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By Y. F. Li

Fengning ilmenite ore is a magnetic deposit in gabbro containing high phosphorus and low titanium, the main minerals in which are ilmenite, magnetite and apatite. The dissemination size of magnetite is so fine that even the percentage of -0.010mm level is up to 36.50%. The fine and vein magnetite are distributed in gangue and ilmenite, so the majority of the magnetite is difficult to be separated from the gangue. Ilmenite is difficult to be recovered by low-intensity magnetic separation even through fine grinding. In high-intensity magnetic separation of ilmenite, the gangue inter-growth with the magnetite and the Fe-containing silicates may be enriched in the concentrate, and the ilmenite of the concentrate will be reduced. Based on the processing mineralogy research, combined gravity-flotation process is suggested to recover the ilmenite. The method is also good to reduce phosphorus in the ilmenite concentrate.

Jan 1, 2014

By Hamid-Reza Manouchehri

"The triboelectric charge attributes of some silicate minerals (i.e., feldspar, quartz and wollastonite) after contacting different triboecharging medium made of different materials were studied. The charge acquisitions by different size fractions of minerals were monitored and accordingly the energetic work function values, i.e., the main parameter determining the entity of triboelectric charges acquired by mineral grains, of the examined minerals were estimated. Moreover the separation behavior of different size fractions of these minerals through the electric field of a laboratory free-falling separator when the mineral grains are charged by different tribochargers were observed and considered as the electrical separation potential of the examined minerals.Furthermore, the role of adsorption of different chemical species on triboelectric charge characteristics and charge acquisition of mineral samples were described from theoretical point of view and the effects of some chemical reagents on triboelectric charge acquisition of the examined minerals were studied. In addition the separation behavior of chemically conditioned quartz, feldspar and wollastonite minerals, using different anionic and cationic reagents, through the electric field of a free-fall electrostatic separator before and after chemical conditioning were monitored.Finally an attempt was made to translate the findings from single mineral systems to a complex silicate ore, containing mainly of feldspars, quartz, and wollastonite. Different separation tests under various conditions were conducted to this complex silicate ore. Before passing through the separation device, the ore sample was conditioned by different cationic and anionic reagents and then was triboelectricaly charged by different tribocharging medium in order to find the effective reagent and tribocharging medium for separating silicates. Besides the role of temperature and humidity of the surrounding ambient in separation behavior were considered."

Jan 1, 2003

By Daniela Campos, Aldo Casali, Gonzalo Montes-Atenas

The understanding of the effect of the major variables influencing the froth flotation performance may allow both to predict and to identify best operating conditions towards optimizing the process efficiency. The aim of this research work is to model the effect of dissolved oxygen onto froth flotation performance. Experimental pilot plant results were obtained from a continuous circuit consisting of a ball mill and a rougher bank of four flotation cells. A series of flotation experiments were run with different conditions of dissolved oxygen keeping constant most of other operating conditions. Variables difficult to control were measured or estimated. A set of mathematical models suggested in the published literature were tested. It was found that the copper recovery results were highly sensitive to the concentration of dissolved oxygen. The latter confirmed the reactions mechanisms associated to the collecting capabilities of current flotation reagents used in the flotation of copper sulfide ores. On the contrary, the results of molybdenum recovery varied non-linearly with changes in dissolved oxygen which could not be explained directly in terms of the computed specific rate constants. The error analysis confirmed that Klimpel continuous model exhibited the best specific rate constant correlation with molybdenum recovery data. Lastly, the classic particle force balance equations indicated that the adjustments of estimated mineral liberation with experimental data exhibited a turning point when passing from highly liberated to low liberated particles. The values of recovery for such turning point correlated well with the concentration of dissolved oxygen. The results indicated corrections due to changes in the dissolved oxygen must be incorporated in future froth flotation descriptions.

Jan 1, 2014

By Chen Dong, Yang Wenwang, Liu Zhineng, Tan Ming

"To meet the requirement of production expanding of a certain potash ore dressing plant in Xinjiang province of China, industrial test of XCF/KYF-50 flotation machine was performed to process potash ore. The tank of XCF/KYF-50 flotation cell is in U shape, 50m3 of volume. This flotation cell is able to suck slurry by itself, and can be arranged on the same base level without high difference. In this paper, two sets of XCF/KYF-50 flotation cells were adopted to replace 8 sets of 8m3 flotation cell in original flow sheet of flotation. Aeration rate, slurry suction capacity, power consumption and slurry suspension are investigated. The measuring results show the slurry suction capacity of the flotation cell is larger than 12.80m3/min and solid particles disperse evenly in the tank without deposition. Industrial test result indicates that the final grade of concentrate is 26.69% at the recovery of 90.95%, which is up to expected performance. XCF/KYF-50 flotation cell has advantages of high flotation efficiency, significant energy saving and reasonable configuration of automatic control system, this kind of flotation cell can meet the requirement of production expanding of this potash ore dressing plant well."

