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By K. K. Kelley, L. B. Pankratz, W. W. Weller

Mullite is a substance of prime importance in ceramic technology . Despite this fact , its thermodynamic properties have received little attention . A Bureau of Mines literature survey disclosed the absence of lowtemperature heat capacity data , the absence of an experimental entropy value for 298.15 ° K , and the lack of heat content data beyond the temperature range from 298° to 576 ° K. Data supplied in this Bureau report fill these gaps in the thermodynamic knowledge of mullite . According to equilibrium phase studies of Aramaki and Roy ,3 the mullite phase melts congruently at 2,123 ± 15 ° K , and the equilibrium crystallinephase composition extends from Al Si2013 to Al6.8 Si₂ Q4.2 . The results in this report are for the stoichiometric composition , Al Si¿Qз . • Heat capacity measurements were made over the temperature range from 50 ° to 298 ° K , and the entropy at 298.15 ° K was evaluated . Heat content measurements covered the temperature range from 298 ° to 1,800 ° K. Heat content

Jan 1, 1963

By Charles T. Chislaghi

An economical, remotely operated (automated), temporary roof support (ATRS) has been developed by the Bureau of Mines for use on a single, fixed-head roof-bolting machine (squirmer) that operates in low coal seams (less than 42 in thick). The ATRS eliminates the need for squirmer operators and helpers to go under unsupported roof to set or remove temporary support prior to or during the roof-bolting cycle--a task that annually accounts for approximately 20 pct of all roof fall fatalities. The ATRS can be adapted to any squirmer used in the U.S. low coal fields. A prototype ATRS was field-tested at Imperial Colliery Co.?s Mine No. 20 in Eskdale, W. Va. The Mine No. 20 amended roof- control plan, which requires the use of the Bureau?s ATRS as temporary support during face bolting, has been approved by the Mine Safety and Health Administration (MSHA), U.S. Department of Labor.

Jan 1, 1982

By S. M. Shelton, W. A. Calhoun, M. M. Fine, T. L. Johnston

"INTRODUCTION An extensive test program is in progress by the Bureau of Mines to determine ways and means of recovering ferromanganese-grade ore 6/ from the wide-spread domestic manganese and manganiforous iron deposits. Samples for testing were received from the Interstate Manganese Co. in northeastern Tennessee, 11 miles west of Mountain City and 10 miles southwest of Damascus Va. The ore deposit occurs in the residual material of the Shady dolomite 7/ as an unconsolidated mixture of hard and soft manganese oxides and clay.Numerous tunnels and pits have developed a large reserve of ore in an area of about 15 acres. One pit 250 by 50 by 20 feet is being mined by rower shovels. The ore is hauled to a washing plant for log-washing, hand-sorting, and jigging. Coarse concentrates from the washing plant are marketed without further beneficiation.ACKNOWLEDGMENTSThe authors wish to acknowledge the assistance of R. F. Fisher, who made the roasting and magnetic tests."

Mar 1, 1942

By E. C. Lane

During the past 15 years the Bureau of Mines has made and published several hundred analyses of typical petroleums and has developed a system of interpreting the analyses and of classifying crude oils. In describing crude petroleum frequent reference is made to the "base" of the oil, a usage the petroleum industry has found convenient. As part of its general study of the characteristics of crude oils, therefore, the Bureau of Mines has developed a system of classifying them according to "base." This system as first published in 1927 was limited to four classes and in its original form is no longer considered adequate. Since the system was first published the Bureau has analyzed a large number of crude oil, including representative samples from nearly every important producing field in the world, and has found that the system of classification could be revised and amplified to advantage. The revised system is presented herein.

Jan 1, 1935

By M. H. Kline

The Chestatee mine is one of several well known pyrite deposits in Georgia that are reputed to carry appreciable quantities of copper with the ore. The deposit is? in Lumpkin County on the Chestatee River, 6 miles northeast of Dahlonega (fig. 1). Old records and reports indicated the probable existence of an extensive unmined ore body, but the mine is inaccessible at present. The Bureau of Mines, after studying old maps and records, decided to cor8-drill along the strike of the lense beyond the limits of the indicated old workings in an attempt to extend the possible reserves. The advantageous location of the property indicates that it could become an economic source of pyrite to be used for the manufacture of sulfuric acid. Iron sinter resulting from the roasting of the ores could be sold at a premium in the Birmingham, Ala., area, and the copper content could be extracted to help replace the nation's depleted resources of this metal.

