Search Documents

By Walter D. Holland

LFE Environmental performed an Industrial Hygiene survey of the Paraho Oil Shale Mining and Processing facility in Anvil Points near Rifle, Colorado, on August 6 and 7, 1975. This survey consisted of an investigation of the underground operations for diesel emission contaminants and of the above ground work areas for all inhalation contaminants other than silica dust. Samples were collected to investigate the following contaminants: respirable dust, total dust, NO2, NO, H2SO4, formaldehyde, CO2, S02 and CO. None of the determinations of contaminants in the underground operations indicate air concentrations exceeding their standards. The results for the samples collected above ground indicate only one operation where the employee's exposure exceeds the standards. It is a welding operation where the standards for total dust and lead are exceeded. Since the survey the employer has installed an exhaust ventilation system which has significantly reduced the welder's exposure.

Jan 1, 1976

By Chase E. Sutton

The porosity of a sand is usually the measure of its capacity for holding fluid, although porosity is sometimes selective; that is, a small percentage of the actual pore space (voids), particularly in fine-grained sandstones, may be isolated by the cementing material which prevents the entrance of fluids under normal conditions. Obviously, however, porosity determinations are essential to an engineering study of underground conditions of an oil field, and a simple and reliable method of obtaining a reasonably accurate figure for average porosity is desirable. This report describes a method suggested by Ruasell,3 which was used by the writer in the preparation of a report on the Texhoma-Gose pool, Archer County, Tex.4 The conditions in this pool were particularly favorable for obtaining an average porosity figure, in that some 30 to 35 core samples of the pay sand were available for analysis.

Jan 1, 1928

By Michael D. Dunn

The Bureau of Mines evaluated a quartz schist formation within the Blue Joint Wilderness Study Area which was identified as having a "high potential" for copper-silver-cobalt-barium resources. Stratiform and remobilized copper occurs near, and bedded barite within, the study area. In addition, the black to gray Proterozoic quartz schist may correlate with the Yellowjacket Formation which contains cobalt-copper-gold-silver deposits at Blackbird, ID, about 30 miles to the south. Eighty soil and 43 rock samples collected across the quartz schist formation were analyzed for gold, silver, copper, cobalt, and barium. During the reconnaissance and sampling, particular attention was given to looking for malachite (copper carbonate) and erythrite (cobalt arsenate, also known as "cobalt bloom"). The sample analyses and geology in this localized area do not provide enough evidence to support the "high potential" designation for copper-silver-cobalt resources. Barium potential still appears high, however.

Jan 1, 1987

By Graham W. Marks, Clyde A. Bridger

"INTRODUCTION An electrolytic process for the preparation of metallic cobalt has been developed recently in the Bureau of Mines Experimental Station at Boulder City, Nev. Chemical analysis shows this cobalt to contain impurities in small percentages, chief of which is nickel. It is desirable to be able to determine these impurities spectrographically. This report is concerned with a procedure for the spectrochemical determination of nickel in cobalt.Previous spectrographic work on cobalt was done by Breckpot and Mevis,/ who used the method of homologous pairs of lines. However, it was felt that a more detailed investigation was needed, employing the method of internal standards.ACKNOWLEDGMENTWe are indebted to B. G. Knickerbockor and his staff at the Boulder City, Nev., station of the Federal Bureau of Mines for their cooperation, and particularly to Richard W. Lewis and Robert G. Sanderson, who prepared nickel-free electrolytic cobalt for us."

Feb 1, 1948

By N. A. Gokcen

In this Bureau of Mines report, appropriate equations correlating the activity of water with the activities of electrolytes in binary and multicomponent solutions have been derived for computer calculation. It was found that the half-integer power series are far superior to the integer power series, for both types of series having the same number of terms. The pro-posed method of calculation is capable of accurately yielding the activities of all components from the measurements of the activity of a single component at various concentrations. This method replaces the cumbersome and objection-able method of graphical integration of the Gibbs-Duhem equation. Two novel methods are proposed for determination of activities of electrolyte solutions important in hydrometallurgy; (1) Water vapor pressure measurement by differential pressure transducers having an accuracy of 0.001 pet, and (2) transpiration method with an inert gas bubbled through concentrated solutions followed by the analysis of the evaporated and redissolved electrolytes with specific ion electrodes having a sensitivity of ±10-10 molal. The first method is suitable for nonvolatile electrolytes, and the second, for volatile electrolytes such as hydrogen halides, HN03, H2S03, etc. The existing methods of estimation of ionic activities have been surveyed, and the best method has been selected, discussed, and summarized.

