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By Robert J. Anderso

Few elements have received more attention and developed greater interest in the last ten years than titanium. The substantially pure metal has been din...ie. cult to isolate, and so far has been little employed oommercially, but the use af alloys and chemical compounds of titanium has increased markedly in recent years. The earlier attempts at preparing pure titanium resulted in various impure forme which, from their metallic appearance, were always mistaken for the metal. Hunter in 1910 isolated pure titanium by the reduction of titanium tetrachloride with sodium. This brief statement is issued by the Bureau of Mines in response to numerous inquiries which have been received concerning titanium. More complete in. formation on the metal may be had by consulting the referenpes appended. The Literature is voluminous and only the more important references are Riven. It has been drawn upon freely in preparing this report; also information was supplied by M. g. Hunter, Arthur Braid, M 1. Schmid, C. M. Johnson, N. B. Hoffman, and de Courny Browne. The pioneer investigator in titanium is A. IL Rossi.

Oct 1, 1922

By Robert L. Rough

The 1954 field tests consisted of six experimental shots in relatively deep holes in a sandstone similar to many oil-bearing sandstones. Water-injection measurements were made before and after each shot to establish the change in conductivity of the fluid caused by the shot. The pressure pulse produced by the shot was recorded in nearby holes to monitor the shot and to determine if any relation existed between the change in conductivity and the nature of the pressure pulse. The results of water-injection tests showed the range of conductivity of fluid before and after shooting with two different types of explosives. Because of the large spread in data for similar shots, not enough information was available to evaluate the differences in increased conductivity produced by the two explosives or any relation between the increased conductivity and the nature of the pressure pulse. However, these results, with the results of other tests involving explosive shots in rock, provide guidance for future research on the oil-well-shooting problem.

Jan 1, 1957

By R. P. Vinson

The Bureau of Mines examined the effects of high humidity and water droplets on the GCA Corp. real-time aerosol monitor (RAM--l). which uses a lO4mm cyclone preseparator. Tests were conducted both in a laboratory and in a full-scale model mine entry. The laboratory tests were conducted in a test chamber saturated with moisture and water droplets. Under these extreme conditions. the RAM-I responded by indicating dust concentrations of 1-1/2 to 2 mg/m3? although the air was dust free. Within the first 2 h of each test. water accumulated in the cyclone and affected the cyclone particle separation characteristics. resulting in readings of 3 to 4 mg/m3. In addition. condensation formed inside the RAM-I case and affected the liquid crystal display (LCD). However. the full-scale mine entry tests revealed that the RAM-I can function ac-ceptably in an atmosphere of water vapor and water droplets similar to the most severe conditions found in an underground mine.

Jan 1, 1984

By R. D. Leitch

The work of the United States Bureau of Mines on stream pollution3 by coal-mine drainage has included a study of seasonal variations in acidity and volume of several streams in Pennsylvania. The acidity of these streams has been determined during the two or three years prior to 1930 and the results may be considered to represent "normal" low water conditions. The summer of 1930, however, was unusually dry and represents what may be termed "extreme" low water conditions on these streams. This report is a comparison of the results obtained for extreme low water of 1930 and for other years. The streams investigated were Buffalo Creek in Somerset County, Indian Creek (lower 5 miles) in Westmoreland County, Little Toby Creek in Elk and Jefferson Counties, Daguscahonda Run in Elk County and West Creek in Elk and Cameron Counties. These will be treated separately in the order given. Most of the descriptive matter and physical data pertinent to the streams and drainage basins are taken from published reports of the Pennsylvania State Water Supply Commission, 1917.4

Jan 1, 1931

By R. D. Leitch

The work of the United States Bureau of Mines on stream pollution by coal-mine drainage has included a study of seasonal variations in acidity and volume of several streams in Pennsylvania. The acidity of these streams has been determined during the two or three years prior to 1930 and the results may be considered to represent "normal" low water conditions. The summer of 1330, however, was unusually dry and represents what may be termed "extreme low water conditions on these streams. This report is a comparison of the results obtained for extreme low water of 1930 and for other years. The streams investigated were Buffalo Creek in Somerset County, Indian Creek (lower 5 miles) in Westmoreland County, Little Toby Creek in Elk and Jefferson Counties, Daguscohonda Run in Elk County and West Creek in Elk and Cameron Counties. These will be treated separately in the order given. Most of the descriptive matter and physical data pertinent to the streams and drainage basins are taken from published reports of the Pennsylvania State Water Supply Commission, 1917.