Jan 1, 1949

By Chas. G. Maier

The bright annealing of copper is an industrial practice of considerable importance. In connection with this process, equilibrium concentrations of carbon monoxide and dioxide, which may exist in contact with copper and cuprous oxide at elevated temperatures, are of interest. Data obtained at the Pacific Experiment Station of the U. S. Bureau of Mines enable estimates of these equilibrium concentrations to be made in two independent ways. Although the publication of final data on one method can not take place until certain further experimental work is accomplished, repeated requests which the Bureau of Minus has had for data relative to the annealing and deoxidation of copper justify the present preliminary report. This paper deals with the calculation of gas concentrations in the reduction of cuprous oxide, using more scientific data which will be published later, and refers especially to those conditions of temperature and concentration of practical implication, and from which critical limits ensue.

Jan 1, 1929

By Wing G. Agnew

It is thought that a brief description of the unique mining and milling procedure at the Doyle nine may be interesting to those engaged in small-scale operations at old mines or in working new ore body adjacent to old workings. It also shows what can be done with r. small capital outlay in working a zinc-lead mine on a small scale; as the operation herein described was begun 3 years ago with four men and it now employs 17 men. The original idea was to mine out any ore left around the edges of some old stones above the water level and to rob pillars after an old stope became filled with waste and tailings. This has been done, and the procedure is still being followed; at the same time a paying lead is being mined toward an area in which churn-drill holes have shown ore. Also, preparations are now being made to do some pumping.

Jan 1, 1936

By F. D. Stevenson

Thermodynamic properties of metal halides and, in particular, vapor pressures have become of great importance in recent years owing to increased application of chemical processing to extraction of metals from their ores. Vapor pressure data serve not only as a valuable source of latent heat of vaporization and fusion values but also differences in metal-halide vapor pressures often provide the basis for their separation by conventional mass transfer operations. This literature search was made to provide a ready reference to experimental vapor-pressure data of metal halides and oxyhalides. Results are reported in two main sections: (1) A tabulation of vapor- pressure references for each of the metal halides (listed by metal) for which actual experimental data are reported (table 1), and (2) a bibliography of the citations. Metal halides and oxyhalides are listed by chemical formula and chemical name, based on the stock4 system. To facilitate location of the references, a listing of the journal titles and their abbreviations follows the bibliography.

Jan 1, 1963

By Jerry E. Olson

In 1988, at the request of the Bureau of Land Management, the U.S. Bureau of Mines studied additional areas, encompassing 11,303 acres, on the east and west sides of the 20,727-acre Badlands study area (Olson, 1987) in order to evaluate their identified mineral resources. The Badlands study area additions are located in Crook and Deschutes Counties, OR, about 10 and 18 miles east of Bend, OR. No mineral resources were identified. The additional areas studied are underlain by Tertiary-and Quaternary-age basalt flows which are largely covered by a veneer of sand and silt. No mines, prospects, mining claims or mineralized areas occur within or near the Badlands study area additions. Slab lava of marketable grade and quantity was not found in either area. None of the study area is of current interest for geothermal resources, but the eastern study area addition has been leased (1984) for oil and gas.

Jan 1, 1989

By Thomas J. Peters

The U.S. Bureau of Mines conducted a mineral investigation, and the U.S. Geological Survey did a geological appraisal of an east portion of the Bear-Marshall-Scapegoat-Swan (BMSS) RARE II area (No. A1485) to provide mineral resource information for land use planning. The Bureau of Mines' investigation consisted of a library and field search for all mineral properties and occurrences, and included a review of Teton County mining claim records. Those records showed two placer claims, the only mining-related activity known in the area. Six reconnaissance pan samples were taken in the vicinity of the two placer claims, the Lone Star and Spotted Horse, located on Hannan Gulch in 1900 and 1901. One sample contained a trace of gold, but there are no identified resources. However, the study area is in the Rocky Mountain Overthrust Belt, which is productive for oil and gas elsewhere. The entire study area is blanketed by oil and gas leases and is currently being explored.

