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By Jerry B. Newby

In the central Ohio area well completions and new production each increased 60 per cent. in 1928 over the previous year. Gas wells increased only 27 per cent. The ratio of dry holes to total completions was unchanged. Ashland County led with 113 completions; a new pool in the shallow Berea sand near Jeromesville stimulated activity. Licking County in the Clinton deep sand territory, however, lead in new production with 972 bbl. Two other deep sand counties followed closely, Coshocton with 831 bbl., and Muskingum with 718 barrels. The Trenton rock or Lima field of northwestern Ohio declined sharply in oil well completions to 130 for 1928 from 210 for the previous year. New production increased from 3000 to 6100 bbl., the increase coming from the Murphy pool in Liberty township, Seneca County. The total of gas wells was unchanged as compared with 1927. The ratio of dry holes to total completions rose from 13 per cent. in 1927 to 27 per cent, in 1928. The largest producer in the Murphy pool made 1200 bbl, in the first 24 hr. The total depth of the wells in this pool averages 1475 ft.; average initial production, 125 barrels.

Jan 1, 1929

Jan 1, 1967

By David Firewick, Daniel Stewart, Richard Rein

Panel caving of the Henderson orebody began in August, 1976. Fifty months later, on September 10, 1980, the cave zone appeared on surface as a steep-walled cavity positioned directly above the initial cave area. Although surface survey data revealed the development of a slight depression over the production area, surface inspection by geologists, three days prior to breach- ing, resulted in no evidence of impending glory-hole development. Geologic factors such as rock contacts and alteration-zone boundaries had little influence on the location of the initial glory hole. Since initial breakthrough, the glory-hole shape and growth have not directionally followed caveline advance because of topography and faulting. Based on periodic data, mine production has resulted in immediate growth of the Henderson glory hole.

Jan 1, 1984

By J. J. Bikerman

In a recent study' of the martensitic transformation of Cu-Zn ß-phase alloys, it was noted that the MS temperature at the surface was raised due to the loss of zinc by volatilization. It seems likely, therefore, that the MS temperature may serve as a guide for the measurement of composition. From a knowledge of the dependence of the transformation temperature on composition, 2 it should be possible to detect variations in zinc content which are less than 0.1 at. pct by measuring the MS temperature throughout the sample. It is unlikely that an electron microprobe analysis could detect accurately such small zinc losses because the presently accepted limits of accuracy of the micro-probe analysis in simple ternary systems are of the order of 2 to 5 pct of the amount present.3 In the present study, a composition gradient was produced by precipitating the a primary solid solution, and reheating for a very short time within the 0-phase field. The nominal composition, in atomic percent, of the ternary ß-phase alloy used, 64.2 Cu, 34 Zn, 1.8 Si, was selected because it had an MS temperature of +4°C, thereby simplifying the experi-

Jan 1, 1968

By S. Mellgren, W. Opie

AN equilibrium state of importance in the process of electrolytically depositing titanium from fused chloride electrolytes is that which exists between titanium metal, titanium dichloride, and titanium trichloride. This can be expressed by the reaction titanium concentration of the solution, temperature, and the proportion of strontium chloride and sodium chloride in the solution. Procedure The general procedure used consisted of the following steps: 1) Development of an analytical method for determining Ti+2 and total titanium. 2) Preparation of batches of fused salt solutions containing various amounts of total titanium, Ti+2 and Ti+3 3) Blending of the prepared batches and excess titanium metal in Vycor tubes and allowing the solutions to come to equilibrium. By blending, solutions with different total titanium content could be prepared and equilibrium could be approached from the high Ti+2 and low Ti+2 sides. 4) Studying the effect of titanium concentration, temperature, and the mole ratio of the solvent chlorides, SrC1, and NaC1, upon the equilibrium.

