke with the required quality characteristics can be produced in top-charged horizontal ovens. In this case, the possibility of using high-volatile coals and in particular coals with low-caking properties is very restricted. Even if high-volatile coking coals have good coking properties, coke produced from such coal alone will not meet the requirements in terms of coke strength. The mechanical coke properties are influenced by the charge coal blend and the coking conditions. In this context, the bulk density of the oven charge is a decisive factor. Research and development in the field of coke production in horizontal chamber ovens aims at improving the specific oven throughput, increasing the raw material basis and introducing environmental protection technologies. The key factor, however, is to guarantee and further improve the rentability of the coke production. It is very important to reduce the cost of the charge coal to a minimum at the same time maintaining or even improving the coke quality.

Aug 17, 2017

By Lidong Teng

ArcSaveTM is a new generation of electromagnetic stirrer (EMS) from ABB for electric arc furnace (EAF) operation. Its goal is to improve the safety, increase the productivity and reduce costs. Electromagnetic stirring in the melt bath during arc furnace operation will affect the scrap smelting, bath temperature distribution, refining reactions, and also the tapping practice. This paper has summarized the investigation results obtained from the first ArcSaveTM system installed in a 90 ton EBT arc furnace in USA. The hot test results show that ArcSaveTM has enhanced the heat and mass transfer in the arc furnace process. This results in a faster scrap melting rate, lower slag superheat during arcing, more homogenous melt bath, higher decarburization rate and higher EBT free opening frequency. ArcSaveTM has also reduced the tapping temperature and tapping oxygen in the steel. This brings a higher scrap yield and saves ferroalloy consumption in the downstream ladle furnace operation. The lower energy consumption, short tap-to-tap time, and consistent furnace operation bring increased productivity and safety.

Aug 16, 2017

By José Francisco Cabello Russo, Késsius Bortolan Menezes, Henrique Dias Gatti Turrer, Denílson Rodrigues de Araújo

With the start-up of the Minas-Rio system, Anglo American, in Conceição do Mato Dentro, MG, in 2014, a methodology was also implemented and certified to perform the tests to obtain the results of TML (Transportable Moisture Limit). Such a parameter provides the maximum moisture content contained in the material that could be transported without the risk of the cargo liquefaction process, which could lead to incidents such as the tipping of ships carrying iron ore concentrate in bulk on the deep water. This means that when loading a ship, the moisture content of the material to be transported should not be higher than the TML reference value, obtained in a physical test and intrinsic to the material. Should this occur the charging may be rejected. From 2014 a downward trend was observed for this reference parameter in the Minas-Rio system, with results approaching the moisture of the filtered product, bringing risks to the operation of the project. In this way, an investigation of the possible causes for understanding this downward trend was required.

Oct 3, 2019

By Andreas Rohrhofer

Reliable high end automation and process optimization systems are main factors for excellent product quality, safe operation and maximized plant performance in the steel industry and its designated environmental plants. Primetals Technologies introduces new automation packages for consequent safe and cost efficient production. Many areas within the steelplant interested to be monitored and measured automatically are not implemented in the automation system due to limited access or technical reasons. A wireless, self-organizing network facilitates wide ranging data transmission in previously inaccessible areas and opens up a wide range of new opportunities. With Fluid Guard a system to detect leakages with highest accuracy and reacts properly for all kind of water cooled circuits is available, improving the safety in steelmaking process. Lance Guard can be utilized for all fully automatic and semi-automatic lance appliances, but is especially suitable for the products of Primetals Sublance Standard/2.0 and LiquiRob applications, since these systems make seamless integration particularly simple. Manual lance appliances may also be tested and diagnosed. Environmental plants have become a main part in steelmaking plants. Highest performance in combination with optimized energy consumption is the main target in Primetals Technologies’ innovations in automation optimization packages for dedusting systems. A new approach for preventive maintenance and operator assistance is introduced with the Acoustic Expert System. In combination with the new Ask cloud based system, Primetals enables a 24/7 monitoring and a whole lifetime observation of any equipment within a steelplant. Furthermore it is now enabled to check the condition of the plant at a fingertip at any time.

Aug 17, 2017

By Francisco Morganti

This report gives in the first part the metallurgical basics for the production of AHSS grades in integrated steel plants starting at the melt shop and ending at the annealing lines of the cold mill. The corresponding process and plant technologies in each production step with its specifics and rules are explained. In the second part by way of example the practical requirements for TRIP 780 steel grade are highlighted like a recipe for process control in the steel plant, hot and cold rolling mill, annealing line and finally skin pass mill. Measuring of mechanical technological properties on samples shows that the specifications according to DIN EN 10268 are fulfilled.

