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By J. B. Stott

The performance of an adiabatic calorimeter for measuring heats of oxidation of coal is assessed and suggestions made for its improvement and calibration. The use of magnetic analysers for measuring small oxygen deficiencies in air is described and three different methods of measuring the output for such a meter are characterised. The occurrence of spontaneous heating in an 800 tonne heap of Wyoming coal is briefly described. The major part of the report deals with the oxidation of Pittsburgh seam and Wyoming subbituminous coal and describes an experiment in which 1 tonne of Wyoming coal is stored in a 5 metre long insulated container whilst air was passed through. Temperature rises, rates of oxygen absorption and gas compositions of the air stream were measured. The report relates the results of these-experiments to a theory of spontaneous heating developed by Stott and Quan which stresses the importance of the moisture content of the coal and the relationship between the heat necessary to evaporate this water to the heat available from coal oxidation. The work was carried out over a five month period and the emphasis is on demonstrating the effects of moisture transfer and confirming the theory of Stott and Quan.

Jan 1, 1980

By J. F. Barkley

"A knowledge of the carbon dioxide (002) content of the products of combustion, particularly from the boiler furnace, is very valuable. An instantaneous indication of the CO2 can be used as a useful guide to efficient burning. A permanent record over a. period of time gives a story to the management which tends to keep the operators more alert. Many instruments that indicate and record CO2 have appeared within the last fifteen years. More are about to appear. Although simple principles involving chemical, physical, or electrical qualities, are being used, there is at present a general feeling of uncertainty about such instruments in the boiler room any instruments are bought, run awhile, then lie idle indefinitely.Inquiries as to CO2 machines continually come to the Bureau of Mines from the general public, as well as from other branches of the Government. Some ten years ago a series of tests was made on certain instruments at that time on the market. The following test was made quite recently on four of the newer types, including one using an electrical principle. The four instruments were installed on one boiler each, according to the instructions of the makers, and the recommended routine attention was given them. The test was of a service nature duplicating the conditions under which the instruments ordinarily serve. The boiler that was available for this purpose was practically banked for some hours of the night. This caused the average CO2 for the entire twenty-four hours to be rather low, although it reached the higher ranges of the instruments during the day.Each day the charts were averaged and the results plotted to form the accompanying curve. The record of each instrument is shown by its particular mark, the dot, circle, cross and square being used in addition there is plotted for each day a rectangular area representing 1 % CO2 in height. The proper positions of this area was determined by means of the Crsat. Where the plotted point for an instrument falls within the rectangel its accuracy is within 1/2% CO2, which is considered satisfactory. Where it falls outside the rectangle, inaccuracy is indicated."

Mar 1, 1925

By Larry L. Anderson

Enormous quantities of organic wastes are produced each year in the United States. The total amount is in excess of 2 billion tons and at least 880 million tons of this is moisture- and ash-free organic material (dry organic solids), representing a potential energy source of significant magnitude that is not being utilized. Bureau of Mines scientists have developed methods for converting these wastes to convenient energy forms. This report itemizes and evaluates for the first time in detail the quantities and sources of moisture- and ash-free organic material contained in manure, urban refuse, industrial wastes, sewage solids, and agricultural wastes in the United States. Furthermore, estimates are presented for amounts of organic wastes collected or concentrated. The potential for fuel, either oil or gas, from both the total organic wastes generated and those collected or concentrated is also estimated.

Jan 1, 1972

By John C. Machisak

INJURY experience and employment data at all metal mines in the United States and Alaska are presented in this Information Circular for the calendar year 1958. This publication covers the metal mining industries, and contains statistical data on injuries and employment pertinent to metal mines, ore-dressing plants, and primary nonferrous smelters, refineries, and reduction plants. These operations report injury and employment information annually to the Bureau of Mines on a voluntary basis. The Bureau is authorized to make requests for such data, and the information submitted contributes immeasurably to the promotion of safety in the metal mining industry. Every effort has been made to make the annual canvass as complete as possible. This publication contains, along with production and development workers, the office employees at the mine location. The metal mines identified in this publication are classified according to the mineral ores mined; that is, copper, iron, lead-zinc, gold-silver lode, gold placer, and miscellaneous metals.