Jan 1, 1983

By Harry W. Campbell

U.S. Bureau of Mines investigation; identified no mineral resources or evidence of mining activity in the Sheep Divide RARE II area. A deposit 10 mi (16 km) southwest of the area contains copper and silver minerals in the Triassic Wild Sheep Creek Formation which probably underlies basalt lava flows covering the study area. Abundant basalt in the area can be crushed and used as aggregate, but suitable deposits closer to markets are widely available No sand, gravel, coal, oil, gas, or geothermal resource, were Identified. INTRODUCTION Location and Access The Sheep Divide RARE II area [10 mi (16 km) west of the Snake River] encompasses 7,100 acres (2,800 ha) of the Hells Canyon National Recreation Area in the Wallowa-Whitman National Forest. Enterprise, Oregon, is located 23 air mi (37 (m) west of the area. Peripheral access is provided by the highway from Joseph to the community of Imnaha, Oregon, then south to the study area by the graveled Upper Imnaha Road (fig. 1).

Jan 1, 1983

By E. C. Lane

This paper is the second report of the results of the United States Bureau of Mines twenty-third semiannual survey of motor fuel marketed in the United States. The first paper, reporting data relating to gravity, vapor pressure, and distillation range of the samples, was published as Report of Investigations 31293. A third and concluding paper giving the results of other tests will be published as soon as these tests have been completed. The present paper deals with the data of the twenty-third semiannual survey presented in accordance with the revised specifications for United States Government motor gasoline. The sample numbers used are identical with those used in Report of Investigations 3129, with additional data included for copper strip corrosion (method 530.22),4 and sulphur content by the lamp method. Three hundred and twelve samples were collected and analyzed in this survey. Two hundred and seven samples were competitive-price gasolines and one hundred and five samples were premium-price motor fuels.

Jan 1, 1931

By E. C. Lane

This paper is the second report of the results of the United States Bureau of Mines twenty-third semiannual survey of motor fuel marketed in the United States. The first paper, reporting data relating to gravity, vapor pressure, and distillation range of the samples, was published as Report of Investigations 31293. A third and concluding paper giving the results of other tests will be published as soon as these tests have been completed. The present paper deals with the data of the twenty-third semiannual survey presented in accordance with the revised specifications for United States Government motor gasoline. The sample numbers used are identical with those used in Report of Investigations 3129, with additional data included for copper strip corrosion (method 530.22).4 and sulphur content by the lamp method.5 Three hundred and twelve samples were collected and analyzed in this survey. Two hundred and seven samples were competitive-price gasolines and one hundred and five samples were premium-price motor fuels.6

Jan 1, 1931

By Jerry E. Olson

In 1986, at the request Of the Bureau of Land Management, the U.S. Bureau of Mines studied the central portion, encompassing 20,727 acres of the 32,261-acre Badlands Wilderness Study Area (OR-005-021) in order to evaluate its identified mineral resources. The study area is located in Crook and Deschutes Counties, OR, about 12 miles east from Bend. No mineral resources were identified. The area studied is underlain by Tertiary and Quaternary basalt flows which are largely covered by a veneer of sand and silt. No mines, prospects, or mineralized areas occur within or near the study area, but some sand and gravel has been removed from alluvial deposits at the east and west sides of the area. Slab lava of marketable grade and quantity was not found in the study area. None of the study area is of current interest for geothermal resources, but the eastern third of the wilderness study area is leased (1984) for oil and gas.

Jan 1, 1987

By D. J. Parker

Du.ring the past two years a number of oases of successful first-aid treatn . .)nt have been reported by or through the employees of the O. s. Bureau of -anes safety cars and stations. Among such cases are the following: At Benbush, w. Va., a boy or 16 years of age who ba.d just started to work in the mines was trained in first-aid by the crew of Bureau of Mines car 8. The local rr.ine superintendent afterwards reported tba.t a few dS¥s later this boy, Melvin Hollingsworht, found droming in a spring a. baby about three years old who bad wandered away fron.. har.e alone. The boy rescued the baby and perf'oxmed artificial re­suscitation upon it, thu.s saving the child's life. The Schaefer method of resuscitation bad bean ta"Ugbt the boy as a routine art of the regular first-aid course.