Oct 30, 2017

By Samuel F. Rodrigues, Clodualdo Aranas Jr., Fulvio Siciliano

The application of thermo-mechanical control processing (TMCP) in hot rolling of steels has become a common routine since the last 60 years. The understanding of the physical metallurgy behind TMCP played a major role in the early developments. Physical and numerical simulation works are performed firstly to derive the fundamental metallurgical knowledge and secondly to conceive existing TMCP practices. In this paper, a summary TMCP techniques is presented. The occurrence of dynamic transformation of ferrite in the austenite region is shown by means of synchrotron light diffraction methods. This phase transformation mechanism is taken into consideration and its effects on TMCP are proposed in an exploratory way.

Oct 1, 2019

By Priscilla Pessin Coppo

The prevention of dental enamel wear has particular relevance for preventive and restorative purposes in dentistry. The wear damage can increase due to salivary disorders and/or parafunction (bruxism); antagonists incisal surfaces become flat and coincident. This study aims to investigate the wear behavior and the related mechanisms in sliding pairs of conformal incisal enamel, with similar values of hardness and fracture toughness, with different applied normal loads and lubricated conditions. Bovine incisors, under pin on flat configuration, were tested in two lubrication condition (dry or with natural saliva) and two applied normal loads (8 and 16 N). The worn surfaces were investigated by 3D profilometry and SEM. The analysis of worn surfaces indicated mechanisms of brittle fracture, but with different severities. Under a normal load of 16 N and dry condition, wear is controlled by a brittle process: microcracking with flake-like wear particles, which results in high friction coefficient (> 0.85), wear rate and wear volume. On the other hand, under a normal load of 8 N and natural saliva, wear took place in the interprismatic region, with consequent exposure of prisms and fracture in localized regions. In this case, the friction coefficient was 16% lower and the wear volume was one order of magnitude lower. Under 8 N and natural saliva, the wear was greater than in the dry condition, probably due to tribochemical reactions.

Jul 31, 2018

By Beatriz Pereda, Ana Clara Fonseca da Silva, Tiago Seixas Bittencourt

Reinforcing steel bars are usually specified based on mechanical properties with flexibility in chemical composition and processing. Most developments, in these steels, are normally focused on alloy and process design to reach minimum cost and conformity to specification. Processing routes using quenching and self-tempering (QST) and accelerated cooling are the most common. Microalloying with V and Nb have been used in rebar. When acicular constituents must be avoided, a combination of Nb microalloying with judicious control of cooling is one of the preferred options. Niobium can contribute to improvement in tensile properties through austenitic grain size control during hot working, precipitation hardening due to carbonitrides or clusters, and hardenability increase. In the present work the alloy design and development processes of a Nb microalloyed steel for rebars are presented. The designed steel has fulfilled the required specification and is under regular production. Austenitic grain size refining – when comparing with the “basic composition” normally used was observed, even without any change in the thermomechanical processing cycle. There are indications that precipitation hardening may also occur. Results indicate that Nb is a good alternative as a microalloying element in rebars.

Oct 1, 2019

By Masakazu Iida

In this article, technologies of unburned Al2O3-MgO (UAM) refractories are demonstrated in terms of microstructure evolution. During operation, Mg2+ diffuses from MgO to Al2O3 through the liquid phase to form spinel (MgAl2O4) network. Molten slag tends to penetrate along the voids in the spinel network structure and spinel dissolves in the penetrated slag. Therefore, maintaining a high degree of spinel saturation in the penetrated molten slag is important. In order to achieve the condition described above, suppression of overall mass transfer through penetrated slag is effective. This is achievable by evolution of complicated spinel network structure with small pore diameter, which increases the flow resistance of molten slag. Thus, optimization of refractory composition and fabricating conditions, with the aim of creating on improved spinel network, is essential. The effectiveness of spinel network improvement was validated by commercial applications. According to the investigation of UAM brick after use, further densification due to heating under restrained conditions was recognized. Hence, it was concluded that the evolution of the spinel network structure in UAM refractories is essential technology needed to improve durability.

