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By E. D. Wilson

A study of factors related to subsidence was specified in a project proposal entitled "Structural Analysis of Block-Caving Operation, San Manuel Copper Mine, Pinal County, Ariz.," approved by the Bureau of Mines early in 1953. This proposal was designed by Charles H. Johnson, then chief of the Base Metals Branch of the Minerals Division, Washington, D. C., assisted by Dr. Leonard Obert, chief of the Applied Physics Branch, Region VIII (now Region V), College Park, Md., and E. D. Gardner, chief mining engineer, Bureau of Mines, Washington, D. C. It read as follows: This project is a study of the mechanics of undercut block caving in a deep ore deposit. The San Manuel is a low-grade disseminated copper deposit containing nearly a half billion tons of ore lying at depths of 500 to 2,000 feet. Development is just starting. Production is to begin in 3 to 4 years (in 1956) at a rate of 30,000 tons of ore a day, or 60,000 tons of copper a year. A Government loan of $90,000,000 /subsequently increased to $94,000,000/ and a long-term Government purchase contract support the capital investment, which will total about $110,000,000.

Jan 1, 1957

By James P. Bennett

The U.S. Bureau of Mines investigated the role of imported natural flake graphites in dolomite-carbon refractories used in steelmaking processes and evaluated carbon fibers as a potential substitute. Varying quantities (1.5-30 pct) of natural flake graphite and carbon fibers were added to test samples. The effect of the additions on modulus of rupture (75°-2,750° F), deformation under load (2,750° F), and air-slag-metal resistance (3,000° F) was studied. Carbon purity of natural flake graphite additions did not influence hot strength, deformation under load, or air-slag-metal resistance. When the quantity of 90-pct-carbon graphite addition varied between o and 30 wt pct, hot strength was highest, deformation under load lowest, and air-slag-metal wear the least at 10 wt pct. As test temperature increased from 500° to 2,750° F, the hot strength difference became less. Carbon fiber additions were limited to 1.5 pct in dolomite-carbon brick. At this level, physical properties were generally comparable to those obtained with natural flake graphite, but were below values obtained with 10-pet-f1ake graphite additions. Carbon fibers are not considered a satisfactory substitute for natural flake graphite.

Jan 1, 1989

By Lawrence W. Scott

The performance of RETIMET metal foam as a flame arrester on explosion-proof enclosures was investigated by the U.S. Bureau of Mines both in laboratory tests and at the U.S. Mine Safety and Health Administration's (MSHA's) Approval and Certification Center, Triadelphia, WV. The objective of this research was to develop a permissible pressure vent for use on lightweight, vented, explosion-proof enclosures. In laboratory tests, four grades of RETIMET, a stainless steel foam material, were evaluated: (1) 45 NC-7, (2) 45 NC-13, (3) 80 NC-7, and (4) 80 NC-13. Explosive gas mixtures were prepared by a dynamic flow system. Ignition was by a low-voltage arc. Each grade of RETIMET metal foam successfully arrested the flame front in all methane-air tests. To evaluate RETIMET metal foam on large, commercial size enclosures,a multi compartmented enclosure was designed and tested in MSHA's explosion gallery in Triadelphia, WV. Extensive explosion testing revealed that a minimum vent-area-to-enclosure-volume ratio of 11.33 in2/ft3 is required to keep internal pressure rises below 3 psig. The RETIMET metal foam functioned satisfactorily in all tests as evidenced by the absence of external ignitions.

