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By Etienne Audibert

No satisfactory theory has yet been advanced to explain what takes place when an explosive is fired in a mixture of firedamp and air. The only means of measuring the' danger is to fire the explosive into the gas mixture and note the effect, but the conditions of firing must be chosen carefully. This report is presented in the hope that it will assist in determining what method to use. The experiments have been designed to show the effect of the principal factors involved in the conditions of firing, and the results give information that seems to have some value.

Jan 1, 1940

By Etienne Audibert

No satisfactory theory has yet been advanced to explain what takes place when an explosive is fired in a mixture of firedamp and air. The only means of measuring the danger is to fire the explosive into the gas mixture and note the effect, but the conditions of firing must be chosen carefully. This report is presented in the hope that it will assist in determining what method to use. The experiments have been designed to show the effect of the principal factors involved in the conditions of firing, and the results give information that seems to have some value.

Jan 1, 1940

By J. P. Baur

The sensitivity of radiochemical techniques makes possible the study of the initial-stage sulfuric acid leaching kinetics of chalcopyrite and other copper sulfide minerals. This Bureau of Mines study of the initial leaching of chalcopyrite used techniques to evaluate the molecular and electrochemical processes. High-grade Transvaal chalcopyrite was neutron-irradiated in a TRIGA reactor4 to produce radioisotopes copper-64, iron-59, and sulfur-35. Dissolution rates were measured in the time interval zero to 60 minutes, during which time significant anomalies were observed. First was an initial period of rapid dissolution lasting a few minutes; second, an arrest or ?plateau? region usually lasting from 6 to 10 minutes; third, a second period of dissolution of lesser rate than the first. The effects of solution variables such as pH, oxygen partial pressure, and ferric ion concentration at different temperatures were measured.

Jan 1, 1974

By C. R. Summers, J. N. Murphy

In response to the Coal Mine Health and Safety Act of 1969, mandatory noise standards have been developed that specify time-noise limits of mine personnel exposure. Most affected by elevated noise levels is the pneumatic roof bolter operator, both in terms of levels near or in excess of 115 dbA and in terms of length of exposure. Therefore, the principal emphasis of this Bureau of Mines report is on pneumatic drill noise control. It is not the intent of this report to suggest any drill redesign; instead, methods are suggested to reduce the noise level by complementing existing machines. An integral muffler system and a separate muffler system were tested in an attempt to lower pneurnaric drill noise levels. Pneumatic drills, when new, operate at about 115 dbA when drilling in sandstone. Using the drill muffler systems, it was possible to decrease the noise level of a 115 -dbA s rope drill to approximately 100 dbA.

Jan 1, 1974

As part of the Phase I study activity, a questionnaire was sent to a representative sampling of mining companies to obtain information on the uses, use conditions, personnel policies and other user concerns associated with front-end loaders. On-site visits to several of the mining companies were also parried out and the questionnaire was used during these visits as well. Five major areas were dealt with in the user questionnaire. These included: 1) Front-End Loader Critique - An open-ended form was employed to permit the mining companies to describe the particular things they liked and disliked about front-end loaders, in general, and/ or specific models in particular. 2) Usage - A form indicating the functions performed by front-end loaders and the numbers, makes and models of front-end loaders being used by mining companies. 3) Environment - A form where the user indicated the various types of conditions encountered in their use of front-end loaders. 4) Personnel - A form for describing factors pertaining to the qualifications of front-end loader operators. 5) Miscellaneous and Comments - A form permitting the user to comment on his feelings toward standardization of front-end loader operator stations.

Jan 1, 1973

By H. W. Gillett

This bulletin is issued by the Bureau of Mines as a contribution to the increase of safety and efficiency in the preparation and utilization of the mineral resources in the United States. Notable among the drains on these resources are the demands made by the nonferrous- metal industries, and in these the losses occasioned in melting brass and bronze are worthy of particular attention. This statement will be better appreciated by a consideration of the size of the brass industry.

Jan 1, 1914

By Terry S. Cory

This report covers magnetic field strength measurements vs range and frequency In low-medium coal mines. Both quasi-conductor-free and conductor-proximity areas were Investigated. The program covered 5 mines, 4 seams, 6 measurement sets, and 3 geographic areas, The results have been summarized In terms of maximum communication range expected per seam and noise condition. Scatter gain Is further explored as a simple measure of energy coupled to conductors.