Jan 1, 1958

By J. B. Newkirk

ABOUT twenty-seven years ago W. bergl discovered that interesting detail could be seen in an X-ray diffraction spot made with a rock-salt crystal if the recording photographic film were held very close to the reflecting crystal. He also showed that much of this detail could be explained in terms of the deformation structure of the specimen. In the same year, 1931, Fox and parr2 reported that X-ray reflections from a quartz crystal were much more intense while the crystal was undergoing piezoelectric oscillation than when it was at rest. This observation was soon confirmed (and explained in terms of X-ray extinction) by Barrett3 in the United States and by Nishikawa et a1.,4 in Japan. During the next few years Barrett refined Berg's method for making X-ray diffraction micrographs and applied it to the study of metallic crystals. He reported this work in the 1945 annual lecture of the AIME.5 Since 1945 relatively little use has been made of the Berg-Barrett (B-B) method for making diffraction micrographs, though considerable interest in investigating subcrystal structures by other methods has developed. Some of these methods depend upon evaporation6 or chemical etching7 and, therefore, suffer from the occasional intrusion of subtle artifacts such as those recently reported by Hooker for leada and Welsh for aluminum.9 Other methods require the introduction of foreign elements which "decorate" the substructure in some way, thereby rendering it detectable by direct" or indirect1'. visual examination. Still others depend upon complex and often highly questionable analyses of X-ray diffraction line profiles. There have also been a number of related X-ray techniques, such as the Lambot,12 Schulz13 and Merlini and Guinier,14 which have proved to be quite useful for specific applications. Some of these methods give a picture of the substructure which is more or less directly related to the shape and the topography of the specimen. The Berg-Barrett method carries this desirable feature to the limit. Closely related to the B-B method are three photographic X-ray techniques recently described by Lang.15 These methods give beautiful pictures of the internal structure of crystals but are limited by the facts that the required apparatus is rather complex, exposure times are long, and the specimen crystals must be thin. An experimental appraisal which I have recently made of the original B-B method has shown that this simple technique is not only inexpensive and convenient, but can give more information than was apparently realized by its inventors. For example, first-order subgrains in iron-silicon crystals were clearly delineated and their relative orientation subject to description. Also defect structures could be seen within the subgrains and in some materials slip bands could be clearly seen with respect to the topography of the rest of the specimen. This much had already been described by Barrett. However, in the present study it was found that the actual sites of individual dislocations which emerge upon the crystal surface could be located. Furthermore, by a simple procedure, the direction (but not sign) of the dislocation Burgers' vector could be defined as well.

Jan 1, 1960

By R. W. Smith

A study has been made of the crushing and grinding circuits by the Portland Cement Association in nine cement plants. Five of the plants used the wet process and four, the dry method. Both raw and clinker grinding were studied in the four dry processing plants. The raw materials used varied considerably from plant to plant. Actual power consumption data were obtained for the majority of the grinding mills in these plants. Previously representative raw and clinker samples had been obtained from the nine plants, and Bond1 and Hardgrove2 grindability tests were run on these samples. All pertinent data concerning the grinding mills, such as mill size and speed, ball charge size and weight, size distribution of feed, and discharge materials were also obtained. Thus it became possible to calculate the actual horsepower used by the various mills, and to compare this figure to the theoretical horsepower as calculated by several different methods.

Jan 4, 1961

By C. H. Mathewson

BeRyllium, magnesium, zinc and cadmium, together with mercury, constitute a coherent sub-group of the periodic system and these metals, excepting mercury, have been studied in sufficient detail by the new X-ray diffraction methods to prove their common adherence to the hexagonal close-packed type of crystal structure with a progressive increase in axial ratio as we pass through the group from beryllium to cadmium. The first four columns of Table 1 summarize the data on crystal structure of these metals reported in the International Critical Tables.' The last two columns are based on results obtained in the present investigation. Twinning has often been observed in zinc and cadmium. The general aspects of this twinning are abundantly illustrated by photomicrographs, diagrams, etc., in the papers by Romig, and Mathewson and Phillips reported to this Institute in 1927.2 A determination of the composition

