Search Documents

By George J. Conroy

To provide data as a basis for proposed acceptance standards and procedures covering permanent splices in trailing cables, the Bureau of Mines conducted testing programs on the flexure life in flat types W and G dc trailing cable splices and ground conductors. Primary reliance was placed on laboratory testing, although some cross comparisons were made at manufacturers' plants and mine operations Besides providing data for acceptance standards and procedures, results of the program should promote the general improvement of commercially available splice kits.

Jan 1, 1977

By A. B. Campbell

The mines in the eastern part of the now active region of the Tri-State zinc district of Missouri, Kansas, and Oklahoma have unusually acid water, which during periods of moderate or no rainfall is used in the mills to replace losses from evaporation, seepage-, and tailings disposal. Its use has caused difficulties by corrosion of equipment and by interference with flotation. The growing importance of flotation, which requires good water, and the increasing troubles caused by the corrosion of the milling equipment have prompted the Mississippi Valley Experiment Station of the United States Bureau of Mines, in cooperation With the Missouri School of Mines and Metallurgy, Rolla, Mo., to investigate the action of the waters on flotation and to undertake to develop means of obviating their harmful effects. The work was under the immediate direction of W. T. Schrenk, consulting chemist, United States Bureau of Mines, and professor of chemistry Missouri School of Mines and Metallurgy, and. Will H. Coghill., supervising engineer of the ore dressing section of the United States Bureau of Mines.

Jan 1, 1932

By Charles Findlay, Stephen Krickovic, J. E. Carpetta

As one of its projects for degasification of major panels of coal prior to mining within them, the Bureau of Mines conducted methane emission studies during development of a set of three headings 1,800 feet in a major coal panel (2,700 by 3,500 feet) which had been completely isolated by sets of main headings for 12 months in the Federal No. 2 mine (Pittsburgh coalbed) in northern West Virginia. Similar emission studies were conducted in the development of two sets of main headings in virgin coal areas nearby. Comparing the two sets of data indicated that the isolated coal panel had been degasified by approximately 70 percent.

Jan 1, 1973

By Lon A. Williams

This report, authorized under Contract Number H0220065, Amendment Number Six, documents the results of an investigation of lighting system modifications and designs for working place illumination in high and low coal entries of underground coal mines. The portable and machine mounted system designs, both modified and prototype, represent a continuation of work performed under Contract Number H0111403, Amendment Number One. See the Final Technical Report dated May 26, 1972 for detailed information concerning this prior Contract. All modified and prototype systems met the performance requirements of Bureau of Mines Specification 2G, as proved by test. In addition, the systems met the requirement for illumination, as specified in the Contract and in the proposed standards which were generated in response to Public Law 91-173.

Jan 1, 1976

By Jerry E. Olson

In 1984, the U.S. Bureau of Mines conducted a mineral survey of the Black Rock Desert Wilderness Study Area (WSA) (NV-020-620), which covers approximately 319,000 acres in Humboldt County, Nevada. About 90% of the WSA is underlain by Pleistocene desert playa sediments; the remainder is comprised of Jurassic-Triassic metamorphic rocks, a Cretaceous intrusive and Tertiary volcanic rocks. Most of the WSA is within a down-dropped fault block of the Basin and Range physiographic province. No mines or evidence of major exploration were identified within the WSA; but five claim blocks within or adjacent to the WSA and zones of anomalous character as defined by the Bureau of Land Management were examined. No mineral resources were identified, but anomalous gold, silver, and indicator element content of samples taken near Pinto Hot Springs indicate resources may exist. Lithium content of samples from near-surface sediments on the desert playa is too low for resources, out geologic conditions are favorable for higher concentrations at depth. Occurrences of zeolites are not considered to be of commercial interest. Approximately 27,000 acres are held under geothermal lease, and most of the WSA is of interest for oil and gas. No evaluation of these commodities was made by the Bureau of Mines

