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By Theo. Koulomzine

"The property of Consolidated Central Cadillac Mines, Limited, consists of 1,103 acres formerly held by Central Cadillac Mines, Limited, and Wood Cadillac Mines, Limited. Both mines have been partly developed to depths of 565 and 1,000 feet respectively, and from 1939 to 1943 they produced gold, with small amounts of silver and tungsten, having a total value of $2,208,528 from 377,489 tons of ore. The average grade of the ore was $5.85 a ton . Less than 10 per cent of the ore hoisted was discarded by sorting. New development work, carried out since the former Wood property has been purchased by Central Cadillac, has shown that the tonnage indicated by mine workings and diamond drilling exceeds 2,000 tons per vertical foot.The property lies between the claims of Kewagama Gold Mines, Limited, and Pandora Cadillac Gold Mines, Limited, and straddles the Cadillac 'break' for a length of nearly 1 ½ miles. The main workings are 1 3/4 miles east of the well-known O'Brien gold mine.GEOLOGYOutcrops are very scarce, with none at all of the most important horizons, so that the general geology shown in Fig. 1 is deduced mostly from underground workings and diamond drilling. Fig. 2 is a vertical cross-section and Fig. 3 a longitudinal section through the ore zone.The ore lies within a belt of Blake River volcanics which is approximately 600 feet wide and is flanked on the north and south, respectively, by Cadillac and Kewagama sediments. All the formations have a nearly vertical attitude. The Blake River belt consists essentially of well sheared volcanic tulfs, but associated with these in the northern part are a number of bands of iron formation and the central part, to a width of 100 feet, is occupied by talc schists, making the Cadillac fault proper. Intruding the volcanics south of the Cadillac shear zone are dykes of two types- finegrained aplite or quartz albitite, and porphyry; both consist essentially of albite and quartz and are distinguishable only by the grain size. They have the general east-west trend of the formations they intrude."

Jan 1, 1954

By Henry Smith, Stu Brown

"The Williams Mine is Canada's largest gold producer, with annual production of some 500 000 ounces of gold from two million tonnes of ore. Highly mechanized and automated underground mining practices are utilized at the property in order to help achieve high levels of productivity and the most cost-effective mining possible.Planning and design parameters for the underground ore handling system at the Williams Mine are described in this paper. Particular reference is made to the considerations that were built into the system to provide maximum operating flexibility through the use of multiple orepass systems, portable low profile jaw crushers, underground conveyors and automated hoisting equipment.IntroductionThe Williams Mine is situated in the Hernlo area of northwestern Ontario, approximately 40 Ian east of the town of Marathon (Fig. I). It is operated by the Williams Operating Corporation, which is owned equally by Teck Corporation and Corona Corporation, and is one of three adjacent properties forming the HernIo gold camp.The mine commenced operation in October 1985 at a nominal production rate of 3000 tpcd. Through an ongoing capital development program, winch was completed in late 1989, the production rate at the property was increased to its current level of 6000 tpcd. This paper describes the mine planning process and the evolution of current mining strategies with particular reference to the underground ore handling system .HistoryGold mineralization was discovered in 1944 in the Hemlo area of Northern Ontario, near the north shore of Lake Superior. A year later, 11 claims were staked over the showing and subsequently patented by the late Dr. Jack Kerr Williams.Over the next 35 years, other claims were subsequently staked, explored and abandoned in the immediate area of the 11 patented claims . In 1980 a predecessor of the Corona Corporation acquired claims adjoining the Williams property to the east. Drilling on this claim group started early in 1981 and intersected the Hemlo orebody in May of that year. In December 1981, Corona Corporation entered into an option agreement with Teck Corporation to explore and develop the property.A drilling program by LAC Minerals on the II patented claims discovered the Williams orebody in March 1982. The mine started production in 1985, pouring its first official bar of gold on December 6 of that year. Corona Corporation was awarded ownership of the Williams Mine conclusively by a decision of the Supreme Court of Canada on August 11, 1989. The court's ruling ended a legal dispute with LAC Minerals over the property initiated eight years earlier."