Jan 1, 1978

By Paul L. Campbell

Investigations by the Federal Bureau of Mines of methods of upgrading tar obtained by low-temperature carbonization of lignite showed that ß,ß?-oxydipropionitrile, ß,ß?-iminodipropionitrile, and ß,ß'-thiodipropionitrile were effective solvents for extracting aromatics (aromatic hydrocarbons plus polar compounds) from coal-tar neutral distillate fractions. Batch extraction showed that these solvents extracted approximately the same percentage of aromatics from various neutral oil fractions boiling between approximately 170° and 350° C. In continuous countercurrent extractions using oxydipropionitrile and iminodipropionitrile, approximately 30 to 35 vol.-pct, and 65 to 70 vol.-pct, of the aromatics in 170° to 350° C. neutral distillate oil were extracted at room temperature when solvent-to-oil ratios were 2:1 and 12:1, respectively. As the concentration of aromatics in the neutral distillate oil fraction decreased, the capacities and, to some extent, the selectivities of these solvents for the remaining aromatics decreased. Aromatics were isolated from the extracts and the solvents recovered by washing the extract fractions with a low-boiling paraffinic hydrocarbon such as heptane, using hydrocarbon-to-extract ratios of at least 2:1. The heptane wash removed most of the aromatics but only part of the polar compounds (compounds containing oxygen, sulfur, and nitrogen) from the extracts. The recovered oxydipropionitrile and iminodipropionitrile, containing polar compounds, were effective in extracting aromatics from neutral distillate oils. The contaminated solvents showed essentially the same capacities and selectivities as the pure solvents.

Jan 1, 1961

By Robert P. Apa

Energy Incorporated has prepared this final report presenting the results obtained from the program for extracting alumina from anthracite culm along with the recovery of energy. This work has been accomplished under the auspices of the U.S. Bureau of Mines with technical coordination through the bureau's Reno, Nevada facility. The objective of this program was to develop a process to recover alumina and energy from Northeastern Pennsylvania anthracite mining waste. The program included Identification of sufficient resources to support a commercial facility, identification of the operating parameters which maximize alumina and energy recovery, the development of a conceptual process design, preparation of material and energy balance(s), and the performance of a system economical analysis. The program was conducted in three major phases. In the first phase the program concentrated on selecting several anthracite culm banks capable of supporting a commercial alumina producing facility. The chosen banks were then sampled and analyzed leading to the selection of two banks which were chosen far testing. The Harry E. and Eckley culm banks were the ones selected. Material from these banks was tested in Energy Incorporated?s Idaho Falls, Idaho testing facility. Parametric testing was accomplished in an eight-inch-diameter fluidized bed test facility. The test program consisted of twelve separate tests. After critical operating parameters were determined, the second phase started: process development in EI's 18-inch fluidized bed test facility. Three material and energy balance tests were completed in this facility. Following these tests a 72-hour demonstration test was performed. The data acquired from these tests were used in the last phase: the process conceptual design and economic analysis. The design basis was a commercial scale facility capable of producing 500,000 tons of alumina per year for 15 years. Based on the test program, It is technically feasible to build and operate such a plant today. The facility would produce, along with the alumina, 81.5 MWe of electricity for outside consumption. A preliminary rate of return indicates that the plant is not feasible with today's economic conditions. An increase in the market price of either the alumina or the electricity is required to provide an attractive rate of return for the facility.

Jan 1, 1982

By J. M. Oestreich

Supercritical water (sew) Is being tested for commercial use 1n several organic extraction systems but little work has been done on the extraction of metals from minerals. This lack of information prompted Bureau of Hines (BOM) research into the sew treatment of minerals. As a result, this research project is intended to serve mainly as a starting point for further experimentation. A simple flow-through reactor was built out of high pressure tubing and used to treat minerals with SCU at 400? C and 3500 to 7000 psi. The research produced four main conclusions: (1) carbonates of copper, iron, and lead convert to oxides; (2) most iron minerals showed alteration to oxides with some iron dissolution; (3) valuable trace elements including nickel, chromium, and others leached to some extent from sea minerals along with some calcium, iron, silicon, and sulfur; and (4) treatment of sulfides extracted elemental sulfur and resulted in several alteration reactions, though with the exception of cinnabar and the iron bearing minerals, the metals in sulfides were mainly insoluble. Surface alterations on many of the minerals show significant changes have occurred in the minerals even when only minor extractions were detected. These surface effects may be very important when used in conjunction with flotation processes since the sew treatment may selectively enhance or suppress a mineral's floatability.

