Search Documents

By Gilmar Zacca Batista

The present work is a part of a comprehensive program that aims to evaluate the girth welding procedures for heavy wall API 5L X65 pipes produced for sour service applications. This article describes the results of toughness, strength and sour resistance of girth welds produced with different welding consumables. The methodology applied included girth welds production with GTAW process for root pass using ER70S-6 consumable and FCAW process for filling passes using E71T- 1CJ and E91T1-GM-H4 consumables. Mechanical tests of Charpy, CTOD, tensile, hardness and stress corrosion cracking were also performed. The E71T-1CJ resulted in a girth weld with tensile and yield strength around 7% lower than the pipe. However, according to the papers analyzed at this study, a value up to 10% of undermatching could be acceptable. The CTOD and Charpy tests showed good toughness and weld metal embrittlement was not observed. The hardness and the stress corrosion cracking tests demonstrated that the consumable ER70S-6 is suitable for sour service. All properties evaluated met the requirements specified by the onshore pipeline standards, showing that the consumables ER70S-6, E71T-1CJ and E91T1-GM-H4 are suitable for the welding of heavy wall X65 pipe with sour service and toughness requirements. If an overmatching is required, the E91T1-GMH4 shall be used to assure a strength overmatching and prevent plastic strain concentration at the weld metal. The results provided by this paper can be used for consumable selection and for welding procedure qualification of pipelines construction when heavy wall API 5L X65 are used for sour gas transportation.

Aug 16, 2017

By Johann-Paul Stemplinger

For lubrication of open gear drives applied in rotary furnaces, often gear greases are used as well as for lubrication of gear boxes in difficult sealing conditions. The selection of the gear grease influences strongly the wear behavior. Investigations with flow greases NLGI 00 were made in a back-to-back test rig determining the weight loss due to wear acc. to the standardised procedure ISO 14635 part 3. Different influences like base oil viscosity, thickener type and additional solid lubricant type were analysed. Only the type and amount of solid lubricant shows a significant influence on the weight loss due to wear. Finally, a linear wear coefficient clT according to the calculation method of the wear amount according to Plewe is derived and can be used to transfer the test results to any gears in practice.

Jul 31, 2018

By Tiago Seixas Bittencourt

Technological developments, associated with the constant worry about the environmental impacts arising from industrial activity, it has driven the development of technologies and practices for efficient fumes and particulates capture arising from the manufacturing processes of steel in steel plants in general. Currently, the electric steelshops in operation with Electric Arc Furnaces (EAF), seek parameterize/design dedusting systems able to retain most of the particulates generated during melting and refining of steel in FEA through configurations of equipment, technologies and parameters operation in order to equalize the antagonistic relationship between effective fumes capture and energy balance of the EAF. The present work gets as a fundamental premise to evaluate critically the possible different settings of the usual dust removal systems, as well as their respective classical parameterizations. The work main purpose is to establish a general rule evaluation technique for dedusting system considering the different modes of operation of an Electric Arc Furnace.

Jul 30, 2018

By Ismael Vemdrame Flores, Lindaura de Souza Cândido D’ Avila, Maurício Covcevich Bagatini, Arthur Felipe Lino Oliveira, Rafael Adriano Lopes Júnior

The use of pellet feed to adjust the chemical quality of the sinter is an alternative to the depletion of iron ore reserves. However, the addition of ultrafine in the sintering process can cause decrease of permeability and consequent drop in machine productivity. In this context, the present work investigated the addition of natural and ground pellet feed, evaluating its effects on cold agglomeration for sintering and quality of quasi-particles produced. Eight typical mixtures with industrial composition were produced in the laboratory, replacing Sinter Feed with different percentages of Natural Pellet Feed (NPF, 91% <150 μm) and Ground Pellet Feed (GPF, 83% <44 μm). The mixtures were subjected to cold agglomeration tests and the quasi-particles produced were evaluated by screening, shatter test, permeability test and disintegration into primary particles analysis. There was a decrease in the mean particle size of quasi-particles and reduce in permeability with addition of the ultrafines. The addition of NPF favored the layering mechanism in larger quasi-particles. The coalescence mechanism occurred for larger additions of NPF and GPF, being more expressive for GPF additions.

Oct 1, 2019

By Sebastien Maillard, Stephane Georges, Thomas Vallee, Stanislas Mauuary

Steel strip manufacturing ever reinvents proposing new grades, requiring to tackle technical limitations of production systems. Primetals Technologies breaks through strip welding by expanding the welder LW21L “Asolid” technology used on low gauges for high-end market such as automotive CAL/CGL. Addressing the usual drawbacks in maintenance, operation and safety of current welding system based on mechanical cutting and CO2 laser welding, the newly developped LW21H “Asolid” technology processes thicker strips up to 7 mm with solid-state laser cutting and welding. This new welder is brought to reality through a scale 1:1 pilot developed, manufactured and tested in Primetals Technologies workshop.