Jan 1, 1985

By L. A. Haas

The U.S. Department of the Interior, Bureau of Mines, is conducting laboratory-scale research to determine the leaching conditions required with sulfuric acid for extracting base metal from a matte with a copper-to-nicke1 ratio of 6 to 1. The matte (61.2 pct Cu, 9.7 pct Ni, 3.3 pct Fe, 21 pct S, and about 5 oz of precious metals per ton) was prepared from Duluth Complex (Minnesota) ore by smelting a bulk sulfide flotation concentrate. The matte was pre leached at atmospheric pressure to selectively extract 20 pct of the nickel, and the undissolved solids were referred to as the matte residue. Autoclave leaching of the matte residue extracted over 95 pct of the nickel, copper, and iron. The remaining leach residue in the autoclave contained over 100 oz of precious metals per ton. The leaching conditions required were matte grind of greater than 98 pct minus 325 mesh, pulp concentration of 50 g/1, total pressure of 100 psig with oxygen at 150° C or 400 psig with air at 180° C, 50 g/1 H2S04, 700 rpm agitator speed, and 6 hours of leaching time. The leaching time was decreased to 2 hours by increasing the agitator speed to 1,300 rpm. Sulfuric acid concentration greater than 50 g/1 did not appreciably enhance the base metal extraction, but with less acid, residues with higher iron concentrations were obtained. Supersaturation of the liquor was prevented at 150° C by using a 1ixiviant that contained 30 g/l Ni and 20 g/1 Cu.

Jan 1, 1979

Geological discontinues in the coalbed, such as faults, sandstone channels, permeability facies, lithotype changes, and large scale partings in the coal seam, can cause intermittent production problems or produce unexpected amounts of water or gas from degasification boreholes. These discontinuities not only can impact methane emissions into the mine workings, especially if they hinder proper and effective degasification of the coalbed but may act as conduits for methane flow from gassy strata into advancing mine workings. The effects of these discontinuities are still under debate by mining and gas production experts. This study presents a numerical investigation using reservoir simulations of the effects of partings and permeability facies and lithotype changes on the production performances of vertical and horizontal degasification boreholes, as well as the emissions during longwall operations. In this work, the grid block was designed in a multi-layer 3-D structure which enabled spatial descriptions of the geometries and properties of the discontinuities within the coal seam. The studied coal seam discontinuities and their properties were distributed arbitrarily within the model. Production was simulated by vertical and horizontal boreholes. Degasification boreholes operated two years prior to start of the mining. The results of this numerical study show that in coal seams with major heterogeneities and discontinuties, the geometry and location of the boreholes are important for improved gas production. These considerations are also important for controlling methane and water inflow into the working environment during longwall mining.

Jan 1, 2008

By Howard D. Jacobs

A bulk sample of oxidized taconite taken from the western Mesabi Range was evaluated by the Bureau of Mines using the Bureau-developed selective flocculation-desliming-cationic (or anionic) flotation process. The raw ore sample containing 32.3 pct Fe was treated by both cationic and anionic flotation. Using the cationic system the concentrates averaged. 37.2 wt-pct of the feed and contained 62.8 pct Fe and 4.7 pet Si02 with an iron recovery of 72.3 pet. With the anionic system, concentrates averaged 37.7 wt-pet of the feed and contained 63.0 pct Fe and 5.3 pct 8i02 with an iron recovery of 73.5 pct. A comparison of reagent costs showed that the cationic process cost 144.1 cents per long ton of crude ore and the anionic process 178.7 cents per long ton of crude ore. Reclaimed water comprised 86 pct of the total water requirement for anionic flotation and 88 pct for cationic flotation. The ore used in this study was one of three samples representing about 3.25 billion tons of oxidized taconite containing from 32 to 36 pct feed iron. Previous study had indicated that selective flocculation-desliming-cationic flotation would produce concentrates from the other two samples of 61.7 pct Fe and 5.1 pct Si02 at 67-pct Fe recovery, and 63.5 pct Fe and 4.3 pet Si02 at 8S-pct Fe recovery. By developing a successful treatment for these ores, the Bureau has insured the availability of technology for processing an amount of raw iron ore which, by itself, would supply U.S iron needs for 50 to 75 years at expected consumption rates.

