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By J. H. Maysilles

The Bureau of Mines is conducting research on various technologies to recover alumina from domestic resources for feedstock to existing aluminum smelting capacity as a means to reduce dependence on imported bauxite, which represents 93 pct of U.S. aluminum requirements. One of the more promising technologies being investigated is the hydrochloric acid leaching of kaolinitic clay. In the hydrochloric acid leaching technology, alumina is recovered from iron-free aluminum chloride leach liquor and separated from impurity elements by sparging the liquor with HC1 gas to crystallize aluminum chloride hexahydrate (ACH). A large-scale crystallizer with a 336-gallon usable volume was constructed and operated to obtain engineering and design data for potential scale up and to demonstrate the ability of the technology to produce specification grade alumina. Test campaigns involving about 1,400 hours of operation were completed. ACH meeting all chemical purity requirements could not be produced by a single crystallization, but was produced by recrystallizing the product from the calcined kaolin clay leach liquor. Product crystals with a size distribution of more than 80 pct plus 100 mesh and 65 pct plus 65 mesh were made at a rate of 10 pounds of ACH/(hr)(ft3). The zirconium tube heat exchanger used to maintain constant process temperature operated with an over-all heat transfer coefficient of 420 to 500 BTU/(hr)(ft2)(°F).

Jan 1, 1981

By David A. Benjamin

In 1986, at the request of the U.S. Bureau of Land Management, the U.S. Bureau of Mines studied part of the 24,600-acre Orejana Canyon Wilderness Study Area (OR-001-078), in order to evaluate its identified mineral resources. The study area, located in Harney County, 76 mi northeast of Lakeview, OR, is underlain by Miocene basalt, rhyolite flows, tuffs, and tuffaceous sedimentary rocks. No mines, prospects, or claims were found within the study area. According to the U.S. Bureau of Land Management, the tuffaceous rocks have a moderate favorability for the occurrence of diatomite and a low favorability for zeolite resources. Also, the rhyolite flows have a low favorability for the occurrence of perlite resources. However, U.S. Bureau of Mines' studies indicate that no metallic or nonmetallic resources are present in the study area.

Jan 1, 1987

By A. Wahab Khair, Nagendra P. Reddy

"This paper presents an analysis of preliminary tests on the effect of in-situ and operating parameters on fragmentation of coal using a specially designed unique automated rotary coal cutting simulator (ARCCS). In these tests coal blocks with an approximate dimension of 18 in. x 15 in. x 6 in. (45.7 cm x 38.l cm x 15.2 cm) were first. subjected to confining pressures, equivalent to in-situ conditions. Such. blocks were then cut by the cutting head of the ARCCS, thus simulating the action of the continuous miner in underground coal mining. During the tests under a particular set of in-situ and operating parameters a number of other parameters such as 1) penetration of bit into coal, 2) penetration resistance (thrust and cutting pressures), 3) rotating velocity of cutting head, and 4) acoustic emission activity in the coal block were monitored. After each cutting cycle the fractured surfaces were photographed and a velocity survey was conducted by using a sonic technique. At the end of each experiment the cutting paths of the bits in coal were photographed using an optical microscope with a camera attached to it. Furthermore, the coal fragments were collected in bags using a vacuum cleaner. These fragments were then sieved for size distribution analysis. The results of the preliminary tests indicated that underground coal cutting can be simulated in the laboratory and the effects of the important parameters, i.e. operating and in-situ parameters, can be studied successfully. INTRODUCTIONThe continuous-mining machines which were introduced in the 1950's now account for more than half the production of coal from underground mines. Unfortunately, these continuous miners, which were designed for increased productivity, have also increased the concentration of respirable dust in mines. As a result, the Federal Coal Mine Health and Safety Act of 1969 was enacted to enforce on the coal operators that the airborne respirable dust not exceed 2 mg/m3, and was intended to reduce the incidence of coal workers pneumoconiosis. This plus the other aspects of the legislation and the subsequent monitoring and enforcement by MSHA made it very imperative that the coal operators provide a relatively healthier and safer working environment for the coal miners. Since 1970, the Federal government has paid over 11.7 billion dollars to more than 470,000 miners with coal workers pneumoconiosis and their survivors (1). These regulations, coupled with the assessment of the continuing burden on miners, the mining industry and taxpayers appear to have provided an impetus for the mining .community towards comprehending the different parameters that influence dust generation and entrainment."

