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By Davey FJ

The Hikurangi Margin of eastern North Island New Zealand represents the feather edge of the over-riding Indo-Australian Plate at its convergent boundary with the subducting Pacific Plate. Towards the south, convergence becomes slower and increasingly oblique, and sediment supply from the Southern Alps becomes increasingly rapid. In this environment a 150 km wide, imbricate thrust, accretionary prism has grown since the Miocene, uplifting slope ridges and basins and a range of coastal hills. Offscraping of thick, axially transported, trench-fill turbidites begins in a zone of proto- thrusts, which extends up to 25 km beyond the principle, slope-toe, deformation front. On the slope, landward tilted, trench-slope basins are separated by ridges. The ridges ride up on thrusts that sole out at a major decollement. The decollement dips landwards at 3 degrees to a depth of 14 km at the coast, where it coincides with an onshore zone of high seismicity. Beneath the decollement, about 1 km of consolidated, oceanic sediment is going under the margin with the underlying oceanic basement. Some of these sediments may underplate the frontal ranges to the west and geochemical evidence of subducted sediment is found in the volcanic zone beyond. A rapid decrease in the width of the accretionary prism to the north is associated with a decrease in sediment supply and perhaps with a dislocation in the downgoing plate. To the south, the accretionary prism narrows, swings westward, and merges into the zone of very oblique collision that marks the transform between mirror image subduction to north and south of New Zealand.

Jan 1, 1987

This paper considers three aspects of cemented fill practice and research in Mount Isa. Firstly, an account is given of the use of Portland cemented hydraulic fill both in MICAF sills and in recovery of major horizontal pillars in the 650 copper orebody, where, during mining, cemented fill has regularly been exposed on unsupported vertical faces up to 90 ft high. In the paper the main considerations are the role and specifications of the fill used but also included is a brief description of fill preparation and placement.Data resulting from a Portland cemented hydraulic fill sampling, curing and testing campaign covering about 18 months of operating practice are presented, analysed, and discussed. These yield information indicating the mode of operation of a fully-automated fill preparation station, as well as a means of comparing field and laboratory strength results. A technique with potential for use as a fill quality control without actual strength testing is also described. The data collected showed that the fill station can operate within tolerances set on product quality, that laboratory and field strength results are comparable, and that rapidly obtained fillsample properties such as moisture content and void ratio can be related to cement content and strength, and hence used for quality control.Results of a fill research programme conducted by the author in Mount Isa since early 1968 are presented involving Portland cemented hydraulic fill and alternative, cheaper additives for cementing hydraulic fill. The most significant alternative to Portland cement is quenched and ground copper reverberatory furnace slag, whIch behaves as a pozzolan, reacting strongly with any available lime to produce cementitious hydrated calcium silicates and allowing Portland cement reductions of at least 50 per cent without strength loss.

Jan 1, 1971

By M A. Faizulin, N G. Stukalova

The present till now practice of averaging of ore by metal content at mining-dressing enterprises does not allow evaluating objectively really existing regularities of dressing process. The processing of large statistical data by specially designed methods has revealed the relationships of extracted mass of metals into concentrates when processing of ore at preparation plants. The analysis of the obtained relationships points to necessity of timely control by flows of ore with due account of different sorts of metal. For this problem solving it is offered to use specially designed methods on carrying out of calendar planning of a mining and shipment of ore at open casts, based on ranked arriving of flows of different sorts ores to preparation plant. The given methods includes economic-mathematical model forming and its implementing by worked out method. The formed model allows taking into account different technological and organisation limits, typical operation conditions of open cast and preparation plants. Using this methods of control of mining operations and designed on its basis the complex of software allows increasing volume of metals, extracting into concentrate, up to two per cent without any additional costs and saving of the existing technological schemes at preparation plant.

