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By Anivaldo Chevane, Leonardo Xerinda, Rogério Sendela, Andre Vilanculos

Moatize Coal Mine is located in Tete Province, in centre of Mozambique. The deposit contains Gondwana allochthonous coals, and has a large amount of mudstone and siltstone banding. Phosphorus levels in the coal can be high which impacts the use of the coals in steel making where phosphorus is considered a contaminant. The Chipanga seam in the Moatize deposit shows considerable variability, vertically within the seam and laterally across the deposit. The data available from the exploration work indicates that the phosphorus is predominantly present as Apatite but the Crandallite minerals also are significant. The concentration of phosphorus varies with coal particle density with the highest phosphorus levels found for the mid density coal which also shows the highest likely levels of apatite or fluorapatite. Crandallite minerals show higher potential concentrations in the Lower density coal..

Oct 3, 2019

By Daniel Wild, Tobias Scheffer, Marvin Laugwitz, Martin Jochum

Leveling is a standard process in the rolling mill to eliminate flatness deviations. The process layout is based on models and the leveling result depends on the accuracy of the material parameters in these models. Even small deviations from the correct assumptions can have a major effect on the final flatness. Thus, after leveling the products may look optically flat, but subsequent to a final cutting process springback occurs due to residual stresses. The objective of this work is to analyze the influence of material parameters and gravity on the flatness after leveling. To evaluate the sensitivity of the process, an FE parameter study is exerted that reveals the influence of fluctuations in material properties in the case that the leveling setup is fixed. Gravity is neglected to not conceal flatness deviations. Examples of this study are rerun in a further step under consideration of gravity to also analyze its influence on the resulting flatness and residual stresses. Finally, to analyze the consequence of the residual stresses, all information of the plate from the previous step are transferred while gravity is suppressed to prompt springback. This study revealed that slight deviations of the material properties can lead to uneven plates in simulations where gravity is not considered. If gravity is taken into account, the unevenness is concealed and the plate seems flat. A springback simulation of the same plate shows that strong residual stresses are still present and would lead to unevenness if e.g. the plate were cut.

Oct 1, 2019

By Anna Carolina Cerqueira Neves

Synthetic fiber has been gradually replaced by natural fiber, such as lignocellulosic fiber. In comparison with synthetic fiber, natural fiber has shown economic and environmental advantages. The natural fiber presents interfacial characteristics with polymeric matrices that favor a high impact energy absorption by the composite structure. However, until now little has been evaluated about the hemp fiber incorporated in polymeric matrices. This study has the purpose of evaluate the impact resistance of this kind of epoxy matrix composite reinforced with different percentages of hemp fibers. The impact resistance has substantially increased the relative amount of hemp fiber incorporated as reinforcement in the composite. This performance was associated with the difficulty of rupture imposed by the fibers resulting from the interaction of hemp fiber / epoxy matrix that helps absorb the impact energy.

Aug 16, 2017

By John Beaumont

The Plate-Steckel mill combines the asset utilization of the strip rolling process with the grade and width range of the reversing plate mill, delivering a broad range of steel products at low cost. Among rolling mill types, plate mills are distinctive in the way that they exploit the metallurgical attributes of their product. The downside of this flexibility, though, is a low level of asset utilization. The Plate-Steckel mill was originally developed to combine the utilization of the strip mill and the width of the plate mill. The Plate-Steckel mill is now setting new benchmarks in accessible grades and applications, whilst pushing the width boundaries of the process. Long experience in the Steckel process control and coiler furnace design is coupled with caster and plate mill expertise to deliver high level of performance in this increasingly important plate and coil rolling technique. Several new design features have been incorporated and the vertical integration of mechanics with process models is the key for better product quality and flexibility at these plants. The use of fully automatic thermo-mechanical rolling using the latest physical models and intelligent sequencing strategies achieves the optimum grain refinement and thus improves mechanical properties. The novel profile and flatness strategy relies on comprehensive physical models and makes use of SmartCrown® as a powerful actuator, enabling large reductions to be taken without risking poor flatness. Throughout the rolling and cooling stages of processing, accurate calculation of the thermal-mechanical state of the product is performed by the temperature monitor. This enables tighter control of the final plate mechanical properties by providing an insight into the plate evolution during the thermo-mechanical processing. Advanced pacing functionalities provide an optimized mill throughput, utilizing new cooling bed charging strategies. Considering the rolling process, process automation applies state-of-the-art model calculations to achieve saleable coil/plate target dimensions even in non steady state rolling conditions.