Jan 1, 1991

By R. P. Viljoen, A. L. Sokolov

"The distribution of mineralized provinces is analyzed on the basis of their genetic link with specific blocks of the earth's crust including ancient platforms, mobile belts and zones of tectonicmagmatic activation. Mobile and fold belts surround the Siberian platform in Russia and the Kaapvaal craton in South Africa, with decreasing age zoning away from ancient platform margins. The main differences in the geological development of the two cratonic areas are: (1) the long period before the final stabilization of the Siberian platform (3600 Ma to 1600 Ma) and the comparatively short period of time for the stabilization of the Kaapvaal craton (3600 Ma to 3050 Ma) and (2) the intensive multiple activation of the marginal zones of the Siberian platform and the tectonicallycontrolled, magmatic sedimentary, intracratonic activity, typical of the Kaapvaal craton. Mineralization of the Siberian platform is largely characterized by marginal reactivation zones of differing ages although mineralized intracratonic Cu-bearing basins of Proterozoic age are also known. Mineralization of the Kaapvaal craton is mainly related to the formation of the intracratonic basins i.e., Witwatersrand (Au, U) and Transvaal (Au). The latter is characterized by multi-age volcanic-intrusive activity including the emplacement of Bushveld Complex (Cu, Ni, Pt, Cr, Au, V). The Siberian platform is characterized by the prolonged development of inherited mineralization from Archean until the late Mesozoic. The main period of mineralization in the Kaapvaal craton is restricted to the middle Proterozoic.The Baykal-Patomskaya and Namaqua-Natal mobile zones occupy similar positions adjacent to the Siberian and Kaapvaal cratons, respectively, and demonstrate similar modes of metallogenic development: i.e., the early formation of exhalative Pb-Zn-Cu deposits during the early stage and magmatic Cu deposits during the late stage. The more remote mobile belt near the Siberian platform, the Trans-Baykal, is characterized by intensive multi-age mineralization (Wo, Mo, Sn, fluorite), related to a period of tectonic-magmatic activation. The Saldania Belt occupies a similar position near the Kaapvaal craton but is known for its poor Au, and Cu mineralization. It does, however, have some similarities with Trans-Baykal Belt in regard to Mo-W bearing granitoids.The phenomenon of interference of geosynclinal, orogenic, platform, and tectono-magmatic activation regimes is known for the Russian section of the Pacific Ocean Volcanic Belt."

Jan 1, 1994

By J. Gillies

"Extraction of Gold in Ketone from a suitably prepared sample of sulphide or siliceous ore or concentrate permits a rapid and accurate determination by Atomic Absorption. Mill test products and exploration development samples are acid-treated to effect complete dissolution of silver, copper, zinc, lead, molybdenum and iron present. Interferences in the determination of molybdenum are described. Results by Atomic Absorption are comparable to those afforded by other acceptable methods.INTRODUCTIONDuring recent years much has been written and discussed concerning Atomic Absorption Spectrometry as a technique for determining the concentration of metallic elements. We would, however, recommend a perusal of the paper presented by J. C. Ingles at the annual meeting of Canadian Gold Metallurgists held in Ottawa, January, 1966. The paper was published in the August, 1966, issue of the Canadian Mining Journal, and contains general information on Atomic Absorption.The purpose of our paper is to present certain specific method procedures for the determination of several precious and base metals normally present in Mine, Mill and Smelter products. Of necessity, analytical results should be as accurate as the most suitable available method permits, whether for metallurgical balance, settlement purpose, ore beneficiation programs, or exploration property development. The success of such programs is relative to the accuracy, speed and economics of the analysis. It is obvious, therefore, that in presenting our paper we consider the technique has achieved the desired evaluation."

Jan 1, 1968

By D. A. MacFadyen, J. J. Brummer, C. C. Pegg

The early identification of a kimberlite dyke and the occurrence of pyrope garnet grains along a section of the Munro Esker north of Kirkland Lake encouraged the search for kimberlites. Subsequent exploration using data from aeromagnetic surveys completed for the Kirkland Lake Initiatives Program (KLIP) resulted in the discovery of five kimberlite diatremes in the area north of Kirkland Lake and another one to the south. These are only a portion of the cluster of pipes found so far that probably occur in the area. Recovery of the diamonds present in four of the pipes yielded 16 stones, the largest being 0.17 carats. Unfortunately evaluation of the pipes is a problem due to the cover of glacial drift, up to 92 m in thickness, which makes it difficult to obtain an adequate bulk sample. A study of their ages, mostly from drill hole samples, suggest that the kimberlite diatremes and other alkaline ultramafic rocks were emplaced along a northwesterly zone of rift structures. These alkaline ultramafic rocks cut across all earlier rock types and have ages ranging from 121 Ma to 173 Ma. The zone of deformation, along which these rocks occur, has been named the Lake Timiskaming Structural Zone (LTSZ), a modification of Lake Timiskaming Rift Valley (LTRV). Ultramafic intrusions which were emplaced along the LTSZ can be traced from the James Bay Lowlands in the northwest to past Belleville on the north shore of Lake Ontario in the southeast, a distance of about 1070 km. As the emplacement of these rock types become known more are certain to be found by drilling selected aeromagnetic anomalies. The project has demonstrated that aeromagnetic surveys can be used successfully to identify covered kimberlite targets.