Oct 30, 2017

By Raquel Húngaro Costa, Jonathan Tenório Vinhal

The demand for natural resources has grown over the years, however, the environment offers a limited amount of these resources for exploration. Then, the investigation of new methods for recovering and reuse some compounds and elements are essential to know later tailings purposes. Zinc is used in corrosion resistance as a protective coating for several products. One of the steps for the extraction of zinc is by flotation process to obtain the concentrated ore, in which a residue is generated. The aim is to characterize this residue, allowing the choice of recovery routes for compounds and elements in future stages. The methods of analysis were Malvern, VA, Eltra and ICP-OES, besides the water content. In this study, a characterization of elemental chemical analysis was performed, in which the main elements presented were: calcium (17.4%), magnesium (10.3%) and iron (7.97%); the water content was 27% and the grain size of the material presented an average size of 50μm. With the presented characteristics the material can be used, after treatment, in the recovery of other compounds for applications in the sector of fertilizers, ceramics and steel industry.

Oct 3, 2019

By Luis Henrique Torres Dantas, Maycon Athayde, Rossano Augusto Pilon Nunes

The objective of this work is to evaluate the physical quality achieved in the iron ore pellets and the temperature profile in the pellet bed by applying an inversion in the flow during the cooling. The firing of pellets requires a minimum residence time in the sintering temperatures of the hematite grains [1]. The applied concept aims at raising this time to pellets located at the bottom of the bed which would provide an improvement in the physical quality of the product. The tests were carried out in a pot-grate type oven and the samples of fired pellets were divided into three aliquots according to the loading position of the pot termed top, middle and bottom, the pellets were sieved and subjected to physical tests and the compared to conventional indurating flow with the same ores and inputs. It was possible to show an increase of 7 to 8% in the compressive strength of the medium and bottom layers, maintaining the top layer results. The objectives of the research were achieved and the tests will be extended to assess the impacts on the mass and energy balance of the indurating machine and its components.

Oct 1, 2019

By J. Bas A. F. Smeulders

Traditional laboratory lubrication tests, including those for cold rolling lubricants often involve measurement of neat oils. To achieve increased levels of test severity, such tests are often carried out at high temperatures and prolonged durations. However, we found that the levels of lubricant degradation and wear in these tests can be much higher than in the field. Moreover, steel rolling is not done with neat oils, but with emulsions, where the presence of water influences film formation, surface chemistry and oil composition in the roll bite. To better approach the situation in the field, and thus to be able to develop rolling oils with improved lubrication performance, several lubrication tests were developed for emulsions: direct measurement of film formation and measurement of Stribeck curves, in which the emulsions can be assessed in terms of their boundary lubrication and elastohydrodynamic behaviour. The key innovation is that also another test method was developed, which focuses on boundary lubrication and wear, and the role of extreme pressure and anti-wear additives. Realistic levels of test severity are achieved in the tribometer by mimicking frictional power intensities and flash temperatures for typical cold rolling or tinplate mills. Test conditions can be adapted according to the mill stand or pass number and other cold rolling process parameters. The emulsions are kept at normal operational temperature. Clear differences could be observed between emulsions of various concentration and composition. The viability of the method is illustrated by a number of field cases, in which a good correlation is demonstrated between the laboratory tests and the performance in a pilot or production mill.

Jul 30, 2018

By Zhi Zhang

The ever increasing demand of high performance rolls in the late finishing stands (F5 – F7) for hot strip mills (HSM) requires better product solutions from roll suppliers. Roll development activities never stop at Union Electric Åkers (UEÅ) in order to meet the requirement. The HYBRID STEEL, a new concept of roll materials especially for the late finishing stands in the HSM, is successfully developed in UEÅ. This paper reviewed the development of previous ICDP as well as enhanced ICDP (eICDP) roll materials, and, the novel HYBRID STEEL roll grade. Rolls manufactured by this new grade have been used in several European mills. A significant improvement over the enhanced ICDP rolls has been observed.

Oct 30, 2017

By Pedro Jorge Walburga Keglevich de Buzin

The steel production in mini mills generates several process residues, among them there is the electric arc furnace dust (EAFD). This residue has as main elements Fe, O, and Zn, being classified as hazardous by the presence of Pb and Cd. Thermodynamic studies related to the formation of mineral species containing Fe, O and Zn elements were carried on due to the influence of these compounds in hydrometallurgical EAFD recycling processes. In recent years, a rise in the chlorine content of this residue was observed, mainly motivated by the increased use of scrap with polymeric impurities containing this element. In this work, based on computational thermodynamics tool FactSage, a general overview of gaseous and minerals species (found in EAFD) formed by Fe, Zn, O, Cl, H and C is shown – representing the organic origin of chlorine. For this study, the PVC polymer was used as the chlorine carrier substance which contaminates the EAF load.

