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By Robson Aguiar de Macedo

O estudo de ligas livres de Pb envolvendo o emprego de junções metálicas sob altas temperaturas tem recebido atenção especial, sendo desenvolvidas novas ligas com qualidade e desempenho adequados. Ligas Bi-Ag consistem em alternativas promissoras para a substituição das ligas de solda contendo Pb para tais aplicações, por isso devem ser melhor caracterizadas sob o aspecto de estruturas brutas de fusão. Assim, o presente trabalho objetiva investigar a liga hipoeutética Bi-1,5%Ag (%em peso) solidificada unidirecionalmente sob regime transitório de fluxo de calor. Será analisada a influência dos parâmetros térmicos de solidificação como velocidade de solidificação (VL), taxa de resfriamento (?) gradiente de temperatura (G) na microestrutura e na evolução de dureza da liga citada. Para determinação do perfil de dureza, foram realizados ensaios de dureza Vickers. Para obtenção e caracterização das microestruturas presentes no fundido Bi-1,5%Ag, fez-se o uso da microscopia ótica e da fluorescência de raios-x. Uma estrutura de dendritas facetadas de Bi circundadas pelo eutético Bi-Ag prevaleceu ao longo do lingote Bi-1,5%Ag. Verificou-se um aumento gradativo dos espaçamentos dendríticos primário (?1) e secundário (?2) à medida que a distância da base refrigerada foi aumentada. Em geral, os valores de dureza diminuíram para maiores valores de ?1 e ?2.

Aug 7, 2018

By Marcelo Braga dos Santos

Visando o estudo da sinergia entre abrasão e corrosão concebeu-se um novo instrumento, permitindo a medição das forças que atuam sobre o contacto. O dispositivo consiste de um equipamento de micro-abrasão por esfera fixa dotada de uma célula de carga de três eixos, e uma célula eletroquímica. Uma membrana protetora flexível foi desenvolvida para isolar a célula de carga, situado no exterior da célula eletroquímica, da amostra no interior da célula. Uma solução corrosiva com partículas abrasivas é continuamente alimentada no contacto entre a amostra e a esfera. Os ensaios de abrasão-corrosão foram realizados simultaneamente em aços inoxidáveis e ferríticos. Também foram executados ensaios de micro-abrasão e corrosão separadamente para avaliar a capacidade do equipamento nos estudos da sinergia entre a micro-abrasão e a corrosão. Para as três condições de ensaios (micro-abrasão, corrosão e abrasãocorrosão) o equipamento se mostrou eficiente em evidenciar a variação nas propriedades do material com excelente repetibilidade. Para os aços austeníticos, as mudanças nas condições de carregamento nos ensaios de abrasão-corrosão induziram variações significativas nas curvas de polarização. A capacidade única de acompanhar as forças que atuam sobre o contato dos processos de abrasão-corrosão pode abrir caminho para novas descobertas sobre o estudo da sinergia na abrasão-corrosão, em especial, a dissipação de energia na interface quantificada através do coeficiente de atrito.

Aug 16, 2017

By Davide Onesti

Electrode regulation is the technology at the heart of the AC and DC Electric Arc Furnace. As such, in the last decade it underwent continuous improvement to maximize the EAF performances, in terms of process efficiency, machine utilization and operator safety. Given this background, Danieli Automation’s efforts in the field of electrode regulation have been focused on fast response to scrap cave-in, compensation of supply variations, automatic resonance detection, transformer protection, dynamic regulation of the electrical and chemical set-points, coordination and control of slagging and foaming agents, arc irradiance supervision. An extensive analysis of operator utilization and feedback was also carried out to develop an innovative system HMI. In this field, the choice of the variables shown to the user is the key aspect to allow a prompt process evaluation by the operator, who can refer to a condensed set of useful data. This paper will describe the innovative features and embedded models of the electrode regulation module (Q-REG+) and the supervision HMI, together with the effects of their application on EAF process efficiency and system usability.

Oct 30, 2017

By Débora Cardoso de Oliveira Silveira, Jean-Christophe Huber, Hamzeh Hamadeh, Kateryna Pastel, Guillaume Brosse

The dynamic behavior of oxygen gas flow, determined by the lance nozzle and blow pattern, is a key factor for determining jet efficiency in BOF Steelmaking. The present work compares the performances of Laval and parabolic nozzles with the aid of the Computational Fluid Dynamics (CFD). The Method of Characteristics (MOC) was applied to design a minimum length parabolic nozzle. The results show that the parabolic nozzle generates more uniform and stable jet, with 2% longer potential core and supersonic length and less shock waves. For the parabolic nozzle, the pressure nearby the nozzle wall is higher, which can protect this region from reverse flow of converter gases and offer longer life for the lance tip. Likewise, the flow rate variations would affect less this nozzle. In addition, the nozzle wear was investigated, and the parabolic nozzle has proven relatively less sensitivity to the presence of this deformity.