Jan 1, 1992

By Bruno Lafrance

Abstract - Quartz veins at the Mufferaw gold prospect and Komis gold deposit, northern Saskatchewan, are examples of oblique-extension veins that crystallized in shear and tensile fractures, which propagated and then opened oblique to their walls during a single continuous deformation event. The Mufferaw gold prospect consists of an interlinked mesh of conjugate shear fractures, tensile fractures, and veins. Oblique-extension veins crystallized in conjugate shear fractures, which opened during dilation of intersecting tensile fractures under the same far-field stress system. At the Komis gold mine, tensile and dextral shear fractures cut across granodiorite dikes. The tensile fractures formed perpendicular to the dike margins during stress transfer from the less-competent country rocks to the more-competent dikes. During extension of the dikes oblique to the bulk extension direction in the country rocks, the tensile fractures were reactivated as sinistral shear fractures. The reactivated tensile fractures and dextral shear fractures opened oblique to their walls, parallel to the bulk extension direction, and were sealed by the deposition of oblique-extension veins during the same deformation event.

Jan 1, 2004

By H. Tokuichi, H. Ohta, K. Sato

A physical separation technique of tantalum capacitors from waste print circuit boards is in a development phase in Japan. A tantalum capacitor consists of an exterior coating of resin (epoxy resin) mixed with silica fillers and a sintered tantalum compact, the latter of which is impregnated with manganese dioxide (MnO2). In this study, we developed a process to recover tantalum oxide from tantalum capacitors by roasting, fluidized-bed separation, and hydrometallurgical treatments. Our aim was to recover tantalum oxide with high purity from waste tantalum capacitors. In this process, the exterior resin was selectively decomposed by roasting without oxidation and pulverization of the sintered tantalum compact at a proper temperature. Furthermore, the decomposed resin with silica filler on the surface of the sintered tantalum compact was mostly removed by fluidized-bed separation. The surface of the sintered tantalum compact was cleaned by ultrasonic irradiation in an acid solution to remove the MnO2 paste as well as residual Ag paste and silica filler. The impregnated MnO2 in the sintered tantalum compact was leached as Mn(II) ions using acid solutions via the reducing effect of tantalum metal to recover purified tantalum oxide.

Jan 1, 2014

By Sarah Bélair, Denis Beltrami, Deka Moussa Ragueh, Valérie Weigel

"Scandium is a highly valuable element belonging to the rare earth elements (REE) but it has different chemical and physical properties from those of lanthanides. This metal is generally used in aluminum-scandium alloys and in fuel cells but the development of its market is slowed down by its high price (more than 1000 US$/kg for a 99.0% grade product). Indeed, the low scandium content in the continental crust (an average of 22 ppm) and the difficulties to extract it selectively from solutions containing high impurity concentrations increase the cost of the recovery processes. Nowadays, scandium is primarily recovered as a byproduct.ERAMET is developing a hydrometallurgical process in Gabon (Mabounié) in which the scandium content in the deposit reaches 10 to 100 ppm. The Maboumine project consists in the extraction and purification of uranium, niobium, tantalum and REE from Mabounié ore. In the frame of this hydrometallurgical project, ERAMET had also studied the feasibility to recover scandium as a byproduct. During the ore leaching, uranium and rare earth elements including scandium are solubilized into the pregnant leach solution (PLS). Among the various methods investigated to recover scandium from the PLS, liquid-liquid extraction using Primene JM-T as extractant was chosen and tested first at laboratory scale and then at pilot scale. Selective stripping of the loaded organic was carried out by using phosphoric acid solution, allowing the selective recovery of scandium from thorium and zirconium partially extracted from the PLS by Primene JM-T under the process conditions."