Jan 1, 2014

By Stephen J. Harker, John Knights, Randolph A. Pax, Glen A. Stewart

"Mineral samples were obtained from different stages of a mineral processing circuit used to extract the copper and gold rich mineralogical phases. The aim of this work is to characterise the quality of the samples at different stages of processing. The samples were taken of the head grade, tailings, cyclone overflow and the final concentrate.Characterisation of the samples was determined using Cu-Ka X-ray powder diffraction and Fe57 Mossbauer spectroscopy. These measurements will be presented and discussed in terms of the enrichment of the ore, showing the removal of magnetite and quartz through the processing, the final concentrate being rich in chalcopyrite and pyrite. This data also shows the utility of Mossbauer spectroscopy to provide mineralogical phase information directly.Mossbauer spectroscopy is a tool to determine the material phases of a sample. It is a nuclear based technique which measures the amount of attenuation of a narrow Doppler shifted source energy as it passes through a sample. The attenuation depends on the amount of resonantly absorbing material in the nuclear radiation path from the source to the detector. Synchronous detection of the doppler shifting velocity and the nuclear radiation count gives a Mossbauer spectrum. By convention, the energy axis of the Mossbauer spectrum is displayed in units of velocity.Figure 1 shows Mossbauer spectra obtained for a sequence of samples throughout a processing plant. These spectra show the removal of magnetite and the concentration of chalcopyrite and pyrite. Optical microscopy results indicated a significant component of bornite not witnessed with Mossbauer spectroscopy. Closer examination showed that optical microscopy assays over estimate the bornite component."

Jan 1, 2003

By Przybycien Krzysztof, Tumidajski Tadeusz

"Materials being the feed to mineral dressing plants are the mixture of ore minerals having different physicochemical properties among others, especially susceptibility on crumbling. During exploitation of material and their preparation to communition the big number of narrow classes comes into being and they have different properties. The determination of common communition laws of multicomponent (on account of size and mineralogy) materials leads to the estimation of mutual influence of narrow classes and their rates, taking into account their endurance and mineral density, on general ratios and their simultaneous crumbling.If we try to accept the grain membership to the certain component as the differing feature, we can write the balance equation as: ( ) ( ) S= = k i i i g x p f x1where: fi – density functions of one type distribution and of different statistical moments (characterising the homogeneous materials grinding), pi – “stirring” proportions of each components, S== k i i p 1 1 . From the point of verification view of detailed versions of this equation the inverse operation should be done: in the base of the components’ mixture grinding results and the results of components grinding the legitimacy of equation should be checked.The using of finished distribution mixtures’ theories to the grinding process analysis allows, first of all, to verify the assumption of grinding independence of individual feed components. Talking more generally it would lead to the comparison of grain size distributions, obtained by individual components grinding from the defined in the mixture distributions theory calculations. One of experimental and calculation results for artificial mixtures of galena and dolomite is presented on figure below (df means distribution function)"

Jan 1, 2003

By Sebastian Fredes, Williams Calderon, Mauricio Toledo, Gonzalo Montes-Atenas

The influence of the temperature on leaching kinetics of copper-bearing minerals has been widely acknowledged: the leaching of copper oxide ores is generally described as exothermic reactions while copper sulfide ores are associated with endothermic reactions. Reports studying the influence of temperature on leaching kinetics at laboratory scale frequently involve the implementation of either fully flooded isothermal systems or jacketed column setups. Nevertheless, at industrial scale controlling or monitoring the temperature or temperature changes is almost impractical. In fact, leaching process is usually a large tonnage operation and changing the temperature of vast amounts of material would require an enormous amount of energy and highly specific heat transfer equipment. Preliminary computations on the amount of energy required to increase the temperature of a heap or dump in 1°C indicates that it would be impossible to find an energy source able to accomplish the task. In order to provide a solution to this matter it is suggested to create an energy managing protocol (EMP) that permits heat up or down the porous body locally taking advantage from the temperature gradients and from the reactivity of different regions within the material as a function of the leaching cycles. The aim of this study is to evaluate different heat transfer regimes in a 1 ton pilot column leach operation. It was found that best results of copper recovery are obtained when heating up the column in horizontal bands starting from the top of the column moving downwards as the leach cycle evolves. The system is expected to be suitable for industrial applications, but further development of the technique is required, particularly in the design of the heat transfer dispositive.