Oct 1, 2019

By Andrew Slifka, Pello Uranga, Douglas Glenn Stalheim

Structural steel final mechanical properties of strength and ductility are predominately generated by the final ferrite grain size/packet size and homogeneity of that ferrite grain size/packet size through the cross-sectional area. Forty to seventy percent of the strength components come from how fine the final cross-sectional ferrite grain size/packet size that can be produced.[1] All the ductility properties of structural steels for a given microstructure are predominately driven by how fine AND homogenous the final cross-sectional ferrite grain size/packet size can be refined.[2,3,4] One key ductility property of structural steels used in construction and energy transmission applications is fatigue. Both low and high cycle fatigue can be realized in these end applications, however, low cycle fatigue is typically the predominate mechanism. In construction applications the environment for fatigue is typically air, such as in wind towers or high-rise building construction. In energy applications, there is an interest in high pressure (5.5 – 21 MPa, 800-3000 psi) gaseous hydrogen as an alternative fuel source to fossil fuels. A project to study the effect of the cross-sectional grain size/homogeneity of a relatively pure polygonal ferrite microstructure on the fatigue performance in air and high-pressure gaseous hydrogen has been developed. This paper will discuss the project strategy, microstructure developed for the project and initial test results.

Oct 1, 2019

By Darina Manova

Plasma assisted surface modification methods have been used to nitride stainless steels in order to enhance hardness and therefore the lifetime of industrial components. Nevertheless, the corrosion resistance is not always preserved since it is very sensitive to the process parameters, either in implantation or in thermochemical diffusion techniques. AISI 316L stainless steel was plasma nitrided using three different techniques: Low Energy Ion Implantation (LEII), Plasma Immersion Implantation (PI3) and conventional DC pulsed plasma nitriding (DCPN). For each method several parameters were tested and some of them were selected to achieve the so called S phase of about 3 µm thickness and no nitrides precipitation. The nitrided layer was characterized with OM and SEM. Hardness was assessed on the surface with Vickers indenter and 25 g load. XRD was performed to characterize the S phase and to detect other phases if present and electrochemical corrosion tests were carried out in 3.5% NaCl solution. Although the S phase thickness in the three groups of samples was comparable, hardness was not and neither was the corrosion resistance. The PI3 samples were the hardest with the best performance in corrosion experiments, resulting in a higher breakdown potential and lower currents.

Aug 8, 2018

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the ex-service condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 52 to 224 MPa producing rupture times varying from 5 to about 3950h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results obtained on a similar plate of the same material in the virgin condition.

Aug 16, 2017

By Luke A. Balzan

Access to information is a key component for making improvements to any process. This is particularly true for all aspects of the iron mining and steelmaking process. The ability to make rapid control decisions can significantly influence process outcomes, including ensuring product specification, mining quality, transportation limits, upgrade factors, waste bypass and direct shipping, among many others. While traditional laboratory methods provide feedback for such processes, having access to analysis results in real-time can lead to positive reactive and predictive control decisions to be made rapidly, leading to significant improvements throughout the process. Scantech has been designing, manufacturing and supplying technological products to the minerals industry since 2002 to enable the availability of such realtime information to a mine or plant, with the benefits being enjoyed by a wide range of operators. This paper provides a summary of the available technologies used in the iron ore and steel industries, as well as providing a case study of their use at an Australian site, and a description of the potential benefits of a range of analysis equipment.

Aug 17, 2017

By Antonio Fabiano de Oliveira

Estudos de laminação com revestimento de cromo e influência nas propriedades foram realizados com o objetivo de aumentar a produtividade dos cilindros. Para tal, foram utilizados cilindros cromados para laminação de chapas de cobre, com amostragem da técnica de réplica epoxy. A compreensão da correlação entre microestrutura e propriedades do material é objeto de grande interesse e, ao mesmo tempo, necessário para aplicação prática na laminação a frio, combinando revestimento e produtividade. O objetivo da pesquisa atual é comparar as propriedades tribológicas do cobre antes e depois da laminação, no cilindro de trabalho e chapa, com e sem revestimento de cromo.

