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By Robert V. Spencer

"This report describes an examination and preliminary exploration of the Magnet Cove Rutile Co. property in Hot Spring County, Ark. The company in 1944 was producing titania for use in-the welding-rod and metallurgical industries but later ceased operations. The deposit appeared to contain potential reserves of rutile ore, and the Bureau of lanes in 1945 conducted an examination designed (1) to obtain samples for ore-dressing tests and (2) to gather information regarding the grade, character, and size of the deposit. This report presents the data obtained by geologic mapping, geophysical surveying, churn drilling, and core drilling. Beneficiation tests are being made at the Bureau of Mines Rolla, No. station, on the samples taken and will be discussed in a later report.The Magnet Cove operation had been called to the attention of the Bureau of Mines, and in view of the potential reserve of titanium-bearing material, it was decided to obtain samples for ore-dressing tests. Churn drilling was selected as a means of obtaining representative samples, and geologic mapping and geophysical surveying were done to throw more light on the nature of the deposit. Subsequently, a few holes were core-drilled.The property contains the NE1/4, W1/2 fractional NW1/4 and 82 acres of the N part of SE of sec. 18, and -29 acres of the SW1/4 NW1/4 sec. 17, all in T. 3 S., R. 17 W., Hot Spring County, Ark. The mine and mill are about 1 mile by graveled road northeast of U. S. Highway 270, a paved road connecting Malvern, 10 miles south and Hot Springs, 12 miles west. The area is served by two railroads, the Missouri Pacific, which passes through Malvern and Hot Springs and the Chicago, Rock Island & Pacific,,has a line connecting Malvern and Hot Springs an passes about 2 miles south of the property. A natural-gas pipe line and an electric power line reach the property."

Sep 1, 1946

By G. R. Fitterer

In the manufacture of steel by any process the refining period involves the partial elimination of the metalloids carbon, manganese, phosphorus, and silicon, by virtue of their reactions with ferrous oxide. At the end of this refining stage the metal consists chiefly of iron in which small amounts of these materials are dissolved. Unless some deoxidizer is added to the steel at this time, the reaction between carbon and ferrous oxide will continue with such force that it is impossible to form sound steal in the ingot molds. Instead, the product will exhibit a marked porosity due to the formation and trapping of carbon monoxide-the product of the reaction mentioned. However, if deoxidizers are added, steel may be obtained which is dense and free from gas bubbles. At the same time the deoxidation products will remain in the steal as impurities. For example, silicon additions form Si02 or combinations of Si02 and FeO. Additions of manganese form deoxidation products consisting of various proportions of MnO and FeO. It is also quite obvious that simultaneous additions of manganese and silicon will form oxide combinations either in the binary system MnO-SiO2 or in the ternary system FeO-MnO-SiO2. Work at the Pittsburgh Experiment Station of the United States Bureau of Mines, in cooperation with the Carnegie Institute of Technology and the Metallurgical Advisory Board, involved the study of such deoxidizing reactions and their products. In this connection considerable information is necessary concerning FeO, MeO, Si02, and Al 203, and their various combinations. Some of the most needed data are the melting points of all of these materials. At the outset of this work ordinary methods of melting point determinations were found to be inadequate for various reasons, and the procedure finally selected involved the use of the micropyrometer with occasional corroboration by quenching methods, The reasons for this selection, together with a description of the apparatus, are given in the following pages.

Jan 1, 1932

By John W. Finch

The Secretary of the Interior acting through the Bureau of Mines and the Geological Survey is authorized by the Strategic Materials (Public No. 117 - 76th Cong., Chapter 190 1st Sess.) to make investigation concerning essential minerals of which the quantities or grades obtainable from known domestic sources are inadequate. The Bureau of Mines, in carrying out its part of this program, may investigate deposits of such minerals in whatever manner may be necessary, in order to determine (1) the extent and quality of the are, (2) the most suitable method of mining and beneficiating it, and (3) the cost at which it may be produced. The essential objective in doing these things is to determine where and how supplies of minerals and metals of which domestic production is usually inadequate might be obtained in a national emergency, even though at higher cost than usual.

Jan 1, 1939

By R. L. Brown

This report, the seventeenth in an annual series, summarizes Bureau of Mines research and technologic work on coal and related investigations for July 1, 1951, to July 1, 1952. It 1s based largely on publications issued during the fiscal year, although 10 some instances data are presented that have not been published previously. Footnote references are given to the publications so that further details on the work may be obtained. Bureau of Mines research on the mining, preparation, and utilization of coal is directed toward developing and encouraging safer and more efficient mining practices and preparing and utilizing coals to the best advantage.