Jan 1, 2016

By B. R. Casement

"Managing safety on the basis of after-the-fact reaction to accidents, can never be more than partially successful. Injuries will occur as long as the underlying potential for them still exists. Unless unsafe actions and conditions are systematically decreased, no program can have more than a short-term success.The pro-active Bullmoose loss control process, instead, focusses on heightening awareness of work habits, to prevent incidents by reducing their potential.Any safety program will be doomed to failure if the development of safe work habits depends on the safety supervisor or a safety committee. At Bullmoose the focus is on the critical actions out of which losses emerge. The successful application of performance-related feedback is achieved by taking safety, health, and environmental concerns into consideration on every level, and, by doing the right thing in every job done.What is an Exceptional Loss Control Program?If an accident in an organization creates a flurry of interest, resulting in ""cracking down"" on violations for a short period of time then an ""exceptional"" loss control program exists. Unfortunately, exceptional here does not refer to the effectiveness of quality of the program but to the fact that the organization is managing loss control by exception. The degree of management attention in an ""exceptional"" safety program varies over a period of time, remaining low as long as the rate of losses stays within management's acceptable control limit (Fig. I). When the losses rise above this, management becomes motivated to begin ""exceptional"" efforts to manage losses. When the rate falls again to within the accepted limit, efforts to control losses take a back seat.Such a strategy guarantees that losses will be tolerated or ignored as long as the actual rate is below the acceptable limit. Simply to lower the limit would not reduce losses, but would result in an increased number of flurries of management attention to loss control. This ""on-again, off-again"" style of management teaches supervisors and others that basic loss control is not as important as are statistics."

Jan 1, 1993

By J. A. Bos, Z. Dai, P. Quinn, A. Lee

A flowsheet is being developed for processing Thompson ultramafic low-grade nickel ores. This type of ore is characterized by high content of serpentinized magnesium silicates which generate slimes during comminution. Flotation of this type of ore proves difficult due to problems associated with the slimes. The flowsheet, based on extensive laboratory and miniplant flotation tests, consists of two key components: desliming by hydrocyclones prior to flotation and using soda ash for pH control in flotation. Satisfactory metallurgical results have consistently been achieved in laboratory full circuit simulation and miniplant tests.

Jan 1, 2009

By John A. Allan

The subject chosen for this paper is not a new one, but the subject matter is so extensive that something new can always be said .about it. We are just beginning to realize how little is actually known about the character of Alberta coal, except for a few general facts. The object of this paper is not to explain that our previous information, in whole or in part, on the coal resources of Alberta, has been incorrect, but rather to present some new facts obtained as a result of recent study in the field and in the laboratory. As field investigation continues the problem of determining the character of a coal seam for any great distance laterally becomes more and more complex. Our present knowledge of Alberta coal deposits should not be discussed before due reference is made to those great pioneers who blazed the trails for later geologists, by recording their observations on the general geology of Alberta. Geologists, to-day, particularly those of us who are striving, year after year, to unravel the mysteries of stratigraphy, palaeontology, and structure, in so far as these are related to the coal resources of Alberta, fully realize our indebtedness to those three trail-makers, Dawson, McConnell, and Tyrrell. Had these geologists not recorded their observations correctly, nor interpreted the broad geological facts contained in Nature's book, with still uncut pages, how much slower would have been the progress of our coal knowledge in the succeeding years. It is true that many of the interpretations given to observations by these pioneers have had to be changed as a result of closer studies, but we must also expect that the geological interpretation from present day observations will be changed by future workers, as Nature's book is read and re-read.