May 1, 1922

By John Durkin

The Bureau of Mines has conducted field studies in coal mines through- out the United States to determine the effectiveness of electromagnetic techniques in locating miners trapped underground following a mine accident. Data from these tests have been used to generate models of expected signal and noise distributions as found above mines throughout the coalfields. These distributions have aided in placing the expected performance of a through-the-earth electromagnetic communications technique into a probabilistic framework. Results show that at a 10-pct false alarm rate, the expected probability of detecting a miner's signal from a depth of 1,000 ft is 54 pct; at 500 ft it is 95 pct. These depths exceed the actual depths of 90 pct and 50 pct, respectively, of U.S. coal mines. Sensitivity studies have shown that at a depth of 1,000 ft, for every 3 db of improvement in signal-to-noise ratio, the probability of detection increases 6 to 8 pct.

Jan 1, 1982

By F. N. Kissell, C. D. Litton

This study ranks the factors impacting survival during a coal mine fire. It bas already been established that reducing time delays is the most important factor in saving lives. Consequently every event during afire is measured in terms d its duration, and the effectiveness d any action taken to improve survival is measured in terms d the time it saves. By ranking actions according to time saved these authors found that a comhination d actions was most effective. This combination was: • installing lifelines. • moderately decreasing air leakage and • decreasing the fire growth rate. Changing ventilation leakage alone was much less effective, as was altering the CO (carbon monoxide), sensor alarm threshold. These results confirm an earlier fault-tree study on escape from mine fires. The fault-tree study bad shown that, with the exception d delays, single factor changes have minimal impact. Significant reductions in fire fatalities only take place with multiple factor changes.

By Ivette E. Torres

For a study such as this, which summarizes and amalgamates much information collected, compiled, and utilized by the numerous U.S. Bureau of Mines country specialists and branch chiefs for inclusion in their country and regional reports that comprise the five other sections of 1992 Minerals Yearbook-International Review, it is clearly impossible to cite all sources of information used in its presentation, but some recognition is due. Generally speaking, this study and its related detailed studies on countries and areas would be much more difficult, if not impossible to complete, without the efforts of the personnel of our counterpart national mining and geological agencies throughout the world. Information that they collect, compile, and then publish, either in their own volumes or those of central statistical agencies in their countries, are the foundations on which this work rests. Thus, our appreciation is expressed to the multitude of persons employed by these agencies for their contributions.

Jan 1, 1994

By D. Montagna

The Kroll-Betterton process for debismuthizing lead is based on adding calcium and magnesium to impure molten bullion to form solid Ca-Mg-Bi inter-metallic compounds that float on the surface as drosses. Present practice in industry is to hand-skim off these drosses, often followed by hydraulic pressing to squeeze out some of the entrapped liquid lead. In an effort to develop an improved technique, the use of an argon-shrouded dipping centrifuge to perform the required phase separation was investigated. Centrifugation experiments demonstrated that the bismuth content of an impure bullion could be lowered from an initial 0.5 percent down to 0.03 percent with a lead recovery of 90 percent, which is comparable to lead recovery after hand skimming of drosses in commercial lead-debismuthizing operations. Centrifugation provides better control in removing drosses, faster operation with less oxidation and relatively little fuming, and recovery of a lead bullion that approaches commercial specifications.

Jan 1, 1972

By C. J. Thompson

In the course of the work currently conducted by the Bureau of Mines in cooperation with the American Petroleum Institute Research Project 48 on identifying sulfur compounds in petroleum, a micromethod was developed (12)5 for catalytically removing the sulfur atom from sulfur compounds. The product is the residual portion of the molecule; the structure otherwise was unaltered except for hydrogenation of any unsaturated bonds that were present in the original compound. Positive identification of sulfur compounds isolated from crude oils is a difficult problem. Direct comparison of properties of the unknown with those of reference compounds is often impossible because of the limited number of reference sulfur compounds available. However, a relatively large number of pure hydrocarbons is available, and the conversion of the sulfur compound to a hydrocarbon enhances the possibility of identification. The technique also can be used to prepare microquantities of scarce hydrocarbons by hydrogenating compounds that are readily available.

Jan 1, 1962