Jan 1, 1962

By Larry A. Haas

Carbonyl sulfide (COS) was decomposed to sulfur and CO in a silent electrical discharge. A threshold of about 4 kv at 60 Hz was required to dissociate the gas in a laboratory ozonizer at 790 torr with electrode gaps between 1 and 5.5 mm. Above the threshold value, the reaction rate increased with increasing voltage with helium or nitrogen diluent. With the latter diluent, higher voltages had to be applied to obtain the same yield in the 4-to 12-kv range. The COS decomposition rate increased with COS concentration, but a saturation value was reached at about 10 pct COS. The reaction rate decreased at low linear gas velocities as obtained at lower gas flows, larger electrode gaps, or larger reactor volumes. Increasing gas temperature also decreased the decomposition rate. The presence of solid adsorbents such as quartz wool, bauxite, or charcoal had no significant effect on the reaction rate. The addition of S02 did not affect the COS decomposition rate, but small amounts of water decreased the reaction rate. Over 50 pct of the COS was decomposed at room temperature and atmospheric pressure in a l7-kv ozonizer using a gas containing 0.9 pct COS in helium flowing at a rate of 0.3 liter/min. The average current was less than 5 ma. This method has possible application in eliminating the toxic air pollutant, COS, which is generated in petroleum refineries and in processes involving reactions between sulfurous and carbonaceous materials. Carbon monoxide that is formed can be further oxidized to CO2 after the collection of elemental sulfur.

Jan 1, 1972

By Kenneth J. Miller

The Bureau of Mines conducted an investigation to improve the flotation response of coals that are difficult to wash by froth flotation. A literature survey and experimentation showed that, for the most part, refractory coals can be floated with oily collectors and frothers. Collector reagent consumption can be minimized and the selectivity of the flotation enhanced by assuring adequate, but not prolonged, reagent conditioning. Where flotation selectivity is especially poor, two-stage rougher-cleaner flotation is recommended. It was concluded that a major problem with refractory coals is predicting when they will appear in a flotation circuit so that supplementary flotation collectors can be added. Coal losses due to variation in the floatability of the feed might be reduced if a nonpolar collector such as kerosine or fuel oil is used along with a frother as general coal flotation practice.

Jan 1, 1977

By Rudolf E. Greuer, Linneas W. Laage, Xinton Chang

INPUT FORMAT INSTRUCTION FILE FOR PROGRAM MFIRE GENERAL RULES FOR DATA INPUT: $THERE IS NO NEED TO DISTINGUISH INTERGER AND REAL NUMBERS. $ $ SYMBOLS FOR NUMERICAL INPUT INCLUDE THE FOLLOWING $ $ 1234567890 -+BLANK $ $ * FREE FORMAT IS ALLOWED. COMMA AND BLANK SPACE CAN BOTH BE $ $ DELIMITERS. SEQUENTIALLY DISTRIBUTED BLANK SPACES ACT AS ONE $ $ DELIMITER. BLANKS ADJACENT TO A COMMA HAVE NO DELIMITING EFFECT $ $ * A ZERO INPUT CAN BE OMITTED BUT NOT THE DELIMITERS EXCEPT WHEN $ $ THE ZERO INPUTS ARE THE LAST ONES ON A LINE. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS "$ IS AN INSTRUCTION $ $ LINE WHICH WILL BE IGNORED IN A PROGRAM RUN. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS NEITHER ONE USED IN THE $ $ ABOVE LIST FOR NUMERICAL INPUT NOR "$, OR WHICH CONTAINS MORE $ $ THAN 3 SYMBOLS OUTSIDE OF THE LIST, IS A COMMENT LINE WHICH WILL $ $ BE SHOWN IN THE OUTPUT FILE. $

Jan 1, 1990

By Bing W. Jong

A bench-scale evaluation of coal and coal waste materials as aggregate materials for use in longwall mine supports was undertaken as part of the Bureau of Mines Health and Safety program on ground control. Performance data were obtained on portland cement concretes (PCC) prepared with coal and coal wastes as aggregate materials. The effects of high-early-strength accelerators on strength and creep and of superplasticizers on strength properties of PCC formulated with coal and coal waste were investigated. Concrete formulated with a high-early-strength accelerator and coal and coal waste has 20 and 40 pet greater compressive strength, respectively, than the control samples without admixture. A concrete formulated with coal waste and the high-early-strength accelerator, using four bags of cement per cubic yard and a water-cement ratio of 1.0, had the lowest creep value of all the coal- and coal-waste-formulated PCC's tested.