Jan 1, 2010

By J. B. Gayle

Because economic and geographic factors have focused particular attention on the use of anthrafines in blends containing Lower Kittanning coal as the low-volatile component, samples from this particular bed were selected for experimentation whenever practical. Carbonizing tests were carried out in accordance with standard procedures, using the Tuscaloosa and sole-heated ovens. Most of the results are in general agreement with those reported by previous investigators. Specific findings are as follows: (1) The effectiveness of anthrafines in reducing coal expansion is such that even highly expanding, low-volatile coals can be carbonized safely with suitable additions of anthrafines and careful control of charge density. (2) Increases in coke size, resistance to shatter, and apparent specific gravity appear to be characteristic for additions up to approximately 15 percent to a fixed base blend. When anthracite of minus-48-mesh size was used and the proportion of low-volatile coal simultaneously increased, these indexes increased only slightly or remained substantially constant. (3) No increase in breeze formation was noted for additions in amounts up to 15 percent. (4) Abradability of coke was increased by additions of anthracite of No. 5 Buckwheat size, but it either decreased or remained sub¬stantially constant when the inert was ground to pass a 48-mesh screen.

Jan 1, 1956

By F. P. Haver

The Bureau of Mines is developing a leach-electrolysis procedure to produce Special High Grade (SHG) zinc from sulfide concentrate without the generation of sulfur oxide gases. Chlorine-oxygen leaching of the concentrate yields zinc chloride (ZnCI2) which, after purification, is electrolyzed in a fused-salt cell to obtain molten zinc metal and chlorine gas for recycle. This paper describes a laboratory-scale investigation made to develop a procedure for electrowinning zinc metal from ZnC12. Zinc chloride by itself is not a suitable electrolyte because it fumes badly above its melting point and is a poor conductor of electricity. Other salts therefore must be added to prevent fuming and improve the conductivity. Optimum results were obtained with a KC1-LiCl-ZnCl2 bath at 500° C, using a current density of 5 amp/in2 and an electrode spacing of 0.5 inch. Under these conditions, SHG zinc was produced at a current efficiency of 94.3 pct and an energy requirement of 1.16 kwhr/lb. Fused-salt electrowinning eliminates the need to handle and melt cathodes and increases the production of metal per unit cell volume through the use of higher current densities than are possible with aqueous electrolysis.

Jan 1, 1976

By D. E. Shanks

The Bureau of Mines surveyed a variety of inorganic ion-exchange materials to determine their suitability for removing valuable accessory elements and troublesome contaminants from metallurgical process and waste streams. Most of the materials, which included molecular sieves, heteropolyacid salts, and hydrous metal oxides, did not give adequate separations, did not have the necessary stability in strong acids or bases, or were not in a physical form suitable for ion-exchange use. Many of the suitable inorganic materials, especially the hydrous oxides, were capable of cation exchange with high capacity only in basic conditions, which caused hydrolysis of most of the cations tested. Multivalent anions, such as arsenate and phosphate, were easily removed from acidic solutions by hydrous oxides. Hydrous zirconia was the best material for this purpose. Multivalent anions were not easily des orbed because of compound formation; therefore, conventional ion-exchange techniques could not be employed. As an alternative approach, hydrous ferric hydroxide was used as a filter material to remove arsenate and phosphate from acid solutions. One gram of arsenic was removed from solution for each 20 g of ferric hydroxide. Ferric hydroxide is preferable to hydrous zirconia for use as a filter material because of low cost.

Jan 1, 1983

By M. M. Tilman

As part of ongoing research to improve mine safety, the Bureau of Mines conducted research on the corrosion of friction rock stabilizer steels in five Missouri lead and iron mine waters. Electrochemical corrosion tests, including evaluation of pitting tendency, were performed on two types of high-strength, low-alloy (HSLA) steels and galvanized steel in four Missouri lead mine waters and one Missouri iron mine water. The tests were conducted at in-mine water temperatures in both air-saturated and deaerated waters. Static, weight-loss corrosion tests were also conducted on HSLA steel specimens in the five Missouri mine waters for 2,900-h duration at average in-mine water temperatures and air-dissolved oxygen contents of 6 to 7 ppm. Corrosion rates determined by the weight-loss tests were roughly comparable with rates determined electrochemically in deaerated waters containing 0.3 to 0.5 ppm dissolved oxygen content. Passivation of specimen (nongalvanized) surfaces in air-saturated waters resulted in very low electrochemically deter- mined corrosion rates. Pitting-tendency was generally higher for both HSLA steels in air-saturated waters than in deaerated waters. Galvanized steel generally exhibited higher tendency to pitting in the deaerated waters than in the aerated mine waters.