Jan 1, 2014

By M. X. Jia

This paper discusses two mineralogy characteristics that may affect the flotation of sulfide ore. The first one, process mineralogy study on a Cu-Ni sulfide ore shows that valleriite and tochilinite are incline to form on chalcopyrite, pyrrhotite and serpentine surface, and the further guess is that the formation of valleriite and tochilinite may also causes the serpentine transform to talc, so the serpentine surface is a phase of talc or a transition phase from serpentine to talc and this enhances the flotability of the gangue minerals. The second discussion on the flotation behavior of the sulfide minerals from the point of view of the mineral semiconductor character.

Jan 1, 2014

By Katarina Theander, Robert J. Pugh

In the flotation process, control of the stability of the froth is extremely critical. In the case where the froth is too stable then mechanical entrainment of particles can occur but in the opposite case, where the froth is too unstable and difficult to skimm-off, then a reduction in recovery can result. In minerals and deinking flotation, commercial fatty acids are used and may act as both both collectors and frothers. However, frequently the fatty acids are mixed with nonionic ethoxylated surfactants to give more effective froth control and increase the flotation performance. It is of interest to note from the surface chemistry literature, that such mixtures may cause synergistic effects in surface activity which may explain changes in bubble size, foaming and carry over of particles. In the present study, we have carried out foaming and drainage experiment with oleic acid and model nonionic surfactants; hexa(ethylene glycol) mono-dodecyl ether, C12E6 and tetra (ethylene glycol) mono-dodecyl ether, C12E4 both in separate and mixed systems. Frothing was carried out in a column, equipped with a series of conductivity electrodes which enabled the water content of the froth to be measured along the length of the column, during various stages of the drainage process. The variation in water content of the froth enabled the process to be characterised by distinct three stages; (a) an entrainment state where the water transfer from the bulk phase to the froth was dominant (b) a steady state when entrainment and drainage are balanced and no water is transferred to or from the froth and (c) the drainage step when drainage predominates and the volume of the bulk phase increases. We also carried out surface tension measurements on the oleic acid/ nonionic systems and related the results to the frothing and drainage performance. From the surface tension data, the adsorption interaction parameter of the mixed systems at the air/solution interface could be calculated and was found to depend on the oleate/ nonionic surfactant ratio. This value was related to the frothing performance and the results indicated a positive interaction parameter for the mixed surfactant systems which could explained the synergistic effects in frothing performance.

Jan 1, 2003

By Y. X. Li

In order to control the pulp level in flotation column which has long time-delay and great inertia, and is difficult to establish an accurate mathematical model, a Fuzzy-PID dual mode controller is applied. This method takes advantage of both strong flexibility and good reliability of fuzzy logic and high precision of PID. With the very stable and reliable process instruments, the control system has a good control performance and results the stable control of flotation column.

Jan 1, 2014

By M. Guo

Coal-based Direct Reduction in Interior-combustion Shaft Kiln (CDR/ISK) is a brand-new technique. Compared with the traditional Coal-based Direct Reduction (CDR) technique, its main character is to use Interior-combustion Shaft Kiln (ISK) as the reactor of direct reduction. After being crushed and grinded, iron ore is made into green pellet, which will be surface-coated by coal fines. Then, the surface-coated green pellet can be directly reduced in ISK. The pellet should not be too dry and should be charged from the top of ISK. Oxygen-contained air should be blasted into ISK to keep the temperature in it higher than 1000 degrees centigrade, at which iron oxide will start direct reduction. The reduced pellet will be discharged from the bottom of ISK and after de-surface-coated, spherical Direct Reduced Iron (DRI) can be gained. The volume of carbon monoxide in the off-gas discharged from ISK is less than one per cent. By using this technique to get one tonne DRI, the consumption of coal is about 300kg of fixed carbon, which is much lower than the energy consumption by using other CDR techniques. There is a lot of complex refractory iron ore in China, which remains unexploited. The iron-bearing minerals in this kind of the iron ore can not be beneficiated economically by present technique of gravity, magnetic, flotation or magnetic roasting because the iron minerals are too very finely disseminated to be liberated, or, the iron minerals are too similar to gangue to be separated each other. By using CDR/ISK, complex refractory iron ore can be directly reduced in lower temperature and all kinds of iron mineral can be turned into iron metal. As the grains of iron metal growing larger during direct reduction, magnetic separation can be used to separate iron metal from gangue mineral, thus high-grade iron metal fines can be gained. According to the experiments, the grade of iron metal fines is above 90 percent and the recovery of iron is higher than 90 percent. The consumption of coal to process one tonne of complex refractory iron ore is only about 90kg of fixed carbon.