Jan 1, 1983

By John R. Reeves

The principal oil aha.le in Indiana ie known as the New Al'baZ\Y shale. It 11 ot Devonian age, and ia usually correlated with, although not certainly of the 1ame age a,, the Antrim shale of northern Michiga.. the Ohio shale of Ohio, and the Chattanooga shale ot Kentucky. Termescae • a."ld Georgia. The nqtmal thickneaa of the formation 1n Indiana 1e a.bout 100 faet, ltbough 1n the region of its out­ cro;l the tall th!::kne,111 io rarely exposed because cf the general d:.p of the strata, which is 11 about 30 feet per mile to the west. With the exception ot thin local pha1e1, the entire thickness is oil shale,

Aug 1, 1922

By Wing G. Agnew, John A. Johnson

"INTRODUCTION This paper is one of a series being published by the Bureau of Mines pertaining to an investigation on the use of stemming in metal mines now being conducted at the Mount Weather Testing Adit. Its purpose is to compare the amount of dust and gases produced as a result of blasting charges of dynamite (1) in drill holes, (2) in bombs, and (3) in mud-cap or adobe shots.ACKNOWLEDGMENTSValuable assistance and advice on stemming were given by members of the staff at the Bureau of Mines, as acknowledged in previous publications. 4/TEST PROCEDUREThe results used for comparison in this report are from dust and gas samples taken after blasting (1) four regular test rounds with no stemming, (2) five bomb shots, and (3) two mud-cap or adobe shots.The four rounds were the standard 26-hole test rounds designed to break 4 feet of rock. The procedure for drilling and blasting these rounds is described in Report of Investigations 3509.Before the regular test rounds were blasted, about 1,200 bounds of fine rock was placed on the steel mucking sheets that covered the end of the adit track; the wails, hack, and floor of the adit were washed thoroughly; and the fine rock on the mucking sheets was completely wetted.Each of the 5 bomb shots consisted of 10 sticks of dynamite tied together and hung at midpoint of the adit, 8 feet from the fall."

Dec 1, 1942

By Richard S. Watt

The Bureau of Mines is often called upon to analyze the demand for various minerals and fuels and to make projections of the future demand. Because minerals and fuels are raw materials and because the demand for raw materials [pends] on the demand for finished goods, these projections are usually [conned] with derived demand rather than final demand. In order to obtain quick [d] reasonably accurate analyses of the demand for mineral commodities, the [reau] developed a method and has used it successfully (31).4 To illustrate the [thod], this report presents a full analysis of the demand for a mineral commodity with enough general theory to permit application of the method to any mineral. Sodium chloride (common table salt) was chosen as the subject of the analysis because the demand for it is less complicated5 and permits a simple application and clear presentation of the method.

Jan 1, 1962

By Walter B. Lenhart

This paper is one of a series on milling methods and costs being. published by the Bureau of Mines. The milling practices and special problems relating to grinding, tailings disposal, and choice of a treatment process at the Cardinal mill are discussed. The property of the Cardinal Gold Mining Co. is about 18 miles southwest of the town of Bishop, Inyo County, Calif., at an altitude of approximately 8,500 feet. The camp has been designated Bishop Creek by the postal authorities. The property comprises 33 mining claims, including fractions and millsite in sections 19, 20, 29, and 30, T. 8 S., R. 31 E. These claims are located in a general way along the strike of a band of quartzite.

