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By W. E. Wallace

Volume-rate-of-flow measurements were made of the flow of mercury through porous samples under conditions of no field, magnetic field transverse to the direction of flow, and transverse magnetic field and electric current to determine if a magnetic method might be potentially useful in the study of pore-size distribution. No change was observed in the flow rate from the application of a magnetic field alone. The application of both field and current produced an electromagnetic pumping action with or against the direction of flow, depending upon the direction of the electric current. This pumping effect was observed to be greater in a rectangular porcelain sample than the calculated value for an equal-Sized open channel.

Jan 1, 1969

By D. K. Ingram

In situ horizontal stresses were measured to determine the influences of geologic anomalies on the regional horizontal stress field in two coal mines in southern Illinois. Stress measurements were obtained near a normal fault having a 121-ft displacement at the AMAX Wabash Mine and a large coalbed want at the Kerr-McGee Galatia No.5 Mine. Horizontal stress measurements were completed using a Bureau of Mines borehole deformation gauge. The average maximum and minimum horizontal compressional stresses at the Wabash Mine were 1,400 and 800 psi, with the direction of maximum stress ranging from N 78° W to N 83° E. At the Galatia No.5 Mine, the averages were 1,500 and 500 psi, with the direction of maximum stress ranging from N 85° E to N 75° E. Generally, the geologic anomalies appear to have no dramatic effect of the regional horizontal stresses. However, subtle differences between stress measurements suggest an influence by the fault zone at the Wabash Mine. The larger anisotropic stress conditions at the Galatia No.5 Mine could be responsible for the increase in kink zones and directional roof failures.

Jan 1, 1988

By David C. Oyler, Hakan Gurgenli, Gregory M. Molinda

Historically, miners have known that roof rocks originally composed largely of mud were prone to slaking and deterioration when exposed to water and humidity. Mine Safety and Health Administration (MSHA) records show that roof falls are more prevalent in summer and late fall. Field data shows higher bolt loads and increased room convergence in summer months. Laboratory data shows that very high internal pressures can be generated by significant strain in clay-rich rocks. In summer months humidities ranging from 70-100% can cause rock strains up to 7%, and rock pressures of 14,000 psi, more than enough to break apart weak shales and fireclays. The National Institute for Occupational Safety and Health (NIOSH) conducted wet/dry immersion cycling of clay-rich rocks. Results show that the rocks most prone to moisture deterioration are fireclays, claystones, and sandy shales, all of which have disrupted bedding. Of the 7 mudrocks with a weatherability index above 40%, none showed consistent fissile bedding. Black shales were surprisingly resistant to wet/dry water immersion cycling. Generally, mixed rocks (stackrock), typically susceptible to horizontal stress, are more resistant to moisture-deterioration. Mine roof rocks tested with moisture sensitivity ratings above 50% (moisture sensitivity index ranges from 0-100 with 100 being the most sensitive) all came from mines which had roof skin problems and used supplemental support to prevent rock fall injuries. Some roof rocks showed lateral variability of moisture sensitivity values, suggesting the need for more samples in highly varying roof rocks. Swelling strains of mudrocks showed that almost all of the swelling occurred in the first 24 hours after immersion. The wet/dry immersion cycling test used provides an accurate, quick and inexpensive method for estimating the moisture sensitivity of mudrocks. With this information mine operators can begin to anticipate hazardous ground and prepare appropriate roof support.

By J. H. Russell

A mathematical modeling method was developed by the U.S. Bureau of Mines for the prediction of the principal equilibrium species in the solvent extraction of nickel. Models were developed for the extraction of nickel from ammoniacal sulfate and carbonate solutions with commercial oxime extractants. Independent variables in the research were nickel concentration, ionic strength, pH of the initial aqueous phase, and extract ants and their concentrations in the organic phase. Results from laboratory shakeout tests compared fairly well with predictions of the equilibrium concentrations of nickel and pH values. For example, the loading of nickel onto the extractant was predicted on average within ±27 pct of the measured values, and the pH to within ± 0.17 pH unit.