Jan 1, 2014

By R. X. Li

The overall flow-sheet of producing chromium (III) sulfate is described in this paper. The suitable conditions of each process such as sintering, leaching, aluminum removal, reduction, and de-composition conditions were experimentally studied. The results show it is reasonable to produce chromium (III) sulfate with the flow-sheet pointed out in this research work. The final product is Cr2(SO4)3 solution contained 150~250g/L Cr.

Jan 1, 2014

By Marianella Perez, Williams Calderón, Gonzalo Montes-Atenas

The lack of fresh water sources, particularly in the Northern part of Chile, has driven the mine sites to search for new and sustainable paths to obtain water resources to run minerals processing operations. Among them, the use of seawater in concentrators appears as an interesting solution to this problem. However, the presence of seawater will have an impact onto the operation, not only because it will enhance corrosion reactions in the equipment installed in a plant, but also because it may affect how particles will effectively be processed across the numerous unit operations existing in the mine site. Among such unit operations, the grinding stage is a highly regarded as it defines the success of the separation of valuable minerals from gangue material in the froth flotation operation. Then, one important aspect to be addressed is to understand how the presence of seawater will affect the different mechanisms acting during the operation of a ball mill. The aim of this research work is to assess the effect of changing the aqueous matrix from process water to seawater in ball mills onto the mill performance. The methodology considered the use of Fluent® software and its capabilities to run numerical simulations with heterogeneous media. On one hand, from the data analysis, it is possible to infer that breakability mechanisms should not be significantly affected. On the other hand, the high ionic strength of the matrix should impact importantly particle transport mechanisms within the mill. Particularly, when transporting finer particles. Rheology results were in agreement with previous published research studies suggesting the suspensions to behave as Newtonian, Dilatant o Pseudo-plastic fluid depending on the amount of fine particles present in the grinding media. The latter will result in changes in the residence time of particles in the mill producing overgrinding or an excess in the circulating loads.

Jan 1, 2014

By N. Raeis Hosseiny, S. H. Bassir

"Chador-Malu iron ore is one of the most important iron mines of Iran.About 98 percent of Fe in the ore is in shape of Magnetite, Hematite, Martite, aqua oxide of Iron and the other irons are with ferrous silicates, actinolite, cholorite and ferrous dolomites. 1% of Fe has replaced in pyrite. The phosphor distribution in the ore is non-hemogenous and its average in the whole of the deposit is 94%. It is in shape of Apatite.This mine contains considerable phosphor, which makes it useless for metallurgical uses. At this mine the phosphor is reduced in the iron ore at two steps. At the first step, magnetic part of the ore is separated from the gangues and phosphors by magnetic separator. At the second step, the ore is enriched by the flotation methods. Experimental flotation methods to obtain the optimum conditions are as follows:• Effect of Starch as Hematite depressant with ATRAC as Apatite collector• Effect of Sodium silicate as Hematite depressant with ATRAC as Apatite collector• Effect of ASAM as Apatite collector with Sodium silicate as Hematite depressant• Effect of ATRAC (BEROL) as Apatite collector with Sodium silicate as Hematite depressant• Effect of ASAM & ATRAC mixture as Apatite collector with Sodium silicate as Hematite depressant• Effect of Kcarbonate as pH-modifier• Final test to Optimize pH, Collector, DepressantAt this research we have found the optimum circumstance of the flotation of Chador-Malu iron ore in order to decreasing phosphors of iron oxide and floating of Apatite to make pure Hematite.To reach the optimum conditions, some tests were done with different amounts of pH, collector and depressant. The results are as follows:"