Jan 1, 1985

By Fred C. Turin, Sean Gallagher, Kim M. Cornelius, William J. Wiehagen

An important part of initiating a site-wide ergonomics evaluation process is prioritizing jobs to be analyzed. While injury data is important, other factors such as worker discomfort and physical exertion requirements, should be considered. This paper describes the use of four sources of data (injury records, the Nordic Standardized Musculoskeletal Questionnaire, supervisor interviews, and management concerns) to prioritize jobs for ergonomic analysis. The approach described integrates the four sources using a decision matrix to prioritize jobs for ergonomics analysis.

By R. P. Beyer

Low-temperature heat capacities and standard enthalpy of formation of copper difluoride (CuF2) were determined by the Bureau of Mines. The low-temperature heat capacities were determined from 11 to 302 K by adiabatic calorimetry. The enthalpy of formation was determined by HC1 solution calorimetry. The standard values of entropy (S°) and enthalpy of formation (?Hf°) at 298.15 K are l8.65±0.03 cal/deg mole and -129.02±0.29 kcal/mole, respectively.

Jan 1, 1978

By Noel N. Moebs

The Bureau of Mines measured surface subsidence above four small coal mine room-and-pillar sections in southwestern Pennsylvania, to obtain preliminary information on the magnitude and character of selected parameters, such as angle of draw and maximum subsidence, which are essential to the development of subsidence prediction methods. Data varied widely at the four sites; this is attributed to local geologic and mining conditions. Surface deformation at each site was of a magnitude normally associated with severe structural damage.

Jan 1, 1982

By M. Copeland

Phase relations of gadolinium alloyed, up to 40 weight-percent (wt pct), with AISI 304-type stainless steel were established. Body-and face-centered cubic iron-rich solid solution phases and several intermetallic gadolinium-containing compounds of variable composition that approximated the formulas Fe9Gd, Ni7Gd2, Ni3Gd, Fe2Gd, NiGd, and NiGd3 were identified. The intermetallic phases Fe9Gd and Ni7Gd2 were noted to melt at about 1,080° C at about 0 to 2 wt pct gadolinium. The melting temperature of Fe9Gd increased with increas-ing gadolinium content to a plateau at about 1,230°C and 30 wt pct gadolinium, and the melting point of Ni7Gd2 decreased to a plateau at 900° C and 30 wt pct gadolinium where Ni3Gd, NiGd, and Fe2Gd coexist. Body-centered cubic iron solid solution was stable from 1 to 2 wt pct gadolinium to higher contents, 30 wt pct gadolinium or possibly more, and face-centered cubic iron up to 12 wt pct gadolinium below 1,200° C. The stability of these phases above 1,200° C was not resolved except for the mel points. A limited number of fabrication variables as well as mechanical and corrosion properties of alloys containing up to 5 wt pct gadolinium were studied. Equilibrating and forming operations were best conducted at about 940° to 1,080° C. Some variability in the yield and tensile strengths of alloys was noted; however, there was a continual decrease in ductility and impact resistance with increasing gadolinium contents. The resistance of gadolinium alloys to corrosion in water at 354° C was about the same as stainless steel.