Jan 1, 1931

By Steven R. Munts

In 1985, at the request of the U.S. Bureau of Land Management, the U.S. Bureau of Mines studied 8,445 acres of the 20,650-acre Tunnison Mountain Wilderness Study Area in order to evaluate its identified mi nerd 1 resources. The study area is located in Lassen County, CA, about 8 miles northeast from Susanville. No mineral resources were identified in the study area based on literature, field observations, and sample results. No mines were operating in or near the study area in 1985, and no mines, prospects, or claims have been located in or within 1 mi le of the study area. The study area is underlain by Pliocene and Pleistocene volcanic units composed of basalt, andesite, rhyolite, and some pyroclastics. No metallic and only nonmetallic commodities are present in the study area. These included stone and sand and gravel. Although substantial volumes of basalt and andesite (stone) occur within the study area, no identified resources of these commodities were delineated. Sand and gravel is not economic because of small occurrence size and lack of local markets.

Jan 1, 1987

By R. Blickensderfer

An impact wear testing machine was devised by the Bureau of Mines that simulates the repeated impact conditions encountered in large milling and grinding operations where breakage and spalling are problems. The apparatus provides data on materials that may help in the design of alloys with improved resistance to deformation, spalling, and breakage. The test blocks are 2 in thick by 6 in by 8 in. Impacts are produced by dropping 3-in-diam balls weighing 4 lb from a height of 10 ft. Tests were run until breakage occurred or to a total of 100,000 impacts. Four types of failures of the test block were observed: (1) cold flow of the bulk material by plastic deformation, (2) flaking of the surface in the impact region, (3) spalling of the block to form a crater in the region of impact, and (4) breakage of the test block into two or more major pieces. The effects of composition, heat treatment, microstructure, and hardness on types of failure are discussed.

Jan 1, 1983

By B. J. Scheiner

The Bureau of Mines investigated an electrolytic technique for oxidizing ore slurried with brine to determine its effectiveness in extracting mercury from ores. Optimization experiments conducted on a 2.5-pound-mercury-per-ton ore resulted in 95 percent mercury extraction with operating conditions of 30° C, a current density of 0.5 ampere per square inch, and a treatment time of 3.5 hours. Corresponding power consumption amounted to 38 kilowatt-hours per ton of ore treated. Amenability experiments conducted on 62 different mercury ores resulted in 90 to 99 percent mercury dissolution from ores containing 0.6 to 20 pounds of mercury per ton of ore, Treatment time ranged from 1 to 7 hours in 4-to 20-percent sodium chloride solutions, and power consumption was in the range of 10 to 50 kilowatt-hours per ton of ore. Pilot mill experiments in a 100-to 200-pound-per-hour extraction plant have been in progress to quantify power and reagent requirements. These data will be reported in a subsequent publication.

Jan 1, 1973

To precondition a stope in advance of mining and thus reduce or prevent rock bursts. Approach Drill deep holes from a mine opening in a radial pattern in the vein and load and blast to fracture, the rock prior to production mining How It Works Preconditioning of a sphalerite galena vein in a hard gangue of quartz and quartzite creates a zone of softer rock that fails by displacement rather than violently as an elastic-battle mass. However, the entire area must he analyzed carefully so that the stress transfer does not cause problems in other workings of the mine A typical drill hole pattern and explosive loading is shown in the sketch. Hole diameter is about 4 inches and a down-the-hole, type drill is used. Drilling speed in hard quartzite is about 12 inches per minute High pressure compressed air (250 psi) is used to run the drill. An overhand cut-and-fill stoping area on the 7700 level of Hecla Mining Company's Star Mine in Burke, Idaho was preconditioned above and below the