Jan 1, 2003

By M. Brozek, W. Pawlos

"The separation of raw materials in the separator with ferromagnetic liquid occurs due to differences in magnetic and gravitational properties of respective components in relation to each other and to the liquid. In the separator with wedge-shaped pole shoes and the working space axis inclined at a certain angle to the horizontal direction, the paths of grain movement at fixed separation conditions depend on its physical properties. Due to this, the levels of grains outlet from the separator working space are differentiated according to differences in their physical properties. The distance between the levels of outlets from the separator working chamber depends on magnetization of the liquid which is proportional to the liquid density, on the magnetic field intensity and the inclination angle of the separator working passage to the horizontal axis. The separation accuracy is higher the larger is the distance between the outlet levels.The paper will present the methods of visual observation and recording of movement paths of coal grains of different physical properties in the paramagnetic liquid which was the water solution of manganese chloride. The paths were recorded with a video camera in the working chamber by means of a specially constructed device, acting as a periscope, which were then transformed into digital images. Experimental movement paths were confronted to the paths obtained in a theoretical way by means of solving differential equations of movement by a numerical method, achieving good compatibility of experimental and theoretical results. The equations of movement were solved with taking into consideration the drag force, expressed by formula for laminar and dynamic conditions of motion.The course of the path of grain movement depends on grain and liquid physical properties, magnetic field intensity and inclination angle of the working space to the horizontal direction. The two latter parameters can continuously control the process of separation."

Jan 1, 2003

By Heribert F. Broicher, Arne Volland

"The analysis of laser-induced fluorescence (LIF) combines remote sensing techniques with laser spectroscopy. Over variable distances different rock types are identified or changes in the quality of one rock type are recognised. LIF Analysers operate non-destructive, non-contact, on-line and in real-time. Installed over conveyors or over driveways the analysers ""look"" at the moving bulk solids 20 times per second and provide in real-time information for downstream sorting, blending or optimisation of processing. LIF Analysers recognise rock types (hardness information or dilution control), degrees of alteration, degrees of oxidation and –semi-quantitative- content of certain minerals in an ore. Only under favourable conditions quantitative assay information can be obtained, as e.g. the phosphorus content of Kiruna type iron ore.The main application of LIF Analysers is seen in big open pit operations, where the muck is trucked to an in-pit crusher and the crushed rock conveyed out of the pit to its respective destination: e.g. the primary high grade ore to the mill, the low grade or oxidised ore to the leach pads and the internal waste to the dumps.In underground mining and especially in block caving operations dilution control is of utmost importance. Here a LIF Analyser mounted on the back of a pick-up truck can be moved from drawpoint to drawpoint and quickly assess the degree of dilution.Closer to the mill the stockpile management based on LIF analysis will lead to stockpiles sorted according to rock type (hardness), degrees of alteration and oxidation. In case of direct feeding rom ore to the mill the knowledge of the type and quality of all the material between the in-pit crusher and the mill facilitates optimisation of e.g. reagent dosage."

Jan 1, 2003

By Chris J. Martin, Nichola A. McKay

"In mid-2001, North American Palladium commissioned a new 15,000 tonnes per day milling and flotation circuit at their Lac des Iles Mine (LDI), one of only two primary platinum group element (PGE) producers in North America. The mill treats an ore containing 2.3 g/t PGE producing a concentrate assaying 300 g/t PGE, at a recovery of roughly 75%.Top-size control crushing is conducted ahead of semi-autogenous milling. A portion of the SABC circuit feed is crushed to –25mm to increase mill throughput. Product from the SABC circuit is fed to flotation. Flotation consists of roughing and scavenging, with the rougher and scavenger concentrates each being reground using vertimills. Cleaner flotation uses two stages of cleaning using mechanical cells, and a third stage using flotation columns, the column tails being scavenged using a bank of mechanical cells. Rougher concentrate by-passes the first cleaner circuit. Reagents added include amyl xanthate collector, dithiophosphate promoter, MIBC frother and a carboxy methyl cellulose-based gangue depressant.SGS Lakefield Research, together with staff at LDI initiated a structured plant optimisation program comprising on-site testing, bench-scale flotation and mineralogical analysis using QemSCAN. The objectives of the mineralogical studies were 1) to identify feed PGM, their size distribution and mineral associations, 2) establish relationships between the PGM mineralogy and PGM floatability, and 3) characterize the culprit silicate minerals diluting the final concentrate.PGM flotation response at Lac des Iles is clearly bi-modal in nature, with about 60% of the PGM floating quickly, to a high value rougher concentrate. The mineralogical work was able to explain the causes of the bi-modal PGM floatability, which in turn created new opportunities for the metallurgists to optimise the circuit."