Oct 1, 2019

By Uwe König

Traditionally quality control of iron ore sinter, its raw materials and raw mixtures has relied on time-consuming wet chemistry. The mineralogical composition that defines the properties is often not monitored. XRD analysis in combination with Rietveld quantification and statistical data evaluation using Partial Least-Square Regression (PLSR) has been successfully established to determine the mineralogical composition and process parameters such as the FeO (Fe2+) content and basicity of iron sinter within an analysis time of less than 8 minutes per sample. Both methods take the full XRD pattern into account and can be simultaneously applied on the same measurement. In addition the Rietveld method was used to quantify the phase content of raw mixtures to monitor the composition of blending beds.

Aug 16, 2017

By Afshin Sadri

One of the main reasons for blast furnace reline is the loss of refractory lining, particularly in the hearth and taphole regions. Intense operation of the blast furnace can result in extensive refractory wear and deterioration. This can then affect the continuity of the operation and the furnace campaign life. Novo-Lipetsk (NLMK) and Hatch developed a systematic approach to monitor the condition of blast furnace hearth linings using Acousto Ultrasonic-Echo (AU-E), a non-destructive testing system developed by Hatch. Continuous and periodic inspections of blast furnaces revealed areas with accelerated refractory deterioration, formation of elephant foot, extent and speed of refractory wear, as well as cracks and other anomalies. Improvement in coke quality, stave washing, the addition of titania, and other changes were recommended and implemented to prolong furnace life while maintaining the intensity of furnace operation. This paper demonstrates how the coordinated efforts between NLMK and Hatch resulted in prolonging the blast furnace campaign life.

Aug 17, 2017

By Luiz Alberto dos Santos

. In this work, samples of the alloy with composition of 50.9 % at. Ni were machined and were subjected to hot tensile test, after the machining all the samples were solubilized so that all were in the same condition during the hot tensile test. The hot tensile tests were performed between the temperatures 350-650°C and the yield stress were between 800 and 597.1 MPa and area reduction between 17 and 75% with respect to the initial area. The test at 350°C shows a fragile fracture characteristic while the hot tensile test above this temperature showed a predominantly ductile fracture. The fragile fracture is evidenced by the river marks that are characteristic of this type of fracture, because in this condition does not promote much plastic deformation. The higher temperatures present ductile fracture, because present the dimples that also characterize this type of fracture. This work shows the temperature relationship in the mechanical properties, more specifically the hot tensile test, in the NiTi alloy.

Oct 30, 2017

By François DUMORTIER

Due to the increasingly stringent requirements and the needs of the automotive industry, galvanizing lines for automotive products have to be modernized and improved. Beginning of 2017, SEGAL, a Tata Steel CGL located in BELGIUM and fully dedicated to automotive market, placed an order to increase the line capacity from 550kt/year to 600kt/year to process a wider range of steel grades and improve the product quality according to automotive requirements. To improve quality, a major revamping of the skin pass was necessary. The objectives were first to increase the work roll diameter from Φ560mm to Φ650mm to be able to transfer the required roughness with low elongation on soft material and second to increase the rolling force and tension to reach higher elongation on high strength steels. The result was the adaptation of the whole skin pass mechanics. Old mechanical elongation system has been replaced by a completely new single AC motor with helical gearbox at each bridle roll. John Cockerill achieved such complicated revamping in a very short time since the shutdown started only 6 month after the contract signature. The shutdown down schedule has been optimized with pre-erection works and the teams working 24/7 to implement all the changes. The complete project (skin pass, furnace, loopers) have been adapted during the three weeks shutdown. Today the customer can use both 560mm and 650mm work roll diameters. Thanks to the use of the new 650mm work roll diameter, the customer is able to make the same elongation using a bigger roll force (average 20% more), which has strongly improved the roughness transfer to the strip and the removal of the defects. SEGAL is really satisfied able to produce and supply higher quality automotive products to his customers.

Oct 1, 2019

By Jônatas Venancio Barbosa, Dagoberto Brandão Santos, Túlio Magno Füzessy de Melo

In this work, the mechanical and metallurgical behavior of titanium added ultra-low carbon (ULC-Ti) steel under hot and warm working conditions was studied by means of dilatometer compression tests. Double compression schedules were performed at temperatures between 700°C and 1000°C, inter-pass times of 0.5-100 s, and deformations of 0.5 and 0.3 in the first and second stages, respectively, with strain rate of 1 s-1. The analysis of the flow curves obtained allowed the evaluation of the softening characteristics of the steel. The softening and microstructure features indicate different restoration mechanisms depending on the temperature range. Static recrystallization with rapid microstructure restoration is observed at temperatures within the austenitic and intercritical field. Strain induced boundary motion and recovery mechanisms apparently control the restoration process in the ferrite region. In general, flow stress curves showed dynamic recovery behavior. Only the deformation in the intercritical region produced a peak in the flow stress curves. Isothermal holding tests associated with single hit compression indicated the presence of dynamic strain induced transformation, accelerating the softening kinetics at the intercritical region.