Jan 1, 2003

The Hodgkinson goldfield contains over 50 separate lodes which have produced 9.7 tonnes of gold from ore averaging 37 g/t. The gold-quartz.lodes are spatially separate from tin and base metal mineralisation, associated with Permo-Carboniferous granitoids in the province. Host rocks consist of sub-greenschist metamorphic grade shale, conglomerate, sandstone, spilite, chert and melange. Oreshoots average 100 x 30 x I m in Size and are contained in cross-cutting quartz. filled with steep-dipping shear zones. Mineralisation in the quartz. consists of gold with minor arsenopyrite, pyrite, galena, and sphalerite with rare calcite. Scheelite and stibnite are aSSOCIated locally but are not necessary proximal or coeval. Alteration is restricted to centimetre-scale phyllic selvedges adjacent to the veins and veinlets.Most of the lodes and vems occur within six main 1.5 x 0.25 km mineralised areas whIch may indIcate separate areas of fluid flow and precipitation. Ore controls differ m melange- and sandstone-hosted lodes but several features are common to all the oreshOOlS. Most of the lodes occur within zones of duauon that are caused by splaymg, refraction through carbonaceous shale-sandstone contacts, or by rolls and changes in strike and dip.Lithologic contacts may act as areas of permeability and chemistry contrast which focus fluid and precipitation. Tensional veins are common between parallel shear zones and curved spur veins occur both in the hangingwall and footwall of the main fissure. Intersections and contacts may have enhanced local fluid flow in many of the areas.

Jan 1, 1991

By C E. Loayza, R M. Pinto, J G. G=mez

The Yanacocha District is located 20 km north of the city of Cajamarca, in the Northern Andean Orogenic belt of northern Peru.Gold production may have occurred as early as Incan times (Paverd, 2000), but modern exploration that began in the 1960s targeted only copper and silver. Newmont Mining Corporation, BRGM and Compa±fa de Minas Buenaventura began exploring for gold in 1983, with Newmont as operator.Initial drilling took place in 1985. By 1992 a reserve of 1.28 million ounces was reported (Teal et al, 2002).Production began at the Carachugo deposit in 1993.Current reserves are 31.7 million ounces at $US 325 per ounce at a grade of 1.03 ppm (Newmont Annual Report, 2003).The operating company, Mineral Yanacocha SRL (Newmont 51 per cent, Buenaventura 44 per cent and International Finance Corporation five per cent) produced 2.85 million ounces in 2003, making Yanacocha one of the largest gold mining operations in the world. The district is made up of a series of epithermal, high sulfidation style gold deposits and one gold-rich gravel deposit (La Quinua), aligned in a NE trend.La Quinua is not discussed in detail in this paper. The bedrock deposits are hosted in a Miocene volcanic package, the Yanacocha Volcanic Complex that also trends NE.Re gional NW striking Andean faults intersect the NE striking Trans-Andean Chicama-Yanacocha structural corridor (Turner, 1997), localising the district mineralisation. These two structural orientations dominate the district, controlling breccia and intrusion locations, and gold mineralisation. Discontinuous EW oriented fracture zones are interpreted as extensional and locally are important in controlling gold mineralisation.

Jan 1, 2004

By N Strong

Cracow is a high-grade; low-tonnage underground gold mine located approximately 500 km north-west of Brisbane in Central Queensland. It is a steeply dipping, narrow vein, epithermal gold and silver deposit that is accessed via a decline from surface. Cracow is owned by joint venture between Newcrest Mining (70 per cent) and Sedimentary Holdings (30 per cent). The orebodies are 5 m wide on average and the ore is extracted via sublevel open bench stoping. Stopes are extracted to a strike of approximately 25 m before being backfilled with waste. Prior to the introduction of electronics, the mine would remove a small amount of the previous backfill out to create a void, and then begin blasting two to three rings at a time, with the ore being extracted between each blast. This method caused the ore to be blasted onto the waste backfill resulting in dilution of the high-grade ore. It also meant that the extraction of each stope took a number of weeks and numerous blasting events. In the fourth quarter of 2005, the mine struck a geotechnically sensitive stope, where all 20 rings had to be extracted in a single shot or risk possible geotechnical problems that could sterilise the ore. Due to the limitations of NONEL« delay detonators the mine could not fire all the rings in a single shot and needed to use an electronic detonator system to extract the stope. Some unexpected benefits to the mine were increased fragmentation, reduced vibrations, reduced dilution, improved efficiency and improved hanging wall and footwall conditions. After the success of this first electronic shot, the mine has since moved to firing all their stopes with electronic detonators. With electronics the mine has been able to fire much larger blasts, and has in fact moved to firing their blasts in the opposite direction, firing towards the draw point instead of into the waste backfill, thus reducing ore dilution.

