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By N. A. Gokcen, R. A. Dodd

Solubility of nitrogen in liquid iron-manganese system at 1550°C and one atmosphere pressure has been determined by a simple method. Results show that the solubility increases from 0.040 pct for pure iron to 1.41 pct for pure manganese. DETERMINATION of the solubility of gases in volatile metals. and alloys by the well-known Sievertsl method is unreliable. This is particularly true for the Fe-Mn system since Mn vaporizes readily from the alloys containing as little as 2 pct Mn, and, upon condensing on the cooler parts of the apparatus, it absorbs large amounts of nitrogen. Further, the condensing Mn vapor interferes with the usual method of temperature measurements with an optical pyrometer.

Jan 1, 1962

By F. Keller, E. H. Dix, L. A. Willey

The consideration of alloying elements for aluminum has led to a series of investigations of the equilibrium relations between aluminum and those alloying elements. Therefore, the aluminum end of the aluminum-antimony diagram has been studied. The general form of the aluminum-antimony equilibrium diagram has been worked out by Campbell and Mathewsi and by Tammann.2 Canlpbell and mathews described principally the beginning of solidification. They found the curve of beginning of solidification rising gradually from the melting point of pure alunlinum to a maximum at about 67 per cent. aluminum. After a slight lowering of the curve at a little greater antimony concentration the curve again rises to a maximum at 18.4 per cent. aluminum, which corresponds to the compound AISb. The curve then drops to the melting point of pure antimony. Tamrriarln explained the maximum occurring at about 67 per cent. aluminum as the result of the slow formation of the single compound AISb. The space lattice of the compound AISb, according to Owen and Preaton,³ is face-centered cubic, the antimony atoms being intermeshed with an identical aluminum lattice. Very little, if any, work has been done on aluminum alloys containing small amounts of antimony. The Present Investigation It has been the purpose of this investigation to determine the solid solubility of antimony in aluminum and also to investigate the eutectic temperature and concentration. The experimental work has been carried out in a manner similar to that described in a previous paper4 from this laboratory.

Jan 1, 1931

By Charles Barron McIntosh

BECAUSE of the well known relationship between a low atmospheric pressure and increased amounts of methane in coal mines, attempts have been made to find associations between low pressures and coal mine explosions. An early study by F. Able disclaimed this relationship. He found that half the explosions took place during a rising barometer when methane content in a ventilated mine would be decreasing. A more recent study by C. L. Hosler revealed a close relationship between anthracite mine explosions and low atmospheric pressure. Bituminous coal mine explosions, where coal dust as well as methane can be exploded, were found to be more closely associated with a rising pressure following a low barometer than with the falling or low pressure period.

Jan 10, 1957

(The following list contains the names of those members of the Institute of whose connection with military service we have only recently become acquainted; it also includes the navies of a few who have recently been promoted or transferred. A complete list was published in the Year Book, issued as a supplement of the Bulletin for March, 1918.) ARNOLD, RALPH, Member of. Board of Tax Reviewers in connection with the administration of the War Revenue Act. BACON, RAYMOND F., Lieutenant-Colonel, Chemical Service Section, N. A., A. E. F. BALLENBERG, A. G., 1st Lieutenant, Ordnance Dept., U. S. A. BARCUS, WALTER J. E., Captain, Gun Division, Ordnance Officers' Reserve Corps. BECKWITH, H. T., Captain, Engineer Reserve Corps, Headquarters Co., 312th Engineers.

Jan 6, 1918

(This list. includes only those who have entered military service within the past month, or whose entry has only recently become known to us; it also includes a few names of those whose titles or assignments have been changed within the month. A complete list will he found in the Year Book mailed with this Bulletin. Another Honor Roll is maintained in the reception room of the Institute.) ALDEN, HERBERT W., Lieutenant-Colonel, Ordnance Dept. ALDER, ALFRED; Engineers' Reserve Corps. ALFORD, NEWELL G., Sergeant, Bureau of War Risk Insurance, Headquarters 84th Division. AMBLER, HARRY A., Lieutenant, 30th Infantry. ANDERSON, GEORGE K., JR., Sec. C, 1st Co.; 3d Officers' Training Camp. AYER, -FRANK A., 1st Lieutenant, 43d Squadron, 3d Prov. Regiment, Aviation Camp.