Jan 1, 1925

By E. Rosseland

Glencore Nikkelverk is operating its Chlorine Leach Process in Kristiansand, Norway, producing nickel, copper and cobalt metals by electrowinning. The copper tankhouse, with an annual capacity of 40 000 tons, is based on traditional technology with copper starting sheets and cast lead anodes. Due to the integration of this copper sulphate process in a nickel chloride refinery, operating conditions are unique. In recent years, operating costs have escalated, and health, safety and environment are top priorities. Test work on a new copper process involving permanent cathodes was therefore initiated in 2007, and a pilot plant was started up in 2012. The objective was to introduce innovative technologies and tailor these to be robust in the Nikkelverk process, to form a basis for a new sustainable copper tankhouse with a high degree of automation. Key learnings from more than 10 years of R&D work is presented, focusing on cathode materials and copper metal deposition including product quality, robotic stripping, coated titanium anodes, electrode contacts and alignment, electrode current monitoring with Hatch HELM tracker technology and acid mist capture using cell hoods with off-gas scrubbing. The new copper tankhouse project was approved in December 2018, and commissioning is planned in 2022. INTRODUCTION The Kristiansand nickel refinery was started up in 1910, processing nickel-copper matte originating from Norwegian mines. It was the first industrial plant in the world to produce nickel by electrolysis using the Hybinette electrorefining process. After roasting to burn off sulphur in the matte, copper was leached and recovered as cathodes by electrowinning with lead anodes. In the first years, the copper cathodes were fire- refined and cast into ingots for sale (Thonstad Sandvik, 2004). The Nikkelverk refinery was acquired by Falconbridge Ltd. in 1929, and since then matte from Sudbury, Canada has been the main feed source. The Hybinette process was in operation until 1975 when conversion to the newly developed Chlorine Leach Process was started (Stensholt, Zachariasen, & Lund, 1986). In this process still used today, nickel and part of the copper in the matte is leached using chlorine gas generated on dimensionally stable anodes in the nickel and cobalt electrowinning tankhouses, as illustrated in Figure 1. The presence of dissolved copper ions in the strong chloride leach solution is essential for effective chlorine absorption and nickel dissolution. To improve copper-nickel separation, slurry from the atmospheric leach is pumped to autoclaves and then to cementation tanks for precipitation of copper as copper sulphide, which is collected in filter presses. The leach residue, also containing the precious metals, goes through a 3-stage wash to remove chlorides before being introduced as a slurry to fluid-bed roasters for sulphur removal. The resulting calcine is then leached in spent electrolyte from the copper electrowinning tankhouse, to dissolve most of the copper and also some nickel, cobalt and other elements. After separation of the leach residue, elements like Bi, Te, As and Ag are removed from the strong copper sulphate solution by reaction with metallic copper in three columns in series filled with cut copper cathodes. The purified solution then passes polishing filters before being mixed with spent electrolyte and returned to the electrowinning cells.

Jan 1, 2019

By C. Arson

We modeled mode I fracture in shale with an equivalent damage zone (CDM), a cohesive zone (CZM) and discontinuous enrichment functions (XFEM). In the Differential Stress Induced Damage model (DSID model) used in the continuum approach the total work input is equal to the sum of the energy released by crack debonding, the energy dissipated by crack opening, and the elastic strain energy stored in the bulk outside of the damage zone. In CZM and XFEM, the overall stiffness of the rock mass in the process zone drops as soon as the fracture starts propagating (unstable fracture propagation), whereas rock elastic properties in the CDM equivalent damage zone evolve smoothly with the displacement imposed at the boundary of the domain. In the CZM and XFEM, fracture propagation stabilizes after a turning point: this point coincides with damage initiation in the DSID model. As a result, the total energy of the rock mass calculated with CDM is about twice as large as in CZM and XFEM. The relative energy components of the rock mass are in the same order of magnitude and follow the same trends in the three models. This numerical study compares the evolution of dissipated energy potentials during mode I fracture propagation, and is expected to provide a basis to predict the amount of energy released by discrete fracture growth vs. damage propagation in the fracture process zone.

Jan 1, 2015

The following guidelines have been recommended by the Diamond Exploration Best Practices Committee established by the Canadian Institute of Mining, Metallurgy and Petroleum. These guidelines are applicable to public companies and their consultants reporting diamond exploration results. In respect of these guidelines, Diamond Exploration Results are results derived from the initial activities undertaken to investigate a diamond bearing prospect or deposit, to generate tonnage, grade and value estimates that cannot be classified as a Mineral Resource or Mineral Reserve. They do not address the earlier stage reporting of geophysical, geochemical or kimberlite indicator mineral results. Public reports of Diamond Exploration Results relating to mineralization not classified as Mineral Resource or Mineral Reserve must address the confidence limits of the result and contain sufficient information to allow a considered and balanced judgement of the significance of the results. The objective of these guidelines is to assist public companies and consultants in making appropriate disclosure of diamond exploration results by reporting in a manner which is: ??Uniform within the diamond exploration industry; ??Consistent with reporting from other industry sectors; ??Comprehensive; ??Unambiguous. The guidelines are not prescriptive. Materiality is the overriding principle that determines the information that should be disclosed. However, where a company or consultant deviates from the guidelines, the disclosure or technical report should state the extent to which the guidelines have not been followed, and the reasons for the deviation. The guidelines do not in any way replace jurisdictional reporting requirements (For example, the requirement for Canadian reporting issuers to comply with Canadian Securities Administrators National Instrument 43-101 by having technical disclosure endorsed by a Qualified Person as defined in that legislation).