Jan 1, 1989

By W. H. Frederic, A. C. Fieldner, W. A. Selvig

"Low-rank coals have a pronounced tendency to disintegrate or ""slack” when alternately dried, and wetted by exposure to the weather. The more readily a coal slacks the greater is its tendency to ignite spontaneously and the more care must be used in its shipment and storage. Lignite slacks very readily when exposed to the weather. Slacking trouble is also experienced in shipping and storing subbituminous coal, but not to the same extent as with lignite. As a rule, bituminous coals are only slightly affected by weathering and in general may be classified as nonslacking coals. The slacking tendency of subbituminous coal is one of the characteristics that is used to distinguish it from bituminous coal. An accelerated laboratory method of test was developed to measure such slacking tendencies. This method was applied to a number of coals, principally from the State of Washington, and the method and the results obtained are given herein.Helpful information concerning slacking tendencies of coal was received from Marius R. Campbell, senior geologist U. S. Geological Survey.Coals that slack readily contain relatively large amounts of moisture. When exposed to the weather such coals lore moisture rapidly. As the coal loses moisture at the surface there is a gradual drift of moisture from the interior of the piece to the surface. If the loss of moisture at the surface proceeds at a faster rate than it is replaced by moisture from the interior of the coal piece, there undoubtedly in greater shrinkage of the coal at the surface as tom-pared to the interior of the piece and stressed are generated in the surface coal.These stresses in the surface coal cause it to crack and disintegrate.Likewise, when the air-dried coal is wetted by rain, the exposed surface of the coal pieces gain moisture more rapidly than the interior of the piece, causing greater expansion in the surface coal and the coal breaks down further. As this process of air drying and wetting is continued when the coal is exposed to the weather, the slacking proceeds and the exposed lumps of coal may disintegrate completely."

Nov 1, 1930

By Motohisa Kanda

The time and amplitude statistics necessary to adequately describe electromagnetic (FM) noise in mines are illustrated through computer software techniques. They are 1) Allan Variance Analyses (AVA), 2) Interpulse Spacing Distributions (ISD), 3) Pulse Duration Distributions (PDD), 4) Average Crossing Rates (ACR), and S) Amplitude Probability Distributions (APD). These statistics are illustrated using data taken from a rather large store of raw analog data recorded in operational mines. The curves generated for the illustrations characterize the noise environment in the mines from which the corresponding data were taken, and should aid in the design of reliable communication systems for such mines.

Jan 1, 1974

By J. R. Wait, D. A. Hill

A survey of the literature on ELF and VLF atmospheric noise has been made. Most measurements have concentrated on the vertical electric field and the horizontal magnetic field rather than the vertical magnetic field which is of interest in transmission between horizontal loops. The limited vertical magnetic field data indicates that the vertical component is generally 10 to 20 dB below the horizontal component. Three laterally inhomogeneous earth models have been analyzed for conversion of horizontal to vertical magnetic field. The rough surface model examines surface effects, the inhomogeneous thin sheet model treats volume effects, and the buried cylinder model treats localized man-made effects. All three models predict the possibility of significant conversion from horizontal to vertical magnetic field. A thin sheet model has also been used to examine transmission from a buried magnetic dipole source. It is found that the pre- dicted fields more nearly model the measured data than does the homogeneous half-space model.

By Lloyd A. Morley

The performance of electrical grounding systems in open-pit metal mines is evaluated, using techniques which are described thoroughly. The normal electrical distribution and grounding practices used in metallic open-pit mines are reviewed and compared with coal mine usage. The results are used to generate the included recommendations for Federal Regulations concerning open-pit metal mine grounding systems.

Jan 1, 1976

By Elbridge W. Gresseth

Rock deformational structures in a deep mine were analyzed by petrofabric techniques to learn (1) the relative magnitude and direction of the principal stresses involved in tectonic deformations prior to mining, (2) the preferred orientation of rock planar discontinuities which define rock anistropy prior to mining, and (3) the relationship of mining-induced rock failure to inherent rock stresses and inherent rock anisotropy. Rock fabric elements used for petrofabric analysis consisted of bedding planes, faults, joints, fractures, foliation, sericite plane (001), quartz axis [0001], quartz deformation lamellae, and microfractures. Structures and structural symmetries from different areas within the mine and from different scales of observation were compared to learn the nature of rock anisotropy and the orientation of the principal stresses defined by rock deformations. Analysis of such fabric as regional and macroscopic faults, b-c joints, quartz [0001], sericite (001), and microfractures, indicate that during the epochs of tectonic deformation, the maximum and minimum principal stresses were horizontally oriented and acted along northwest and northeast axes, respectively. This condition of regional stress appears to have continued during folding and the associated period of faulting. The most recent tectonic deformation represents a rotation of the minimum principal stresses into a vertical position, as shown by the development of a tensile joint system, quartz deformation lamellae, and microfractures. Good interscale correlation and statistical homogeneity of tectonic fabric indicate a stress field homogeneity in this area during tectonic deformation. Rock physical anisotropy is genetically associated with tectonic fabric and consists of preferentially oriented planar discontinuities intersecting along a nearly vertical axis. The mining-induced deformations were correlated with the inherent rock anisotropy which either directly controls or greatly affects their development. This phase of rock deformation shows a greater degree of stress field heterogeneity than was the case with tectonic deformations This is explained as a result of nonconfinement afforded by underground openings and the increase in ground stresses due to mining activity"