Jan 1, 1979

By J. J. Jakosky, D. H. Zellers

"IntroductionThis paper is the seventh of a series describing an investigation being conducted by the Bureau of Mines on underground communication. A review of past work and results obtained has been published. The present paper deals with a study of line-radio or wired-wireless methods of communication, herein electrical energy is transmitted by metallic conductors.The use of line-radio over metallic conductors has been practiced for a number of years, and at present is being used on a large scale in long-distance carrier-current telephone and telegraph. The early work of the U. S. Army Signal Corps and the Bureau of Standards in using ordinary radio transmitting and receiving apparatus for communication over metallic conductors was been descried. Later publications describe commercial applications, and an excellent treatise and resume is given by E. Colpitts and C. B. Blackwell.Scope of ReportThis report contains (1) a discussion of the chief factors affecting carrier-current transmission, with particular reference in application to underground communication for mines; (2) a description of typical underground circuits used for power and lighting; and (3) description of apparatus used and results obtained in line-radio experiments in coal mines near Pittsburgh, with circuit diagrams, and conclusions as to power requirements and limitations for mine use."

Apr 1, 1925

By F. E. Brantley

Optimum autoclaving conditions were determined for separation of iron and manganese values from pregnant leach liquor produced in extracting manganese from low-grade umber are. The umber was leached with a synthetic anolyte similar to a recycle solution, used in manganese electrolysis cell operations, that had been renewed with ferrous sulfate and sulfuric acid. The equipment used and results obtained are presented for the several conditions employed. The kinetics of the separation were studied. Rate equations were derived for the formation of solid ammonium-manganese sulfate, (NH4)2 Mn2 (S04)3.

Jan 1, 1968

By D. J. Bauer

Solvent extraction separation of light group rare-earth elements in a quaternary ammonium compound-chelating agent system was demonstrated in single-stage studies, Typical separation factor values obtained were 93 for lanthanum-praseodymium, 5.4 for praseodymium-neodymium, and 11.6 for neodymium-samarium. These values are significantly higher than those obtained using organophosphate extractants. Further studies in a 20-stage countercurrent mixer-settler resulted in the production of 99 percent lanthanum (oxide basis) at 96-percent recovery. Subsequently, 88 percent of the neodymium with a purity of 92 percent was recovered in the raffinate.

Jan 1, 1971

By Charles H. Parr

A testing program was conducted to determine the suitability and reliability of adhesives and polycarbonate lenses for extended use in luminaires in mine environments. Polycarbonates were exposed, for periods up to 36 months, to four environments including ultraviolet light, humidity, intermittent water spray, and heat of either 180°F or 407 in various combinations. Rod impact tests on the exposed lens material indicated, that polycarbonate functions well under all 180°F environments and could be used with confidence for periods exceeding the test period, for as long as ten years, with a suit) able safety factor employed in design. The specimens exposed at 240°F showed decreased toughness after 24 months' exposure. Extrapolation of these data was deemed to be risky. A 462-day compatibility test between polycarbonate and six hydraulic fluids was run on stressed PC beams. One fluid caused beam breakage in less than one day, while three caused breakage at intermediate times. Two fluids exhibited essentially no effect on the PC when compared to a control. Epoxy and silicone adhesives were tested as lens adhesives and sealants. Three epoxy combinations tested showed low and erratic failure stresses. A room-temperature-cure silicone adhesive functioned extremely well for time periods up to 36 months and temperatures u2 to 240°F.

Jan 1, 1985

By Richard W. Lewis

Domestic production of greensand (glauconite) increased 15 percent in quantity and 13 percent in value compared with that of 1964. Since only two firms were in operation, statistics on production and sales for the year are not reported in order to avoid disclosure of individual company confidental data. The average annual production for the 5-year period 1961-65 was 4,306 tons valued at $200,200. The material was marketed for use as a soil conditioner and a water softener. An article of mineralogical interest was published concerning the New Zealand glauconites.2

Jan 1, 1966

By Carlton E. Brown

This report contains information on the relation between and precision or reproducibility of counts (light-and dark-field) of the dust in liquid from simultaneous impinger, midget-impinger, electric-precipitator, and filter-paper samples. The impinger was the main sampler used from about 1922 to 1939 by industrial hygienists in the United States for collecting samples of unhygienic dust from the atmospheric environment of workers. The midget-impinger, a small modification of the preceding impinger described in 1937, has been the sampler used most since about 1939. Electric precipitators5/6/ have been used to a limited extent, mainly by the Bureau of Mines in the laboratory, for obtaining results comparable to impinger results. A filter-paper sampler for obtaining results comparable to impinger results has been described by Brown. All these samplers have a high collecting efficiency for particles larger than 1 micron in diameter revealed by the usual light-field counting procedure. However, their collecting efficiencies are quite variable for the smaller particles revealed by the dark-field counting procedure used in this study. Published information on the relation between the results of these samplers is limited and scattered. Summaries of some of this information are given in this report along with some previously unpublished information.