Jan 3, 1918

By W. C. Knopf, G. Samsel

For several years International Minerals & Chemical Corp. has used a radiation method to assay potassium content of products from potash and feldspar beneficiation. The procedure is rapid, accurate, and inexpensive and is easily handled, if necessary, by nontechnical personnel. Data are presented to show the accuracies that may be expected if the technique is used for control of pilot plants or large- scale plants. Natural potassium is composed of three isotopes -K39, K40 and K41. Five other isotopes, artificially produced, have been detected. In natural potassium only the K40 isotope, with a half life of 1.4 x 109 years, is radioactive. Its modes of decay are beta and gamma rays, positrons, and x-rays. Only the more abundant beta rays, however, are important in radiation measurements using geiger tubes.

Jan 10, 1958

By Thomas A. Wright

No symposium on die casting could be complete without consideration of the methods of formula and impurity control. No consideration of control would be complete without discussion of that new tool of the analytical chemist and inspector, the quartz spectrograph. Just as there is an increased appreciation of the possible applications of the die-casting process and of die castings, so too is there, slowly but surely, of the spectrograph. At present the role of the instrument might well be compared with that of brass or magnesium die castings. Neither is as widely understood or known as they will be. Product specifications are increasing and are getting more explicit and often more rigid. The designer, metallurgist and production engineer or superintendent will be forced to depend more and more on the chemical laboratory. Sampling, as well as analyses, testing and inspection problems will grow. The chemical laboratory must meet its increased responsibility and use of the spectrograph will become more common. Advantages of increased precision, greater speed, lessened labor and often lower costs cannot be ignored. It will be the purpose of this paper in part to outline the respective fields of chemical and spectrographic analyses and to indicate where one may overlap the other and in part to indicate certain possible sources of contamination of zinc-base die-cast alloys in particular. COMPOSITION Aluminum.-Aluminum die castings are expected to conform to the specifications of the American Society for Testing Materials1† and the Society of Automotive Engineers2. The A.S.T.M. has recognized seven

Jan 1, 1935

By Ralph H. Sweetser

At the joint session of Blast Furnace and Open Hearth Committees, April 7, 1937, at Birmingham, the subject of the quality of basic open-hearth pig iron was so well presented and discussed from so many different viewpoints that it was the general opinion that progress had been made and that such meetings were conducive to the advancement of the art of making pig iron of the right quality for the open-hearth man to produce the most satisfactory quality of steel. It was agreed that there is a decided differentiation between the chemical analysis of pig iron and the "quality" of pig iron. Paul J. McKim said that open-hearth furnace operators frequently make reference to certain types of iron as "bad iron," "dirty iron," "cold metal," etc., claiming that when using these irons, although they are within specified chemical analysis, it is impossible to produce quality steel. Mr. McKim gave a list of the suggested causes of those "certain types" of bad irons that have a thoroughly respectable analysis but a thoroughly disreputable character. Another open-hearth man, P. A. MacIsaac, of Nova Scotia, said that: The effects of iron that is below standard in analysis or in that mysterious property called quality, are well known to all open-hearth operators. It has been shown that iron of this type results in the production of steels on which the rcjections of finished product run high. What is to be done about it? I would say that the burden of producing high-quality iron should be placed squarely on the shoulders of the blastfurnace man, even as that of making good steel is shouldered by the open-hearth man. It is the purpose of this paper to bring out into the open this "mysterious property called quality"; that is, in those "certain types" of basic pig iron that make it impossible to produce quality steels; and at the same time to point the way for the blast-furnace man to be able to shoulder the burden that Mr. MacIsaac and all other open-hearth men and foundry-men have placed upon him. Silicon, sulphur, phosphorus and manganese are not the guilty elements because these are known, specified and usually kept within the

Jan 1, 1938

By Ralph H. Sweetser

At the joint session of Blast Furnace and Open Hearth Committees, April 7, 1937, at Birmingham, the subject of the quality of basic open-hearth pig iron was so well presented and discussed from so many different viewpoints that it was the general opinion that progress had been made and that such meetings were conducive to the advancement of the art of making pig iron of the right quality for the open-hearth man to produce the most satisfactory quality of steel. It was agreed that there is a decided differentiation between the chemical analysis of pig iron and the "quality" of pig iron. Paul J. McKim said that open-hearth furnace operators frequently make reference to certain types of iron as "bad iron," "dirty iron," "cold metal," etc., claiming that when using these irons, although they are within specified chemical analysis, it is impossible to produce quality steel. Mr. McKim gave a list of the suggested causes of those "certain types" of bad irons that have a thoroughly respectable analysis but a thoroughly disreputable character. Another open-hearth man, P. A. MacIsaac, of Nova Scotia, said that: The effects of iron that is below standard in analysis or in that mysterious property called quality, are well known to all open-hearth operators. It has been shown that iron of this type results in the production of steels on which the rcjections of finished product run high. What is to be done about it? I would say that the burden of producing high-quality iron should be placed squarely on the shoulders of the blastfurnace man, even as that of making good steel is shouldered by the open-hearth man. It is the purpose of this paper to bring out into the open this "mysterious property called quality"; that is, in those "certain types" of basic pig iron that make it impossible to produce quality steels; and at the same time to point the way for the blast-furnace man to be able to shoulder the burden that Mr. MacIsaac and all other open-hearth men and foundry-men have placed upon him. Silicon, sulphur, phosphorus and manganese are not the guilty elements because these are known, specified and usually kept within the

