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By Rogério Felício dos Santos

Nitriding of metallic materials using electric discharges generated during electric discharge machining (EDM) is a recently developed technique. The aim of this paper was to correlate mechanical properties of a nitrided layer produced in AISI 4140 steel by EDM nitriding with the type and amount of nitrides. A conventional die-sinking EDM equipment and electrolytic copper electrodes were used to generate the electric discharges. The electrolyte was a solution of urea in deionized water. Knoop microhardness profiles assessed the variation of hardness along the nitrided layer, whereas the elastic modulus of this layer was measured using nanoindentation tests. Optical microscopy and X-ray diffraction (XRD) were used to characterize the nitrided surface. The results showed the formation of a nitrided layer containing iron nitrides with average thickness of around 25 µm. The amount of nitrides reduced from the surface towards the centre and these results correlated well with microhardness profiles obtained.

Jul 31, 2018

By Edo Engel

Blast furnace No. 3 at Zaporizhstal in Zaporozhye is rebuilt in 2016-2017. The Ukrainian company is targeting increased production and availability, mainly through the use of new technology. Zaporizhstal awarded a contract for a new Top Charging Unit to Danieli Corus, after comparing all available technologies. Reliability of the chosen charging device is pivotal, since long outages may be required for maintenance/replacement jobs, which strongly affects the availability of the blast furnace. This article describes the Top Charging Unit including DANCU (Danieli Charging Unit) - a robust hydraulic system. The main focus employed by Danieli and Danieli Corus during the development of this system has been availability and maintainability of equipment. This chute type charging unit has only few major moving parts, none of which is complex or vulnerable. The article also describes the main challenges of the project at Zaporizhstal, such as the use of hot sinter.

Oct 30, 2017

By Francesco Toschi

The Special Bar Quality family comprises a wide range of steel grades, mainly requested by the automotive, energy and engineering sectors, for applications where significant performances are required (eg. stresses, temperatures, working cycles, etc.). To meet these requirements it is necessary to reach a precise control of both the mechanical characteristics and metallurgy structures along the whole production chain. For semi-product with large dimensions, such as equivalent diameters around 300 mm, this is traditionally obtained through a manufacturing route which comprises the casting in ingots followed by reheating, forging and rolling. After 2010, new processes were investigated and technologies developed to replace the ingot route with a continuous casting followed by controlled high-reduction rolling. In these processes a seamless integration of CCM with rolling is implemented so to obtain the precise control of material flow, applied deformation and working temperatures. By using the proper combination of rolling diameter, speed and applied reduction, a very good control of the metallurgy structure across the whole section can be obtained, so to also remove the internal discontinuities ("voids") generated during the continuous casting. These processes, which can be defined "forging-like", are applicable to several grades also with large semi-product dimensions (300 mm and more). Besides, removing the ingot route means increased yield and productivity, which is very beneficial to the economical management of the plant. An example of this "forging-like" process is represented by the high-reduction blooming stand installed by Acciaierie Venete in the Padova-Camin mill. This article describes its main concepts as well as its technology and process features.

Oct 30, 2017

By Karl K. Bagger, Felipe Bertelli

The competitive scenario of steel industry requires studies and developments to improve manufacturing processes focusing on increasing productivity and reducing costs. The practice of coating rolls for cold rolling with the chrome aims to increase the rolling campaign, reducing their wear by increasing the surface hardness, which guarantees a greater homogeneity in the surface of the rolled products. The present paper presents a study on the effect of the chromium coat on a forged steel rolls on the wettability of a SkinPass solution. The hardness of the coated layer and the contact angle were measured for two concentrations of solution on two types of surfaces, comparing the coated and uncoated surfaces. The results show that there is an influence of the coating on the wettability of the fluid when comparison are made with chrome coated and uncoated materials, being verified through tests in Goniometer. The productivity of the coated rolls showed higher productivity than the uncoated ones.

Oct 1, 2019

By Nestor Cezar Heck

Aim of the present work is to continue the theoretical evaluation of the slags of the fundamental system CaO-SiO2-CrOx-MgO (Ca-O-Cr-Si-Mg quinary system) at the temperature of 1,873 [K], with the help of a computational thermodynamic tool. Driving force for this and the previous research works is the understanding of chromium losses from the molten bath into the slag. Especially motivating is the presence of solid phases in the slag, since they may prevent refractory degradation and help in the production of foaming slags. Nevertheless, Cr-bearing solid phases can lead to Cr losses, being therefore detrimental. Determination of the states of thermodynamic equilibrium for this system using a slag with fixed composition as a start material were made using MgO amount as variable. Results show the impact of the MgO content on the equilibrium phases (molten metal, liquid slag, solids) and their composition for this system.