Jan 1, 1949

By Steven R. Davis

Dear Interested Party: Subject: Notice of Intent to Solicit Outside Opinions Regarding Amendments to the Rules Concerning the Leasing of State Owned Lands for the Mining of Metallic Minerals The Department of Natural Resources, Division of Minerals, is seeking outside opinions concerning the leasing of state owned lands far the mining of metallic minerals. Enclosed for your information in a copy of the Notice of Intent to Solicit Outside Opinions Regarding Amendments to the Rules Concerning the Leasing of State Owned Lands for the Mining of Metallic Minerals.

Jan 1, 1994

By H. P. LeVan

The Bureau of Mines has developed a technically feasible continuous single-stage leaching and thickening system for extracting manganese from umber by a sulfuric acid-ferrous sulfate process; the cocurrent leaching and thickening system proved simpler to operate and control than the countercurrent leaching and thickening system developed earlier" Related tests investigated the use of a centrifuge to replace thickeners for separating the product liquor from are residues and compared several chemical agents for removing iron from the pregnant manganese leach solutions. Results of Some exploratory autoclaving tests are also given.

Jan 1, 1972

By J. P. Walsted

The lack of an iron-smelting industry in the Pacific Northwest places the ferrous metals industries under an economic handicap. No iron-smelting enterprises, now dormant, had been operated successfully. Iron made at both of hoes installations proved to be satisfactory for normal pig-iron uses. Electric power and reductants acre available in the area. Power from the dames now completed and. those being constructed insures present and future needs for basic industries. Subbituminous coal, close to the main supply of iron ore, insures ample reluctant for all smelting requirements.

Jan 1, 1954

By F. B. Tough, B. H. Scott

"Petroleum engineering is a comparatively new branch of engineering, with which few people, even petroleum operators and mining engineers, are thoroughly familiar. Petroleum engineers are responsible for the accurate keeping of well logs and all pertinent data upon formations encountered, for the careful analysis of such information, and recommendations as to most suitable places for drilling, for detailed study of methods of drilling, casing, and so on in order to obtain maximum production for a minimum cost.The Bureau of Hines has from time to time carried on work in all branches of petroleum engineering in the various fields of the United States. Such work is also being carried on extensively by the California State Mining Bureau, which has in its employ a number of men who have had, besides their technical training, actual experience in oil field work. This is about the only state at the present time which is carrying on this work in a definite way. It has therefore been the practice of the employees of the Bureau of Mines to go to other states and give such advice and assistance as might prove of value in development work and in prolonging the production of the fields."

Jan 1, 1920

By John M. Devine

The oxygen bomb-is used extensively for determining sulphur in petroleum, although it has been suspected that the results obtained with this method are somewhat lower than the true varies. In this paper are compared the results given by the oxygen-bomb and Carius methods, the latter being generally accepted as the standard procedure for the determination of sulphur in organic compounds. The Carius determinations given hero were made in connection with a special study of this method.4 Only petroleum oils of the less-volatile type are covered in the present work. Summary and Conclusions. When used with oils containing 2.3 to 0.15 per cent of sulphur the oxygen-bomb method gives results that are consistenly if slightly lower than those obtained with the Carius method. This variation, for the oils used, amounts to 3.1 per cent (on tae basis of sulphur present) for the sample containing 2.47 per cent of sulphur, and gradually increases (as the percentage of sulphur in the oils decreases) to 7.3 per cent for the oil containing 0.15 per cent of sulphur. With the oils studied the presence of ammonium nitrate in the bomb does not influence the results materially.

Jan 1, 1928

Develop a safe, nonpolluting power source for underground mining equipment. Approach The Bureau of Mines and EIM-CO Mining Machinery International entered into a cost-shared project to develop and demonstrate a novel power source for mining. An underground mining utility truck was equipped with an ultra-low-emission hydrogen-fueled engine and a safe, metal hydride fuel storage system. How It Works The nonpolluting hydrogen engine and a "solid-state" (metal hyride) hydrogen fuel storage system were combined to power a utility mining vehicle. An 85 horsepower diesel engine was convened to burn hydrogen. The engine was converted by equipping it with a spark ignition, lowering the compression ratio, turbocharging, and adding an ahercooler and a parallel fuel induction system. Parallel induction provides two intake paths, one for hydrogen and one for air. It avoids intake-manifold backfiring by keeping the hydrogen and air separate until they enter the cylinder.