Jan 1, 1981

By R. Ward Stahl

Fire has been one of man's most useful tools through the ages and certainly is a "must" for industrial progress but when uncontrolled is one of the most destructive agencies. This fact is even more important in a coal mine, where many persons and much expensive equipment are confined in a relatively small area. Means of escape from a burning area, as well as from the products of combustion, are often limited; and in many instances the entire surroundings are combustible. Numerous mine fires, which resulted in a high death toll and great financial loss through the years, have caused mine owners to search for the best fire-fighting equipment; much of this has been installed, the quantity depending largely upon the experience of the individual companies or neighboring mines in certain coalfields. A mine owner or operator has meager published information on the actual fire protection afforded and systems of fire-fighting inaugurated in the coalfields, by which he could compare his efforts and get some idea of the adequacy of his own protection. To further general knowledge of the subject, it was decided to survey a representative number of mines in the field and show what has been accomplished. Representative mines were selected in various coal beds; some had similar tonnage, so comparison could be made if desired.

Jan 1, 1957

By Frank D. Lamb

"INTRODUCTION The use of beryllium and its alloys has come into prominence in the last 15 years and increased considerably during the war. In contrast to other light metals, such as aluminum and magnesium, beryllium is relatively hard, has a high melting point (1,285° C.), and other properties that make it resemble steel in many respects. It has a specific gravity of 1.85, is only slightly heavier than magnesium (specific gravity 1.74), and is appreciably lighter than aluminum (specific gravity 2.7). Its lack of ductility prevents its use as a structural material, but this difficulty may be overcome in the future by the use of various alloy forms. The only important commercial alloy in which beryllium is used today is with copper. The addition of small percentages (1/2 to 2 percent) of beryllium to copper imparts properties to the alloy that make it desirable for use in springs carrying electrical current, particularly at high temperature. Many other uses of berylliam are known, and new uses are being found constantly that make the metal of increasing interest.Possibly the main factor preventing the use of more beryllium is the lack of a large source of beryllium ore. Many beryllium minerals are found as minor constituents of natural deposits, some of the more common ones being beryl (Be3Al2(Si03)6), chrysoheryl (Be A1204), helvite (3(Mn, Fe) Be Si04. MnS), and phenacite (Be2Si04). Of the known beryllium minerals, beryl is by far the most common and has been found distributed rather widely throughout the world. It usually occurs associated with granitic rocks and is commonly found as a constituent of granitic pegmatite."

Mar 1, 1947

By Kenneth L. Rubow, Virgil A. Marple, Bruce K. Cantrell

"In a cooperative study by the University of Minnesota and the U.S. Bureau of Mines, diesel exhaust and mineral dust concentrations have been measured for aerosols generated in the laboratory and in five underground coal mines. Three mines utilized diesel-powered haulage equipment and two used all-electric equipment. Two source apportionment techniques have been applied to differentiate between the mineral dust and diesel exhaust aerosol concentrations measured. The first technique, using a micro-orifice, uniform deposit impactor (MOUDI) for size selective sampling, is based on modeling aerosol size and the premise that the diesel exhaust portion of the aerosol is predominantly submicron and the mineral dust portion is mostly greater that one micrometer in size. The second technique, Chemical Mass Balance (CMB) modeling, was used to referee the analysis of diesel exhaust and mineral dust aerosol concentrations from the size selective sampling results.The MOUDI size distribution data were modeled to obtain parameters describing the fine and course fractions of the sampled aerosol and to estimate the contributions to each mode from both mineral dust and diesel exhaust aerosol sources. The results showed the size distribution of the mixed aerosols exhibited two definite modes with the minimum between the modes occurring at 0.8 µm. Less than 5 pct of the coal mine diesel aerosol was found in the coarse size fraction. CMB analysis confirms the original premise for using aerosol size to separate diesel exhaust and mineral dust aerosol during sampling.Based on the results from the size selective sampling, a personal diesel aerosol sampler has been developed for measuring diesel aerosol mass concentrations. Th.is sampler uses an inertial impactor to size separate the respirable aerosol at 0.8 µm. All material less than 0.8 µm is collected on an after filter for subsequent gravimetric analysis."