Oct 1, 2019

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Milan Terčelj, Matej Drobne, Urška Klančnik, Peter Fajfar

The study of oxidation behavior of High Chromium Steel material used for surface layer of work rolls was carried out. Specimens taken directly from the roll were subjected to thermal fatigue in the temperature range between room temperature and 500 °C up to 700 °C by using thermo-mechanical simulator Gleeble 1500D. Our observation was focused on the impact of oxidation as a principal mechanism of degradation of the roll’s surface layer - mainly on the characteristics of oxidation propagation in relation to the test temperature and microstructure constituents characteristics of the material. Oxidation is considerably accelerated by certain characteristics of eutectic and primary carbides, i.e. their size (area), composition, morphology, orientation regarding to the water-cooled surface, etc. In the presented paper selected cases where emphasized oxidation takes place are investigated, analyzed and explained. Obtained results thus represent a contribution to explanation of conditions which lead to acceleration of oxidation behavior that in turn can lead to chipping or even early spalling of material from the roll surface layer.

Oct 1, 2019

By Lucas Monteiro Corrêa e Lopes, Carolina Carvalho Nunes, Nathalia Luiza Nascimento de Carvalho

The characteristics of each ore make it impossible to predict the quality of a flotation concentrate without exploratory tests. The research begins with laboratory batch tests, and then, after advances in the determination of process conditions, the complexity of the tests increases in order to evaluate new parameters. The closed cycle test (LCT) simulate circuits with load recirculation and the greatest difficulty of this test is to stabilize the circuit and achieve equilibrium. Depending on mass availability, the types of tests that offer the highest reliability and informations about flotation in an ongoing process are mini-scale or pilot-scale tests. This work aimed to compare the results of the flotation tests in three scales (batch test, LCT and mini pilot) for the Bonsucesso ore, a new deposit, owned by Nexa Resources, that has sphalerite, zinc ore, and galena, lead ore. In the open flotation circuit of galena was obtained 27.57% content with 26.70% recovery, in the LCT test the content was 31.54% with 64.64% recovery and in the mini pilot reached 51.22 % content with 65.51% recovery. In the open sphalerite flotation the zinc content was 55.51% with 77.35% recovery, in the LCT test the zinc content was 56.71% with 84.42% of recovery and in the mini pilot of 50.02% content with 94.54% recovery.

Oct 3, 2019

By Rogério Felício dos Santos

Nitriding of metallic materials using electric discharges generated during electric discharge machining (EDM) is a recently developed technique. The aim of this paper was to correlate mechanical properties of a nitrided layer produced in AISI 4140 steel by EDM nitriding with the type and amount of nitrides. A conventional die-sinking EDM equipment and electrolytic copper electrodes were used to generate the electric discharges. The electrolyte was a solution of urea in deionized water. Knoop microhardness profiles assessed the variation of hardness along the nitrided layer, whereas the elastic modulus of this layer was measured using nanoindentation tests. Optical microscopy and X-ray diffraction (XRD) were used to characterize the nitrided surface. The results showed the formation of a nitrided layer containing iron nitrides with average thickness of around 25 µm. The amount of nitrides reduced from the surface towards the centre and these results correlated well with microhardness profiles obtained.

Jul 31, 2018

By Gigliola Salerno

The carbon-epoxy composite has high specific resistance and strength, which means specific applications. However, its behavior under compressive stress could be decreased by delamination, needing more detailed studies. The main purpose of the present work is to verify the mechanical properties in bending process considering two different fiber orientations. The composite materials were made by woven fibers and epoxy resin. Primarily, the carbon fiber fabrics suffered a superficial physical treatment called silanization, in order to developing a better chemical adhesion between fibers and resin. After the superficial treatment, the layers were embedded with epoxy resin. The composite resin’s cure was made in a Fanem heater, model 320, during 1 hour at 120°C at 1.5 bar; subsequently the specimens were cut by water jet. Specimens oriented in 0°/90° and 0°/90°/45 were manufactured and taken to bending tests, accordingly to the ASTM E855 and D790 standards, in an universal testing machine MTS – Material Test System, full capacity of 250 kN. It was concluded that all specimens failed by tension. Specimens with internal void volumes results in lower flexural modulus and those with presence of fracture mechanisms, like delamination, showed lower strength values. Scanning Electronic Microscopy demonstrated the damages involved during bending process.