Jul 30, 2018

By Steven G. Jansto

Carbon content and continuous casting parameters affecting solidification behavior, such as super heat, mold level fluctuation, heat transfer, fine grain chill zone depth and other process solidification parameters directly influence the surface and internal quality of the steel strand. The carbon content, resultant fine grain chill zone depth, the equiaxed-columnar transition zone and the strain energy are the primary drivers that govern hot ductility behavior. These factors influence the propensity for crack formation during the unbending section in the continuous casting process. Elements such as microalloys exhibit secondary or tertiary root causes for crack formation and are not the primary crack formation root cause. This solidification research identifies that the traditional hot ductility as measured via the percent reduction in area (%RA) at elevated temperature grossly overstates the minimum ductility required to assure crack-free casting of microalloyed steels. The strain at the ultimate tensile strength exhibits a very high correlation coefficient with strain energy while an extremely low correlation coefficient is exhibited with %RA.

Oct 30, 2017

By Walter Hartig

Rogesa is operating two medium sized Blast Furnaces, No. 4 and No. 5 at Dillinger integrated steel works plant. The history of the results of the cooling concepts of the intersection between tuyère belt and bosh shows failures at both furnaces. At the 3rd reline of No. 5 Blast Furnace in 2010 changes were made to improve the cooling efficiency of the mentioned area. Two rows of copper cooling plates were installed. After commissioning and a short operating time hot spots occurred in the area of the cooling plates. The decision was taken to develop a new cooling concept together with Paul Wurth Umwelttechnik GmbH, Essen-Germany by replacing the cooling plates by one row of a short copper stave. The duration of the shutdown to perform the work was only 17 days including salamander casting. The operational results after the commissioning are very satisfying with outstanding performance of the new bosh cooling system.

Aug 1, 2018

By Francisco Morganti

The market requirements which strip processing lines have to deal with have altered significantly within the last decades. Particularly, the production has to be economical and ecological efficient and processing lines have to cover a broad product portfolio. Already existing plants either directly or indirectly are competing with new plants, which are equipped with the latest technologies. The “Special Strip Processing Equipment” is designed to be integrated easily and within small downtime phases in existing lines. All single machines can be delivered in short time “ready-to-perform” with a tested and proved automation system. Thus, the competitiveness of existing lines can be increased immediately with less effort. To find out which machines can be reasonably implemented SMS group offers an “Efficiency Check”. A special proceeding is used by experts to find out quickly which machines will have the largest effect on the efficiency of the line while demanding at the same time the smallest expense.

Aug 17, 2017

By Jean-Philippe Houde

The Blast Furnace Campaign lifetime is highly depending on the wear progress of the hearth lining. This progress is monitored in general through single and double thermocouples at the cold side of the lining. This type of monitoring becomes ineffective as soon as heat resistance will be formed in the refractory lining. Paul Wurth’s monitoring system, consisting of MTP-Sensor and Heat Flux Probes, is able to identify such heat resistances to give a true hearth lining wear. Since last year Paul Wurth is also able to install safely those MTP-Sensor and Heat Flux Probes on running blast furnace without salamander tapping, thanks to a newly developed cooled core drilling device. Blast Furnaces that are equipped with Paul Wurth’s monitoring system have optimized their campaign lifetime as they received right information upon the true wear lining such as detection of heat flux transfer failure, detection and monitoring of brittle layer or detection of hot spot.

Aug 16, 2017

By Giulio Antunes de Medeiros, Leonardo Martins Silva, Giselle de Mattos Araújo, Rayla de Souza Caldas

To analyze the direct reduction of self-reducting briquettes producted with different electric arc furnace dust contents, three sets of homogeneous mixtures were produced with elephant grass biomass, iron ore, cement and furnace dust in increasing levels, which were submitted to thermogravimetric tests in muffle furnace and TGA furnace at variable temperatures and times. The curves of degree of reduction were obtained and the reduced briquettes were analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results showed that the reducibility of the agglomerates is diminished by the increase of furnace dust, with variations of this result at higher temperatures. The observed microstructures were spherical particles, porous structure or whiskers. Based on XRD results, it was considered probable that the decrease of the degree of reduction with the increase of furnace dust content is related to the reaction between hematite and zincite, which is expected to be controlled by zinc diffusion.