Jan 1, 1990

By James V. Kelly

During the winter of 1946 and the spring of 1947, the Bureau of Mines conducted an investigation and drilling program in the vicinity of the village of Fairplay, Wis. Fifteen diamond drill holes totaling 2,457.6 feet of bore were completed. This work was part of a general study of the zinc-producing area of southwestern Wisconsin and had the particular purpose of investigating a structural trend, determined by the Federal Geological Survey, in an area some distance from known ore bodies or active mines.

Jan 1, 1948

By W. A. Stickney

The Bureau of Mines conducted beneficiation and smelting studies on siliceous offgrade manganese samples to indicate effective methods of manufacturing silicomanganese from materials that cannot be economically beneficiated to meet General Services Administration (GSA) specifications for stockpiling. Laboratory and pilot-plant flotation tests were conducted on 2 samples, 1 from the waste-tailings dump of the Domestic Manganese & Development Co , Butte, Mont., and the other from the Nettie mine in the Butte-Philipsburg area. Smelting tests were made on the combined concentrates from the pilot-plant flotation tests and on part of the tailings sample The flotation scheme found to be adequate in laboratory tests and later in the pilot-plant tests consisted of flotation by a fuel oil-tall oil emulsion in an acid circuit (pH )-1-.8 to 5.0). The oil-emulsion reagent flocculated the manganese minerals and selectively floated them from the siliceous gangue, In the pilot-plant flotation test on Butte-mill tailings 90.1 percent of the manganese was recovered in a concentrate that analyzed 32.6 percent Mn, 4.8 percent Fe and 28.1 percent Si02. In the test on Nettie mine ore 90.8 percent of the manganese was recovered in a concentrate that analyzed 36 6 percent Mn, 5.5 percent Fe, and 26-4 percent Si02.

Jan 1, 1956

By P. A. Wasson

The investigation described in this publication was conducted by the Bureau of Mines to determine the effectiveness of the anionic silica flotation method on goethitic iron-bearing materials from the Cuyuna Range, Minn. Samples used in this investigation were a composite of drill core from 13 holes, and 3 samples from lean ore stockpiles. These samples are believed to be typical of the mineralization occurring in an area with a potential reserve of several million tans of submarginal iron ore. Results from batch tests showed that the iron-bearing minerals could be effectively concentrated by flotation removal of the siliceous gangue. The drill hole composite yielded laboratory flotation concentrates from locked tests containing 56.8 percent Fe and 6.1 percent silica, with an accompanying iron unit recovery of 94.2 percent. Concentrates containing 52.4 to 53.7 percent Fe also were produced from the lean ore stockpile materials; corresponging iron recoveries ranged from 71 to 79 percent in the batch tests, with the possibility remaining for additional recovery of iron from the middlings.

Jan 1, 1963

By V. Castranova, T-M. Ong, V. Vallyathan, M. J. Keane, W. E. Wallace Jr.