Jan 1, 1991

By Stephen E. Stewart

This document presents the explosion-proof enclosures used severity of certification tests solutions to linear transient thermal and stress analyses of in underground mines. The results were used to assess the for enclosure windows relative to possible loads occurring in the actual mine environment. Cast iron electric light enclosures with polycarbonate and glass windows were analyzed under steady state thermal conditions (light burning) and for thermal shocks corresponding to an internal explosion (ignition of volatile mine gas) or external quenching (mine water spray system). Thermal shocks to the enclosure, caused by ignited gases or water spray, were applied via a series of load steps in the transient analysis. The temperature dependence of material I properties and of the film heat transfer coefficients were included in the model. The work demonstrates that thermally induced stresses are strongly influenced by the way the window is mounted in the enclosure. It also shows that the MSHA Thermal Shock Test, if performed on an unsupported lens (or window), produces lower stresses than the lens (or window) may experience in the mine environment.

Jan 1, 1984

By Virgil A. Marple

The primary purpose of this contract was to evaluate methods and techniques by which the size distribution acid concentration of mining-related dusts can be measured. One result has been the development of a portable, battery-operated optical particle counter/ multi-channel analyzer system which can he used to determine the size distribution and concentration of mining aerosols. One important aspect of this program has been the development of a calibration technique which relates the output of the optical particle counter to the penetration of the particles through an impactor: This results in a calibration curve in terms of the aerodynamic or Stokes' diameter or the aerosol particles. Using this technique, calibrations were performed on coal, silica, Arizona road dust, potash, and rock dust (corer ore) aerosols. Another task of this program was the calibration and evaluation of the GCA respirible dust monitors (RMD) 101-1 and 301. The results of evaluation showed that the instruments were within the manufacturer's specification of ±25% of the true mass concentration up to about 15 mg/m , if the dust particles were in a size range from about 0.7 to 10 µm aerodynamic diameter. Particles smaller tan about 0.7 µm were not collected by the instrument and particles larger than about 10 µm were lose in the inlet. Other tasks included performing field studies in cooperative research programs with the Bureau of Mines personnel, development of a portable polystyrene latex generator for use in optical particle counter calibrations in the field. The incorporation of impactor classification devices on the inlets of aerosol mass measuring instruments to give mass size distributions, and a study of the density of coal particles as a function of the particle size.

Jan 1, 1977

By H. Miller

In recognition of the need for a portable low-profile hard rock crusher, the Bureau of Mines sponsored the development of such a unit capable of moving up as the face advances. By allowing primary ore reduction at or near the mine face, the advantages of conveyor haulage From the face as demonstrated in soft ore and coal mines, could be realized for hard rock Brines as well. This report presents the results of a development and testing program for such a portable low-profile crusher, designed by Eagle Crusher Company and called the M44. The unit has an extremely low vertical profile considering its size and capacity. The crushing jaws, which form the crushing lumber, are inclined, with the lower jaw mounted for eccentric movement relative to the stationary upper jaw. This provides efficient crushing while also forcing material through the crushing chamber. As a result, the inlet feeder can be disposed horizontally. To facilitate correct processing of different materials, the size of the discharge opening and the action of the movable crushing jaw are variable. The unit also incorporates a feeder hopper and discharge conveyor that provides for efficient ore handling through the machine. Tests demonstrated the M44 Crusher's high capacity, efficiency and reliability. During testing, it crushed over 120,000 tons of materials of up to 32,000 psi compressive strength at production rates in the 200-350 tons/hour range. The unit operated smoothly under simulated low-headroom conditions, and Proved readily transportable.

Jan 1, 1983

By D. E. Traut

A fluidized countercurrent ion-exchange system was developed, operated, and evaluated by the U.S. Department of the Interior, Bureau of Mines. The system consisted of integrated multiple-compartment absorption and elution columns in which the solution flows were continuous except for short periods when resin increments were withdrawn. The exchange of uranyl carbonate between a simulated in situ uranium leach liquor and a strong-base ion-exchange resin together with the subsequent elution with an ammonium chloride solution was studied. The effects of the number of sections, section height, amount of resin withdrawal, solution flow rate, and column diameter were investigated. The kinetic and equilibrium relationships for the absorption and elution steps were also examined. The experimental data indicate a strong interdependence between variables. Solution retention time appears to be a major limiting variable in the absorption process, while resin residence time is the determining factor in the elution process. The column was efficient over a range of conditions, but close control was needed for optimum operation.