Oct 30, 2017

By Steven G. Jansto

Carbon content and continuous casting parameters affecting solidification behavior, such as super heat, mold level fluctuation, heat transfer, fine grain chill zone depth and other process solidification parameters directly influence the surface and internal quality of the steel strand. The carbon content, resultant fine grain chill zone depth, the equiaxed-columnar transition zone and the strain energy are the primary drivers that govern hot ductility behavior. These factors influence the propensity for crack formation during the unbending section in the continuous casting process. Elements such as microalloys exhibit secondary or tertiary root causes for crack formation and are not the primary crack formation root cause. This solidification research identifies that the traditional hot ductility as measured via the percent reduction in area (%RA) at elevated temperature grossly overstates the minimum ductility required to assure crack-free casting of microalloyed steels. The strain at the ultimate tensile strength exhibits a very high correlation coefficient with strain energy while an extremely low correlation coefficient is exhibited with %RA.

Oct 30, 2017

By Evan Thomas

It has been shown before that liquids can slip at a solid boundary, which prompted the idea that parallel-surface bearings can be obtained by the use of alternating slip and non-slip regions in the direction of fluid flow. The amount of slip at the wall depends upon the surface tension at the liquid - solid interface, which in turn depends on the chemical composition of the surface and its roughness. In the present study a heterogeneous surface was created by coating half of a circular glass disc with a coating repellent to glycerol. A rotating glass disc was placed at a known distance above the coated stationary surface and the gap was filled with glycerol. With the top surface moving in the direction of slip to non-slip region, a pressure build up can be theoretically predicted. The pressure gradient in the two regions is constant, similar to that in a Rayleigh step bearing, with the maximum pressure at the boundary. In order to accurately measure the force generated by the pressure increase, a load cell was attached to the heterogeneous disc. Experiments were conducted by varying both sliding speed and distance, and the resultant load carrying capacity was measured and compared with theoretical calculations. This allowed the slip coefficient of the coated surface to be evaluated.

Jul 31, 2018

By Priscilla Pessin Coppo

The prevention of dental enamel wear has particular relevance for preventive and restorative purposes in dentistry. The wear damage can increase due to salivary disorders and/or parafunction (bruxism); antagonists incisal surfaces become flat and coincident. This study aims to investigate the wear behavior and the related mechanisms in sliding pairs of conformal incisal enamel, with similar values of hardness and fracture toughness, with different applied normal loads and lubricated conditions. Bovine incisors, under pin on flat configuration, were tested in two lubrication condition (dry or with natural saliva) and two applied normal loads (8 and 16 N). The worn surfaces were investigated by 3D profilometry and SEM. The analysis of worn surfaces indicated mechanisms of brittle fracture, but with different severities. Under a normal load of 16 N and dry condition, wear is controlled by a brittle process: microcracking with flake-like wear particles, which results in high friction coefficient (> 0.85), wear rate and wear volume. On the other hand, under a normal load of 8 N and natural saliva, wear took place in the interprismatic region, with consequent exposure of prisms and fracture in localized regions. In this case, the friction coefficient was 16% lower and the wear volume was one order of magnitude lower. Under 8 N and natural saliva, the wear was greater than in the dry condition, probably due to tribochemical reactions.

Jul 31, 2018

By Franco de Castro Bubani

Cu-base alloys (Cu-Zn-Al, Cu-Al-Be, Cu-Al-Ni), depending on their composition, have martensitic transformations that can be thermally or mechanically induced between a metastable structure called austenite and one or more metastable structures called martensites. In single crystals, depending on the specific composition of the alloy and the crystallographic orientation of the tensile axis, martensite-martensite transformations can be mechanically induced. The hysteresis associated to these martensite-martensite transitions is usually much greater than the one associated to the austenite-martensite transformation. Thus, martensite-martensite transitions are potential candidates for energy dissipation in a mechanical damper. Possible applications that would benefit from high hysteresis include seismic damping devices, dampers for satellites and the aerospace industry, defense and others. We present pseudoelastic cycling results of alloys submitted to different thermal treatments. Our conclusions highlight the fact that, under certain conditions, Cu-base alloys deliver better damping performance than commercially available SMAs and even the new Fe-base SMAs.

Aug 7, 2018

By Hervé Thomasson

Siemens VAI has made an important Research & Development effort since 10 years on laser welder field. The last step of this program was in 2010, the evolution of its laser welder range by implementing the solid state technology with laser cutting and welding. Since this step, 8 welders were produced by Siemens VAI. Now after more than 1 year of industrial feedback, the results are showing a high level of performances on very demanding processing lines for a large range of products from Silicon steel to High Strength Steel with DP and TRIP grades. This laser welder concept using laser cutting and welding through solid state laser source is also proposed by Siemens VAI for pickling lines and tandem mills with significant advantages compared to standard solution.

Jul 30, 2018