Jul 30, 2018

By José Hamilton Resende Tavares, Késsius Bortolan Menezes, Mariana Vieira de Moura

Sampling and its representativeness is of significant importance in process control and decision making in the mineral sector. In this way, the present work seeks to compare different methodologies for the sampling of the iron ore from Anglo American. Through a sample of 120 kg, representing the industrial flotation circuit feed, samples obtained by the method of long pile, random sampling and rotary sample divider were analyzed, being the latter adopted by the company. In this case, after sampling, the material obtained through each method was subjected to the same sequence of characterization tests and the difference between the results statistically analyzed. Through such analysis it was observed that the random sampling method showed high values of variability and is therefore considered as unsatisfactory when compared to the other methods tested. In addition, rotary sample divider also showed parameters slightly superior to the long pile method. This study confirms the importance of appropriate sampling systems and procedures systems in the pursuit of reliable results.

Oct 3, 2019

By Michel Rodrigo Luiz, Glaucio Augusto Polini, Leonardo de Souza Melo, Giovani Rodrigues, Giardini F. Lazzarin

ArcelorMittal's pickling and cold rolling line has been demanded to increase production since the installation of equipment in 2015. In addition to improving productivity related to these new equipment, several additional jobs were planned and executed on equipment already installed has been carried out in order to improve the efficiency of the line. The present work exposes what was done in the scale breaker (tension leveler) to improve the availability results of the section and consequently of the line.

Oct 1, 2019

By Günther Staudinger

Aperam is a global player in producing of stainless, electrical and special steel qualities. The steelmaking plant in Timoteo Brasil is equipped with one AODconverter for stainless steel and one MRPL-converter for special steel production. The MRP-L converter is almost in operation for 20 years. In order to improve production Aperam decided to install a new converter with increased reaction volume equipped with DANIELI state of art technology. This paper describes the major changes and improvements of the new converter installation.

Aug 16, 2017

By Priscila Tavares de Paula, Márcia Mika Saito, Henrique Gonçalves Teixeira, Felicio de Freitas Simoões

In this paper a sample of the apatite flotation from Cajati-SP was studied. Four alternatives of depressants were analyzed: corn starch, cassava starch, sodium hexametaphosphate with corn starch and sodium silicate with corn starch. The cassava starch had a gain of 7.5% in the metallurgical recovery and a collector consumption 13.8% greater than corn starch. Alternatives with hexametaphosphate and silicate sodium had a loss of 6.7% and 7.8% in recovery respectively in comparison with corn starch.

Oct 3, 2019

By Constantino Capurro

For certain applications, coarse titanium nitride (TiN) precipitates can be deleterious for the final properties of the material. Hence, in order to better understand the mechanisms involved in the generation of these precipitates, a thorough characterization of the particles observed in steels with different titanium and nitrogen content was carried out. Samples from liquid steel (tundish), continuous casting billets and final product were evaluated using an Automatic Particle Analyzer (APA) coupled to a Scanning Electronic Microscope (SEM). The location, frequency, size distribution and composition of the different particles observed were assessed. While only few TiN precipitates were observed in liquid steel samples, the density of this type of particle significantly increased in the continuous casting billets samples. Particles ranging from 1 to 10 µm were mainly found in the interdendritic zones of the as-cast structure. The density of TiN particles observed in these samples did not change after re-heating and rolling operations. A model to predict TiN precipitation during solidification was developed. A reasonable agreement was found between model results and measured data. Results of this analysis confirmed that the precipitated fraction of TiN increases as the product of steel Ti and N contents rises.

Oct 30, 2017

By Cesar Santos, Marcelo Duarte Silva, Ediron Antônio Lage, Fábio Silva dos Santos

Ceramic filtration technology, despite consuming about 90% less energy than conventional vacuum filters and producing clean water ready for reuse, faced a big challenge that put in doubt its technical and economic viability. In 2015, the production of pellet feed in this last stage of the process of the Minas-Rio Complex of Anglo American was impacted by deep fillings in the filter medium. The chemical regeneration process indicated by the filter manufacturers did not have the necessary effect. SUEZ then carried out a research work on the potential causes and indicated specialty chemicals. After an intense work of the Anglo American technical team supported by SUEZ, an efficient regeneration methodology was developed. From this reference, SUEZ received another 03 similar challenges with ceramic filters. Among them, the Herculano Mineração Dry Stacking pioneer project, which until 2017 could not process more than 20% of the tailings generated in the pellet feed concentration process. Following adaptations in the regenerative methodology as a function of the mineral characteristics facilitated by the development of a pilot backwash system, success was achieved, providing a condition for production of 3.0Mtpy without the use of tailings dam and with continued decline in the unit cost of the tailings filtration operation.

Oct 3, 2019