Jan 1, 1953

By Martin Hertzberg

The Bureau of Mines 8-liter flammability system was used to study the effectiveness of a variety of powdered inhibitors in preventing the propagation of explosions of coal dust or methane in air. Over 35 different chemical additives were evaluated against Pittsburgh seam pulverized coal. The least effective inhibitors were the carbonates, which required mass additions in the range of two to three parts inhibitor to one part of coal dust in order to prevent propagation. The most effective inhibitors were the derivatives of ammonium phosphate, which were effective quenching agents at additions of only one part inhibitor to four parts of coal dust. Alkali halide powders were of intermediate effectiveness. These laboratory-scale results are in good agreement with full-scale mine experiments in all cases where detailed comparisons have been made. Data were also obtained for the effectiveness of several of the same powdered inhibitors against methane-air explosions. Their relative order of effectiveness and the concentration ranges required for quenching the gas explosion are comparable to those measured for coal dust explosions. Data are also presented for the effectiveness of N2 and CF3Br addition. Some preliminary data are also presented for powder addition to methane burner flames. Those data are compared with other burner data and evaluated in terms of their relevance to explosion tests.

Jan 1, 1982

By R. H. Sprute

This report describes Bureau of Mines laboratory test results in electro-kinetic dewatering and consolidation of metal-mine mill tailings from five mines in the Coeur d'Alene, Idaho, district. Classified (coarse) tailings, slimes, and unclassified material were separately tested. Tailings were placed in 0.3 ft3 plexiglass models, and dc potential was applied until dewatering ceased. Time-oriented measurements of water removal, changes in resistivity, and power consumption were recorded during the dewatering process. Moisture content and density of the dewatered material at test end indicated the method to be generally effective for all materials examined, but best results were achieved with well-mixed unclassified tailings.

Jan 1, 1974

By Wilbert J. Huff

The organization of the Explosives Division has been outlined in two preceding publications.3/ The activities of the various units for the fiscal year 1939 are described hereafter: I. INFLAMMABILITY OF GASES AND VAPORS DETERMINATION OF EXPLOSION HAZARDS OF COMBUSTIBLE GASES AND VAPORS IN MINES AND INDUSTRIES (a) Determination of Limits of Inflammability of Gases and Vapors The following hitherto unpublished limits of inflammability were determined during the past fiscal year.

Jan 1, 1939

By Wm. F. Netzeband

"The mode of ore occurrence and the methods and costs of mining at one of the zinc-lead mines in the Tri-State zinc and lead district, Oklahoma, are presented in this paper for the information of mine operators in other districts.No. 2 mine property was acquired by lease in 1918 after some 30 holes had been drilled and a shaft had been sunk to the 305-foot level by the first lessees. After acquisition of the lease, the present operating company drilled a rich ore body on the 260-foot level and in 1920 started sinking two shafts. Production was begun late in 1921, and the mine has been operated more or less continuously to the present time.The mill has a capacity of 400 tons in 10 hours, the usual length of the mill shift in the district.The geology of Mine No. 2 is very similar to that of Mine No. 13 except that the Cherokee shale is thicker, ranging from 80 to 160 feet, and all the formations are correspondingly deeper, the Short Creek oolite horizon here being at a depth of about 300 feet. The oolite has not been found on this property, but the lime comes in at about the level at which the oolite should appear.The ore deposits of Mine No. 2 occur in the brecciated and bowlder ground above the Short Creek oolite. The main or 260-foot level is about 40 feet above the oolite horizon, and the lower or 300-foot level is immediately above it.The ore deposition is controlled by a zone of shearing and fracturing, and the mineable areas are divided into two distinct runs which have a northwest trend with a lean or practically barren area dividing them. This characteristic has controlled the mining to a large extent, for it enables the mine superintendent to locate the large pillars in lean ore and leave only small pillars in the richer ore. Figure 1 shows the outlines of the ore body and the pillars.The ore on the main level occurs disseminated throughout the jasperoid breccia as patches or lenses in the jasperoid, or cementing massive bowlders of jasperoid breccia and chert. The ore of the lower level is more of the bowlder type than that on the main level and occurs chiefly cementing the bowlders but also with some disseminated ore in the jasperoid breccia.The gangue minerals are jasperoid breccia, chert, and dolomite. Calcite is found in minor quantities. Sphalerite is the principal ore mineral; galena is found only in minor quantities around the edges of the ore body. When galena is encountered in this ore body, the limit of the ore can be expected.The exploration and estimation of ore reserves at Mine No. 2 are similar in many respects to the methods used at Mine No. 1.4After the mine was opened up and the general character of the ore deposit had been determined, drilling operations were concentrated along the trend of the shear zone. Later drilling has proved what appears to be a parallel shear zone or an offset of the zone now being mined."

