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By M. M. Tilman

The Bureau of Mines investigated the precipitation strengthening of lead¬-base alloys containing 0.5 through 4 weight-percent combined Cd plus Sb. The Cd and Sb were alloyed in a 1-to-1 atomic ratio which maintained compositions along the quasi-binary section Pb-CdSb. Tensile properties, creep rates, and stress-rupture values were obtained on alloys in the aged condition. The highest tensile strength was observed in an alloy of Pb-3 CdSb, After aging for 6 months at 90°±3° F, this alloy had a mean tensile strength of 8,950 psi with 15-percent elongation. An aged alloy of Pb-1 CdSb exhibited a steady state creep rate of 1.2 X 10-3 percent per day at a stress of 500 psi and a temperature of 90°±3° F. Times to rupture at stresses up to 4,000 psi and at a temperature of 90°±3° F were obtained for some compositions.

Jan 1, 1970

To produce industrial-grade titanium castings by processes that are nonpolluting and lower cost than the currently used rammed-graphite process. Approach Foundry-grade zircon and olivine sands, bonded by waterglass or bentonite, are used to make shell or rammed molds which require relatively low-drying temperatures and do not generate noxious fumes during drying or casting. Procedures Three separate processes have been developed which meet the stated pollution and cost goals. These are: 1. Waterglass-bonded rammed zircon or olivine sand molds are dried at 480°F, zirconia washed, redried, and used in an inductoslag or skull-casting furnace. 2. Waterglass-bonded zircon or olivine sand shell molds are formed at 560°F, cured at 620°F, zirconia washed, dried at 480°F. and used in an inductoslag furnace. 3. Rammed zircon and olivine sand molds are bonded with western bentonite, zirconia washed, dried at 980°F, and used in an inductoslag or skull-casting furnace.

Jan 1, 1981

Develop a machine which can accurately simulate both the breathing and metabolic functions of a human being. The advantages of such a machine over a human being for testing of respiratory protective devices lie in its ability to quantify metabolic input, its repeatability, and the lack of a need to deal with the vagaries of human subjects. Breathing simulation has been widely achieved throughout the world but metabolic simulation has not. Approach Utilize the latest computer technology and place the complex portion of the system in software, leaving the mechanical portion as simple as possible. How It Works The concept for the automated breathing and metabolic simulator (ABMS) was developed through a research contract with the Pennsylvania State University. The ABMS utilizes a continuous removal/replacement concept to simulate metabolic functions, with breathing and metabolic functions being controlled by a computer. The mechanical portion of the machine is simple; the complexity of the system lies in its computer software which is not subject to maintenance problems.

Jan 1, 1987

Use water-jet-assisted cut-ting technology to reduce the exposure of mi ne workers' to respirable dust. Approach Install water-jet-assist on mining machines and evaluate its impact on respirable dust. How It Works Water-jet-assisted cutting involves a mechanical cutting bit working in combination with a moderate pressure (generally up to 10,000 psi) water jet directed just in front of, or through, the bit tip. One of its advantages is reduced dust generation because the jet wets the face of the material being cut more efficiently than a conventional low-pressure water spray, thus capturing much of the dust before it ever becomes airborne. It also removes loose cuttings ahead of the bit before they are pulverized by the bit into respirable dust. Total water consumption is about the same as for conventional low pressure dust control water spray systems. However, there is some increase in power consumption because of the energy needed to provide the high pressure water.

Jan 1, 1987

Reduce potential for steering errors during tramming of articulated vehicles, particularly when the operator is seated to the rear of the machine pivot point and is tramming in reverse. Approach Position-sensing and feedback cylinders were applied to the steering cylinders of two S&S cleanup tractors to cause the steering-control lever to match the orientation of the vehicle sections. The vehicles were tested in two working mines. How It Works A position-sensing cylinder (see Figure 1, Item A) is attached to one of the steering cylinders in the cleanup tractor steering system. As the steering cylinder piston rod is actuated by movement of the control lever, hydraulic oil flows from the position sensing cylinder to the feedbck-cylinder (B), causing the feedback-cylinder piston and rod to move. The outside end of the rod repositions the the steering-control lever until its angular position corresponds to the orientation of the vehicle sections.