Jan 1, 1965

By E. G. Noble

The effects of HBr concentration and temperature on the solubility and hydration state of AlBr3,' CoBr2, PbBr2, MnBr2, KBr, and NaBr were investigated by the Bureau of Mines. Saturated aqueous solutions of the AI, Pb, K, and Na bromides were sparged with HBr gas at 20°, 40°, and 60° C, and saturated solutions of Co and Mn bromides were sparged at 20° C. Increased HBr concentration caused decreased salt solubility because of the common ion effect for all the investigated bromides except PbBr2. Aqueous solubilities at 20° C were, in percent, 51.7 for AlBr3, 53.2 for CoBr2, 1.1 for PbBr2, 59.6 for MnBr2' 39.5 for KBr, and 47.4 for NaBr. At 60° C, the solubilities were, in percent, 53.3 for AlBr3, 2.2 for PbBr2' 46.0 for KBr, and 53.8 for NaBr. Solubilities in solutions sparged to HBr saturation at 20° C were, in percent, 0.5 for AlBr3, 42.0 for CoBr2, 32.2 for PbBr2, 21.0 for MnBr2, 0.6 for KBr, and 0.3 for NaBr. At 60° C, the solubilities at HBr saturation were, in percent, 1.8 for AlBr3, 41.4 for PbBr2, 1.3 for KBr, and 0.4 for NaBr. CoBr2 precipitated out to a minimum solubility of 27.2 pct at 28.7-pct-HBr concentration. Further increases in HBr concentration increased CoBr2 solubility because of the formation of bromide complexes. PbBr2 in-creased in solubility as HBr concentration increased.

Jan 1, 1988

1. Alford, N.G. quantity, of timber used in soft-coal mines and how much will be needed for the future. Gives a table of estimated increase in mine timber consumption in the future. A.I.M.E. Separate. 1336-C 1924. 2 Clark, B.M. The forest and the mine. Rept. Conference of Wood-Using Industries, Harrisburg, Pennsylvania. Apr. 13-14, 1921, pp. 58-62. Describes experience of a Pennsylvania mining company in depletion of timber supply and conservation methods adopted.

Jan 1, 1925

"Correlatina Lung Crackle Usina Holographic lnterf erometryAli Afshari, MS, West Virginia University, 1989The Effect or Surfactants on Suppression of Non-Wettable ParticlesAli Alaboyun, MS, Mineral Engineering, The Pennsylvania State University, 1989Geochemical Characterization of Kerogem, ShaJes, and Coal .Refme ~ted with Allegheny Fonnationof Cases of Northern West VirginiaDick Andre, MS, West Virginia University, 1987Particle Concentrations in a Hazelton Inhalation ChamberShahram Bavani, MS, West Virginia University, 1985Use and Potential of Luer Holographic Interferometry and Subsidence Model Study of an Underground.Room and Pillar MineRichard Begley, MS, West Virginia University, 1984Development of a Mechanistic Model for Prediction of Subsidence in a Longwall MineRichard Begley, PhD, West Virginia University, 1990.Redesign of Micro-Orifice Unifonn Deposit ImpactorSteve Behm, MS, University of Minnesota, 1991A Fracture Mechanics Study of Crack Propagation Mechanism in Coal: The Mechanics of Fine FragmentFonnationZ. T. Bieniawski and R. Karl Zipf, Jr., Mining Engineering Department, The Pennsylvania State University,University Park, PA. Final Report, October 1, 1988A Mathematical Model for the Prediction of Ambient Dust Concentrations in Mine AtmospheresR. Bhaskar, MS, Mining Engineering and Operations Research, The Pennsylvania State University, 1984Spatial and Temporal Behavior of Dust in Mines-Theoretical and Experimental StudiesR. Bhaskar, PhD, Mining Engineering, The Pennsylvania State University, 1987Experimental Studies of Dispersion and Deposition of Fane Particles in a Wind Tunnel and Mine AirwayKlaus Bode, MS, Mining Engineering, The Pennsylvania State University, 1991Perf'onnance of the High Yield Technology PM - 100 - Particle 11ux MonitorRobert Caldow, MS, University of Minnesota, 1987Development of Improved Methods for Monitoring and Control of Diesel Particulate in an Underground CoalMineD. H. Carlson, B. C. Cornilsen, P. L. Loyselk, X. Shan and J. H. Johnson, Michigan Technological University,Houghton, Ml. Final Report, June 15, 1991"

Mar 1, 1992

By William R. Barton

Sampling to determine development potential of beryllium deposits was conducted at 31 New England localities. A total of 54 additional areas where the geochemical environment appeared favorable were sampled to determine if economically interesting percentages of beryllia (BeO) might occur. Newry Hill-Plumbago Mountain, Maine, Iron Mountain, N.H., and Long Island, Maine, were investigated in some detail to determine the size and grade of deposits. The mineralized pegmatites at Newry Hill-Phunbago Mountain are extensive but very low grade; at Iron Mountain the ore bodies are very rich but of small volume; at Long Island beryl occurs with molybdenite, wolframite, and scheelite, but the tonnage of ore was not determined.