Jan 1, 1978

By Walter Frank

The purpose of the work covered by this contract is to develop a ground and pilot conductor connector which will significantly improve mine trailing cable splice performance. This work compliments the work completed under Contract 00357100 on the development of crimp connectors for the phase conductors of trailing cables. A brief discussion on splice problems is presented as an introductory means and substantiates the need for the development and test programs outlined in this report. As with the phase development work, the ground and pilot connector work is essentially of an empirical nature. As a result time is devoted to explaining the derivations of the test procedures used. In order to familiarize the reader with connector terminology a section is devoted to a glossary of pertinent terms. The connector design effort includes connectors for splicing ground and pilot conductors. A distinction is made between connectors suitable for splicing round and flat ground configurations. The same also applies to the pilot conductors. During the course of this work, much time has been devoted to the question of suitability of round cable configurations for trailing cable applications. This is discussed in detail along with resulting conclusions and recommendations. A field test program was conducted in order to confirm ground and pilot connector laboratory data. This testing also determined the viability of the connector designs and recommended installation techniques in a mine environment.

Jan 1, 1979

By Wils L. Cooley

The report covers tests and criteria for the establishment of safe grounding systems for coal mines. The work deals primarily with under-ground coal mines, but much is applicable to surface mines as well. Included is an extensive guide to grounding and bonding procedures for mine surface substations. Xit-Rods are evaluated and shown to deviate from manufacturer's claims. An analysis shows that very long cables are difficult to monitor using audio frequency ground-check techniques. A method is developed to detect failing cable splices without removing the cable from service. Simulation and measurement are compared for a technique to detect bad rail bonds, and an assessment is made of grounding techniques for dc face equipment.

Jan 1, 1979

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Jan 1, 1981

By Donald E. Redmon

This Bureau of Mines report reviews injury experience in the nonmetallic mineral industries (except stone and coal) for 1968-69. For each of the years, 23 tables summarize disabling work injuries by department, source of injury, extent of disability, part of body injured, and nature of injury. Correlative information on employment, worktime, and operating activity is also presented.

Jan 1, 1973

By D. R. Flinn

A newly developed chemical conditioning technique, which greatly simplifies the preparation of plating baths for the electrodeposition of titanium diboride (TiB2) coatings, is described in this report. The new plating technique was used to prepare samples of titanium diboride (TiB2) coatings on three types of substrate materials. These samples were then evaluated in both low- and high-speed wear-test programs to determine the wear resistance, microhardness, and adhesion of the coatings. In general, it was found that the wear resistance of the coatings is independent of substrate. Scanning electron micrographs have shown that the coating wear surfaces are very smooth, suggesting slow and continuous removal of the coating during the wear test (that is, adhesive wear). Adhesion between the coating and all substrates was excellent. Microhardness results show that the TiB2 coating is harder than alumina, with a hardness value exceeding 5,000 kg/mm2 measured in one test. The results of the wear tests show that TiB2 coatings have relatively poor wear resistance compared with alumina in low-speed unlubricated sliding environments, but exhibit wear properties comparable with alumina in high-speed unlubricated sliding environments.

Jan 1, 1981

By J. B. Zadra

Tungsten metal, chemically equivalent to commercial grade, is produced by electrolysis of impure tungsten compounds or scheelite in an alkali, phosphate or borate electrolyte. A preliminary investigation of fused-bath electrolysis shows the effect of electrolyte composition, temperature, and current density on current efficiency, yield, crystal structure, and purity of product. Experiments show that tungsten can be electrowon from scheelite in a fused alkali, phosphate, or borate bath with similar results. Studies on electrolyte composition show that the addition of sodium chloride is essential to both electrolytes in treating scheelite. Although its main function is to react with or flux the CaO, it also increases the bath fluidity. Temperature studies revealed optimum ranges between 900° and 1,100° C.; 900° C. proved satisfactory for tungsten trioxide, and 950° to 1,050° C. for scheelite. Current efficiencies were satisfactory for all current densities ranging from 10 to 57 a./dm.2. Yields were 400 to 650 g./kw.-hr. over the same current-density range. Crystal size and purity of the product are functions of temperature, current density, and amount of impurities in the electrolyte. Deposited crystals vary in shape from spherical grains to clusters of dendritic hexagonal needles, and in size from smaller than 35 to 570 microns. The purity of the tungsten metal produced ranges from 99.7 to 99.94 percent.

Jan 1, 1959

By Jose P. T. Agapito

Several underground coal mines currently operating in the Beckley District of West Virginia are experiencing serious roof and floor problems. A significant portion of the estimated two billion tons of coal resources may be lost as a result of these ground control problems. Preliminary studies by the Bureau of Mines indicated that these problems are due in part to a high horizontal stress field. During this contract study, a field program was conducted to quantify the horizontal in situ stress. A total of 14 overcoring sites (using the Bureau of Mines strain-relief overcoring technique) in five mines were drilled producing 53 data sets. Analysis of the data was done to provide in situ horizontal stresses for each of the five mine, and for the district as a whole. Stress data indicate horizontal stresses far in excess of that predicted by theory and in some cases, up to six times the estimated vertical stress. In addition to the field testing, a detailed computer modeling study was conducted using finite element and boundary integral (displacement discontinuity) methods. Verification of in situ stresses was obtained by the models and analysis of various development geometries, mining methods and remedial techniques were conducted. Recommendations for reducing ground control problems and future studies are presented.

