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By R. O. Dannenberg

The Bureau of Mines investigations described in this report were undertaken to devise a process to economically recover precious metals and copper from low-grade, complex electronic scrap generated in large quantities by military and civilian electronic operations. Leaching with various media is applicable to certain selected items of electronic scrap but cannot be practically applied to complex mixtures of scrap. A process comprising incineration, caustic leaching to remove aluminum, smelting with a siliceous slag, and electrolysis recovered 99.9-percent-pure copper metal and anode slimes assaying more than 7,000 ounces per ton of combined precious metals. Silver, gold, and copper recoveries were 93, 95, and 87 percent, respectively. Cost analysis indicated that an alternative process using direct smelting of the scrap to make assayable products for sale to a custom smelter would provide better overall financial returns.

Jan 1, 1972

By D. Harrington

Fine ventilation was discussed. much more 15 to 20 years ago than it is now, yet today there are tendencies in connection with ,-line ventilation (in fact, numerous ventilation systems have been installed in recent years) indicating that the lessons learned by bitter experience in the past either have been forgotten or lave not been brought to the attention of the present generation. Possibly, the mining min of today considers that conditions have changed so much that experiences of the past cannot be repeated today. At any rate, it seems desirable to restate some of the principles of mine ventilation that were understood more or less in the past and to call attention to some danger in connection with present-day trends or practices.

Jan 1, 1939

By Bruce I. Thomas

In 1943, the Bureau of Mines investigated the occurrence of cassiterite in the gravels of Morelock Creek which flows into the Yukon River 32 miles east of the confluence of the Yukon and Tanana Rivers in central Alaska. Samples of the gravels were obtained by churn drilling test pitting, shaft sinking, and open-cut mining. The gravels along Morelock Creek are about 6 feet in depth and covered with about 2-1/2 feet of overburden. The overburden is frozen, but the underlying gravels are not. Cassiterite, with gold and other heavy minerals, is usually concentrated in the first 2 feet of' gravel above bedrock and in some places penetrates into joint planes in the bedrock. The various methods of obtaining samples are discussed, and drill logs and analyses are tabulated in this report.

Jan 1, 1948

By Leonard Obert

[Tng occasional. rock noises in a nice caured by brc,*ing and ripping of the back, settling, and other cailscr, are well-known tc~ a11 mining en- gineers. These noises oftcn prececte certnin tpes of rock failure as such are used to e certain event a; w:,rnlngs. Senides t5ese audible rock noisee t'nere are, l?o\;evpr, even Iprger nw.iber of' s;Lba.J^;li5le rock mis~s, which must; be piclcell UT with sole type of vi-urr,tion rnicroyhoce and qli- fied in order tnnt :hey n;ny e heard. It v:zs s~v;,yestec" Ir, an evlier ? ,I a.ldible noises Ifureau of I.lines s~zb:ic;et.iod that n stud:r of t!ler;c! *- t mig!!t be useful ir. de temining roc^ movemrnt 3 preceding failure.]

Jan 1, 1941

By Leonard Obert

[Tng occasional. rock noises in a nice caured by brc,*ing and ripping of the back, settling, and other cailscr, are well-known tc~ a11 mining en- gineers. These noises oftcn prececte certnin tpes of rock failure as such are used to e certain ev';ent a; w:,rnlngs. Senides t5ese audible rock noisee t'nere are, l?o\;evpr, even Iprger nw.iber of' s;Lba.J^;li5le rock mis~s, which must; be piclcell UT with sole type of vi-urr,tion rnicroyhoce and qli- fied in order tnnt :hey n;ny e heard. It v:zs s~v;,yestec" Ir, an evlier ? ,I a.ldible noises Ifureau of I.lines s~zb:ic;et.iod that n stud:r of t!ler;c! *- t mig!!t be useful ir. de temining roc^ movemrnt 3 preceding failure.]