Jan 1, 2008

By Kidman B. E

The Fitzpatrick area is the deepest section of the North Mine, with the orebody located between 1450 and 1800 m below the surface and some 600 m NE of the main No. 3 Shaft orebody and separated from it by the intensely sheared Globe Vauxhall Shear Zone. Development towards the Fitzpatrick area commenced in 1977 after earlier initial exploration drive development. However, it was not until 1982 that mining in the Fitzpatrick area actually began with the silling out of No. 36 level at a depth of some 1600 in. Since that time mechanised cut and fill mining from an incline ramp system with connecting stope accesses has progressed some 25 m above No. 36 level. Initial sill development on No. 37 level at 1660 m depth also commenced in July 1987 to further develop the Fitzpatrick area.

Jan 1, 1988

By G Showers, R Triglavcanin

The complexity of understanding the whole thickening process to achieve real performance improvements cannot be underestimated. The last significant change in feedwell design was more than 15 years ago with the introduction of self-dilution systems û firstly with OutotecÆs Autodil, followed by FLSmidthÆs E-Duc. Now, following many years of extensive in-house research, including close collaboration with AMIRA and the CSIRO, Outotec has launched the next generation Vane Feedwell. The Vane Feedwell has been globally patented and installed at various sites. This paper briefly outlines the feedwellÆs development using CFD modelling and its subsequent performance in a æreal lifeÆ site installation. Plant results of the first commercial Vane Feedwell, in a mineral sands application, are discussed. The Vane Feedwell was retrofitted so comparative data of pre- and post-installation is shown.

Jan 1, 2009

The occurrence of metallic minerals in Australia to the time of the proclamation of South Australia as a Colony in 1836 was unknown. It is, therefore, perhaps, surprising that British settlers arriving in the Coromandel included among their number a German scientist Johannes Menge who had been appointed by the South Australian Company to the post of Mine and Quarry Agent and Geologist on 1 July 1836. His instructions were to `explore the natural productions of the Colony above and below ground and to superintend the working of quarries of stone and slate, the boring for water, metal, lead, coal and other mines at a salary of ú150 per annum for one year and for as much longer as the Company require your services not however exceeding five years'. In the event, he was to have little influence on those matter.

Jan 1, 1993

The efficient development and exploitation of an orebody relies on an understanding of the mineral characteristics of the deposit. This information is valuable throughout the mining cycle - during exploration, assessment, testing, design, operation and rehabilitation. Problems can arise at each stage if there is an inadequate appreciation of the mineralogy involved and its effects on the treatment process. Modern image analysis systems now permit a more quantitative understanding of the mineralogy of an ore to be gathered. Where previously the metallurgist had to rely on qualitative information to guide technical decisions, it is now possible to give numerical estimates to the compositional and textural properties which govern the mineral concentration processes. Ore samples can be characterised according to modal abundances, mineral grain size parameters and mineral associations, all of which affect the liberation and concentration of the values. The paper will discuss the application of quantitative process mineralogy by considering a number of case studies. These include: ore characterisation to assist in exploration, assessment and mine planning; modal analysis of complex mineral suites to assist in the evaluation of ores, the deportment of values between products and the recovery or loss of these values; liberation analysis for ore testing, plant optimisation and performance monitoring; and characterisation of tailing to guide estimates of leachability, stability and rehabilitation options.

Jan 1, 1998

By Blom MS

Two well-developed styles of mineralization occur in the Nevados del Famatina mining district, Famatina ranges, La Rioja province, Argentina. Porphyry molybdenum- copper-gold mineralization and high level acid sulphate alteration/mineralization (Nevados del Famatina) are related to intrusion of the Pliocene Mogote rhyodacite porphyry complex. High sulphidation epithermal mineralization (La Mejicana) is developed peripheral to the Nevados del Famatina deposit. Both are hosted mainly by the Ordovician Negro Peinado metapelites.At Nevados del Famatina, five mineralized fracture events have been identified and correlated with four distinct alteration assemblages. Stage I (barren quartz) and stage II (molybdenite¦sphalerite¦pyrite) mineralization are associated with a K-silicate alteration assemblage of K-feldspar+biotite+quartz+magneti te¦ilmenite¦anhydrite. Stage III (bornite+pyrite+sphalerite+molybdenite ¦chalcopyrite¦idaite) and stage IV (chalcopyrite+pyrite +sphalerite+gold¦tennantite-tetrahedrite) mineralization are related to a quartz-sericite assemblage of quartz +phengite+illite+pyrite+rutile. Stage V mineralization is divided into two substages. Stage Va (chalcopyrite +pyrite+sphalerite¦ tennantite-tetrahedrite ¦ tellurides ¦ gold ¦enargite¦famatinite¦stibnite¦molybdenite) is related to a sericite-clay assemblage of quartz+illite+kaolinite ¦montmorillonite¦alunite. Alunite-kaolinite alteration (alunite+pyrophyllite+kaolinite+ aluminum - phosphate -sulphate minerals ¦illite¦fluorite¦corundum¦anhydrite) occurs in the upper part of Nevados del Famatina associated with the later stage Vb (quartz+famatinite +chalcopyrite+covellite + chalcocite ¦ marcasite ¦ enargite ¦ luzonite¦sphalerite¦melnikovite) mineralization.