Aug 16, 2017

By Débora Cardoso de Oliveira Silveira, Jean-Christophe Huber, Hamzeh Hamadeh, Kateryna Pastel, Guillaume Brosse

The dynamic behavior of oxygen gas flow, determined by the lance nozzle and blow pattern, is a key factor for determining jet efficiency in BOF Steelmaking. The present work compares the performances of Laval and parabolic nozzles with the aid of the Computational Fluid Dynamics (CFD). The Method of Characteristics (MOC) was applied to design a minimum length parabolic nozzle. The results show that the parabolic nozzle generates more uniform and stable jet, with 2% longer potential core and supersonic length and less shock waves. For the parabolic nozzle, the pressure nearby the nozzle wall is higher, which can protect this region from reverse flow of converter gases and offer longer life for the lance tip. Likewise, the flow rate variations would affect less this nozzle. In addition, the nozzle wear was investigated, and the parabolic nozzle has proven relatively less sensitivity to the presence of this deformity.

Oct 1, 2019

By Saul Garcia Hernandez

The research work objective is to study a new ladle shroud internal design to reduce the slag emulsification in the tundish during ladle transient periods. A 3D mathematical model of the tundish was created to solve the fundamental equations, a turbulence model, and a multiphase model. The results show that using a conventional ladle shroud, the fluid is delivered with an excessive amount of kinetic energy being dissipated inside the tundish bath, generating strong mixing flow patterns and entrapping a massive amount of slag. In the other hand, the proposed ladle shroud dissipates the kinetic energy before the fluid enters the tundish promoting less intense mixing patterns; thus, the amount of slag emulsification is reduced significantly. Consequently, if the internal design of the ladle shroud is able to dissipate the kinetic energy before the fluid enters the tundish, it shall be possible to reduce considerable the slag emulsification and the slag opening area.

Aug 17, 2017

By José Ricardo Nunes de Macedor

Com o crescente zelo ambiental, os polímeros biodegradáveis ganharam importante papel no mercado mundial. Em especial, o amido é um destaque por apresentar preço baixo e alta demanda, contudo possui grande fragilidade mecânica e os seus filmes são muitos hidrofílicos. Outro importante polímero biodegradável é o poli(ácido lático) que possui, alta resistência mecânica e transparência, quando comparado com o amido termoplástico, permitindo sua aplicação em embalagens alimentícias. Contudo, o PLA ainda possui custo elevado, quando comparado ao amido e até commodities, como o PET, PP e PE. Estudos com algodão, material em grande produção e baixo custo, retratam ganhos nas propriedades mecânicas sem perda da biodegradabilidade em compósitos. Assim, este trabalho objetivou preparar, por meio de homogeneizador termocinético KMixer e prensa térmica, placas de compósitos de PLA contendo amido (0, 3 e 5% m/m) e fibras de algodão in natura processadas (0, 10 e 20% m/m). As amostras foram caracterizados por espectroscopia na região do infravermelho com transformada de Fourier (FTIR), ângulo de contato estático e ensaios mecânicos (módulo de Young, resistência à tração e alongamento na ruptura). As análises mostraram que a adição de fibra de algodão compensa a perda de resistencia à tração ocasionada pela adição de TPS. Tanto a fibra como o amido aumentaram a molhabilidade do compósito.