Jan 1, 2003

By Joseph Kelly, Christopher Kelsey

This revolutionary super-fine crusher has the unique capacity to generate fine and ultra-fine products from single stage reductions of coarse or fine mineral feeds. The crusher consists of a rotating compression chamber and an internal gyrating mandrel. The axis of rotation of the shell is displaced relative to the axis of the vertically mounted mandrel. The inner surface of the compression chamber is machined as double cone frustums at an angle equal to the displacement angle. Crusher feed is accelerated into a compacted particle bed, which lines the inside of the compression chamber. The depth of the compacted bed progressively increases until the mandrel is engaged. The mandrel is then free to rotate with the compression chamber. Continued feeding increases power draw and triggers the counter rotating mandrel gyration drive. The gyrating mandrel delivers multiple compressions at high pressure to the rotating particle bed. High concentrations of energy are harnessed within a small active volume over short retention times. The combination of extraordinarily high power intensity and extreme compressive force results in primary compressive fracture and induced secondary tensile failure. The axially displaced rotation of the compression chamber effectively distributes the breakage forces throughout the particle bed. This paper covers open circuit, pilot trials on magnetite, perlite, garnet, marble and a copper/pyrite concentrate. Particular emphasis is placed on the extraordinary results achieved with trials on zircon and highly refractory fly ash. The extreme duties were deliberately chosen to demonstrate the crusher’s application scope and potential to impact capital operating and maintenance costs as the technology matures. Super-fine crushing, once considered impracticable has the potential to offer compelling options for the generation of ultra-fine products.

Jan 1, 2014

By Q. J. Liu

The flotation circuit and the reagents of the all-sliming flotation about low grade and hard operation on zinc oxide ore are researched in the paper. The results indicated that there are many types of zinc minerals in this ore, and the composition is very complex. They include hemimorphite, smithsonite, hydrozincite and so on. The ore is seriously sliming. In light of the ore properties, three kinds of flowsheets have tested. They are gravity concentration (cleaning tables), flotation, combined process of gravity concentration and flotation. The test showed that the recovery of zinc is only 17.08% in the gravity separation. In combined process of gravity separation and flotation, the recovery of zinc concentrate is close to 70%. But the flow-sheet is complex and hard to control in the production. The floatation circuit is feasible. In the test, it pay attention to investigate the new combined reagent which is used in selective all?sliming flotation process. The effects of slime are eliminated by the multi-loop treatment of middling. In flotation, the final recovery of concentrate is 88.76%; the grade is 29.50%. The recovery of physical ore is 93%; and the recovery of -10mm fraction is more than 65%.

Jan 1, 2014

By Peter N. Holtham, Mary M. Ng

"Resistivity measurements of minerals in the laboratory are commonly made with a low DC voltage source. Common test voltages specified in the ASTM Standard D257 are 100, 250, 500, 1000, 2500, 5000, 10000 and 15000 V, however 100 and 500 V are the most frequently used. Resistivity results obtained in the laboratory have been used to infer the electrical behaviour of minerals undergoing electrostatic separation. However because the voltages employed in electrostatic separation in the plant are of the order of thousands of volts, typically greater than 15000 V, whether the laboratory results are applicable as a predictor of plant performance is a critical question. It is unclear whether resistivity values taken at a low voltage are characteristic of those seen in electrostatic separation, in which the minerals are exposed to a much higher voltage. No definitive answer could be found in the literature.In this work, the resistivities of zircon, rutile and ilmenite were measured in a corona field for the first time. The measurement principle was based on a technique developed to measure fly ash resistivity in electrostatic precipitators, however the test apparatus and findings are novel.Resistivities of rutile and zircon were found to be easy to measure. The values measured in a corona field were several orders of magnitude less than those obtained with a dc voltage of 100 V. Evidence of back corona was observed with zircon. When the voltage drop was greater than the sample layer could withstand a localised electrical stress developed, resulting in a voltage breakdown, at which point a sudden surge of corona current (back corona) was detected in the sample layer. Rutile, on the other hand, exposed to the same conditions as that of zircon (i.e. same temperature and applied voltage) did not exhibit any sign of back corona. Its resistivity across the range of test voltages (14 to 33 kV) remained fairly constant."

Jan 1, 2003