Jan 1, 1990

By S Miller, R Smart, J Thomas

Single-addition and sequential net acid generation (NAG) experiments were carried out on natural and prepared samples with varying contents of organic matter and pyritic S. Results show that carbonaceous matter can produce significant quantities of organic acids during peroxide oxidation in the NAG test, which leads to overestimation of acid-forming capacity and misclassification of benign samples as potentially acid forming (PAF). Organic matter effects were most pronounced in samples with low S (less than 0.5 per cent) and total organic carbon (TOC) contents of greater than seven per cent. The single-addition NAG test will tend to overestimate acid potential in samples with little or no pyrite and high organic matter content, potentially leading to sample misclassification. High pyritic sulfur samples tend to show little difference in single-addition NAG acidities with increasing organic matter, and it appears that pyrite is preferentially oxidised by peroxide when present in significant concentrations (greater than one per cent pyritic S). In sequential NAG tests overestimation was greatest in samples with little or no pyrite, but highly carbonaceous (>20 per cent TOC) pyritic samples were affected in later stages as the pyrite was depleted. A modified NAG method is proposed to account for the relative proportions of pyrite derived acidity and organic acidity in a given NAG solution.

Jan 1, 2003

It is proposed to deal with those raw materials which are produced in South Australia to meet the needs of the country's steel industry. They are chiefly, iron ore, limestone and quartz.Iron ore and limestone are fed to the blast furnaces of Newcastle and Port Kembla together with coke to produce the hot metal charge for the open hearth steel furnaces.They are also qsed in the raw state in the steel furnaces to assist in the conversion of the hot metal to steel. The iron ore is quarried from' Iron Knob and shipped from Whyalla to Newcastle and Port Kembla, whilst the limestone is supplied from the deposits at Rapid Bay and shipped in the same manner.Quartz is used in the manufacture of ferro-silicon, an alloy which is added to the ladles of molten metal tapped from the open hearth furnace in the case of almost every grade of steel. It is obtained from a quarry situated between Iron Knob and Whyalla, and shipped to Newcastle.IRON OREWith the exception of several small quarries situated at Breadalbane, Cadia, Cowra, Crookwell, Michelago, Jerrawa and lerraama in New South Wales, the iron ore requirements of Australia's steel industry to date have been met from Iron Knob and the Middleback Range in South Australia.Several of the small deposits in New South Wales were worked during the war years of 1941-44 during the shipping emergency and produced 1,355,417 tons, compared with an output of approximately 43,000,000 tons from Iron Knob between 1901 and 1949.

Jan 1, 1951

Railway cuttings require the highest care in design and construction, as the pro- bability of failure concept does not allow any risks to be taken with hundreds of lives being dependent on continued stability. The usual geological influences on stability such as bedding dip and faulting are often discus- sed, but other major problems may come from the presence of sheet joints, cross joints differential weathering and seasonal or daily changes of ground water level. The design of rail cuttings has taken little note of the problems imposed by cons- truction methods, and low cost quarrying methods may seriously weaken a designed shape. The presence of berms and drainage ditches is often difficult to achieve as blasting imposes cumulative stresses and jointing on rocks. Contractors face difficulties in bidding extensive rock cuttings as variations in rock properties are often concealed and overshoot- ing the toe of a batter can easily occur. Modern blasting methods offer some solutions, but the best guide to safe successful cuttings is extensive investigation and the continued involvement of engineering geology at the stages of feasibility, design, construction and maintenance. Two case histories show the influence of folding, faulting and construction methods in the case of slope failure and slope stability.