Oct 30, 2017

By Steven Gillgrass

Gerdau Monroe has installed and commissioned the Tallman Supersonic Carbon Injection system (TSCi™) for use in their 135-ton Electric Arc Furnace (EAF) located in Monroe, MI. TSCi™ is an innovative injection system with the primary aim of improving injection carbon delivery to the steel bath by increasing efficiency. It is proven technology with installations at numerous steelmaking facilities all over the world. Results from installation and commissioning of TSCi™ at Gerdau Monroe will be reported as well as on-going trials and optimization efforts. Standard injection systems deliver carbonaceous material from a vessel to the EAF using air where it is injected through a lance pipe or oxy-fuel burner. Using this method, material delivery to the EAF is limited by the pressure and velocity of the transport air. Loss of efficiency can be observed by looking at the quality of the injection carbon stream during operation or by measuring loss on ignition of EAF slag or off-gas system dust. TSCi™ uses a patented design and proprietary technology to improve delivery of carbonaceous material to the EAF. Using this method, savings at Gerdau Monroe were realized by reducing the amount of carbon used in each heat while maintaining or improving upon existing foamy slag practice. As well, significant savings were achieved as a result of reduced FeO content in the slag and improved recovery of iron. Additional savings can be realized by using a smaller mesh material to take advantage of lower material cost and higher injected surface area. Other inherent benefits to improved injection carbon include lower energy and electrode consumption, reduced refractory wear and reduced maintenance cost.

Oct 30, 2017

By Jean-Paul Simoes

The development of the blast furnace over the last years lead to a substantial increase in production capacity and productivity. This development triggered an evolution of the cooling systems in order to cope with the raising heat loads. The excellent protection of the shell by copper staves allowed blast furnace operators to achieve campaign lifetimes of more than 20 years. However in recent years some blast furnaces have experienced severe wear of the copper staves due to abrasion. The influences of the blast furnace design as well as of the operation conditions on this premature wear have been analysed and the mechanisms leading to the wear will be explained. New developments in the copper stave technology are part of the solution for avoiding premature wear during periods with less favourable conditions. The protection mechanisms made available by the new design extend the inherent protection mechanisms of copper staves to these periods. BFXpert® system is the ideal tool for the monitoring of the process data, the process models and the recommendations given by Sachem® support the operator in choosing efficient operation points. The charging with a Bell Less Top® (BLT) allows an accurate controlling of the blast furnace with regard to the optimization of the gas distribution. High performance operation together with long campaign lifetimes are thus made possible.

Aug 1, 2018

By Julián Andrés Ortiz González

This work presents a series of experiments of Fatigue Crack Growth (FCG), which are intended to provide evidence about the main parameter controlling this phenomenon, whereas still no agreement about this, since the Paris´ theory is based on the principle that FCG is controlled by the ?K and the Elber´s theory says that the driving force is ?Keff. For the development of the experiments, some DC(T) specimens were machined with two different thicknesses: 2 and 30 mm to perform FCG tests in plane stress and plane strain state, respectively. Besides this, all FCG tests were carried out with a constant ?K e Kmax, measuring the strain with a Strain-Gage bonded on the back face of the specimen and seven Strain-Gages located on the crack growth path. The data needed to measure the crack opening load, and the ?Keff, were collected through a program developed in Labview. Finally, the data post-processing was carried out based on the ASTM standards and several articles of recognized authors in this field, in order to compare the two positions with the experimental data, and this way conclude which is the most consistent theory with the observed behavior.

Aug 16, 2017

By Gabriela Pereira de Miranda

Este estudo teve por objetivo avaliar a soldabilidade a pontos entre os aços 22MnB5 e Dual Phase da classe de 800 MPa de limite de resistência (DP800), ambos com 1,8 mm de espessura. A intenção foi determinar os parâmetros adequados de soldagem para esse tipo de junta soldada, que vem sendo progressivamente utilizada na estrutura de veículos automotores, em virtude do uso crescente de peças fabricadas a partir do aço 22MnB5, submetido ao processo de estampagem a quente (hot stamping). Foram avaliadas as propriedades mecânicas através de ensaios estáticos de cisalhamento e de tração cruzada, em juntas soldadas produzidas a partir da variação do tempo de soldagem e da força aplicada pelos eletrodos. Percebeu-se que as juntas confeccionadas com o tempo de soldagem com múltiplos pulsos (9/2/9/2/9 ciclos) e a força de 5,0 kN obtiveram os melhores resultados em cisalhamento. Em contrapartida, os corpos de prova produzidos com a força de 6,5 kN atingiram os maiores valores em tração cruzada. Independentemente dos parâmetros aplicados, todas as condições avaliadas permitiram alcançar o valor mínimo de carga de ruptura necessária para garantir a qualidade de uma junta soldada a ponto entre os aços avaliados.

Aug 16, 2017

By Jorge Ivan Sabogal Paz

Con este trabajo se desarrolló un sistema para eliminación de un olor no característico en CO2 captado como subproducto industrial de un proceso de producción de alcohol por fermentación de jugos de caña de azúcar. Al incrementarse la producción, este CO2 comenzó a presentar un olor Dulce que afectaba la calidad insabora por lo cual en este trabajo se reporta el diseño y análisis de un sistema de eliminación de este olor no característico basado en sistemas de lavado. optimizado por sistemas de control automático. En los resultados se reporta el efecto en la disminución de los olores no característicos de distintos sistemas con respecto a su eficacia técnica e impacto.