Jun 1, 1988

By F. D. DeVaney

The low-grade deposits of manganese ores along the Missouri River near Chamberlain, S. Dak., are known to contain one of the largest reserves of manganese in the United States. Manganese occurs as concretionary nodules ranging in size from 13 inches in their longest dimension to particles finer than 65-mesh. The nodules are embedded in soft, wet shale, which contains little manganese. The removal of nodules from the low-grade shale is a simple mechanical problem; the question is primarily to determine the lowest-cost method of separation. This report purposes to present data acquired by experimenting with samples of the ore, which form a basis for suggesting methods of concentrating manganese nodules.

Jan 1, 1942

By F. D. DeVaney

The low-grade deposits of manganese ores along the Missouri River near Chamberlain, S. Dak., are known to contain one of the largest reserves of manganese in the United States. Manganese occurs as concretionary nodules ranging in size from 13 inches in their longest dimension to particles finer than 65-mesh. The nodules are embedded in soft, wet shale, which contains little manganese. The removal of nodules from the low-grade shale is a simple mechanical -problem; the question is primarily to determine the lowest-cost method of separation. This report purposes to present data acquired by experimenting with samples of the ore, which form a basis for suggesting methods of concentrating manganese nodules.

Jan 1, 1942

By R. W. Huber

While conducting an investigation on electrolytic reduction of magnesium oxide in 1943, it became necessary to obtain accurate data on the conductivity and density of various mixtures of fused chlorides. AZ the required information was not available in the technical literature, or there were inconsistencies in the data from several investigators, an independent study was made at the Bureau of. Mines laboratory at Salt Lake City on the conductivity and density of the molten chlorides MgCl2, CaCl2, BaCl2, KCl, and NaCl and the binary mixtures of MgCl2 with the other four chlorides. Studies were also made on the binary system KCl-CaCl2 and on certain portions of several ternary systems. Measurements covered a temperature range from the melting point to 1,000° C. The results of this study were reported in an intra-Bureau report prepared early in 1944. Since then the Bureau of Mines has received several requests for data on fused chlorides; the results of the previous study, therefore, are being published to make the data available.

Jan 1, 1952

By D. C. Dahlin

The Bureau of Mines investigated the Ketchem Dome tin prospect in east-central Alaska to evaluate the tin resource. The studies included field investigations, mineralogical characterization, and concentration of the tin-bearing minerals. The tin mineralization consists of cassiterite (Sn02), which occurs as grains disseminated in a greisen (quartz-mica) matrixo A bulk sample from the largest and best-developed greisen vein exposed at Ketchem Dome contained 0.51 pct Sn. Concentration of the cassiterite by gravity table methods resulted in a product that contained 56 pct of the tin at a grade of 41.4 pct Sn. The mineralization exposed at Ketchem Dome is typical of greisen found in the area and elsewhere in interior Alaska.

Jan 1, 1987

By E. C. Hoeman, W. C. Stoecker, R. C. Redfield

"INTRODUCTION Industrial sands, characterized by specific physical and chemical proportion, are,essential new materials for the manufacture of glass, sodium siliante and other products. Sands of suitable characteristics are used extensively for molds and cores in the casting of metals as a granular medium in municipal water filters, as abrasives, as traction sand to prevent the slipping of driving wheels of self-propelled vehicles on trucks and in various ceramic and other structural forms. In addition to the use of common silicon sands in concrete, cement, and mortar, special sands find use in sand-lime brick oxychloride cement, and flooring, for coating prepared roofing, and for placing ware in saggers although sand for sandpaper has been mostly displaced by other harder mineral or synthetic grains, other abrasive uses are numerous and include sandblasting stone sawing, glass burnishing and finishing."