Jan 1, 1938

(This list includes only those who have entered military service within the past month, or whose entry has only recently become known to us; it also includes a few names of those whose titles or assignments have been changed within the month. The last complete list was printed in Bulletin No. 131, November, 1917. A complete Honor List is maintained in the reception room at the office of the Institute:) AARONS, J. BOYD, Captain, 4th Reinforcements, 11th Infantry, Australian Imperial Force. AHBE, F. R., Captain, 33d Engineers. AMBLER, HARRY A., 30th Infantry, Camp Greene, Charlotte, N. C. ALFORD, NEWELL G., Sergeant, Headquarters 84th, 9th Division, Camp Zachary Taylor, Ky. ANDERSON, ALEXANDER, Lieutenant, Royal Garrison Artillery. ANDREWS, CLARENCE W., 1st Infantry Co., Officers' Training Camp, 83d Div., Camp Sherman.

Jan 2, 1918

By Raymond A. Bradbury

The first diesel-powered Scooptram has now been in service for 21/2 yr at the I-C mine of Martin County Coal Corp. It has become the workhorse of the operation, being used around the clock many days. The fleet of nine 20-ton capacity Teletrams used behind three Jeffrey Heliminers now have more than 1 1/2-yr experience in the Coalburg mine. They have been exposed to some difficult conditions which, include steep grades, water, mud, and rutted roadways. These units have proven to he both rugged and powerful. The safety components and shutdown systems make these haulage units very safe for underground coal mines. A clean-burning engine, a satisfactory exhaust conditioning system, and good ventilation are the keys to maintaining a safe and healthful atmosphere for the underground operators and other employees.

Jan 1, 1976

By Irving Hale

The superiority of electric power for mining purposes was recognized in a general way as soon as the electric motor be-

Jan 1, 1897

By K. J. Anusavice, R. T. DeHoff, H. Oikawa, J. J. Pinajian

STUDIES of nickel self-diffusion and impurity diffusion in pure metals and alloys have, for the past two decades, employed predominantly the nickel radio-However, because of the low energy of the emitted particle, careful and time-consuming techniques must be used to obtain reproducible measurements. In our studies of nickel diffusion into copper, we have recently used Ni66 [Td1/2: 55 hr; : 0.20 Mev (100 pet)] which decays to it much more suitable as a tracer because of the presence of the high-energy y radiation from the cu66 daughter. Although the half-life of Ni66 is appreciably shorter than that of Ni63, the useful working lifetime of a small quantity, " 10 mc, is about 1 month. preparation bf Ni66. he Nis6 radioisotope was produced at Oak Ridge National Laboratory by means of a double (n,y) reaction:

Jan 1, 1969

By W. P. Haynes

DuRing 1939. there were no discoveries of oil and gas in Rumania worthy of mention. and the only important extension was the anticipated

Jan 1, 1940

By Elmars Ence, Harold Margolin

A. J. Goldak and J. Gordon Parr (University of Alberta) —While we appreciate the difficulties involved in any investigation of this system, and we wish to congratulate the authors on their comprehensive efforts, there are several aspects of their paper that are not clear to us. 1) If the 6 phase is, in fact, isomorphous with Ti3Sn, it should not be designated Ti,Al. An 4B structure cannot be isomorphous with an ordered structure of the DO type. Anderko et al.' suggested that the structure be called Ti3A1, and we believe this to be a more reasonable designation. The confusion is compounded when the authors designate the phase Ti3Al—yet the composition limits of this phase (according to their diagram) are approximately Ti,A1 and Ti,Al. Further, while Pietro-kowsky is said to have pointed out that the structure of the 6 phase is isomorphous with Ti3Sn, we understand that this was only a suggestion that was not confirmed. Margolin and Ence do not appear to have presented any evidence to support the suggested isomorphism. 2) In referring to the precipitation observed microscopically during the initial breakdown of high A1 a during quenching, the authors state that "such precipitation is not likely to be detected by Debye-Scherrer techniques". We suspect that if the precipitate was visible by optical microscopy, it must have at least one dimension of the order of 1 or greater, and would therefore be readily detected by diffraction techniques. 3) The authors state: "The basis for this suggestion (that 6 forms peritectically P + L—6) is the observation that the ,'3 + 6 and 6 phase fields were