Jan 1, 1941

[1.1. The provisions of this code are minimum provisions and are designed to minimize hazards to life and property in and about underground coal mines where electrical equipment and circuits installed used. They indicate the Steps necessary in the selection, installation, operation, inspection, and maintenance of electrical equipment and circuits to obtain proper safeguards in reducing electric shock, fire, explosion and other hazards. Surface as well as underground installations were considered in formulating the code and, unless otherwise stated, each provision applies equal to both underground and surface installations. This code does not apply to buildings and installations not directly connected with mining operations, nor does apply to strip-mining operations.]

Jan 1, 1952

By George S. Rice

A novel method of extinguishing a mine fire in a stowed or gob-filled area by employing liquid carbon dioxide under high pressure eras used recently with success at the President (Prasident) coal mine, Bochum, Germany, as reported by P. Cabolet in Gluckauf (Apr. 24, 1937, p. 393) The use of carbon dioxide gas as a fire-fighting agent in surface plants and in ships is now general practice in the United. States, but when it has been tried for extinguishing fires in mines in large areas more or less confined by stoppings it has not been successful. Examples of the latter method of attempting to fight mine fires are given in Bureau of Mines Bulletin 229, Fifty-Nine Coal-Mine Fires; How They Were Fought and That They Teach, by G. S. Rice, J. VT. Paul, and 14. VT. von Bernewitz (1927). The reason for its nonsuccess may be either that the stoppings are not tight or that the roof and pillars are more or less fissured and enough air passes into the area to sustain a slow fire, whether of spontaneous origin or produced by gas explosion or other source of ignition.

Jan 1, 1937

By J. E. Conley

Available statistics show that the demands of the American chemical industry for sodium sulphate have been increasing slightly in recent years. The supply from domestic sources, particularly In the form of byproduct salt cake from the acid manufacturers, has been tending to decrease due to the growing manufacture of synthetic acid. Both hydrochloric and nitric acids are being synthesized from their elements. The natural result has been that a smaller amount of salt cake is available. Simultaneously, the expansion of the Kraft paper industry, especially in the South, has brought about greater demand for sodium sulphate in that section. This dean is being met by domestic byproduct salt cake, by imported German sodium sulphate made from potash waste liquors, and by favorable situated domestic deposits of Glauber salts and tile anhydrous salt, thenardite. No shortage of natural sodium sulphate exists in the United States, but usually such deposits occur in semiarid regions far removed from transportation facilities and from markets. Moreover, the major portion of the natural deposits is Glauber salt or mirabilite (Na2SO4 ? 10H20), which must be dried or dehydrated in order to meet consumer requirements. The water of hydration represents, roughly, 55 percent of tae total weight of the crude salts and therefore has a very important influence on transportation costs. In marry instances the cost of getting, even the dehydrated product to market is the deciding economic factor. Therefore, the recovery oil production of anhydrous sodium sulphate from plant-.waste liquors or from natural brines of suitable composition might be economically feasible. The U.S. Bureau of Mines, at its nonmetallic Minerals Experiment Station, New Brunswick, N. J., has, for a number of rears, been investigating the commercial possibilities of treating the complex saline mineral polyhalite (K2SO4?NgSO4?2CaSO4?2H20) for the recovery of potash and magnesia. Certain proposed processes (1, 2, 3, 4)4/ yield waste liquors that contain the bulk of the magnesium and sulphate originally combined as magnesium sulphate in the polyhalite molecule. Sodium chloride In limited concentrations is also present, as extensive beds of salt occur in strata overlying the polyhalite deposits. A typical waste liquor would contain:

Jan 1, 1936

By J. E. Conley

[Available statistics show that the demands of the American chemical industry for sodium sulphate have been increasing slightly in recent years. The supply from domestic sources, particularly in the form of byproduct salt cake from the acid manufacturers, has been tending to decease due to the growing manufacture of synthetic acid. Both hydrochloric and nitric acids are being synthesized from their elements. The natural result has been that a smaller amount of salt cake is available. Simultaneously, the expansion of the Kraft-paper industry, especially in Lie South, has brought about greater demand for sodium sulphate in that section. This demand is being met by domestic byproduct salt cake, by imported German sodium sulphate made from potash waste liquors, and by favorably situated domestic deposits of Glauber salts and tile anhydrous salt, thenardite. No shortage of natural sodium sulphate exists in the United States, but usually such deposits occur in semiarid regions far re¬moved from transportation facilities and from markets. Moreover, the major portion of the natural deposits is Glauber salt or mirabilite (Na2SO4?10H20), which must be dried or dehydrated in order to most consumer requirements. The waters of hydration represents, roughly, 55 percent of tae total weight of the crude salts and therefore has a very important influence on transportation costs. In marry instances the cost of getting even the dehydrated product to market is the deciding economic factor. Therefore, the recovery or production of anhydrous sodium sulphate from plant-waste liquors or from natural brines of suitable composition might be economically feasible.]

Jan 1, 1936

By Wing G. Agnew, John A. Johnson, McHenry Mosier

"INTRODUCTION AND CONCLUSIONSThe first three reports of investigations 5/ in this series, pertaining to the investigation of stemming at the Mount Weather Testing Adit dealt with the dust produced by blasting, the effect of stemming on gases generated by blasting, and the relative advantages and disadvantages of different types of stemming and no stemming when used with 60-percent ammonia gelatin dynamite.This report covers an investigation of the length of stemming material through which a primer will fire and detonate a charge of dynamite, such as a missed hole.The practice of drilling a new hole a foot from a missed hole to blast out the missed hole should be prohibited. It is dangerous, as is evidenced by the number of miners killed through drilling into missed holes. It is even more hazardous in a mine on a multiple-shift basis, in which the same miners do not drill succeeding rounds."

May 1, 1942

By Jesse L. Hoyer

A Bureau of Mines turbomill was evaluated for use in the production of high-purity, ultrafine x-Sic powders suitable for advanced ceramics that could substitute for high-temperature alloys containing critical materials such as chromium, cobalt, and nickel. The effect of milling param-eters, such as type of dispersant, temperature, pH, and gas environment, on the milling of x-SiC was studied. The addition of dispersants improved the grindability of x-SiC. Of the six dispersants studied, the best results were obtained with Mara-sperse N-22. Grinding efficiency was also increased when the x-SiC was milled in a basic slurry and at elevated temperature. Gas environments did not appear to affect grinding of x-SiC. Optimum grinding efficiency was obtained at 50° C in a slurry at pH 9.5 with Marasperse N-22 as the dispersant. Under these conditions, minus 100-plus 200-mesh x-SiC was ground to 80 pct less than 1 um in 4 h.

Jan 1, 1987

By W. A. Haley

This is the second of a series of publications that describes the progress of mechanical longwall coal mining in the United States in which a German coal planer was employed.3/ Details of the equipment, a description of its operation, and the results obtained in mining the experimental panel were published in the preceding report. Experimental mining with the planer in the first panel showed an improvement in performance over conventional mining methods at the coal company's Stotesbury 11 mine. The work, which was begun on an experimental basis, soon proved successful, and the coal company purchased the equipment for continued use. Two panels, adjacent to the first, were developed and mined with the planer. Each of these panels was shorter than the preceding one because water seepage from a surface creek limited development. On completion of mining in the third panel, the planer equipment was moved by the cooperating company to a nearby mine operated in the same coal bed where a large area of coal suitable for planer mining is available.