Oct 1, 1945

By Francis Church Linxoln

"This property was explored as part of a general investigation of zinc-prodccing areas of southwestern Wisconsin at a time when an effort was being made to increase the production metals important to the Nation's war program. This report describes the work that was done and presents the data obtained.ACKNOWLEDGEMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the and that they make the greatest possible contribution to national security and economy. It is the policy of the bureau to publish the facts developed by each exploratory protect as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metallurgical Branch, P., G. Knickerbocker, chief, analyzes samples and performs beneficiation tests. Both these branches are under the supervision of Dr. R. S. Dean, assistant director. Special acknowledgment is due Professor G. H. Pett, of the Wisconsin Institute of Technology at Platteville, Wis., Jack Tracy, manager of the Mifflin Mining Co., and J. M VanMatre, representative of the Defense Property, for their assistance in the work. Acknowledgment is also due to A. F. Agnew and A. V. Heyl, geologists of the Federal Geological Survey, for furnishing geologic interpretations and lithologic studies of the drill-hole sections. All drilling was done under the immediate supervision of Francis C. Lincoln and M. Howard Berliner, project engineers, Edward P. Barrett, district engineer, Minneapolis, and E. D. Gardner, regional engineer, of the Bureau of Mines."

Sep 1, 1946

By H. K. Kutter

The pressure pulse generated by an underwater spark \vas investigated in relation to its potential use for rock fragmentation. The study established (1) the relation between the peak discharge current and the peak wave pressure; (2) the relationships among the peak wave pressure, the discharge voltage, and the spark gap width; (3) the type and pulse duration of the generated wave; (4) the percentage of energy transmitted in the spark as a function of spark gap width and discharge voltage; and (5) the percentage of energy converted into the pressure wave as a function of gap width and discharge voltage. Spark-generated fractures were studied in two-and three-dimensional rock and plastic specimens. The laboratory results indicated that the pressure pulse generated by an underwater spark is a potential practical tool for rock fragmentation. The paper contains an appendix describing the capacitive pressure gage specially developed for the laboratory tests.

Jan 1, 1969

By Rudolf E. Greuer, Linneas W. Laage, Xinton Chang

Data or input files are used to describe the mine's ventilation system and physical characteristics necessary for ventilation calculations as well as the physical or mechanical disturbance to be modeled and simulated Data files are organized into lines of categories or groups of information Each line contains multiple sets of information or data items Data lines are read by the program, and the data items provide information to the program variables The data file is in American Standard Code for Informa¬tion Interchange (ASCII) format, sometimes called a DOS text format Creation or modification of a data file is accomplished with text editor software Most word pro¬cessors are also capable of making the required ASCII type files A sample data file and its associated output are included in appendix B. When selecting software for editing the data files, the user should be aware that the software will also be used for viewing the output of the simulation The output file can be quite large (several megabytes), if a lengthy simulation is performed The output can be sent to a printer for a hardcopy fisting, however, the user should also be aware that most printers currently used with PC's print at rates of 100 to 300 characters per second and large output files may take several hours to print Viewing the output with a text editor can save much time and paper DATA FILE MANAGEMENT The data files describing the event and mine to be simulated can reside either on a floppy disk or in a directory on the hard disk drive When the program starts, the user is prompted for the data file location and name The user response is in the form of a standard DOS path and file name For example, if the data file is on a floppy disk located in drive B and the disk has a directory MYMINE with the data file MYDATA DAT in that directory, then, at the prompt

Jan 1, 1990

By Jack C. White

As part of an investigation of the production of alumina by the nitric acid leaching of kaolinitic clay, the Bureau of Mines designed, built, and tested a fluidized-bed system for the calcination of aluminum nitrate nonahydrate to alumina, while recovering nitric acid. The calciner consisted of an 8-in-square by 36-in-tall vessel containing 18 in of fluidized solids. Molten aluminum nitrate, sprayed directly into the fluidized solids, formed sandy, granular alumina by growth of successive layers on fluidized particles. Solids were fluidized in a dense bed at temperatures of 250° to 500° C with steam, air, or mixtures thereof. Decomposition of nitrate ranged from 4 to 10 pet during single-pass steam or air fluidization, respectively. Alumina dust losses and low throughput are significant unsolved problem areas.