By William A. West

One manifestation of anelastic properties in solids is the mechanical elastic aftereffect, which may be described briefly as follows: If a stress is applied to a solid body, a deformation or strain is produced. On removal of the stress, this deformation disappears, at least in part. As a first approximation, this appearance or disappearance of deformation usually has been considered instantaneous. Actually, however, for a very wide variety of substances, on application of stress the instantaneous deformation is followed by a further slow yielding, which continues, although at a rapidly diminishing rate, for as long as the stress is applied. Similarly, on removal of the stress, the instantaneous recovery from deformation is followed by a further slow recovery, which continues, although at a rapidly diminishing rate, often for a long time. This latter phenomenon has been called the "elastic after-effect." Experiments upon the elastic after-effect in metals, when properly designed and when properly interpreted, are capable of giving quite precise information regarding the relation between stress and strain in the various constituent parts of the metal. For example, if certain parts of the metal, such as grain boundaries or slip bands, behave in a viscous manner—that is, if therein—the relaxation spectrum will contain lines or bands associated with the relaxation of shear stress within these parts. No attempts have heretofore been made to utilize elastic after-effects for obtaining such detailed information. The purpose of the present paper is to explore the possibilities of properly designed and interpreted experiments on the elastic aftereffect in metals. Since new procedures and principles are employed in this study, an attempt has been made to record each step taken. Elastic after-effect observations are susceptible of simple interpretation only when the stress level employed is so low that all effects are linear with the stress. Just how low the stress level must be can he determined only by experiment. An advnntage, other than simple interpretation, is associated with low stress levels. When all effects are linear, derived quantities, such as the relaxation spectrum, are independent of the stress distribution. It is, furthermore, possible to employ the type of deformation that is most convenient from the experimental standpoint; for example torsion. It appears that in experiments involving both loading and unloading the following would be observed: I. Instantaneous deformation, recoverable instantaneously in whole, or in part. 2. Delayed deformation, recoverable slowly in whole, in part, or not at all. 3. Permanent deformation, the difference between total deformation and total recovery. In the work here described, unloading experiments only were made. Wires were

Jan 1, 1947

By William A. West

One manifestation of anelastic properties in solids is the mechanical elastic aftereffect, which may be described briefly as follows: If a stress is applied to a solid body, a deformation or strain is produced. On removal of the stress, this deformation disappears, at least in part. As a first approximation, this appearance or disappearance of deformation usually has been considered instantaneous. Actually, however, for a very wide variety of substances, on application of stress the instantaneous deformation is followed by a further slow yielding, which continues, although at a rapidly diminishing rate, for as long as the stress is applied. Similarly, on removal of the stress, the instantaneous recovery from deformation is followed by a further slow recovery, which continues, although at a rapidly diminishing rate, often for a long time. This latter phenomenon has been called the "elastic after-effect." Experiments upon the elastic after-effect in metals, when properly designed and when properly interpreted, are capable of giving quite precise information regarding the relation between stress and strain in the various constituent parts of the metal. For example, if certain parts of the metal, such as grain boundaries or slip bands, behave in a viscous manner—that is, if therein—the relaxation spectrum will contain lines or bands associated with the relaxation of shear stress within these parts. No attempts have heretofore been made to utilize elastic after-effects for obtaining such detailed information. The purpose of the present paper is to explore the possibilities of properly designed and interpreted experiments on the elastic aftereffect in metals. Since new procedures and principles are employed in this study, an attempt has been made to record each step taken. Elastic after-effect observations are susceptible of simple interpretation only when the stress level employed is so low that all effects are linear with the stress. Just how low the stress level must be can he determined only by experiment. An advnntage, other than simple interpretation, is associated with low stress levels. When all effects are linear, derived quantities, such as the relaxation spectrum, are independent of the stress distribution. It is, furthermore, possible to employ the type of deformation that is most convenient from the experimental standpoint; for example torsion. It appears that in experiments involving both loading and unloading the following would be observed: I. Instantaneous deformation, recoverable instantaneously in whole, or in part. 2. Delayed deformation, recoverable slowly in whole, in part, or not at all. 3. Permanent deformation, the difference between total deformation and total recovery. In the work here described, unloading experiments only were made. Wires were

Jan 1, 1947

By Fritz F. Prugger, Peter R. Jones

This paper considers some of the main aspects of underground mining in the flat, rich, but deep lying deposits of Saskatchewan. It briefly describes the pertinent geological features as they relate to mining and the practical de-stressing techniques used to allow productive extraction in the high stress environment present in many of the province’s mines. Mining layouts, materials handling, and the evolution of some of the world's largest mining equipment are examined.