Jan 1, 1981

By William A. Vogely

STRIKES in the steel and copper industries adversely affected production in the minerals industry in 1959. Because of an excellent first half of the year and rapid recovery of production after the steel settlement, most statistical indicators were higher than the recession-recovery year 1958. Domestic production of metals declined by 9 percent, but nonmetals (except fuels) increased by 8 percent. Ferrous-metal mine production was down 8 percent, and base-metal mine production was off 11 percent. Employment was high during the first half of the year, but averaged lower than in 1958. Stocks continued to decline as a whole, but crude metal ore stocks actually increased. The indexes of stocks at yearend were still high as compared with 1955. Prices were firm throughout the year. A new index of average unit mine value is presented for the first time in this review; it showed a very slight decline in average mine realization for 1959. The percentage share of supply from imports increased in some commodities, due in large part to the shutdown of domestic iron, steel, and copper industries.

Jan 1, 1960

Improve the safety of salt mine workers by providing a means for quickly identifying areas within the mine that?s how an increased potential for gas and salt outbursts. Approach Outbursts occur in salt mines when a high-pressure pocket of gas is intercepted during the mining process, resulting in a sudden and sometimes catastrophic expulsion of gas and salt. In one case, the amount of gas released through such an event caused an explosion that resulted in five fatalities. The U.S. Bureau of Mines has designed and developed a gas outburst prediction system that can quickly determine the potential instability of areas within rock salt mines. The determination is based on noise measurements obtained from samples of the salt as they are dissolved in water. This system improves upon technology currently available because it provides information in only a few minutes instead of in several days. In addition, present prediction systems are not only time consuming, but expensive because they require laboratory conditions and highly trained personnel to operate them and determine results.

Jan 1, 1989

By J. D. Marchant

As part of its mission to assure the maximum recovery and use of the Nation's mineral resources, the Bureau of Mines, investigated an improved procedure for producing rare earth-silicon alloys. For example, a charge consisting of 681 grams of mixed rare-earth oxides, 309 grams of ferrosilicon (75 wt-pct Si), and 182 grams of aluminum metal along with a flux consisting of 681 grams of CaO and 45 grams of MgO was reacted at 1,500° C in an induction furnace. Good slag-metal separation was achieved. The alloy product contained, in weight-percent, 53 RE, 28 Si, 11 Fe, and 4 Al with a rare earch recovery of 80 pct. In current industrial practice rare earth recoveries are usually about 60 pct in alloy products that contain approximately 30 wt-pct each of rare earths and silicon. Metallurgical evaluations showed the alloys prepared in this investigation to be as effective in controlling the detrimental effect of sulfur in steel and cast iron as the commercial rare earth-silicon-iron alloys presently used in the steel industry.

Jan 1, 1980

By Raymond P. Maloney

The Rhyolite mercury prospect is on the south flank of Juninggulra Mountain--a large rhyolite intrusive in the Kuskokwim River region about 36 airline miles northwest of Red Devil, Alaska. Bulldozer trenching by the Bureau of Mines exposed bedrock at intervals in a 2,000-by 3,000-foot area where previous prospecting by the owners had disclosed abundant float and several in-place stringers containing cinnabar in widely varying amounts. The additional trenching indicated that the mercury mineralization in the limited area investigated was confined to erratically distributed short stringers and to small lenses, occurring in discontinuous zones in numerous silica-carbonate dikes and sills or along their altered contacts with sedimentary rocks. The geologic relationship of the mercury-bearing silica-carbonate dikes and the nearby rhyolite intrusive is similar to that existing at several other mercury mines and prospects in the. Kuskokwim region. The depth of over-burden and the presence of permafrost were serious obstacles to bulldozer trenching, and only a comparatively small part of the mineralized area was thus investigated.