Aug 8, 2018

By Maria Carolina Andrade Teles

Uma fibra natural apresenta características interfaciais com matrizes poliméricas que favorecem a absorção de alta energia de impacto da estrutura compósita . Este trabalho procura avaliar a resistência ao impacto deste tipo de matriz de poliéster com reforço de fibras naturais. As fibras de Fique foram misturadas com resina de poliéster sob pressão em um molde metálico, e curada à temperatura ambiente durante 24 horas . Amostras padrões foram preparadas até 30% em volume de fibras Fique alinhadas ao longo de todo o seu comprimento, estas amostras foram então testadas com ensaio de impacto Izod do pêndulo e as superfícies de fratura examinadas por microscopia eletrônica de varredura, MEV. A resistência ao impacto aumenta substancialmente com a quantidade relativa de fibra de Fique como reforço do compósito . Isto pode ser atribuído a uma descolagem preferencial da interface fibra / matriz , o que contribui para uma elevada energia absorvida.

Aug 17, 2017

By Sebastien Flament

More and more Hot Strip Mills are facing defects on their products that lead to a rejection of complete product batches by their customers. Several of those defects are induced by excessive work roll degradation. This paper is focussed on the understanding of work roll corrosion and oxidation mechanisms in a hot strip mill. Several laboratory trials (Hot rolling simulator, cyclic oxidation) have highlighted important factors influencing corrosion of work rolls as well as helping the understandings of oxidation of a work roll in the roll bite and along the roll circumference in a stand. The attention is focussed on several elements present in water used in HSM for direct roll cooling (e.g. chloride, bactericides, sulphates, phosphates) and their effect on roll surface degradation. The second part of this paper is focused on the understanding of work roll oxidation along the roll circumference. The effects of roll composition, roll temperature, water composition and water temperature have been studied in order to understand the oxidation/corrosion mechanisms in a HSM.

Aug 16, 2017

By Patrícia Mundim Campos Faria

The process of particle size reduction by grinding is inherently inefficient and involves high capital and operating costs. In particular, ball milling is one of the important unit operations in the iron ore pelletizing process. The mill product, due to its physical properties, determines the efficiency of subsequent stages of classification, filtration and pelletizing, thus impacting the quality of iron ore pellets. The work demonstrates the application of the population balance model in the optimization of a full-scale ball mil circuit grinding pellet fines with the aim to evaluate the optimal solids concentration to improve iron ore pellet quality. Initially, detailed experimentation was carried out in a 25.4 cm diameter batch mill and a relationship for mill scale-up using a linear population balance model in wet grinding systems was established. The selection and breakage parameters and the specific selection functions were determined for pellet feed iron ore. It was possible to identify the non-normalizable nature of the breakage functions of the ore studied, which were modeled properly. Afterwards, as a result of incorporating the specific selection functions and breakage functions into the linear population balance model, it was possible to predict product size distributions in the pilot and plant scale mills (0.416 and 5.18 m diameter, respectively) from data obtained in the 25.4 cm diameter mill. Finally, with this scale-up procedure it was possible to appraise the plant scale optimization via laboratory scale grinding mill tests. The effects of changing percent solids were assessed in order to improve the industrial mill performance and the optimal value should be in the range from 76 to 80%.

Aug 1, 2018

By Shibu John

The COREX® process is beside the FINEX® technology the only industrially realized alternative to the blast furnace route for the production of hot metal. Changes in the raw material sector in respect of decrease in quality, strictly enforced environmental laws and positive operation results of COREX® reference plants make it worth to carefully re-evaluate the COREX® technology in comparison with the traditional blast furnace technology. Integrated Plant concepts based on COREX® offer solutions for future challenges of the iron- and steelmaking industry, which include: economical hot metal production; efficient and highly economic export gas utilization (power generation, DRI production, syngas production for chemical products); lower raw material cost, higher raw material availability; environmental friendly high grade steel production. The economic evaluation of different COREX® gas based plant concepts in comparison with the traditional blast furnace route shows that the COREX® technology is highly competitive in the challenging iron and steel producing environment.