Jan 1, 1954

By Frank J. Wiebelt, Spangler Ricker

"INTRODUCTION Bauxite, in Appalachian Alabama, occurs in the Rock Run and Goshen Valley districts in Cherokee County; in Nences Creek Valley near Jacksonville; near Anniston in Calhoun County; north of Fort Payne in DeKalb County; near Ashville in St. Clair County; and near Talladega in Talladega County.In February 1942, Preston E. Cloud, Jr., assistant geologist, Federal Geological Survey, began a study of these bauxite deposits and the geology relating thereto.The Bureau of Mines established field headquarters at Piedmont, Calhoun County, in July 1942. Mineral agreements covering a total of 11,097 acres were executed with 15 landowners in the Rock Run district; 38 in the Goshen Valley district, covering 7,575.5 acres; and 3 in the Nances Creek Valley district, covering 988.5 acres. Drilling was done on.the properties of 9 land¬owners in the Rock Run district, and on the property of 1 landowner each in the Goshen Valley and the Nances Creek districts. Drilling began October 26, 1942, and ceased on May 17, 1943.Power drilling was supplemented by a labor crew that drilled hand-auger holes in shallow deposits and sampled .old shafts, mines, and mine dumps.In all, 222 holes for a total of 13,250 feet were drilled. Of these toles, 88 penetrated bauxite but too low in grade to constitute ore."

Mar 1, 1948

By A. Bartkowiak

The lower flammability limit of methane at 0 p.s.i.g. and ambient temperatures is 5.6 volume percent in chlorine, 5.2 in oxygen, and 5.0 in air. The corresponding upper limit values are 70, 60.5, and 15 volume percent, respectively, so that the range of flammable mixtures is greater in chlorine than in oxygen or air. The lower flammability limit of ethane at 0 p.s.i.g. and ambient temperatures is 6.1 volume percent in chlorine, 3.0 in oxygen, and 2.9 in air. The corresponding upper limits are 58, 66, and 12.5 volume percent, respectively. In this instance the range of flammable mixtures is greater in oxygen than in chlorine or air. Generally, the limits of flammability for both methane-chlorine mixtures and ethane-chlorine mixtures widen with increases in temperature and pressure.

Jan 1, 1960

By Wesley A. Grosh

The Valzinco mine, Spotsylvania County, Va., is a lead-zinc deposit with minor quantities of copper. The property was reopened n 1942 by Panaminas, Inc. The Bureau of. Mines, in an effort to increase the reserves of the deposit to justify greater production, diamond-drilled nine holes totaling 4,213 feet during 1943. Drilling by the Bureau delimited the original ore body and discovered another ore body on the hanging-wall side, which was being developed by the company at the close of the project.

Jan 1, 1949

By W. H. Emens

[This circular is one of a series dealing with tie development and equip¬ment of small and medium size mines, and with the costs of such work prior to productive operation. The preparation and publication of these papers by the Bureau off Mines has been made possible through the cooperation of various min¬ing and development companies. The bureau of Mines has published a series of circulars dealing with min¬ing methods and costs at a large number of producing nines in the United States, Canada, Mexico, an, other countries. Unit costs of development work, shaft sinking, (rifting, crosscutting, tunneling, and raising are usually much higher in the preliminary development of a property than during its productive life.]

Jan 1, 1933

By Frank L. Hess

In 1876 cassiterite was identified in the placer gold from the northern Black Hills, and such a mixture could have come only from Nigger Hill or one of the streams draining the hill, because in no other hart of the northern hills have cassiterite anti gold been found together. Nigger Hill is in western Lawrence County, South Dakota, and on it is the little camp of Tinton. The Wyoming line runs along the west side of the hill and crosses the ridge which is the hill's continuation about miles north-northwest of Tinton.