May 1, 2003

By W. Dan Hausel

"Hundreds of diamonds have been found in the United States. The majority of the discoveries occurred during the 19th century as a by-product of placer gold mining. Most of these early diamond finds have no known source, and in many cases are situated in areas unfavorable for diamond exploration based on current models that require kimberlite or lamproite to be emplaced in a stable Archean craton or Proterozoic craton margin.Diamonds have also been recovered in situ from lamproite at Murfreesburo, Arkansas, from kimberlite in the Lake Ellen region of Michigan, and in several kimberlites in the Colorado–Wyoming State Line district. Unverifed reports also suggest that diamonds may have been recovered from other related intrusions at a number of localities in the United States.IntroductionTo date, diamonds have been recovered in situ from kimberlite in the Colorado–Wyoming State Line district and from a kimberlite in Michigan. Additionally, diamonds have been recovered from lamproites in Arkansas. Diamonds have also been reported from kimberlite in Kansas, and from peridotite in New York and Maryland. However, these latter reports have not been verified."

Jan 1, 1995

By P. E. Auger, J. E. Gill

"The zinc deposits to be described are in Lemieux township a few miles south of the Tabletop mountains, in the central part of Gaspe peninsula, Quebec. Although they have not been worked, they constitute a potential source of zinc and lead and structurally are of considerable interest.GENERAL CHARACTER OF THE OCCURRENCEThe deposits are in sharp-walled quartz-carbonate veins and breccia zones carrying locally, and in varying amounts, sphalerite, galena, pyrite, marcasite, chalcopyrite, and specularite. Those so far investigated strike generally north-south, have steep dips, and cut through sediments of Lower Devonian age, mostly calcareous argillites or siltstones. Wall-rock alteration is negligible.BROADER STRUCTURAL FEATURESThe principal known occurrences are in the south-central part of a dome structure measuring 6 by 5 miles. The argillaceous sediments are overlain, on the flanks of the dome, by sandstones and lavas. These have been stripped from the central part of the dome, revealing the veins in the argillites beneath. The veins formed after the volcanics, but the fractures and breccia zones in which the deposits formed are confined mainly to the argillite series, presumably because of the greater strength of the lavas.The argillite series is cut by dykes, sills, and small stocks of diorite and acidic 'porphyries' that are older than the veins.THE FEDERAL HILL AREAThe distribution of known veins is shown in Fig. 1. The characteristic features of the veins are well illustrated by the Federal Hill area shown in Figs. 2, 3, and 4, and described below."

Jan 1, 1954

By A. David MacPhail

"Highland Valley Copper is a large volume producer of copper and molybdenum concentrates. Production is by conventional truck and shovel operation combined with an extensive ore handling in-pit crushing and conveying system.Grade of the two orebodies is low at 0.4% copper and 0.007% molybdenum and this demands a production rate in excess of 260 000 tpd at a stripping ratio of 1: 1. Mining cost has to be kept at minimum levels to keep the mine profitable and thus, it is necessary to keep in the forefront: of technology. As well as the in-pit crushing system, the mine has pioneered the use of shovel weighing coupled with a state-of-the-art dispatch system.Maintenance of the equipment is carried out at the on-site mine maintenance shop with assistance from local shops for engine and wheel motor rebuilds and other large jobs such as those requiring stress relieving. Shovel and truck rebuilds are undertaken by mine crews. Both long- and short-term planning is designed and scheduled in the mine engineering section. Outside consultants are used to assist in slope design, reclamation and blasting technology."