Aug 17, 2017

By Tiago de Abreu Siqueira

CO2 geological storage is one of the current technologies developed worldwide to reduce industrial emissions of carbon dioxide to the atmosphere. Two main mineral types of deep geological reservoir could be contemplated for CO2 storage: sandstone reservoirs and carbonaceous reservoirs. Geochemical reactivity of a dolomite-calcite mineral compound and magnesite pure mineral was studied with a set of nine experiments per crushed mineral phase with two saline solution and with mQ water and three temperatures: 50°C, 90°C and 150°C. Experiments were performed in batch reactors with 250 bar of CO2 partial pressure during 24h to assess the effect of temperature and salinity in constant CO2 pressure. Solid characterization was performed by XRD and solution analysis by ICP-OES. Acidification of solutions due to CO2 dissolution in water is the main source of reactivity in the system. Proton concentration increases and causes partial dissolution of initial dolomite, calcite and magnesite and release of Ca2+ and Mg2+ cations in solution. Bicarbonate anion (HCO3) concentration also increases due to CO2 dissolution in water and carbonate minerals dissolution. Temperatures of 90°C and 150ºC increase the kinetic of reaction and the dissolution of minerals and cations release in solution. New carbonate crystalline phase precipitates as a Ca, Mg solid solution between dolomite and calcite pure poles.

Aug 8, 2018

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019

By Carolina Gomes Dias Ribeiro

The modern composite materials, especially those reinforced with synthetic fibers such as glass and carbon, have been used since last century to attend the demands required by most technological fields, from home appliances to aerospace. Natural fibers composites with biodegradable polymer matrices are considered environmentally friendly materials and currently accepted as possible substitutes for synthetic composites. These green composites can be safely discarded or composted at the end of their life without harm to the environment. Another alternative for synthetic composites is to apply natural lignocellulosic fibers as reinforcement of conventional polymer matrices and already used in the automobile industry. In addition to the environmental and societal advantages of the green composites, the lignocellulosic fiber reinforced conventional polymer composite also has economical and technical advantages. In the case of a fiber collected as a waste, the price of the composite can be considerably lower than “fiberglass”. Furthermore, with high strength lignocellulosic fibers such as sisal, ramie and malva the specific strength of a composite may approach that of “fiberglass”. Therefore the objective of the present work is to investigate the mechanical behavior of polymer matrix composites reinforced with high volumes of natural malva fibers subjected to tensile stresses.

Aug 16, 2017

By Mathias Woydt

The tribological and mechanical properties of binderless and metal-bonded niobium carbides (8 or 12 vol.-% of Cobalt, 12 vol.-% of Fe3Al) are presented. Rotating disks made of niobium carbide bearing hard metals were mated against alumina (99.7%) under unlubricated (dry) unidirectional sliding tests (0,1 m/s to 12,0 m/s; 22°C and 400°C) as well as in oscillation tests (f= 20 Hz, ?x= 0,2 mm, 2/50/98% rel. humidity, n= 105/106 cycles). Microstructure and phase compositions were determined as well. The tribological data obtained were benchmarked with different ceramics, cermets, hard metals and thermally sprayed coatings, where NbC bonded with 8% and 12% Co presented above 8 m/s the lowest wear rates so far in such a benchmark. Binderless NbC (HP-NbC1) and the metal bonded NbCs exhibited low wear rates under dry sliding associated with high P?V load carrying capacities. NbC-based hard metal bonded with 12 vol.-% of Fe3Al resulted in a higher hardness level than for 12 vol.-% cobalt. The tribological profile established revealed a strong position of NbC bearing materials under tribological considerations and for closed tribosystems against established reference tribo-couples.