Jan 1, 1983

By H. F. Yancey

PHYSICAL properties have been used for a long time in characterizing different kinds of coal, and physical properties, such as friability and slacking, have been included with chemical properties in grouping coals according to the widely used system of classification adopted by the U. S. Geological Survey. Nevertheless, the usefulness of physical properties for classifying the different ranks or kinds of coal has been limited because it has not been possible to express these properties in definite form as numerical values. Because of the present wide interest in the formulation and adoption of a satisfactory system of coal classification, the Northwest Experiment Station of the U. S. Bureau of Mines, in cooperation with the College of Mines of the University of Washington, has recently completed a study of the physical and chemical properties of approximately 100 different coals ranging from lignite to, anthracite. PURPOSE AND SCOPE For this investigation samples were collected in approximately 45 mines and prospects in Washington and 23 mines in other states. The following studies, in addition to proximate and ultimate analyses, were made of the samples: Determination of (1) friability, (2) slacking or weathering characteristics, (3) yield of products by low-temperature carbonization in a laboratory retort, and (4) agglutinating value. Most of the coals examined were subjected to each of the tests enumerated, but with coal of some ranks this was unnecessary in some instances, and in others it was not feasible to do the work involved.

Jan 1, 1932

By H. D. Peterson, G. E. Butts, J. F. Spisak

In 1978, Anschutz Mining Corp. began efforts to develop the Madison Cobalt Project in southeast Missouri. Preliminary metallurgical studies indicated that intermediate grade cobalt products, suitable for shipment to existing refineries, could be recovered from the sulfide mineralization of the ore body. However, tolling and freight charges were significant, as the refineries were located outside the US. These refineries would not satisfy the goal of strategically insulated production of superalloy-grade cobalt. The acquisition of proven, readily available refinery technologies was then evaluated. However, licensing costs were substantial and the "proven" technologies were not directly applicable to the unique chemistry of Madison materials. Faced with these challenges, Anschutz, in conjunction with the Colorado School of Mines Research Institute, embarked on an effort to develop a sulfate-based separation and refining process. CSMRI performed bench-scale and continuous pilot experiments on solutions generated through other pilot campaigns conducted by Lurgi, Hazen Research, and Sherritt Gordon. The results indicated that cobalt could be selectively extracted from sulfate media using a new generation of organophosphates. The solvent extraction system produced a solution suitable for electrolysis of high-purity cobalt. Preliminary cost studies indicated the novel process was competitive with other refinery systems. Plans to develop the detailed engineering-design information required to commercialize the process were abandoned when the price of cobalt collapsed to less than $17.64/kg ($8.00 per lb).

Jan 1, 1985

By John B. Malcom

The discovery of tungsten-bearing quartz outcrop- pings in Vance County, N. C., by the Hamme brothers in 1942, made international news in the mining industry and was, in fact, one of the major ore discoveries made in the U.S. during the last 25 years. Operations began at the Hamme mine in 1942, but after 16 years of successful operation, the mine was closed down in 1958 under adverse market conditions. By that time, it had produced nearly 20 million lbs of metallic tungsten. Because of the square-set timber mining method then in use, mine operating expenses were high, actually representing 78% of the total operating expenses at the property. In timber work alone, 160 men were employed. Approximately 500,000 bd ft of timber were placed monthly at a direct supply cost of $1.00 per ton of ore mined.