"Inhalation of certain forms of silica, asbestos and some other respirable dusts can result in pulmonary fibrosis, characterized by destruction of the surfaces of alveoli and respiratory bronchioles. Fibrous thickening of the alveolar septa decreases the lung's capacity for gas exchange.Pulmonary macrophage damage by respired dust may initiate the fibrotic response.In one proposed mechanism, dust particles interact with the plasma membrane of a macrophage. This damages the cell or induces some hyperactivity of the cell, resulting in excessive release of lysosomal enzymes and reactive forms of oxygen (1). These reactive enzymes or radicals then damage the alveolar surface epithelial cells. A second mechanism has also been pro¬posed (2,3) in which dust damage to the macrophage causes the release of mediator substances which induce pulmonary fibroblast cell proliferation and increased collagen synthesis. This produces fibrous tissue in the terminal air spaces (4,5).Mineral surface interactions with plasma membrane lipoproteins have been proposed as a mechanism of lytic damage of pulmonary cells by silica dust in numerous models (6,7). The significance of dust surface proper¬ties has been further revealed in studies showing significant changes in dust induced cytotoxicity as a function of dust surface crystallinity and organic or inorganic contamination or coating of mineral surfaces (8,9). Such modification of the mineral surface might interfere with surface sites responsible for the toxicity of dusts for pulmonary macrophages, thus interrupting the early stages of the process of fibrosis.In vitro cellular assay systems using erythrocyte hemolysis or the release of macrophage cytosolic or lysosomal enzymes following dust challenge, have been used to analyze the initial mechanism of dust damage to cells. However the ability of these assays to predict the pulmonary disease producing potential of various dusts is imperfect owing to some ""false positive"" results. These assays as performed are therefore questionable models for the initial lesion in pneumoconiosis or silicosis. In particular, kaolin frequently is found to have comparable biological activity to silica quartz in these assays (10,11).Silica and kaolin have distinctly different fibrogenic potentials. Silica is highly fibrogenic, resulting in both acute and chronic silicosis (12). Some epidemiological data and animal experimentation data have indicated that long term exposure to kaolin can result in pneumoconiosis; however, kaolin is relatively benign as compared to silica (13-18). Kaolin is also of interest because it is one of the major mineral inclusions in Eastern U.S. bituminous coals. We have observed that exposing respirable sized native silica or kaolin for two hours to pulmonary macrophages results in a greater enzyme release for kaolin exposures, on a dust mass basis. Exposure of erythrocytes to the dusts also results in greater levels of hemolysis by kaolin for equal mass respirable dust doses. Therefore, these results do not correlate positively with known disease inducing potentials of the two dusts.Characterization of physical and chemical surface properties of dusts involved in occupational exposures, and characterization of the alteration of those surface properties which are likely to occur upon deposition of the dust in the lung, should improve the identification of respiratory disease hazards.Inhaled dust particles deposited in the lower respiratory tract will come in contact with pulmonary surfactant. This surfactant forms a surface film on and emulsion in the liquid hypophase coating of the alveoli and respiratory bronchioles. The primary constituent of this pulmonary surfactant is the lipid diacyl glycerophosphorylcholine, lecithin (19). Because this lipid is also a major component of cell membranes, it is possible that surfactant can interact with mineral dust to alter its Interaction with macrophages and other pulmonary cells and, thus, it"

Jan 1, 1988

By W. J. Kroll

The production of beryllium metal and its alloys is one of the most difficult tasks in metallurgy. In this report we shall examine the progress made in this work- in the last 15 years; taking into account the outstanding publications, including; those of the patent literature, and the information obtained during our 20 years? experience with this metal. The difficulties experienced' in producing elementary beryllium derive from the physical nature as well as from the chemical behavior of the metal and its compounds. Its oxygen affinity is about the same as that of calcium and a little higher than that of magnesium. Its chlorine affinity is much lower than that of magnesium, about equal that, of manganese, and little higher than that of aluminum. The sulfur and nitrogen affinity is probably almost the same as that of calcium for these elements, and beryllium carbide is probably more stable than aluminum carbide, A14C3. The intermetallic affinity of beryllium may be given in descending order, as follows: Nickel - copper - iron. It forms eutectics with -aluminum and silicon as well as with silver. It does not alloy with magnesium and only partly with calcium. Its oxide melts at 2,570° C., but CaO and BaO form readily fusible eutectics with BeO(65).3/ No igneous solvents are known for BeO, which behaves id this regard like Mgo. The beryllium silicate is a strong compound, the aluminete much less so; however, CaO easily displaces Be in the heated mixtures. The Anhydrous chloride hydrolyzes, and it cannot be made from aqueous liquors. It sublimes at 488° C, and melts at 405° C., The fluoride, which, is very Soluble in water, hydrolyzes also, but a kind of oxyfluoride of the approximate formula 2 BeO?5 BeF2 can be made from solutions by dessication. The fluoride melts at 800° C, and boils above 1,100° C. It forms very stable double fluorides with alkalifluorides, which have very low melting points and are fairly soluble in water. They are more stable than the analogous fluosilicates and the sodium fluoaluminate cryolite.