Jan 1, 1978

Provide a method for obtaining in situ measurements of coal cutting forces which are needed for mining machine design. Approach A portable in-seam testing device is carried to the face of an underground coal mine heading to measure the cut-ting force encountered by a continuous miner pick directly at its maximum depth of cut. How It Works The tester frame is attached directly to the coal surface with four one inch diameter threaded studs resin-bolted into 1-1/4 inch diameter holes which are drilled 30 inches deep. Spherical nuts and washers compensate for misalignment between the bolts bearing plate, and traverse beams. Spacers can be placed over the studs to assure that the traverse beams remain in the same plane. Cutting forces are applied by a hydraulic cylinder that moves the pick of the tester through a twin-chain arrangement which gives a 20-inch cutting stroke with

Jan 1, 1982

Determine safe practices for surface mine blasting near pressurized gas, oil, and water transmission pipelines. Background Surface mine blasters regularly have to address the issue of how blasting affects transmission pipelines that run near and sometimes through their permit areas. Regulatory approaches to blasting have ranged from no regulation at all to strict limits intended to prevent cosmetic cracks in plaster interior walls of homes, but they have not directly addressed the impact of blasting on nearby pipelines. Concerned with both productivity and safety, the mining industry and its regulators have requested guidance on safe practices for mining near pipelines. The Pipeline Research Group of the American Gas Association has sponsored studies of the effects of small close-in blasts because of vibration concerns related to the installation of new pipes into existing pipeline right-of-ways. By contrast, the recent study in which the U.S. Bureau of Mines (USBM) took part is the first addressing large-scale mining blasts.

Jan 1, 1995

Continuously monitor air-borne radon daughters that are a hazard to underground miners. Approach A beta detector continuously counts beta activity collected on a filter paper to allow calculation of exposure in working level units. How It Works At each Site a constant flow pump draws mine air through a fiberglass filter located in front of a beta detector (pancake type Geiger Mueller tube), Radioactive particles (products of the radon 222 gas emanating from the mine walls) collect on the filter and decay, releasing alpha and beta particles as well as gamma rays. A portion of the beta particles penetrate the Geiger tube window and create electrical pulses in the tube. These pulses are then amplified and sent by a coaxial type or shielded electrical cable to a central monitor located some distance from a working level detector. At the central monitor incoming Signals are amplified and fed into two channels, (See the block

Jan 1, 1979

Provide means for rapidly re-establishing ventilation control in metal mines after blasting, for emergency applications, and for routine temporary use. Approach Two quickly-installed, parachute-like stoppings have been developed and tested by the Bureau's Pittsburgh Mining and Safety Research Center. How the Parachute Stopping Works The parachute stopping can be fastened to an existing anchor point, opened, and effectively block the air flow, in less than two minutes. Because the parachute stopping tends to be self-scaling, its performance is generally better than that of conventional fabric stopping. However, the periphery of the parachute stopping must be longer than the periphery of the mine opening, Figure 1 shows the parachute stopping deployed in a mine entry. To reduce leakage during routine use, the cloth at the periphery of the parachute stopping can be adjusted and then anchored at several points as necessary. This extra adjustment can also be done after the initial installation during mine rescue or mine recovery.

Jan 1, 1977

By Ann G. Kim

The Bureau of Mines investigated factors that influence the formation of methane and other hydrocarbon gases in coal, which is an integral part of the coalification process. Coalification begins with a biogenetic stage in which plant debris decomposes and peat is formed; methane and CO2 are the predominant gases produced during this stage. During the diagenetic stage of coalification hydrogen and the hydrocarbon gases methane, ethane, ethylene, propane, propylene, butene, iso-and normal butane, and pentane are formed by dissociation of the organic material. Methane may also be produced by a secondary reaction of hydrogen with unsaturates or by the reduction of CO2. The gas contained in coalbeds is a mixture of methane, C2 through C5 alkanes, CO2, O2, N2, H2, and He; its heating value is equivalent to that of natural gas. The gas content of coal depends on many variables, but an empirical relationship between adsorptive capacity, rank, and depth has been observed.