Jan 1, 1968

By George S. Koch

In preparing diamond-drill core samples for assay at the Homestake mine, Lead, S. Dak., 5-foot intervals of core are processed through three stages, crushing, grinding, and pulverizing, and portions of the core material are discarded after splitting at each stage of preparation. Then two 1-assay-ton fractions are taken from the pulverized material and assayed. This report investigates alternative methods of sample preparation. The consequences of crushing, grinding, and pulverizing all rather than part of the core are appraised through the statistical analysis of assay results from 118 5-foot intervals of core. Evidently, a substantial improvement in precision at small additional expense is obtained by grinding most or all of the core before splitting. Pulverizing all of the core would be desirable only if doing-so would cost less than assaying five random splits from each interval. Graphs and tables detail appropriate procedures to obtain specified precisions. The experimental design and methods can be applied to similar problems in preparing core and other geological samples.

Jan 1, 1972

Two coal seams were selected and the conceptual designs were based on the geological and physical conditions typical of these seams. As a result of the screening process presented below, the two coal seams selected were the Lower Kittanning Seam in central Cambria County, Pennsylvania and the Pittsburgh Seam in northwestern West Virginia and southwestern Pennsylvania. SELECTION PROCESS FIRST SCREENING OF LONGWALL OPERATIONS The list of longwall operations prepared in Phase I and included in the Phase I report, was used as the basis for a first screening. From this list it was determined which longwall operations were not in the Appalachian coal fields and not in a coal seam of the thickness range of 42 to 72 inches. The first screening eliminated 30 of the listed operations, leaving 48.

Jan 1, 1976

By David A. Monaghan, Kenneth R. Maser, Adi R. Gurdar, D. Randolph Berry

7. Development of Acoustic Seal Checking System The acoustic approach was shown in Section 4 of this report to be the most promising concept for checking the seals. This section describes the development of this concept into a working hardware system to be used later in the field test program. This development effort included: (1) Theoretical analysis of the acoustic behavior in the mine using acoustic modeling- techniques. (2) Experimental determination of acoustic patterns in mine passages. (3) Refinement of the theoretical model. (4) Verification of final theoretical predictions in the quarter-scale laboratory model of a mine passage and seal. (5) Development of system specifications. (6) Development of the Acoustic Prototype Seal Checking System. 7. 1 Analysis of the Acoustic Seal Checker Concept The acoustic seal checker concept is based on a model which combines corridor acoustics and hole transmission theory. The idealized model for the mine sealing application is shown schematically in Figure 66. A high intensity acoustic- source is located in a corridor at a, position adjacent to the location to be sealed. The acoustic signal transmitted through the seal is monitored by a microphone pick-up placed on the opposite side.

Jan 1, 1973

By I. Liebman

The Bureau of Mines conducted research to develop triggered barrier systems for protection against gas explosions that can occur in underground coal mines during the use of continuous miners. Several extinguishing agents were tested in barriers at a simulated mine face. Water, powered by pressurized nitrogen, was found to be efficient in stopping fully developed gas explosions, but it had little effect against the explosion during its incipient stage. Hybrid combinations of currently known extinguishants, however, were successful against incipient explosions. Three hybrids that were developed and tested consisted of Halon 1301, combined with either an aqueous foam solution, water, or a dry chemical powder. The three hybrids were found to be more efficient than any constituent alone. Results of the tests point to a synergism between the hybrid components, and indicate that the Halon aids in dispersing its constituent and also converts the aqueous foam solution into a stable fine foam and the water into fine drops.

Jan 1, 1978

By Frank S. Wartman

"The experimental flotation work described in this paper was undertaken to test the conclusions derived from a previous microscopic and chemical study of several samples of converter slag. That study3 resulted in the conclusion that approximately 90 per cent of the copper content of a converter slag wad in either the sulphide or metallic form, and that if the slag were cooled slowly the copper-bearing material would be in particles of such size that they would be freed from silicate and magnetite grains by grinding the slag to pass a 150-mesh sieve. If this were true, it should be possible to separate the copper-bearing grains from slowly cooled, converter slag by the flotation process.Many attempts, of which the author has seen no published account, have been made to treat slags, especially converter slags, by flotation. In every case these trials have been made with chilled slags, in which, as shown in the preceding report, the copper-bearing material is top finely disseminated, to be freed by any reasonable degree of grinding.The flotation tests described in this paper have shown that it is possible to recover by flotation about 30 per cent of the copper content of a converter slag containing 3 per cent copper and to obtain flotation concentrates which have a copper content of 35 per cent.Acknowledgment is made to G. L. Oldright, supervising engineer of the section of nonferrous metallurgy, U. S. Bureau of Mines, for valuable assistance and direction; to W. A. Sloan for chemical analyses; and to Alfred P. Towne for assistance in experimental manipulation."

Apr 1, 1931