Jan 1, 1962

By Mark S. Redfern, Kim M. Corneliusa, Christopher A. Hamrick, Sean Gallaghera

Coal miners often handle heavy electrical power cables, weighing up to 10 kg per meter. These cables are manually lifted and attached to the mine roof to prevent damage from mobile underground equipment. Data suggest that workers who commonly perform cable handling tasks experience a high rate of lost time back injuries. In this study, six male underground miners performed a total of 12 cable-hanging tasks in standing, stooping, and kneeling postures, during which kinematic and ground reaction force data were collected. Reductions in vertical work space were found to result in a linear increase in the peak moment experienced by the lumbarspine (p<0.05). In restricted postures, peak moments were not significantly different in stooping vs. kneeling postures (p>0.05). Average lumbopelvic flexion during the tasks was highest in stooping conditions, followed by standing and kneeling exertions (p<0.05). Implications of this data with respect to design of cable handling tasks are presented and discussed. Keywords: Biomechanics, posture, low back pain, restricted workspace, mining

By Chas. F. Jackson

The annual reports of the supervising engineering of the nine sections comprising the Mining Division are assembled in the following pages and constitute the annual report of the division. In planning activities, the aim is to adapt them to changes in conditions, in the needs of the mining industries, and in the public interest; those current activities that contribute most to problems of present concern are emphasized, investigations of less immediate importance being recessed, if necessary.

Jan 1, 1940

By Chas. F. Jackson

The annual reports of the supervising engineers of the nine sections comprising the Mining Division are assembled in tie following pages and constitute the annual report of the division. In planning activities, the aim is to adapt them to changes in conditions, in the needs of the mining industries, and in the public interest; those current activities that contribute most to problem of present concern are emphasized, investigations of less immediate importance being recessed, if necessary.

Jan 1, 1940

By K. K. Kershner, J. G. Donaldson

This investigation was conducted to obtain data on optimum conditions for chloridizing metal sulfides . Salt- roasting galena at 450° C for 8 hours chloridized 75 percent of the lead ; in an equal time of treatment at 750° C , the process chloridized 42 percent of the zinc in sphalerite . Hydrogen chloride at 500° C completely chloridized galena in 15 minutes , and at 600° C converted all of the zinc in sphalerite to the chloride in 4 hours .

Jan 1, 1963

By A. N. Fried

One of the important problems confronting oil producers in appraising the possibilities of secondary recovery in many California fields is the effect of viscosity on oil recovery by water flooding. In January 1954 there were 554 fields and/or pools, in the State, that produced 1 million barrels daily, and 138 of these pools produced approximately 267 thousand barrels daily of heavy crude oil having gravities below 200 API. Many of these fields are nearing the end of their primary economic life and still have high residual-oil saturations, a favorable factor in water flooding. The crux of the problem is whether or not enough oil can be recovered from these fields by water flooding to make the operation economically successful. Some experiments on the relationship between viscosity and oil recovery have been made by other investigators, but in most instances the viscosity of the oils used in the experiments was lower than the viscosity of the oils found in many of the heavy-oil fields in California. A study was undertaken, therefore, to determine the relationship between oil viscosity and recovery over a wider range of viscosities and to compare the experimental results with those predicted by theoretical calculations.

Jan 1, 1955

By John H. Soule

Appreciable quantities of sine and lead orus have been produced from the West. Pinos Altos district of Grant County, N. sex. This area was visited many times by engineers of the Bureau of ines. D. H. Johnson and 4. R. Storms visited the district in haren 1943 in connection with an acrenu road to toe wines. M. H. Storma again visited the area in July 1943 in connection with a hetals Feserve Corporation loan on the Routen-Thomas

Apr 1, 1948

By William G. Pariseau

Elastic-plastic finite-element simulation of cut-and-fill stoping in deep, narrow veins shows substantial quantitative agreement with field measurements of stope closure and fill pressure made at two mines in the Coeur d&apos;Alene mining district of northern Idaho. The simulation procedure, validated by field data, was used in an analytical study of vein-wall closure and sill-pillar stress as influenced by fill modulus, rock modulus, and premining stress. Ratios of closure and pillar stress in the filled stopes to closure and pillar stress in the unfilled stopes are used as prediction indices for fill performance. In general, the support capability of fill increases dramatically as the ratio of fill modulus to rock modulus approaches 1. A significant reduction in closure .from the open stope--up to 75 percent--occurs with a relatively low-quality 10-ksi-modulus fill (rock modulus of 1,000 ksi). However, a higher quality fill is needed to achieve a substantial reduction in pillar stress from that of the open stope. A 100-ksi-modulus fill reduces pillar stress in both the 36-foot and l6-foot pillars (vein width is 10 feet) by about 50 percent relative to the open stope.

Jan 1, 1976