Aug 17, 2017

By Alessandro Pigani

Over the last 25 years the thin slab casting and rolling process has been gaining a major market share in the production of hot rolled strip, progressively eroding the areas previously of exclusive domain of conventional mills. This is mainly thanks to the competitiveness of the process over conventional ones, and to the growing ability of this technology to cover the majority of market niches, well beyond the boundaries of the commodity market. After having significantly contributed to the continuous expansion of this production mode and after an extensive campaign of theoretical research and physical testing in reference plants, Danieli has progressively developed over the years a new generation of thin slab casting and rolling layout, marking a new phase in the evolution of this process. The new step-ahead is epitomized by the name QSP-DUE. This configuration belongs to the Quality Strip Production (QSP) family, which is Danieli’s strip-quality-oriented thin slab based plants. The innovative features of the process are embodied in the acronym DUE, which stands for Danieli Universal Endless (Danieli patented technology – US patent n. 8087449, January 3rd, 2012). What makes this new concept different is the ability of “universal” rolling modes thanks to the fact that, now, within one single plant it is possible to perform coil-to-coil, semi-endless and endless rolling modes, making this plant a major technology innovation compared to the previous generation.

Aug 16, 2017

By Sara Hornby

After almost half a century of experience in using DRI/HBI in electric arc furnaces (EAFs), and taking into account the decrease of natural gas cost in the USA, it is interesting to revisit some trends and controversial issues around this alternative iron source. This paper reviews aspects like the evolution of iron ore quality and its influence on EAF operation; DRI stockpiling and transport, regarding the risk for selfcombustion; optimum charge design; cold DRI/HBI charging (fifth hole, bucket, transporter); hot charging (ways and results); carbon content, metallization and silica in DRI/HBI, and its influence on EAF operation and performance; oxygen / carbon balance; chemical energy and DRI/HBI charge.

Aug 16, 2017

By Edo Engel

Whereas only a handful of decades ago, typical blast furnace working volumes were below 1000 m³, such furnaces are currently designated compact or even mini blast furnaces. For certain business cases, however, small furnace sizes remain an attractive option. Decades ago, this size blast furnace would have produced a maximum of 0.3 Mtpa with its 600 m³ working volume over a campaign of up to four years. The current state of technology and operational know–how will allow a similarly sized furnace to produce over 0.7 Mtpa while achieving the multiple decade campaigns that have become familiar to steel producers in full sized operations. This level of productivity, but especially the reliability and supply security associated with mature technology, allows for integration into minimills or taking a first step towards a full scale BF–BOF integrated mill. Steel producers considering such scenarios, which are typically attractive for emerging economies, are confronted with fundamental decisions, one of which is for the technological basis for the compact or mini blast furnace to be included in the plant. This article addresses some of these decisions from an operations–based perspective. A small number of case studies is included.

Aug 16, 2017

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019

By Piezanowski Ludivine

With the aim to reduce the hot metal production cost, ArcelorMittal Gent decided to integrate more ores with finer particle size distribution in the raw material mix for the production of blast furnace sinter. As a consequence of such an increase of finer material in the sinter raw mix, the sinter machine productivity and the quality of the sinter are affected. In order to compensate this impact, modern granulation technology can be employed. Within this context, ArcelorMittal Gent has invested in a vertical intensive mixer. The equipment was placed before the existing drums, with a function of “mixer”, whereas the drums are fully optimised for the nodulizing process. The paper presents the results of the industrial operation during the commissioning phase of the new equipment. Gradually increasing the proportion of fine material in the sinter raw mix has made it possible to compare the performances of the old system using drums for mixing and pelletizing with the new system using an intensive mixer combined with a nodulizing.

Aug 1, 2018

By Santiago Faucher

Molten slag from pyrometallurgical furnaces is tapped at high temperature, carrying a large amount of thermal energy. But the common slag dumping and water granulation methods used for slag treatment do not permit energy recovery. Furthermore, water is present in these processes and while operations are designed to minimize risks of steam explosions, from the contact of slag with water, these common slag handling practices have never been inherently safe. Common handling practices do permit some slags to be sold, but often in low volumes at low prices. Dry granulation offers advantages over these common slag handling practices, including the production of by-products, the recovery of thermal energy, and the eliminated consumption and safety hazards of water. For these reasons, there have been various studies in dry granulation and heat recovery, but most have never been brought to commercial scale due to scalability and cost challenges. Ecomaister- Hatch has developed and brought to commercial scale a reliable and simple dry granulation and heat recovery technology. Here we review common slag handling practices, the developments in dry slag granulation over the last three decades, introduce the Ecomaister-Hatch dry slag granulation process, and elaborate on future applications of the technology in the processing of argon oxygen decarburization and blast furnace slags.

Aug 17, 2017