Jan 1, 1938

By Donald W. Mitchell

Research shows that water neutralizes the explosion hazard of coal dust when present in sufficient quantity and when intimately mixed with the dust. The quantity of water required to neutralize coal dust and coal-rock dust mixtures is about equal to the limiting moisture adsorptive capacity of the dust; the adsorptive capacity increases with increase in the fineness and volatile content of the coal. Pools of water or high atmospheric humidity do not reduce the explosion hazard. Although wetted dust is less dispersible than dry dust, poor dispersibility cannot be relied on as the sole safeguard against explosion. Dust mixtures that contain water in excess of their limiting adsorptive capacity are dispersed and ignited by severe initiation sources. Pure coal dust adsorbs water with difficulty and retains water poorly; adsorption and retention is increased by the addition of rock dust the coal; the rock dust agglutinates wetted coal and assures that incombustible is present should drying occur. Therefore, it is advantageous to rock-dust wet areas in bituminous coal and lignite mines. When coal-rock dust mixtures are wetted and subsequently dried, the explosion hazard is about the same as for dust which was not wetted.

Jan 1, 1962

By Paul L. Michael

Roof warring signals from eleven underground coal mines (principally in the Pittsburgh seam) were studied and analyzed. The character of individual acoustic warning signals is shown to be dependent on spectral distribution of energy. Reverberation tires (pulse decay rates) were found to be usually between 0.1 and 0.5 seconds. Listening tests were conducted to assess the miner's ability to discriminate speech and roof talk signals in noise and in quiet, with and without ear protectors and with various levels of hearing loss. The ability to detect roof talk is shown to be generally degraded while wearing car protection in quiet, although, if car protectors are worn only when required by high noise levels, the ability to detect roof talk will be preserved at its maximum.

Jan 1, 1972

By John C. Edwards, Gene F. Friel, John J. Opferman, Robert A. Franks

As the use of deep -rut mining increases, there - expected to be a greater demand for methane (CH,) measurement devices capable of scanning working faces al depths in excess of 10 m to alert mine personnel of hazardous concentrations of CH and to satisfy regulatory requirements. Remote optical devices offer the most promise to satisfy these objectives while the operator remains safely under supported roof. A second¬-generation remote Optical methanomeor (ROM) bas been designed and Is undergoing laboratory evaluation at the National Institute for Occupational Safety and Health. It operates on the principle of differential absorption of the "u;' fundamental absorption band of CH, centered at 3.31 um in the infrared region of the spectrum. The new instrument differs from the previous prototypes by the replacement of the two hand pass differential absorption technique of measurement with a single filter gas correlation technique and a refinement of the amplifier and gating circuitry used within the unit. This results in a more accurate isolation of the CH, spectral absorption band centered at 3.31 um. A specially designed 0.4m-diam variable-length gas mixing tunnel was constructed and instrumented with CH4 sampling capability to calibrate the ROM. Experiments have demonstrated the ability of the detector to respond to various conditions of CH, (pn•m) at distances as great as 12 m. Thermal radiation generated within the instrument is the controlling factor in the drift of the output signal nod, therefore the reliability of the instrument. Several approaches to reduce this extraneous radiation interfering moth the infrared detector, described, such as the installation of a fan in the instrument and thermoelectric coolers on the detector's beat sink. Implementation of this technology will significantly improve the safely of miners.

Jan 5, 1997

By James P. Bennett

To improve construction materials for emerging chemical and metallurgical technologies, the Bureau of Mines is investigating the acid resistance of ceramic materials. In the study described here, eight commercial ceramic materials comprising two red shale, two fire clay, a silica, a silicon carbide, a carbon, and a high-alumina brick were evaluated. Samples were exposed to 20 wt-pct HC1 at 50° C for 110 days. The test apparatus designed to evaluate the materials is described. Changes in chemical and mineralogical composition, cold crushing strength, volume, and weight, and leach rates of AI, Ca, Fe, K, Mg, Na, Si, and Ti ions were monitored. In general, the statistically significant physical property changes that occurred were small. In many cases, no changes were detected.