May 1, 1929

By Ernest J. Conway

Seventy-four human factors research and development projects were identified for possible Bureau funding. The projects were based on (1) literature surveys, (2) reviews of accident statistics and reports, (3) interviews with equipment manufacturers, MSHA, and Bureau personnel, and (4) site visits to 26 mines. The projects are divided into the following categories: those related to (1) mobile equipment, (2) maintenance shops and areas, (3) plants and mills, (4) organizational factors, (5) safety programs/data, and (6) training. The projects were rated by industry and MSHA people in terms of benefit to the industry. Projects were placed into three categories of priority. The highest priority contained 25 projects with 26 in Category 2, and 23 projects in the lowest category.

Jan 1, 1982

By Daniel L. Ng

This Bureau of Mines report describes the results of scanning electron microscopic (SEM) studies of the combustion residues of carbonaceous dust particles resulting from explosions and thermal ignitions in laboratory and full-scale mine tests. The dusts studied varied widely in rank and volatility: Pittsburgh seam bituminous coal (35% volatility), Pocahontas seam bituminous coal (16% volatility), anthracite (7% volatility), graphite, and diamond. The most systematic explosion studies were performed in an 8-L chamber with narrow size distributions of Pittsburgh coal dust with surface mean diameters of 2, 22, and 84 pm. Experiments were conducted mainly in air, with some data obtained in 50% 02. Observations of the bituminous coal explosion residues showed particles with rounded edges, particles with blowholes, and some cenospheres. The lower volatility dust residues showed fewer changes from the original, unburned dust. In addition to the experimental studies, results of SEM observations of residues from a mine explosion disaster are reported. Comparison of such residues with those from the laboratory and experimental mine explosions can help investigators determine the extent of dust participation in the disaster and in identifying the possible ignition sources.

Jan 1, 1983

By G. F. Skala

Additional testing of two prototype instruments for the discrete detec­tion of submicrometer particles in metal and nonmetal underground mines is described. The detectors are designed to utilize properties of submicrometer particles to distinguish between those produced by fires from mine ambient particles primarily resulting from diesel engine exhaust. One instrument is based on the ability to pyrolyze fire produced parti­cles, but not diesel exhaust particles. An alarm is produced when the ratio of pyrolyzed to unpyrolyzed particles exceeds a preset value. The other detector utilizes a continuous flow ion chamber preceded by a denuder to remove charged particles. Discrimination against diesel produced submicrometer particles results because the diesel particles are naturally more highly charged than fire produced particles. In-mine testing was conducted over a period of several months. Both in­struments exhibited an ability to discriminate against diesel exhaust. However, problems with the recording equipment, and with the instruments themselves, due to large ambient dust particles, prevented enough data from being obtained to choose between the two methods. Recommendations to correct the problems are made.

Jan 1, 1982

By Joseph E. Chilton, Robert J. Timko, Charles D. Taylor

No regular monitoring of methane is required in areas of gassy coal mines outby the mining face. Methane ignitions that have occurred in mine outby areas indicate the need to provide better protection to workers. Handheld methane monitors are now used by some miners to make periodic measurements of methane at the working face. The IYONI II gas detector which is incorporated into a miner’s cap lamp and worn on a miner’s helmet can continuously provide an alarm signal whenever methane levels exceed a set level. Tests were conducted to evaluate the performance characteristics of this methane detector by measuring response times with methane gas supplied through a calibration fixture or adaptor. Other response time tests were performed with the detector in an environmental test box. Performance was also evaluated in a full scale test gallery where face methane emission and underground ventilation were simulated. Procedures for calibration by response time measurement of the IYONI II detector have been developed. In limited testing, the IYONI II detector was found to reliably detect the presence of 1 percent by volume methane.

By S. J. Rodgers

This report presents the results of in-mine studies to determine the severity of dust sources in conventional mining operations. Three underground coal mines were surveyed using gravimetric samplers and GCA RAM-1 continuous dust monitors. Two additional mines were surveyed using only GCA RAM-1 monitors. Data on dust control methods were acquired during the survey, also. The results indicated that cutting/drilling and loading out were the dustiest operations during a conventional mining cycle. Roof bolting, shot firing and product transport were less severe dust sources.