Jan 1, 1980

A computer program for the static load analysis of linear elastic structures is presented. It is the product of a two-year project for the development of a efficient program for the analysis of mine-type structures. The report is divided into two parts. The first part explains the general method of analysis, the computer program organization and the most significant numerical techniques used. The second part is a user manual for the computer program. The FORTRAN IV computer program deck and example problems were transmitted separately to the sponsor. Request for a copy of the program should be directed to the Bureau of Mines, Denver Mining Research Center.

Jan 1, 1972

By Stephen Krickovic

Air quantity-pressure and methane concentration surveys were conducted by the Bureau of Mines in accessible portions of an area being pillared in a Pittsburgh coalbed mine in West Virginia. These included two mined-out and three active butt headings and a bleeder system. The particular mine workings were started in virgin coal directly from a set of main headings; the main reason for the study was the difficulty usually encountered in adequately bleeding the gobs under such conditions. Although the two separate return airways in each active butt heading and the North and 1 Left bleeders contained acceptable methane concentrations (0.01 to 0.78 percent in the butts and 0.73 to 1.0 percent in the bleeders) with significant total methane removal (109 cfm in butts and 631 cfm in bleeders), there were relatively large areas in the gobs with possible minimal airflows. This condition appears to have developed from lack of systematic regulation of the airflow across the gobs and appears to indicate the existence of considerably more methane in the probably low flow areas in the gob.

Jan 1, 1973

By M. P. Board

The U.S. Bureau of Mines, under a cooperative agreement with Hecla Mining Co., conducted a rock mechanics study at four widely spaced horizons in a deep mine shaft in northern Idaho. The objective of the project was to measure and analyze rock deformation and lining behavior during construction of a deep shaft in a high in situ stress field within an isotropic rock mass. Rock mass displacements were monitored with multiple-position borehole extensometers. Liner stress and strain were measured with concrete pressure cells and embedment strain gauges. This report discusses the general trends and magnitudes of data from the four test sites, and relates the data to a proposed anisotropic constitutive model for the rock mass. A design procedure is then outlined for specifications of liner thickness and support installation sequences for future shaft sinking.

Jan 1, 1989

By H. W. Lang

The Bureau of Mines conducted an investigation to observe the effect of cetane improvers upon nitrogen oxides concentration in diesel exhaust gas. Amyl nitrite and amyl nitrate were used as additives to the fuel used in a four-cycle, single cylinder type test engine. It was concluded that nitrogen oxide concentrations were not enhanced at fuel-air ratios above 0.03 pound of fuel per pound of air.

Jan 1, 1969

By John B. Umhau

[This !m-i~!.al survey giver, statistice.1 data res;?~dirf ~:rimay ard ?eco~- dqr or scmn tin used in thL: United St,ztas by industries an? incluclcz d;ta on stop&apos;ics, ~urchares, ard plnrt losr.c.5. It is :i ml:anwe of consq~tion in terms of fir.is1icd -prcd.~cts nz6.e iry initid ti11 Sabric:,.torc,, that is, aon- cerns that purchzse virc,in zni s~col~d&apos;l~y i.i.5 ti:; 01&apos; tin c;cra.. rav materi,als ar,d co:lrrert them into !ror?ucts such F!: ti:i plz.te, ~lloyr;, and. c?hemic?ls; comy~nias ;~urchn.&apos;.ii~; alloys, ch:rr.ic,~l::, or tin vl?.tc fcr furthcr a:mflzc- ture ?rc: ~-.f>t i~ci~~dcd. Tilit r~lqe:;tionrr::ire submit tod to consunern ar,nt:incd no dofinition of rnr.oncl.:ryr me$.-i; but, ovrirq to ti~i-: a~counti~ procedure used s.l~o~c-:t 1&apos; thu scrnn hac i~-.rtergol:e ch?rri?~ of ovinerzhip or titlo, thc rc!coverod t! n !its b~en i-c<;,r(it.!rj L.S r,e~3r;d:q met.1. Tbv tin content ~f ]

Jan 1, 1938