Jan 1, 1978

By J. E. Dooley

Reference mass spectra and analytical correlations for 20 alkylcycloalkyl sulfides and two dicycloalkyl sulfides are presented 'to provide information that will facilitate the identification of sulfur compounds occurring in natural or synthetic mixtures. Reference spectra indicate relative intensities in addition to parent and base peak sensitivities. Analytical correlations establish the ionic species that reflect major fragmentation paths for the com-pounds studied. Specifically, the correlations show that base peaks are formed by several different processes: (1) Cleavage of the bond a to the ring, (2) fragmentation of the alkyl chain, and (3) fragmentation of the ring plus fragment contribution from the alkyl chain. Useful correlations for deter-mining alkyl chain length involve the CnH2+3S+ and CnH2n+1 + ions. CnH2n-2+ and CnH2n-1 S+ ions reveal the number of carbon atoms in the cyclic ring. Other important ionic species are also discussed.

Jan 1, 1970

By R. P. Vinson, Abdurrahman Cetinbas, Joseph Cervik, M. G. Zabetakis

The periphery of longwall panels in the Pocahontas No. 3 coalbed is characterized by a zone of reduced permeability that inhibits the natural drainage of methane. A residual gas pressure of 105 psig was measured after 1 year in an isolated block of coal measuring 340 by 1,100 feet. The buildup of gas pressure within such large blocks causes methane problems during plowing operations. However, natural drainage holes drilled during development have been found to reduce the gas content of the coal in this coalbed by over 90 percent. The effect of water infusion on dust during plowing operations was investigated using existing methane drainage holes. These holes were cleaned of debris and a pipe was grouted into the hole for water infusion of the panel. Both total and respirable dust levels were reduced by 40 to 79 percent. Water infusion of the panel proved more effective than did the use of a plow-mounted spray sys tem.

Jan 1, 1974

By D. R. Douslin

This report describes an inclined-piston pressure gage that operates from a zero-pressure datum level. The gage is adaptable to accurate vapor-pressure measurements in the low and intermediate pressure range, 0.01 to 40 mm (mercury). Residual friction in the oil-lubricated piston-cylinder combination is eliminated by a unique oscillatory method that is free of end thrust on the piston and allows the full sensitivity of the gage to be realized. The axial component of the weight-to-area ratio of the piston is determined by measuring the angle of inclination with a goniometer that can be read to 1 sec. Accuracy of the gage proper is estimated to range from 0.001 to 0.012 mm from lower to upper pressure limits. Its highest practical sensitivity is about 0.0005 mm. As a test, the vapor pressures of ice and water were measured in the range -30° to +20° C.

Jan 1, 1963

By W. M. Myers

[The principle of the application of electrolytes for deflocculation of fine materials in order that impurities may settle out, and the subsequent flocculation of the suspended particles by a different reagent, is well known and has been applied successfully to clays. Flocculation is also applied with success to ore slimes. Thus certain electrolytes, particularly alkalies added to a suspension of colloidal particles cause deflocculation so that, suspension may be-maintained indefinitely. The addition of bother electrolytes particularly acids, on the contrary produce's flocculation and the articles produce's are rapidly precipitated from suspension leaving a clear liquid above: the precipitated mass. Salts of trivalent elements such as aluminum act similarly. Due to its cheapness the double sulphate of aluminum and potassium, ordinary alum, has been used extensively for treating clays. These properties of electrolytes. and. their utilization in the commercial: preparation of clays have been described in publications of the Bureau of Mines.2]

Jan 1, 1927

By Howard C. Turnage, Dana T. Updyke

An evaluation was made of one of several improved underground communication systems sponsored by the U.S. Bureau of Mines. The system evaluated was installed in a typical metal/non-metal room and pillar mine and utilized UHF repeaters connected to a unique distributed antenna and passive reflector system which provided mine-wide communications. A microprocessor controlled data collection system was assembled and installed for the evaluation. Data consisting principally of times and durations of messages and identities of the originating transceivers was collected between February and August of 1982 (6 mos.). Analysis of the data shows that the principal benefits are reduction in time required for unscheduled maintenance and repair, enhancement of safety, and better coordination of production activities. A cost benefit analysis shows a net benefit over cost, although it is also concluded that the capacity of the system is greater than can be justified by current activity in the mine.