Jan 4, 1962

By Wilbur Nelson

Little drilling has been done in Kentucky and Tennessee in 1923, with the exception of the Kettle Creek area on the Kentucky-Tennessee line. Oil prices fluctuated between $2.86 and $1.36 Per bbl. for light oil. The Kentucky production was slightly over 8,000,000 bbl., being 1,000,000 bbl. less than during 1922. Tennessee production was approximately 8500 bbl., being a decrease of 1000 bbl, over. 1922. During 1923, the first producing well was brought in, in Clay County, Tenn. Production in Tennessee will undoubtedly increase considerably in 1924, and Kentucky production will probably increase slightly. THE year 1923 has been a dull period in oil development in Kentucky and Tennessee, with the exception of the Kettle Creek area along the Tennessee-Kentucky line, in Clinton and Cumberland Counties, Kentucky, and Clay County, Tennessee. The price of oil during the year has been so low that wildcatters have shown little interest in drilling. At the beginning of the year, light oil sold for $2.31 per barrel and medium oil for $2.06 per, barrel. Prices increased to the highest point for the year in February, when light oil brought $2.86 per barrel and medium oil, $2.61. In April, prices had declined 35 c. while in May an additional decline of 25 c. went into effect. During June, prices declined 20 c. per barrel; during July, 45 c. per barrel; remained stationary during August and September, and dropped during November and December to the low price of $1.36 per barrel for light and $1.21 for medium oil. At present, an increase of 29 c. has brought the price of light oil up to $1.55, and indications are that the price will continue to increase during the coming months. It can readily be seen that during 1923 the price of oil was such as to prevent any drilling except that necessary to hold leases and to maintain production enough to take care of overhead expenses.

Jan 3, 1924

By Wm. R. Webster

This is a contribution for the proposed new discussion on the physics of steel. The former discussion on the subject started with the consideration of five papers presented at the Chicago meeting in 1893, and continued for several years. The Suggested Lines of Discussion, prepared by Doctor Howe, covered a wide field and added greatly to the success of the work. Naturally, the first step in a new discussion will be to remodel and bring up to date the old Suggested Lines of Discussion so as to embody all the important advances in the metallurgy of steel that have a bearing on the physics of steel and keep the papers and discussions within the field of work undertaken. This paper will be devoted to the practical application, in rolling steel, of the effects of carbon, phosphorus, and manganese on its tensile strength, with some suggestions on further research work. Dr. J. E. Stead, in his paper Influence of Some Elements on the Mechanical Properties of Steel,' gave a complete review of all that had been done during the past thirty years. He gave full credit to all investigators who worked on these lines, also their results, with his views on same, and in many cases his own results. All of this data and much new valuable information were put in convenient shape for reference and study. To do this required a great deal of work, which is fully appreciated by the steel manufacturers and investigators. The variations in the values given by the different investigators for the increase of the tensile strength of steel for each 0.01 per cent. of carbon, phosphorus, and manganese were largely due to the steels they worked on, the large or small variations in the amount of the elcments present, and the omission to take into consideration all the factors, from the blast furnace through to finished rolled material, that affect the character of the steel. For instance, a poorly made dirty steel requires considerably more carbon to give the same ultimate strength than a well-made clean steel with the same phosphorus and manganese content.

Jan 1, 1922

By Wm. R. Webster

This is a contribution for the proposed new discussion on the physics of steel. The former discussion on the subject started with the consideration of five papers presented at the Chicago meeting in 1893, and continued for several years. The Suggested Lines of Discussion, prepared by Doctor Howe, covered a wide field and added greatly to the success of the work. Naturally, the first step in a new discussion will be to remodel and bring up to date the old Suggested Lines of Discussion so as to embody all the important advances in the metallurgy of steel that have a bearing on the physics of steel and keep the papers and discussions within the field of work undertaken. This paper will be devoted to the practical application, in rolling steel, of the effects of carbon, phosphorus, and manganese on its tensile strength, with some suggestions on further research work. Dr. J. E. Stead, in his paper Influence of Some Elements on the Mechanical Properties of Steel,' gave a complete review of all that had been done during the past thirty years. He gave full credit to all investigators who worked on these lines, also their results, with his views on same, and in many cases his own results. All of this data and much new valuable information were put in convenient shape for reference and study. To do this required a great deal of work, which is fully appreciated by the steel manufacturers and investigators. The variations in the values given by the different investigators for the increase of the tensile strength of steel for each 0.01 per cent. of carbon, phosphorus, and manganese were largely due to the steels they worked on, the large or small variations in the amount of the elcments present, and the omission to take into consideration all the factors, from the blast furnace through to finished rolled material, that affect the character of the steel. For instance, a poorly made dirty steel requires considerably more carbon to give the same ultimate strength than a well-made clean steel with the same phosphorus and manganese content.