Jan 1, 1938

By Jeanne A. Zimmer, Brad Smith, Steve Viles, Andrew B. Cecala

A recent report evaluating silica exposure levels in the metal/nonmetal mining industry noted that bag packaging and loading are some of the occupations at the greatest risk. In addition to dust problems, the bag-stacking process is labor intensive, making lost-time injuries common due to back fatigue and strains. During the bag-stacking process, a significant amount of dust can be generated, mainly from product on the outside of the bags and from dust escaping the bag valve upon impact of the bag on the pallet. In an effort to address dust-exposure and back-fatigue issues, Malvern Minerals Co., Hot Springs, Ark., made two major improvements to its ground silica stacking facility. First, the company purchased a semi-automated bag palletizing system (Figure 1). With this system, the bag stacker does not lift the bags, but slides them across a metal table. Small jets of air exit through perforations in the table top (similar to an air hockey game), allowing workers to more easily slide each bag into the proper position. After each layer of bags is completed, the table slides open, and the entire layer of bags is loaded onto an underlying pallet. The table then closes, readying it for another layer of bags. After the entire pallet is loaded, the unit delivers the pallet to a shrink wrap and forklift pick-up area. In addition to this semi-automated palletizing unit, Malvern Minerals purchased an Overhead Air Supply Island System (OASIS) to lower the bag stacker's dust exposure. The OASIS takes outside air, directs it through MEASURING RESPIRABLE DUST The bag stacker's respirable dust exposure was monitored using a RAM-1 instantaneous dust monitor to evaluate the impact of the various changes on the palletizing process and dust-control equipment. The bag stacker wore a vest that held the 10-mm Dorr-Oliver cyclone, which classifies the respirable portion of dust. Flexible tygon tubing was used to connect the cyclone to the RAM-1 dust unit, allowing the bag stacker to perform the palletizing process with minimal interference. The RAM-1 measures respirable dust concentrations by light scattering with a sensing chamber. This device closely simulates gravimetric measurements when calibrated for a specific dust. This instrument is ideal for comparative evaluations, as was the case in this study. Since the RAM-1 is not an MSHA-approved instru¬ment for dust compliance sampling, the dust concen¬trations listed in this article should be used as a com¬parative value of respirable dust concentration and not to determine actual dust concentrations from a com¬pliance standpoint.

This pamphlet and the enclosed video describe a safe, effective and economical method for removing dust from work clothes. Background Information Dusty work clothes can increase a worker’s exposure to respirable dust. Respirable dust is usually considered to be particles having an aerodynamic diameter of 10 microns or less and able to enter and deposit in the gas-exchange region of the human lung. A former U.S. Bureau of Mines report documented a 10-fold increase in worker dust exposure on a number of separate occasions from dusty work clothes.* It was found that once clothes become contaminated, they are a continual dust source until cleaned. The only MSHA approved method to clean work clothes requires a HEPA-filter vacuuming system which is very time consuming and difficult to perform effectively. Therefore, most workers use a single air hose (not MSHA approved) which can elevate dust levels for the worker, co-workers, and the work environment. A substantial amount of engineering technology has been developed that, when applied, can significantly lower respirable dust exposures of workers at mineral processing plants. But even with these improvements, some workers continue to exceed their permissible exposure limit. Elevated exposures increase the potential for developing debilitating or fatal lung diseases. ?e clothes cleaning method described within is an example of a continuing effort to reduce the potential for developing these lung diseases. Information about engineering research by the former U.S. Bureau of Mines and NIOSH can be found online at www.cdc.gov/niosh. ?is website can also be used for obtaining NIOSH information about health hazards associated with crystalline silica.

By L. R. Burdick, J. F. Barkley

"The agglomerating index of coal is an index based upon the nature of the coke residue left when the standard volatile-matter determination of the well-known proximate analysis is made. In this determination a small amount of coal is heated in a container to about 950° C. (1,742° F.), at which temperature the volatile matter is driven off, leaving a coke formation. The coke residues for various coals are quite different in physical structure: and, for some time past, work has been done on studies of the nature of these residues in connection with the coking of coal. In 1934 Gilmore, Connell, and Nicolls proposed use of the agglomerating index for indicating the dividing line between noncaking coals and those having weakly caking properties. 4/ Its use was adopted in the standard classification of coals by rank as a requisite physical property index to differentiate semianthracite from low-volatile bituminous coal and also high-volatile ""C"" bituminous from subbituminous ""A"" coal, as shown in table 1, the standard coal classification adopted by the American Society for Testing Materials and the American Standards Association. 5./In studying the agglomerating properties of coals based on the coke residue the Bureau of Mines has adopted the notation given in table 2. Coals that in the volatile-matter determination give a coke residue either in the form of an agglomerate button that will support a 500-gram weight without pulverizing or a button that shows swelling or cell structure are considered to be agglomerating."

Nov 1, 1938