Jan 1, 1979

Nickel ores from three different mines, Digger Rocks, Cosmic Boy and Flying Fox, are treated at the Forrestania concentration plant. The ore types vary from oxidised supergene ores to primary pyrrhotite+pentlandite ores. Mineralogical investigations on the ore and process samples have been carried out in different stages of process development. One of the studies was done with the samples collected from the flotation circuit in 19 June 1994 when the Cosmic Boy ore was processed. The process products were screened, and the size fractions were analysed for the main elements by appropriate analytical methods. Mineralogy of the products was studied microscopically and composition of the sulphides was analysed with an electron microprobe. Liberation of the main sulphides in the flotation feed was determined with the point-counting method, and weight percentages of the minerals were calculated using chemical and mineralogical data. The typical sulphide assemblage of the Cosmic Boy ore is violarite, pentlandite, pyrite, pyrrhotite and chalcopyrite. Violarite dominates over pentlandite (ratio being 70 per cent to 30 per cent), and pyrrhotite is strongly replaced with pyrite and magnetite. One of the most common mineralogical features of this ore type is secondary magnetite, which occurs as narrow rims in porous violarite or in association with secondary pyrite. Serpentine, talc and chlorite are the main gangue minerals. In the milled feed (76 per cent -74 ¦m) locked particles between nickel and iron sulphides are common. About 41 per cent of total pentlandite occurs as pure liberated particles, and 33 per cent as locked grains with violarite. Liberation degree of violarite is 55 per cent, and the most common type of locked particles is violarite+magnetite, carrying about 20 per cent of total violarite. To achieve a recovery of 80 per cent for pentlandite, all the particles containing at least 50 vol-% pentlandite should be floated into the nickel concentrate. Correspondingly recovery of 80 per cent can be reached for violarite if all the particles containing at least 65 vol-% violarite are floated.

Jan 1, 1996

By Hegedus M

The Hydrogeological Survay of the bauxite mines in Hungary was establisned 30 years ago. The goal of the HS has been to collect the all available date needed to solve the hydrogeological problems of bauxite mines. The results of activity of the HS have been summarized in the annual reports-. This report is going to present a few methods to evaluate the hydrogeological properties of fissured, karstic rock ie. the evaluation of drilling mud losses, the statistics of core samples evaluated by a special computer program for calculation the porosity and permeability of the rocks. An experimental injection test is presented together with the development of a new portable instrument to get signes of the water table change during the injection test in every two second. It can be proved that the flow around the well may be a transient one if the yield of the injection exceeds a definite one (Figure 2.). It was observed that the permeability calculated from the pumping test date may be 1.2-1.6 time higher than it coming from the injection test. A practical example is presented also how to use the results of the HS for designing the dewatering of a new mine together with an analogous computer model to forecast the yield expectable for making the drift tunnel. A suggestion based on the hydrogeological feature has been done for the dewatering without using electric energy (see Figure 3.-6.).

Jan 1, 1988

By Hoberg H, Schnieder FU

The disposal of residues from coal preparation and processing will to an increasing extent require investigation and consideration of the environmental problems resulting as a consequence of this. Different authors (Diingelhoff and Plankert, 1983; Hasenpatt, 1985; Szczepanska and Twardowska, 1987) have concentrated primarily on the content and the mobilisation of inorganic contaminants such as chlorides, metals and heavy metals from spoil tips, while no publications have yet been found on the question of a possible emission of organic contaminants (PCB, PAH, HC HC) from processing residues. Here the flotation residues in particular are able to bind larger quantities of organic contaminants by physi-sorptive means because of their large specific surface and, after disposal, to be re-emitt than into the environment. The flotation agents used in coal flotation are mixtures of technical distillation products with a correspondingly fluctuating composition. As Hey, 1986 showed, they may contain, in addition to the main components (n-alkanes, alcohols, surfactants), over 50 individual trace substances. In conjunction with the structural-chemical similarity of the individual components, this complicates the quantitative analysis of individual components considerably. For the analysis of hydrocarbon content of flotation products by means of extraction with organic solvents in accordance with DIN 38408, H18, the difficulty arises, besides the insufficient sensitivity at low concentrations, that geogeonic hydrocarbons are extracted from the coal as. well and the analysis results are thus falsified. These problems were overcome by the application of the 14C radiotracer method where certain components of the flotation agents are marked with radioactive carbon (14C). By measurement of the radioactivity of solid and liquid samples, the concentration of the marked substance can be measured very sensitively and precisely, whereby the accumulative measurement of similar organic substances is ruled out. Thus the reaction path of certain substances in complex reagent mixtures such as flotation agents can be traced excellently and the conceivable environment burden resulting from flotation tailings disposal can be estimated. In this paper, the adsorption behaviour of typical components of coal flotation agents are investigated for different coals and types of gangue material, the reagent content of flotation concentrates and tailings, as well as the mobility of the reagents adsorbed onto solids. The knowledge of adsorption and desorption mechanisms of unpolar hydrocarbons emulsified in water to solids are also of particular interest for the understanding of processes of organic soil contamination and for the further development of washing processes for oil-contaminated soils.