Jan 1, 1992

By G. Vibert Douglas

IN a previous paper by Douglas and Gillies (1), a simple field test was given for gold. Later work by the present writers, and by others who have kindly written to us, shows that the test is not as satisfactory as it was hoped. In many cases, the gold mirror is completely obscured by a dense precipitate which, up to the present, it has been found impossible to remove. After many attempts, we have temporarily given up the iodine test and have been working on a simple pyridine reaction based on the work of Putnam, Roberts, and Selchow (2): The ore to be tested is ground to a fine flour. Place half a gram of this powdered ore (an amount that will cover a Canadian ten-cent piece, not heaped) in a six-inch test-tube and add 5 c.c. of aqua regia. The aqua regia. should be made up on each occasion, using four parts of hydrochloric acid and one part of nitric acid, both concentrated. Shake the solution in the test-tube for about one minute and allow to settle until dear. The rime to settle may be 30 to 60 minutes. When dear, a drop of the solution is with-drawn with a fine, dean eye-dropper or capillary tube and placed on à small glass plate. A slide such as is used for mounting rock sections is suitable. Now place an equal sized drop of pyridine solution on the plate beside that of the aqua regia solution to be tested. The pyridine solution, containing nine volumes of hydrogen bromide to one volume of pyridine, can be made up in advance and carried in a glass-stoppered bottle. Join the two drops with a glass thread or fine, dean stick, and allow the merged drops to stand undisturbed. I t is well to place the slide on a piece of white paper so that the presence of the crystals which may form can be easily seen. The time for their formation will vary with the amount of gold present, but the slide should be allowed to stand for at least 30 minutes before negative results are reported. A hand lens of at !east ten magnifications is essential. If gold is present, minute red crystals will form around the margin of the drops as these drops slowly evaporate.

Jan 1, 1938

By L. Xia, B. Hart, K. Douglas1, S. C. Chelgani

Development work to optimize a flotation flowsheet for rare earth element (REE) recovery is underway. The original approach used alkyl phosphates and phosphoric acid ester as collectors to concentrate REE minerals. To improve REE recovery, hydroxamates as alternative collectors were investigated. In this paper, micro flotation of REE minerals using salicylic, benzoyl and naphthoyl hydroxamates is reported. Unlike phosphonic collectors, slime removal does not show a significant effect on REE recovery when using hydroxamates as collectors. Among the three hydoxamates, the grade of La, Ce, and Nd for concentrates produced by salicylic hydroxamate is the highest. The recovery response with naphthoyl hydroxamate is similar to that of salicylic hydroxamate; good grades for La, Ce, and Nd, less effective for Nb, Y, and Zr. The data indicated an affinity by salicylic and naphthoyl hydroxamtes for LREE over the HREE minerals. In comparison, benzoyl hydroxamate indicated an affinity for Nb, Y, and Zr. Temperature effects on REE recovery were also studied. The grade and recovery of REEs generated by flotation using a mix of salicylic and benzoyl hydroxamates at room temperature was almost identical or even better relative to the recovery using naphthoyl hydroxamates at elevated temperature.

Jan 1, 2014

By J. W. Matousek

"More copper concentrates are treated in flash smelting furnaces than by any other process, and such furnaces are located in most of the world's major copper producing areas. Except for perhaps two furnaces treating chalcocite-type materials, little difference is seen between the grades of the concentrates being smelted. Within individual smelters, even less variation in feed grades is found. This is both accidental and intended. Many furnaces treat concentrates from captive ores, and these tend to be of relatively constant composition over long periods. Toll smelting operations blend concentrates to ensure delivery of feeds of fixed compositions to their furnaces to avoid upset conditions. Matte grades vary between flash smelting furnaces, but most commonly, these are the result of differences in operating practices rather than because of differences in concentrate grades. This paper reviews an industrial flash smelting test in which the copper content of the furnace feed was intentionally altered over a wide range. IntroductionExcept in a few copper mining regions of the world, the principal copper mineral is chalcopyrite (CuFeSz). This results in the almost universal production of concentrates containing 25070 to 30% copper (and similar amounts of iron and sulphur). Many operators of copper flash furnaces spend their entire metallurgical careers smelting concentrates of essentially fixed grades. This is true both of smelters treating concentrates from captive mines and those processing concentrates on a toll basis. From the production staff's point-of-view, the less variation in grades seen by the furnace, the better. Fixed analyses of concentrates and constant feed rates produce consistent quantities of matte at a consistent grade for processing by the converters. The result is, even in smelters treating a variety of concentrates, efforts are expended in sampling and blending to ensure feeds of relatively uniform compositions being sent to the furnaces."

Jan 1, 1993