Jul 31, 2018

By Osmar de Sousa Santos

NiTi shape memory alloys (SMA) have been widely used as construction materials due to their shape memory and superelastic properties. Usually the application of the NiTi alloy is in the wire form, which is ideal shape to make springs, orthodontic arc-wire and endodontic files. Since our research group (ITASMART) started producing NiTi wires, it was noticed that NiTi SMA produced by Vacuum Induction Melting (VIM) presents carbon contamination, which is due to the melting process. Therefore, alloys rich in carbon remove titanium from matrix, forming precipitates of TiC (titanium carbide). Also, Ti2Ni precipitation removes titanium from the matrix and these two precipitates TiC and Ti2Ni can produce internal volumetric defect in the wire drawing process. Seeing the importance of NiTi wires as base of many applications, this work studies the formation of volumetric defects caused by precipitates in the wire drawing process of a NiTi wire drawn down to 0,39 mm in diameter.

Aug 8, 2018

By Fernanda Ferrante, Wagner Reis Modesto Ribeiro, Eduardo Pena Carvalho

CSN Mineração S.A. is the second largest exporter of iron ore in Brazil and is among the five most competitive in the market. Casa de Pedra currently has an approximate production capacity of 30 million tons per year. The fleets of small trucks 6x4 and 8x4 models are responsible for the ore movement, traveling an average distance of 10 km between origin and destination. 116 trucks of this size are used in CSN Mineração for the handling of products. Every month this fleet consumes an average of 550,000 liters of fuel. The objective of the work is to do a fuel consumption analysis by truck through the embedded telemetry system. The reports generated through this system provide the specific consumption of each equipment and also the specific consumption of each Driver. As reports are generated it is possible to assess which equipment had a higher specific consumption and, in this case, the respective trucks with greater consumption are directed to the Maintenance team for analysis and action in the event that a problem is identified in the equipment. At the same time, the analysis of the drivers who had the highest specific consumption and conducted a practical and theoretical training, addressing the techniques for a safer and therefore economical direction, is carried out. In 2019, the economy of fuel consumption type S10 was 204 thousand liters, which represents 9% of all consumption foreseen for the period.

Oct 3, 2019

By Flávio Túlio Busatto, João Bosco Mendes, Marcio de Souza Lana, Raphael Dias de Medeiros, Gabriel Nazareth G. Alcoforado

The sintering process begins at the ignition stage of the surface layer of the mixture to be sintered. This ignition is performed through the heat supplied by a furnace, called "Ignition Furnace", and this burn must have sufficient heat potential to start the agglomeration process. As a result of the horizontal movement and the flow of air passing through the material, this surface firing front is transported until reaching the lower zones of the bed, thus producing the sinter. The higher the calorific value of the fuel used, the more efficient (lower fuel consumption and higher temperature) is the surface burning, thus raising the mechanical strength of the product during the process. Due to variations in fuel quality, keeping the ignition temperature controlled becomes a challenge, so, in this work, a study on the combustion of coke oven gas (COG) was carried out, evaluating not only its stoichiometric but also the most adequate control strategy, in order to maintain the working temperature and still optimize the yield and quality of the sinter produced. Mathematical knowledge, automation, control and industrial combustion were used in order to achieve the expected results.

Oct 1, 2019

By Alessandra Spaghetti

Rolling small-diameter hot wire rods at high speeds with conventional laying head pipes can wear the pipe out frequently and affect quality and consistency in the final product. Laying head upgrades using Sandvik SAF2507LHP™ (UNS S32750) tubes make possible to achieve optimal metallurgical properties, smooth coil formation and easier coil handling. Operators can also avoid unwelcome shutdowns due to frequent worn pipe changes and turndowns. Sandvik have been developing different customers and understand their process needs. The suitable selection materials that are able to withstand high levels of wear better than low alloy and carbon steel grades that are commonly used in industry is very important to improve the quality and increase productivity. UNS S32750 tubes were demonstrably superior to low alloy and carbon steels when used in Laying Head Pipe system regarding tubes lifetime, reducing replacement, production interruptions and increasing reliability.

Aug 17, 2017