Jan 1, 1982

By John L. Edwards, Anthony T. Iannacchione

There has been a persistent need to forecast roof falls so that miner’s exposure to hazardous underground environments can be minimized. Several monitoring techniques have been developed and are used today with varying levels of acceptance in the mining industry. This paper examines the potential for monitoring microseismic emissions activity as a means of forecasting roof falls. The use of this activity to forecast roof falls has drawn only limited attention, resulting in a lack of published field performance data. This deficiency is being partially addressed by analyzing data obtained during longwall mining at Moonee Colliery in 1998. The Moonee data base contains a wealth of information concerning roof fall forecast parameters and the seismic alarm criteria used to develop these forecasts. Four seismic alarm criteria were developed and used by Moonee with varying degrees of success. Roof falls were forecasted 73% of the time with average forecast times of 54 minutes. Ninety percent of the predicted roof falls had a warning time, i.e., the time between warning and roof fall event, of greater than 1 minute. The fraction of forecasted roof falls decayed logarithmically as a function of warning time, until only 20% of events were predicted more than 100 minutes prior to roof falls. False alarms occurred in 50% of the warnings. Many of the false alarms were quickly followed by a cessation in mining which could have temporarily halted the on-going failure process. If mining had continued immediately after the false alarms, a roof fall may have occurred soon after. The microseismic activity collected from Moonee Colliery demonstrates that techniques to forecast roof rock instabilities in underground mines are possible.

By F. D. DeVaney

In the course of the investigation by the U. S. Bureau of Mines and the Missouri School of Mines and Metallurgy at the Mississippi Valley Experiment Station at Rolla, Mo., on the beneficiation of the low-grade manganese ores of the country, some samples from the Cuyuna District, Linn., have been examined. The work was done under the direction of W. H. Coghill, supervising engineer of the Mississippi Valley Experiment Station. Joseph and Kinney in writing about the relative importance of Minnesota deposits of low-grade ore compared to the total reserves say: "***It has been estimated that 26 to 35 million tons of ore contain 5 to 35 per cent of manganese, and the total domestic tonnage is from 75 to 48 million tons. The mean of these values is 30.5 million and 42 million tons, so it is seen that about 75 per cent of the reserves are in Minnesota." The manganese-bearing ores of the Cuyuna district maybe roughly grouped into two classes. The most abundant ore is of the low-silica, low-manganese, and high-phosphorus type called brown are. The other type is the so-called black ore, which is characterized by a higher manganese and silica content and by a lowe phosphorus analysis than the brown ore. As a general rule the brown ore carries less than 10 per cent of manganese while the black ore contains about 15 per cent and sometimes as high as 22 per cent of manganese.

Jan 1, 1930

By H. Kenworthy

A zinc-pyrite ore from the Gray deposit in Jo Daviess County, Ill., was successfully concentrated on a laboratory scale. Initially, drill cuttings were submitted for separation of zinc and iron concentrates. Subsequent to mine development, a large sample of coarse ore was submitted to ascertain its amenability to sink-float treatment to produce a low-grade zinc-iron concentrate and discard a clean tailing. The samples of ore were submitted to the Rolla Metallurgical Branch by the Mining Division of the Federal-Bureau-of Mines. They were obtained during the recent war as a part of the extensive government program to increase metal production through exploration for new mineral deposits and investigation of old mineralized areas. The first sample consisted of about 3,000 pounds of drill cuttings collected, during the Bureau?s churn and diamond- drilling program. The second sample was taken at a later date, after Tri-State Zinc, Inc., had opened the deposit and commenced milling the ore. This sample consisted of a ?ton-of mill feed crushed through 2 inches and collected over a period of 3 days.