Jan 1, 1962

By James Terry Duce

Production of oil in Bahrein for the war years was as follows: YEAR BBL PER YEAR Prior to 1939 . . . . . . . . . . . . . . 22,287,055 1939 . . . . . . . . . . . . . . . . . . . . . . 7,588,554 1940 . . . . . . . . . . . . . . . . . . . . . . 7,073,919 1941 . . . . . . . . . . . . . . . . . . . . . . 6,794,157 1942 . . . . . . . . . . . . . . . . . . . . . . 6,240,627 1943 . . . . . . . . . . . . . . . . . . . . . . 6,571,609 1944 . . . . . . . . . . . . . . . . . . . . . . 6,713,795 1945 . . . . . . . . . . . . . . . . . . . . . . 7,308,938 Total to Jan. 1, 1946 . . . . . . . . 70,578,654

Jan 1, 1946

By B. Foley

IN THE first report1 disks of steel of known composition and history were exposed, under carefully prescribed conditions, to impacts of explosion products resulting from the explosion of 50-gm. charges of explosives having well-determined rates of detonation, or to impacts of a weight of known mass, falling through measured distances. There were available at the Bureau of Mines Experiment Station five explosives, having rates of detonation of 5716, 4470, 3190, 2296, and 1523 meters per second. It being desired to continue this exposure downward, and no explosives with a lesser rate of detonation being at hand, resort was had to the impact of a falling weight, the differences in the velocity of impact being attained by varying the height from which the weight was allowed to fall. It was expected by this means to demonstrate experimentally that the development of Neumann bands was determined by the suddenness of the deformation of the metal in which they were produced. But while progressive deformations were obtained with the explosive arges, the falling-weight method failed because the tup was ogressively deformed, also the disks were so flattened as to be unfit for metallographic examination. A return, therefore, has been made to the use of explosives as the source of energy, an air-gap being interposed between the charge of explosive and the disk, as the effect diminishes as the function of the distance between the charge and the object on which the products of its explosion, or the shock wave from its detonation, impinge. The details of the arrangement of the tests by the air-gap method were the same as those described by Foley and Howell,2 except that after the system had been set up and the desired apparent specific gravity for the explosive

Jan 2, 1926

By R. H. Singleton

ThE purpose of this investigation was to determine the effect of cerium upon the nonmetallic inclusions found in cast and wrought steel containing various amounts of sulfur, oxygen, and nitrogen. Interest of the Physical Metallurgy Laboratory of the Watertown Arsenal Laboratories in this type of research was stimulated by the reports from industry that rare-earth metals imparted beneficial effects upon the mechanical properties of steel, but that the mechanism was not understood. Berry and Dorvel' found that misch metal improved the impact properties of aluminum-killed cast steels. They reported that the rare earths modified the intergranular-film type nonmetallic inclusion, present with aluminum as the sole deoxidant, to a randomly distributed globular type. Lilliequist and Mickelson2 observed the improvement of ductility and toughness of quenched and tempered cast steels through rare-earth additions. They also observed the change from angular to duplex inclusions when rare earths were present. They con-

Jan 1, 1960

By E. J. Schmitz

The existence of copper-ores in the Permian measures of Texas has long been known, and these ores have been, from time to time, the object of geological researches and mining

Jan 1, 1897

(This list includes only those who have entered military service within the past month, or whose entry has only recently become known to us; it also includes a few names of those whose titles or assignments have been changed within the month. The last complete list was printed in Bulletin No. 131, November, 1917. A complete Honor List is maintained in the reception room at the office of the Institute.) BANKS, HAROLD P., 2d Lieutenant, Ammunition Train, 2d Division, U. S. A. BARKER, L. M., Co. B., 62d Infantry. BENHAM, W. M., Sergeant, Co. H, 158th Infantry. BOUDWIN, WALKER J., Co. C., 25th Engineers, Camp Devens, Ayer, Mass. BOWLES, MARTIN F., 2d Lieutenant, Co. B., 355th Infantry. BURG, ROBERT S., Instrument Sergeant, Headquarters Co., 340th Field Artillery, N. A. CHALMERS, JOHN W. P.; Signal Depot, Royal Engineers. CHETNEY, P. C., Corporal, 340th Field Artillery, Headquarters Co. CLARK,. WILL L., Federal Fuel Administrator for Arizona. COFFEY, George W., Lieutenant, Engineer Section, Officers' Reserve Corps.

Jan 1, 1918