Jan 1, 1993

By Tuckey SH, Wake BA, Ariti J

Astute exploration on the northern Minahasa Peninsula, North Sulawesi, resulted in the discovery of the Toka Tindung, Pajajaran, Blambagan and Araren low-sulphidation quartz-adularia vein and stockwork gold-silver deposits. Combined, these deposits have estimated mineral resources in excess of I Moz gold at an average grade of 2.8 gAu/t and 7 gAg/t and are known as the Toka Tindung Gold Project. Gold typically occurs as fine grained electrum and is often associated with acanthite. The structurally controlled mineralised veins are hosted by Late Pliocene plagioclase and pyroxene-phyric basaltic andesite volcaniclastics and flows which form part of the Early Miocene to Pleistocene Sulawesi-East Mindanao Arc. Silica-adularia alteration dominates the volcaniclastic host of the Toka Tindung deposit. K-Ar dating of vein adularia indicates a 2.16 ¦ 0.04 Ma mineralisation age. Relatively narrow envelopes of silicification and argillisation surround the chalcedonic silica, quartz and adularia veins, stockworks and breccias at the other three deposits. Remnant hydrothermal breccias, chalcedony and anomalous arsenic, antimony and mercury indicate these gold deposits were part of a mineralised geothermal system.As of June 1997, Aurora Gold Ltd is finalising a feasibility study on exploitation of the four deposits and treatment of ore through a centrally located conventional CIP plant. Subsea tailings disposal is anticipated. Favourable metallurgy of the ore and logistics of the project area assist in minimising capital requirements.

Jan 1, 1997

THE slag from the blast furnaces having been granulated, a representative sample is taken to the sample mill. It is then dried, crushed through a 100-mesh screen, intimately mixed, and packeted for assay purposes.METHOD OF ANALYSISINSOLUBLEWeigh 1 grm. of the finely-pulverized slag into a 3t-in. casserole, moisten with a little water to prevent sticking, cover with a clock glass, and add 20 cc. of hot acid (1 HNOs, 3 HCI, 4 H2 0). Evaporate slowly to dryness on a hot plate and bake (without overheating) until all the gelatinous silica is dehydrated. Cool, add 20 cc. HCI (1-1), and boil gently for several minutes; filter into a 300-cc. beaker, cleaning out the casserole thoroughly with a rubber-tipped glass rod. Wash residue with hot distilled water and transfer it to a No. 1 porcelain crucible. Dry, ignite, cool in a desiccator and weigh as total insoluble matter. Dilute filtrate to 200 cc. and neutralize some of the excess HCI with NHa.OH. Warm, and pass H2S for 15 min. Filter and wash withhot water. Boil off H2 S, oxidize with 5 cc. HNOll , reduce bulk of the solution by evaporation. to about 100 cc., and transfer to a 250 cc. flask.SILICAFuse insoluble residue over a blast lamp in a platinum crucible with three or four times its weight of anhydrous carbonate of soda, for 10 to 15 minutes, or until decomposition is complete. Cool, and extract fusion in an 8-in. evaporating dish with HCI (1-1); rinse crucible and cover with distilled water, and evaporate to dryness over a water bath. Take up dry mass with 10 cc. strong HCI, and then.

Jan 1, 1922

By Bartosiewicz H

A method for the determination of the gas content of coal seams is presented which improves upon existing methods. The method makes use of a gravitational technique for measurement of the gas desorbed. The amount of lost gas is estimated by determining an empirical relationship relating the desorption of gas with time for each sample separately. This is to replace the assumption that desorp- tion follows a square root law with time. Laboratory investigations have been conducted which indicate that the square root desorption law does not hold good for carbon dioxide. Results of investigations on various factors influencing the technique are presented. It is shown that co-efficients of the empirical equation are dependent upon the elapsed time and the period of observation. Data about gas pressure measurements is presented and it is concluded that gas pressure can be approxi- mated to 0.6 times the pressure below a column of water equal to the depth of cover. This estimate is good enough for adsorption tests to evaluate desorption co-efficients. The technique for repressurisation of the sample,

Jan 1, 1982