Jan 1, 1945

By S. D. Maksimovic

The use of vertical surface degasification boreholes with bleeder systems and the use of a timbered bleeder system to degasify gob areas were studied by the Bureau of Mines. This report describes three gob degasification studies conducted in the Pittsburgh coalbed. One study was conducted to determine the number of panels degasified with one large borehole. The study showed that the borehole provided degasification for three panels. Another study was conducted during the retreat of a 35-acre panel with a single-entry and a two-entry bleeder system and a large surface borehole. A major portion of methane emitted from the panel was carried away by the bore-hole, leaving the bleeder entries relatively free of methane. The last study was made to determine the effectiveness of a timbered bleeder system. The bleeder entries successfully degasified the gob area when enough entries were available and adequate pressure was available to force the air through roof falls.

Jan 1, 1980

By C. A. Komar

The Bureau of Mines has undertaken an investigation to determine possible applications of acoustic energy at sonic and ultrasonic frequencies to improve ultimate recovery from oil reservoirs. A literature search was conducted to provide background information for initiating laboratory research. The purpose of the literature search was to review the uses that have been made of acoustic energy in the petroleum industry and to select procedures and techniques that could be applied to the solution of petroleum production problems. The characteristics (68)3 of ultrasonic energy make it potentially useful to a variety of industrial and experimental applications. Pulse techniques (99) are common in the testing of materials where inspection is accomplished by propagating an ultrasonic pulse through the material. Viscosity measurements (45) are made by interpreting changes in the absorption of sound as it is propagated through a flowing liquid. Cavitation phenomena (93) produced by high-intensity ultrasound in liquids have been used extensively in industrial cleaning, machining, impact grinding, and aluminum soldering operations.

Jan 1, 1963

By Eric R. Bauer

The U.S. Bureau of Mines, in cooperation with a southwestern Pennsylvania coal mining company, BethEnergy Inc., Mine No. 60, Eighty-Four, PA, recently assessed the feasibility of using pre driven recovery rooms (open entry recovery) when longwall mining to increase the productivity of the coal extraction process. Two recovery entries, one 200 ft long and another 600 ft long, were supplementally supported with bolts, channels, and wire mesh, and either fly ash-cement piers or fiber cribs, then mined into by the longwall face. The recovery entries showed little deterioration as the supports provided adequate resistance to the front abutment loading. Compared with conventional recovery methods, the fullface recovery room allowed for panel extraction to be completed nearly 17 days faster and to reduce face equipment move time by 1-1/2 days. The potential productivity increase accompanying recovery rooms is greater than the cost of supporting a fullface recovery room. The fullface recovery room provided over 18 additional production days and the opportunity to mine nearly 68,400 st of coal per year per panel mined.

Jan 1, 1989

By R. A. Beall, W. E. Anable

The purification of hafnium by electron- beam melting at moderate energy inputs and at low pressures was examined in detail . Most metallic impurities and hydrogen were removed in the first few minutes of operation ; oxygen , carbon , and nitrogen were removed at a slower rate . Samples treated by electron bombardment suffered a small loss of weight and a gradual lowering of hardness . The magnitude of each change varied with the energy input and the duration of the melt . Analysis of the data confirms the loss of oxygen as a hafnium monoxide . Approximate activity coefficients for other contaminants are given .

Jan 1, 1964