Oct 1, 2019

By Larissa Agrizzi Ronqueti

The effect of coiling temperature on selective oxidation behaviour of binary and ternary iron-based model alloys containing different contents of Si or Mn were investigated by SEM and SIMS. The experiments were carried out with a temperature ranging from 450 °C to 700 °C, under N2-5%H2 gas flow with a Dew Point of -3.3°C, for different durations. SEM images of binary iron-based model alloys revealed a decrease of grain boundary oxidation depth with increasing Silicon or Manganese content. At 530°C and 600°C SIMS results showed no Silicon diffusion toward surface, contrary to the results analyzed for Fe-x%Mn. Tests results and Wagner’s theory application (specific cases Fe-0.2%Si and Fe-0.5%Si) showed that grain boundary oxygen diffusion coefficient “DoGB” is almost 60 to 70 times faster than oxygen bulk diffusion coefficient. These results helped to broaden knowledge of single-element effects on grain boundary oxidation, in addition, will contribute of the future works in new steels with complex alloy compositions.

Aug 17, 2017

By Luke A. Balzan

Access to information is a key component for making improvements to any process. This is particularly true for all aspects of the iron mining and steelmaking process. The ability to make rapid control decisions can significantly influence process outcomes, including ensuring product specification, mining quality, transportation limits, upgrade factors, waste bypass and direct shipping, among many others. While traditional laboratory methods provide feedback for such processes, having access to analysis results in real-time can lead to positive reactive and predictive control decisions to be made rapidly, leading to significant improvements throughout the process. Scantech has been designing, manufacturing and supplying technological products to the minerals industry since 2002 to enable the availability of such realtime information to a mine or plant, with the benefits being enjoyed by a wide range of operators. This paper provides a summary of the available technologies used in the iron ore and steel industries, as well as providing a case study of their use at an Australian site, and a description of the potential benefits of a range of analysis equipment.

Aug 17, 2017

By Leandro Augusto Viana Teixeira, Márcio Francisco Dill Junges, Adauto Caldara

Innovation in the mining industry is critical when facing ever growing challenges, like the need to increase safety, reduce social and environmental impact, deal with commodities price fluctuations among others. However, successful innovation is not only the product of technological innovation, but it is also dependent on Innovation Management, which consists of changing the way a company fosters innovation, creating a new structure able to leverage technology knowledge and the ability to convert this knowledge in value. This paper presents a restructure option for innovation that focus on R&D development linked to business needs and company strategy. This new system was approached based on four fundamental blocks for innovation management (Approach, Organization, Resources and Metrics), showing how the technology master plan and a management tool are able to bring together all aspects necessary for the proper operation of the system. The new system confirmed the importance of having the initiatives organized as innovation roadmaps, connecting techno-scientific development with the company needs through the use of KPIs that are relevant to the business.

Oct 3, 2019

By Fabio Lerbach

The Powder Charcoal Injection in the main burner of the rotary kiln of Pelletizing Plant aims to reduce natural gas consumption and consequently cost reduction with thermal energy. This paper presents the technology, the injection process and the advantages of using powder charcoal to substitute natural gas.

Oct 30, 2017

By Stanislas Mauuary

Price pressure is a real challenge on the stainless steel market. With market globalization, increase production capacity and exorbitant raw material, the margins are squeezing for stainless strip producers. Primetals Technologies offers a wide range of advanced technological solutions to secure the margins of our customers. Our solutions, implemented with professional project management, allow an optimum coil to market time, securing then the return on investment for the investor. Among the possible lever used to optimize the production route, one drastic step can be made to cut rolling time and cost by replacing the common 20-Hi mill stand reversing process by state of art high capacity X-HI® stands in continuous rolling line. Other source of savings can be implemented by integrated several process steps together (rolling, annealing, pickling, skin passing), achieving then savings on stocks and logistics while coil processing is reduced to fraction of hour. Additional solutions can also be implemented on the new, as well as existing line, like maintenance free solid state laser welder, skin-pass and tension levelers, in-line inspection system coupled with process and quality management system.

Aug 17, 2017

By Bruno Alves Resende, Antonio Adel dos Santos

Temperature, microstructure and dimensions are the main material parameters to be controlled during hot rolling of steel. Although thermal mathematical models have long been developed and applied for hot strip rolling, each Hot Strip Mill (HSM) must have its own model adapted to its facilities. Thus, a mathematical model for temperature evolution during rough rolling has been developed for the Usiminas HSM at Ipatinga Plant. The model achieved a high level of accuracy, which was assessed by comparing measured values of temperature at the hot strip mill entry with the calculated ones, the difference ranging from 9°C to 17°C. Application examples have shown that the slab can be occasionally stopped before start of rolling for as long as a couple of minutes without compromising its further processing. On the other hand, if the transfer bar stops after rough rolling even for short time, further processing in the HSM can be hindered, due to excessive temperature drop. In case of such abnormal line stop, the model can be used as a tool for decision-making to either continuing the planned rolling schedule or to changing the route, thus improving the overall rolling process.