Jan 1, 1949

By Carl Belser

This report on tungsten in Ouray, San Juan, and San Miguel Counties, Colo., is one of a series describing results of studies on the tungsten potentialities in Region III, Bureau of Mines. The San Juan tungsten deposits occur in an area of 250 square miles, centering near the common corner of Ouray, San Juan, and San Miguel Counties (fig. 1). Field work supporting these studies was done in May 1954. Bureau of Mines reports prepared from investigations made during World War II and under the Defense Production Act of 1950 were reviewed.

Jan 1, 1956

By S. J. Page, R. A. Jankowski, J. A. Organiscak

The U.S. Bureau of Mines investigated the relationship of bituminous coal seam parameters and the amount of airborne respirable dust generated at longwalls. Dust and coal samples were obtained from 20 longwalls operating in geographically representative coalfields throughout the United States. Statistical analyses of coal seam parameters and airborne respirable dust measurements indicate a likely causal relationship between seam type and respirable dust. Low-ash, high-volatile coal seams were associated with higher airborne respirable dust levels. A negative linear correlation (significant at the 95-pct confidence level) was observed between the seam's ash content and airborne respirable dust, explaining up to 18 pct (R2 = 0.18) of headgate dust level variation and up to 15 pct of tailgate dust level variation. Volatile matter was found to have a positive linear correlation with tailgate dust level, explaining 16 pct of the variation. Further data examination indicates that these relationships with dust are most likely nonlinear, because of improved R2 values over the linear correlations. However, a notable portion of longwall dust production is influenced by other operational parameters, so additional research under more controlled conditions is needed to determine the seam's causative functions.

Jan 1, 1992

By Forrest T. Moyer

INJURY experience and employment data are presented in this chapter for metal and nonmetal mines, stone quarries, sand and gravel pits, iron blast-furnace slag plants, and metallurgical plants (including ore-dressing and nonferrous reduction plants and refineries) in the United States. Employment and injury experience data for all mineral industries are given in volume II. The 1962 figures are preliminary summations which are subject to revision. They were compiled from all reports from producers received by the Bureau of Mines through April 15, 1963. The data for metal, nonmetal (except well and brine operations), stone, and sand and gravel operations were collected by a mandatory reporting system under the provisions of the act of September 26, 1961, Public Law 87-300 (75 Stat. 649). The act authorized the Secretary of the Interior to study the various aspects of safety in metal and nonmetal mines (excluding coal mines) and report the findings 2 years sub-sequent to the enactment of the law. Data on nonmetal well and brine plants and nonferrous reduction plants and refineries were reported voluntarily by the operators. METAL MINES Preliminary data for the metal mining industry comprise reports on 1,871 mines and pits. The combined fatal and nonfatal injury-frequency rate was 31.95 per million manhours in 1962, a decrease of 8 percent from the similar rate of 34.54 in 1961. Metal operations reported a total of 61 fatal and 3,201 nonfatal injuries.

Jan 1, 1963

By E. Morrice

High-purity lanthanum metal was prepared by electrolysis of La003 in a LaF3-LiF-BaF2 bath at 950° C. The requisite bath temperature for the deposition of molten metal was maintained by supplying the heat as current directly to the electrodes. A current efficiency of about 60 percent was obtained. The lanthanum nodules contained carbon and oxygen as major impurities. The total impurity content was from about 0.1 to 0.2 percent.

Jan 1, 1962

By Robert J. Timko, Charles D. Taylor, Edward D. Thimons, Tom Mal

A test system was developed for measuring airflow in the National Institute for Occupational Safety and Health (NIOSH) ventilation gallery using a three-axis ultrasonic anemometer. The gallery was used to simulate face airflow conditions in underground mines having a blowing curtain. Airflow data collected at multiple sampling locations between the face and the end of the curtain were used to draw airflow profiles for different curtain setback distances, intake flow quantities and entry widths. In addition, methane was released at the face, measured at the sampling locations, and displayed as methane distribution in the area between the curtain and the face. Entry geometry had a significant effect on airflow patterns, and the flow patterns affected the distribution of methane in the entry. Flow measured at and parallel to the face was a good predictor of methane dilution and removal within two feet of the face.