Jan 1, 1986

By Rudolf E. Greuer, Linneas W. Laage, Xinton Chang

INPUT FORMAT INSTRUCTION FILE FOR PROGRAM MFIRE GENERAL RULES FOR DATA INPUT: $THERE IS NO NEED TO DISTINGUISH INTERGER AND REAL NUMBERS. $ $ SYMBOLS FOR NUMERICAL INPUT INCLUDE THE FOLLOWING $ $ 1234567890 -+BLANK $ $ * FREE FORMAT IS ALLOWED. COMMA AND BLANK SPACE CAN BOTH BE $ $ DELIMITERS. SEQUENTIALLY DISTRIBUTED BLANK SPACES ACT AS ONE $ $ DELIMITER. BLANKS ADJACENT TO A COMMA HAVE NO DELIMITING EFFECT $ $ * A ZERO INPUT CAN BE OMITTED BUT NOT THE DELIMITERS EXCEPT WHEN $ $ THE ZERO INPUTS ARE THE LAST ONES ON A LINE. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS "$ IS AN INSTRUCTION $ $ LINE WHICH WILL BE IGNORED IN A PROGRAM RUN. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS NEITHER ONE USED IN THE $ $ ABOVE LIST FOR NUMERICAL INPUT NOR "$, OR WHICH CONTAINS MORE $ $ THAN 3 SYMBOLS OUTSIDE OF THE LIST, IS A COMMENT LINE WHICH WILL $ $ BE SHOWN IN THE OUTPUT FILE. $

Jan 1, 1990

By M. M. Jones

A procedure for the spectrophotometric determination of uranium has been developed in support of minerals research being conducted by the Bureau of Mines. Uranium is separated from the sample by tributylphosphate extraction from acid solution containing added aluminum nitrate and (ethylene dinitrilo)-tetraacetic acid solutions. The colored uranium-dibenzoy1methane complex is developed in the organic phase by adding an ethanol solution of dibenzoylmethane buffered with triethanolamine. Absorbance is measured at 410 nanometers, and the response is linear up to at least 100 micrograms U30S in the aqueous aliquot taken for analysis. Aliquots containing as little as 8 micrograms U30S may be analyzed with relative errors no greater than ±5 percent. For aliquots containing at least 35 micrograms U308, relative standard deviation at the 95-percent confidence level is about ±2.2 percent. Appropriate procedures are given for analyzing a wide variety of samples.

Jan 1, 1980

"INTRODUCTIONMany of the facilities and much of the equipment available to the Generic Mineral Technology Center for Respirable Dust are highly specialized and therefore, unique to the universities associated with the Center as illustrated in FIGURES 30 through 39.For example, a sample bank of 1300 U.S. coal specimens housed in the Coal Research Section, Deike Building of The Pennsylvania State University has been characterized for physical, elemental, mineralogical and maceral compositions. The results of this research have been used to initiate a study of the relationship between pneumoconioses and coal properties. Selected samples from this bank have been used in animal (primate) studies at the Milton S. Hershey (Penn State) and West Virginia University Medical Centers. These laboratory facilities for research in the medical and biological disciplines is state-of-the-art and includes a primate colony where dust research is currently underway. The Materials Research Laboratory and the Rock Mechanics Laboratory at PSU, and the Mechanical Systems Design and Control Laboratory, the Rock Mechanics Laboratory and the Mine Electronic System Laboratory at WVU are equipped for fundamental research on dust generation and characterization. While the majority of respirable dust research projects fall into these two categories, dust generation and characterization and interaction of dust and lung, there are other laboratory facilities available to the Center which are unparalleled in the type of equipment and expert personnel that they contribute to the program. The Mine Particle Laboratory located at the University of Minnesota and the Diesel Engine Laboratory at Michigan Technological University are examples. They house equipment and instrumentation that is unique to these facilities. much of it having been developed specifically for dust research by the research scientists there. The dust collection equipment and the fine particles measurement, characterization and analysis apparatus are essential to research in the areas of dust collection, particle characterization and diesel particulates. In addition to university laboratories, the research facilities of the National Institute for Occupational Safety and Health (NIOSH) are available to the Center through its relationship With West Virginia University."

Aug 31, 1989