Jan 1, 1983

By Harold M. Smith

This report presents a complete qualitative picture of knowledge of the composition of petroleum as of April 1965. The material is presented in detail on two imaginative maps--one, the Hydrocarbon Hemisphere, depicts the hydrocarbons that have been identified in petroleum; the other, the Heterogeneous Hemisphere, shows the sulfur, nitrogen, and oxygen compounds that have been found. All compounds are placed on the maps according to boiling point. The accompanying text illustrates by structural formulas the several types of hydrocarbon and nonhydrocarbon compounds identified, presents some quantitative data, and points out the possible geochemical significance of a number of the compounds. The possibilities of the Petroleum World of the future are discussed as a function of needed research,

Jan 1, 1966

By George D. Drechsler

The purpose of this review is to provide an analysis of the supply and demand for coal in Europe in 1955-56 and estimates of future growth in European requirements as a medium for appraisal of the effects and benefits to the economy of the United States. This review stems from observations and evaluations made in contacts with Government and industry representatives of the principal countries of Europe and is based on detailed data selected from the established flow of unclassified economic and statistical material originating in overseas areas for use and deposit in the Bureau of Mines, Foreign Solid Fuels Section. This material includes current reports and analyses prepared by the United States Foreign Service, official reports of individual countries, foreign industry and trade publications, and the committees of the several European organizations engaged in continuing review and study of problems relating to fuels and energy. The review is presented in four sections: 1. Discussion of the more important factors relating to the present and future fuels and energy position of Western Europe.

Jan 1, 1957

By S. R. Wilson

[The Anniversary-Bucky pegmatite is one of the largest, dikes in the Quartz Creek district, 21 miles east of Gunnison, Colo. The major dike consists of quartz-albite pear pagmatite and graphic granite with many quartz masses as individual cores occurring within the dike. A mining operation on one of the largest core areas has exposed several mineralogic cones directly associate with the core. These zones, including the large- units of the dike, are quartz pegmatitc, quartz-perthite pegmatite, perthite pegmatite, muscovite-feldspar -quartz pegmatite, quartz-albite pegmatite, and perthite-quartz (graphic granite) pegmatite. Muscovite and beryl are found in the muscovite-feldspar-quartz zone and are the only two products that have been marketed. Other potential products are perthite, graphic granite, and possibly small quantities of columbite-tantalite, monazite, and related radioactive minerals. The Bureau of Mines drilled two diamond-drill holes during April 1950 to investigate the largest and cost promising core area. This, report describes the results of this drilling.]

Jan 1, 1953

This report describes the work performed by Mine Research Company in developing a prototype mobile roof shield during 1971-1972 for the U. S. Bureau of Mines, along with background information leading to the design decisions adopted for the project. In addition, the report evaluates the choice of design and analysis and the results of the project in terms of future possibilities of mobile roof support systems. The report begins with the discussion of the problems of designing, building, and using mechanical and hydraulic roof support in coal mines. It then gives a historical summary of past work with discussions of the design choices made for previous roof support systems.

Jan 1, 1973

By David C. Oyler

Methane-drainage holes must be completely filled by grout before mining to prevent the emission of large quantities of gas during mine-through, which would constitute an explosion hazard. In November 1980, seven horizontal holes at the multipurpose borehole, a small-diameter shaft drilled as a Bureau of Mines coalbed methane-drainage installation on the property of the Federal No. 2 Mine, Monongalia County, WV, were plugged using a sodium silicate gel grout. This report de- scribes the grout mix and the use of the grout at the multipurpose borehole, and discusses the results observed upon mine-through of the holes in early 1981. Cost data for the sodium silicate grout are also presented.

Jan 1, 1984

By J. A. Zimrner, R. J. Tirnko

The roles of main mine fans in underground mines are to induce airflow and continuously re- move hazardous gases and dust. While most larger mines use multiple fans to accomplish these tasks, many smaller mines employ only a single fan. This paper concentrates on those mines having only one fan to provide ventilation needs. If this fan should cease to function, it is likely that methane concentrations will in- crease in some areas of the mine. As a safety precaution, Federal Regulations require that personnel must be- gin evacuating the mine within fifteen minutes after fan stoppage. Powered haulage can be used to transport workers to the mine portal as long as travel is through areas where hazardous levels of methane are not expected. To determine where methane will accumulate along haulageways during a fan stoppage, air samples must be taken at specific areas and analyzed for hazardous gases. During this study, procedures were developed for measuring methane levels along the haulegeways that are used to exit a mine following stoppage of the main mine fan. Methane levels were measured in four different mines at selected underground locations during four planned fan stoppages. In these mines the measurements taken only at the specified locations showed that, if workers had used electrically powered haulage to exit the mine following a fan stoppage, the methane accumulated along haulageways during fan stoppages would not have significantly increased the risk of an ignition.

By Leon W. Dupuy

Marquette's first reported the existence of iron In Missouri in 1673. Recorded production wan begun in 1815, increasing in size and importance until 1888, when the low price of iron resulting from Minnesota's production of high-grade ore caused most of the operators to close down. Missouri's iron production came from three types of ore: (l) Brown ores, including the deposits of primary and secondary limonites in southeast and southwest Missouri, (2) hematites of the filled sinks, including the ores of Central Ozark district, and (3) specular ores in porphyry, including the deposits of the St. Francois Mountains.

Jan 1, 1949