Jan 1, 1968

By Amanda Azman, Richard Hi Danie/son

Ultimately, the most important product of a hearing conservation program is the prevention of hearing loss, not the amount of hearing protection that has been purchased or whether employees are attending their annual training sessions. Audiometric testing directly reveals whether hearing losses are actually occurring in a plant. With audiometric data, we can assess overall program effectiveness, alert workers of impending hearing loss, and reveal potential employer liabilities for compensable hearing loss. Without the ability to efficiently analyze audiometric data or produce effective reports, our programs become fruitless and unproductive. Consequently, ifaudiometric data are such vital end-products, then effective audiometric technologies serve as the prime architect and generator of these fundamental data. These technologies, consisting ofaudiometers, associated peripheral hardware, and database/reporting software, deserve our consideration.

To determine the effectiveness of multiple types of fire sensors for early and reliable mine fire detection. Background The National Institute for Occupational Safety and Health (NIOSH) has evaluated the effectiveness of multiple types of fire sensors for early mine fire detection and nuisance signal discrimination. Reliable early fire detection in underground mine can be hindered by false fire alarms produced by carbon monoxide (CO) and smoke particulate emissions from diesel equipment, welding, and metal-burning activities. Another false fire alarm source is the cross-interference of hydrogen (H2) produced by battery-charging operations with a CO sensor's chemical cell. Workers can learn to ignore repetitious "false" alarms associated with these emissions. This jeopardizes their safety in the event of a mine fire.

Sep 1, 2002

Determine the site specific flow behavior of leachants and groundwater during development, production, and restoration phases of an in situ leaching operation. Approach A computer program has been developed which simulates the hydrologic activity associated with in situ mining. Various user options enable modeling of many of the site specific geologic conditions and well field specifications that affect the hydrology of solution mining. How It Works In situ hydrology is modeled, using a closed-form solution to the three-dimensional, partial differential equation that describes changes in hydraulic head as a result of pumping from leachant Injection and recovery wells. Model capabilities include arbitrary well patterns and pumping schedules, partially penetrating well screens, directionally anisotropic permeability and natural groundwater flow, in either

Jan 1, 1981

By Bill M. Stewart, Philip W. Patton, Curtis C. Clark

Handling materials in underground mines continues to be a major safety problem. To help reduce materials-handling injuries, researchers at the Spokane Research Laboratory of the National Institute for Occupational Safety and Health are investigating those materials-handling tasks in underground mines that appear to generate a high number of injuries. Data from the Mine Safety and Health Administration for the years 1989-1999 were studied to find out if there were any trends in materials-handling accidents and if so, to determine what tasks were involved and the sources of injuries. Several underground coal and metal mines we revisited to document innovative materials-handling technologies. Considerations for safety training and mechanization needs for continued reduction in materials-handling injuries are described.

By H. E. Powell

A series of alkyl-dithiocarbamic acid amine salts was prepared and tested as collector for slimed lead minerals contained in the waste material from a commercial lead ore concentrator. The reagents, members of a homologous series differing only in the number of alkyl radicals in their structure, were prepared by reacting stoichiometric amounts of primary amines and carbon disulfide in a cold alcohol solution. Subsequent purification was by recrystallization from absolute ethyl alcohol solution. Evaluation was through froth flotation of a mill tailing containing 0.2 percent lead. Results show that maximum recovery (38 percent) was obtained with the reagent containing 8 alkyl radicals, but that maximum rougher concentrate grade (4.8 percent) was obtained with the reagents of intermediate number of radicals.

Jan 1, 1962