Jan 1, 1982

By Peter Kovalchikb, Gregory Colec, Syd Peng, R. J. Matetic, Jeffrey Petersond

Mine Safety and Health Administration (MSHA) data indicates that the roof bolting machine is third among all equipment and second among equipment in underground coal mining whose operators exceed the MSHA-PEL (Mine Safety and Health Administration-Permissible Exposure Limit). In response to this, the National Institute for Occupational Safety and Health (NIOSH) has conducted a study to reduce overexposures of noise to operators of roof bolting machines. An important segment of the research is to determine, characterize and measure sound power levels radiated by a roof bolting machine during different drilling configurations. The determined sound power levels generated during the drilling cycle are of major interest because the levels represent the overall sound power generated by the machine. These sound power levels, determined from laboratory tests, can be used to accurately assess the effectiveness of proposed controls for reducing noise exposure to roof bolting machine operators. By using the sound power level results obtained from the laboratory and a commercially available acoustical modeling package, a method for predicting sound pressure levels to roof bolting machine operators for differing drilling types and parameters could be determined. This paper provides a method for predicting sound pressure levels at the operator’s position of a roof bolting machine in an underground coal mine using sound power levels determined in the laboratory. To determine validity, underground coal mine data was also collected to compare predicted and measured sound pressure levels. The results of the predicted sound pressure level data were the same as the underground measured results. This research will provide the mining industry with a valid method for predicting a roof bolting machine operator’s noise dosage underground given any type of drilling configuration or drilling method utilized from laboratory testing.

By V. B. Royer, C. H. Harty

"MANGANESE-SILOCON ALLOYS AS DEOXIDIZERSThe basic open-hearth process for steel mining requires large amounts of oxidized iron for oxidation of the elements carbon, silicon, manganese, and phosphorus which are to be removed from the metal. Some of this oxidized iron (FeO) dissolves in the metal during the refining process, Subsequent to the elimination of the elements named, a considerable amount of dissolved iron oxide must be removed before the metal may be cast into ingot form. The elements generally used, for iron oxide removal, or deoxidation, are silicon, manganese, and aluminum. Silicon and manganese are always alloyed with iron, either singly or in combinations of various compositions. Aluminum generally is used in a commercially pure state and sometimes in complex alloys. A double deoxidizer of manganese and silicon alloyed with iron for furnace deoxidation has been the subject of an extensive cooperative investigation between the United States Bureau of Mines, the Carnegie Institute of Technology, and the Metallurgical Advisory Board. Certain grader of steel, especially low-carbon rimming steels, require a low-carbon deoxidizer to keep the finished steel within the carbon specification after deoxidation. ACKNOWLEDGMENTThe authors wish to acknowledge the assistance of J. F. Sanderson and S. S. Johnston in the analysis of the alloys used in this work.PURPOSE OF WORKThe need for definite information as to which compositions of manganese and silicon within a certain manganese-silicon ratio and when alloyed with iron would have an allowable carbon content for the particular grade or type of steel on which the deoxidize is used, prompted the undertaking of this investigation to determine the solubility of carbon in manganese, silicon, and iron alloys within the region bounded by 10:1 and 4:l manganese to silicon ratios. These data should be of value to the manufacturer producing such"

May 1, 1934

By J. Mitchell Linne

The principal mineral commodity in the Orleans Mountain RARE II area (No. 35019) is gold. Gravel deposits along the Salmon River contain placer gold. Lode gold with associated silver is contained in quartz veins. Many placer mining claims have been located within the study area in the Salmon River district. Four placer patents totalling 230 acres were issued for claims on the Salmon River between Lewis Creek and Forks of Salmon. On this same reach of river, adjoining and overlapping the study area boundary, approximately 3.3 million cu yd (2.5 million cu m) of gold bearing gravel with values ranging from $0.51 to nearly $5 per cu yd (50.66 to $6.50 per cu m) (gold valued at $400 per troy oz), are contained in three placers, the Bloomer, Pot Luck, and Horn (table 1). Within the study area boundary there are approximately 950,000 cu yd (726,000 cu m) of gold bearing gravel in these three placers. These three mines yielded nearly 12,000 oz (373,000 g) of gold and more than 300 oz (25,000 g) of silver between 1872 and 1913.

Jan 1, 1982

By J. C. Fowler

The field testing of the Seismic Mine Monitor System is described. This system consists of nine geophones buried about 40 feet deep over a ten-square-mile area, the amplifiers and electronics needed to get the signals to the mine office, and a central processor unit to detect and locate explosions and large roof falls. Since the problems associated with the original installation were solved, this system has worked for 2 1/2 months. The system has detected roof falls in the pillar areas and has located blasts as small as 114 pound of dynamite. The location accuracy has, in general, been within 250 feet. The system is now being used to gather long-term data on the seismic activity of the mine.

Jan 1, 1974