Oct 1, 2019

By Armando Vazquez Arredondo

Tenova Goodfellow Inc. has successfully installed the proprietary EFSOP® (Expert Furnace System Optimization Process) system in over 80 installations worldwide. For over 15 years, the EFSOP® System has successfully achieved its main objective of improving performance and operating costs through the reduction of electricity, oxygen, methane, injected and charge carbon use. Using the off-gas information provided by the EFSOP® System, Tenova Goodfellow Inc. has now developed a solution for detecting abnormal water events within the EAF steelmaking process. When water form enters the EAF, it immediately forms into water vapor (H2Ogas) and a proportion of the resulting water vapour will further react and dissociate to H2. Effective water detection technology must be capable of detecting BOTH forms of water; H2Ogas & H2. Tenova Goodfellow has the technology to measure in real time and simultaneously H2Ogas & H2. This paper will provide a summary on how the EFSOP Water Detection Technology® is used during the EAF operation. Details regarding the technology, software, alarm rate and information on sensibility water trial tests will be provided within this paper.

Aug 16, 2017

By Leandro Seixas Bicalho, Raphael Alcantara da Costa, Pedro Martins de Almeida Rollo, Eduardo Tres, Anderson D. Thomazini

Usual pelletizing process requires the use of iron ore within a given range of particle size. The pelletizing plants often have comminution circuits composed of ball mills and roller presses to meet the granulometric parameters. Aiming at the partial removal of grinding operations and elimination of wet ore processing, the present study evaluated the pelletizing of two samples of ore with lower surface area: (1) sample with only one passage into the roller press (specific surface area of 997 cm²/g) and (2) “in natura” sample as fed to the pelletizing plant (specific surface area of 450 cm²/g). These experiments were conducted with the use of bentonite and the products E/PE MIN 070/19 and E/PE MIN 090/19, made available by Clariant for this purpose. The results indicated that conventional bentonite is not efficient for coarse particle agglomeration. On the other hand, the products E/PE MIN 070/19 and E/PE MIN 090/19 achieved good performance. Considering a sample with only one passage into the roller press it was possible to form pellets similar to those produced in the conventional process.

Oct 1, 2019

By Hamilton Ferreira Gomes de Abreu

Os aços maraging apresentam baixo teor de carbono e possuem uma estrutura cristalina martensítica tetrágonal de corpo centrado (TCC). Estes aços oferecem uma combinação única de alta resistência mecânica e boa tenacidade à fratura. Nesse trabalho, foi realizado um estudo in situ de radiação síncrotron na busca de avaliar a estabilidade da austenita revertida no aço maraging 18%Ni grau 300. Um corpo de prova do aço em estudo com dimensões padronizadas foi solubilizado a 840°C por 1 hora e resfriada ao ar. Em seguida foi aquecida a uma taxa de 10°C/s até 630°C, mantendo-se então nesta temperatura pelo tempo de 12 minutos. Posteriormente a este tratamento, a amostra foi resfriada até a temperatura ambiente a taxa de 15°C/s. Em cada estágio de ciclo térmico foi realizada medidas de radiação síncrotron com comprimento de onda (? = 1.0332 Å). As frações volumétricas das fases austenita revertida e martensita presentes em cada etapa do ciclo térmico foram calculadas utilizando o método de comparação direta e através da área integrada relativa aos picos das fases. A estabilidade mecânica da austenita revertida sob carga externa foi estudada usando radiação in situ síncrotron.

Aug 16, 2017

By Camila Valentina Ribeiro Portilho

O processo siderúrgico necessita de tijolos refratários resistentes ao choque térmico em virtude das inúmeras solicitações térmicas, além de solicitações mecânicas e químicas. Refratários C exibem excelentes propriedades tecnológicas e boa resistência ao ataque de escórias, embora sua resistência ao choque térmico seja limitada, sendo utilizados em válvulas siderúrgicas. Este trabalho visa analisar refratários Al2O3-ZrO2 com adições de microssílica, que pode melhorar eminentemente sua resistência ao choque térmico, pelo fato da microssílica apresentar uma eficácia no empacotamento da massa após mistura e ainda pela possível formação de mulita in situ através da reação com alumina. A possibilidade de formação de mulita in situ proporciona superior resistência à fluência e excelente resistência ao dano por choque térmico. Utilizou-se alumina, 5% de zircônia monoclínica e teores de 15, 25, 35 e 50%.p de microssílica. Os corpos de prova foram prensados a 7 toneladas, sinterizados a 1600°C/2h e caracterizados quanto a resistência ao choque térmico, propriedades tecnológicas pelo método de Arquimedes, resistência à flexão á temperatura ambiente, análise microestrutural utilizando microscopia eletrônica de varredura e análise mineralógica através de difração de raios x.

Oct 30, 2017