Jan 2, 1983

By Hal H. Engel

This publication was written in response to numerous requests for information about the Federal Bureau of Mines' "Demonstrated Lecture on Flame Propagation and Permissible and Explosion-Proof Electrical Equipment." The requests came principally from: (1) Persons wanting to know more about the demonstration before requesting it for groups they represented; (2) persons wishing advance information to help publicize a meeting where the demonstration was to be given; and (3) members of audiences desiring something to help them remember the salient points, facts, and figures presented during the lecture and demonstration. The purpose of the demonstration that accompanies the lecture is to show: (1) Variations in flame speed and pressure at various percentages of flammable gas within the flammable range; (2) effect of flame speed on the "pressure piling" within the area confining the mixture; and (3) the application of flame speed and pressure piling to the combustion of surrounding gas and to the design and maintenance of electrical equipment used in hazardous locations.

Jan 1, 1960

By D. E. Hirsch

The Bureau of Mines, as a part of American Petroleum Institute Research Project 60, Characterization of the Heavy Ends of Petroleum, has made extensive use of gel permeation chromatography (GPC). Data developed in this study were used to develop several correlations that greatly expanded the usefulness of GPC and the data have been used as an aid in the interpretation of mass spectra (MS). GPC retention volume data on pure compounds were used with molecular structure to develop correlations that can be used to accurately predict retention volumes, molecular volumes, densities, chain lengths, and ring numbers of many components of petroleum without resorting to further laboratory experimentation. Conversely, the correlation can be used to select or reject some compounds from several possible compounds that are indicated on the basis of MS analysis. The utility of these correlations in compound type characterization is demonstrated by showing their application to 330° to 550° C fractions from a low-sulfur and a high-sulfur crude oil.

Jan 1, 1974

By Michael G. Pojar

This Bureau of Mines report estimates the population of the principal types of machinery in use by the coal mining industry during 1982 in surface and underground mines. Estimates were arrived at using 1976 coal equipment population estimates as baseline data with modifications made for new mine development, expansion, and closure occurring during 1976-82. Estimates were broken down into 3 regions which included all 26 coal-producing States. Modifications made to the baseline data were computed using (1) actual equipment information when available, plus (2) equipment information hypothesized from representative generic mine models, which were predicated on mine size and mine method. Roughly half of the equipment fleet at new or expanding coal operations was known; the remainder was hypothesized. The mine models used to generate equipment information are included in this report, along with the hypothesized equipment use data. The equations and various factors used to determine the equipment adjustments for mine closings, new mine openings, and small coal mine operations are also identified.

Jan 1, 1986

By W. H. Oppelt

Converting small-particle lignite to a stable, storable fuel of relatively high heating value was investigated. The fuel was prepared by thermal pretreatment of the lignite in an 8-inch i. d. rotary-drum retort, then the pretreated material was pelletized in an experimental 15-inch-i. d. rotary-drum pelletizer. Pelletizing tests were made with both starch and bituminous binders. During the first phase of the project, the quantity, composition, and heating value of products from the thermal processing of Kincaid lignite from Burke County, N. Dak., in an B-inch i. d. rotary-drum retort were investigated at a series of temperatures from 250° to 950° F. to establish optimum conditions for preparing feed material for pelletizing. To determine the response to thermal treatment of different lignites, 5 other lignites from Divide, McLean, Mercer, and Stark Counties, N. Dak., and 1 lignite from Saskatchewan, Canada, were processed at 700° F.

Jan 1, 1958

By William O. Vanderburg

Tis paper describing the mining practices at the Cold Springs mine of the Wolf Tongue Lining Co. at Nederland, Colo., is one of a series of similar papers prepared by the Fureau of kines on mining practices, methods, and costs at various mines in the United States. The writer acknowledges the assistance of William Leach and William T. Todd, manager and mine superintendent of the Wolf Tongue Mining Co., respectively, in the preparation of this paper.

Dec 1, 1932