Jan 1, 1922

By Howard A. Meyerhoff, J. Earl Frazier

It is not known when silica sand was first noticed along the north coast of Puerto Rico, but the first mention of its occurrence was made in 1922, by N. L. Britton,1 who described its presence in isolated patches extending from Loiza westward beyond Manati. Further observations were made in 1925 and 1926 by Meyerhoff,2 who extended the known occurrences still farther westward to the low hill belt in the Quebradillas limestone immediately south of Hatillo. The extraordinary purity of the sands, which in most localities exhibit no contamination from the non-siliceous materials surrounding them, was quickly appreciated, and the feasibility of utilizing them for the manufacture of glass was investigated, initially by the Committee on Mineral Resources3 and later (1936) by the Puerto Rico Recon-structionAdministration and by H. C. Ray, mining engineer of the Insular Bureau of Mines. In 1934 samples submitted to the Hazel Atlas Glass Co., of Washington, Pennsylvania, were reported to have the composition as shown in the table on column two. Appreciation of the quality of the sand prompted geological and quantitative studies of the deposits, as well as cornmercial investigations to determine the feasibility of utilizing it locally or on the mainland for the manufacture of glass containers. Distribution of the Sands The quartz sands consistently lie within the outcrop area of the Quebradillas limestone, the youngest of the Miocene formations in the Tertiary coastal plain that fringes the northern coast of the Island. Many of the deposits are closely associated with limestone outcrops, but some appear to be embedded in lagoonal sediments at some distance from rock exposures, and at least one deposit, near Dorado, has been reworked by waves and littoral currents. With this single known exception, the deposits consist of irregular, patternless patches of white sand, which have sharply defined contacts with the surrounding material. Although patches of sand are present in a 90-km. belt that is not more than 5 km. wide, extending from Loiza to Hatillo, they attain maximum size, purity and number in the north central coastal area between Dorado and Barceloneta. Fifty separate deposits have been mapped in Lago Tortuguero and to the south of it, some as small as 50 ft. in diameter but

Jan 1, 1948

By J. Earl Frazier, Howard A. Meyerhoff

It is not known when silica sand was first noticed along the north coast of Puerto Rico, but the first mention of its occurrence was made in 1922, by N. L. Britton,1 who described its presence in isolated patches extending from Loiza westward beyond Manati. Further observations were made in 1925 and 1926 by Meyerhoff,2 who extended the known occurrences still farther westward to the low hill belt in the Quebradillas limestone immediately south of Hatillo. The extraordinary purity of the sands, which in most localities exhibit no contamination from the non-siliceous materials surrounding them, was quickly appreciated, and the feasibility of utilizing them for the manufacture of glass was investigated, initially by the Committee on Mineral Resources3 and later (1936) by the Puerto Rico Recon-structionAdministration and by H. C. Ray, mining engineer of the Insular Bureau of Mines. In 1934 samples submitted to the Hazel Atlas Glass Co., of Washington, Pennsylvania, were reported to have the composition as shown in the table on column two. Appreciation of the quality of the sand prompted geological and quantitative studies of the deposits, as well as cornmercial investigations to determine the feasibility of utilizing it locally or on the mainland for the manufacture of glass containers. Distribution of the Sands The quartz sands consistently lie within the outcrop area of the Quebradillas limestone, the youngest of the Miocene formations in the Tertiary coastal plain that fringes the northern coast of the Island. Many of the deposits are closely associated with limestone outcrops, but some appear to be embedded in lagoonal sediments at some distance from rock exposures, and at least one deposit, near Dorado, has been reworked by waves and littoral currents. With this single known exception, the deposits consist of irregular, patternless patches of white sand, which have sharply defined contacts with the surrounding material. Although patches of sand are present in a 90-km. belt that is not more than 5 km. wide, extending from Loiza to Hatillo, they attain maximum size, purity and number in the north central coastal area between Dorado and Barceloneta. Fifty separate deposits have been mapped in Lago Tortuguero and to the south of it, some as small as 50 ft. in diameter but

Jan 1, 1948

By Kirby D. Mellegard, Ralph A. Wagner, Paul E. Senseny

Six creep laws for salt, each fitted to the same laboratory data base, are used in a numerical model of the deformation of an opening in salt to determine the influence of creep law form on the predicted closures. Results show that predicted closures can be very sensitive to the functional form of the creep law chosen to model the laboratory data.

Jan 1, 1982