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The variety and sources of sampling errors have been studied since the late 1800s, but the pioneering work of Pierre Gy in the 1950s provided insights into sampling as an error generating process. Total sampling variance is a measure of the total sampling error, but disaggregating the variance into its component parts is problematical. Ten sources of error and error generating processes have been identified, some of which can be eliminated through rigorous application of the principle of correct sampling. Others can only be minimized but never eliminated. Three principal questions relating to the appropriate mass of a sample, the fragment size of the sample and the size of the associated error are addressed. These questions relate principally to the Fundamental Error (FE), the only error that can be estimated before the sampling event. Aspects of constitutional and distributional heterogeneity are examined, as are the essential components of Gy?s formula including the shape factor (?), the granulometric factor (g), the mineralogical composition factor (c), and the liberation factor, l. Applications of Gy?s equation to the problems of sampling in the minerals industry are explained using real-life examples. The approach to sampling taken by Pierre Gy provides an excellent inferential relationship between the mass of material to be sampled, the size of the fragments being sampled, and the relative variance of the sampling error. It also provides solutions for three of the main problems associated with the Theory of Sampling.

Jan 1, 2007

By F. Botha, J. S. Adams, W. T. Ruhmer

The report describes the Amuran project in the Welkom area, which is being conducted by six members of the Anglo American Group. The project comprises three plants for the flotation of pyrite, a twin-stream uranium plant in which 'high-grade' slimes and pyrite can be leached separately, a pyriteburning sulphuric acid plant, and a plant for the recovery of gold from calcines. Details of these plants including capital costs and estimated production are given. Mention is made of the adsorption of gold onto activated charcoal and wet high-intensity magnetic separation as possible suitable processes for these residues.

Jan 1, 1978

By A. P. Van Wyk, G. Pirnaar

The effect of vanadium on the susceptibilities of chromium and chromium-nickel steels to reversible temper embritlement was evaluated. The steels investigated were approximately equivalent to steels of as 970 Grade 708A42 and as 970 Grade 817M40, the major difference being that molybdenum had been replaced by vanadium in various concentrations. It was found that the vanadium had a detrimental effect and, in al the concentrations tested, enhanced the susceptibility to reversible temper embritlement of both the chromium and the chromium-nickel steel. The detrimental role played by vanadium in reversible temper embritlement is explained by a consideration of the effect of vanadium carbide, as well as of free vanadium, in solid solution in ferrite.

Jan 1, 1987

By B. Kenealy

A typical deep shaft is President Steyn No. 2 in the Free State, where 9 tonnes of ore are hoisted at about 15 metres per second from 2378 metres below surface. The skips and attachments each weigh 7 tonnes and they are connected by 43 tonnes of rope, so that to hoist the 9 tonnes of payload, a total of 66 tonnes is accelerated from stand still to 55 km/h for each cycle, using an average of 3185 kilowatts of power in the process. The cycle time for the hoisting is 3.22 minutes. The peak power consumption is 6954 kilowatts, which determines the size of the motor used. Is this the right approach? Are larger skips moving at higher speeds the answer? Is there another way?

Jan 1, 1996

By R. D. C. Shone

Consideration is given to the technical and economic feasibility of freeze desalination as a technique for the simultaneous provision of ice to cool deep mines and for the desalination of mine water. Freeze desalination has not been developed fully or commercially. For sea-water applications, it may not offer significant advantages over other methods of desalination but, for the unique mining application, a single dual purpose plant that produces desalinated ice could offer significant cost savings over combinations of separate desalinators and ice-makers. The current status 01 freeze desalination is reviewed, and the important aspects relating to mines are discussed. Some freezing processes that could be suitably modified are described. The possible use of conventional ice-making machines for desalinating mine water is also discussed.

Jan 1, 1987

By E. Wolmarans

Dowding, Reynard and Associates Mineral Projects (DRAMP) was approached by the ARM/Lion Ore JV during July 2006 to conduct a feasibility study and control budget estimate for a new greenfield project for their NKOMATI Nickel mine 45 km east of Machadadorp. The scope included the evaluation and review of previous studies as well as a techno-economic trade-off on four possible comminution circuits ranging from conventional crushing and ball milling to fully autogenous milling. The following document encapsulates the thought process, decisions and the references used in selecting the final comminution route for the new 375 ktpm MMZ concentrator. Apart from the pilot test work performed, design simulations from a number of sources, performance results from a recently commissioned 100 ktpm MMZ concentrator, together with an understanding of the geology and mineralogy of the orebody and possible variations in the characteristics of the orebody over the life of mine were assessed. The results from all the above-mentioned work indicated that it would be possible to treat the MMZ ore at the desired throughputs to the desired grind sizes in a fully autogenous grinding (ABC-type) circuit. Autogenous milling is generally considered to be one of the higher risk milling circuits. This is mainly due to the fact that the ore, which is utilized as the grinding media, could be variable in terms of hardness and mineralogy/geology. Nevertheless, it is a very popular route as the cost benefits, more specifically the operating cost, are normally very attractive. This is especially the case when large low grade orebodies are evaluated. In North/South America, autogenous and semi-autogenous grinding circuits have been successfully employed during the past 20 years on large scale low grade operations. Taking all the above factors into account, the DRA/Nkomati project team recommended an autogenous circuit with the option to add steel to both the primary and secondary mills (if required) for the new operation in order to create the opportunity for significant operating cost savings. One has to bear in mind that all the new design simulations and decisions are based on previous work and potential unknown variations within the orebody will never be fully understood until the pit is operational for some time.

Jan 1, 2009

By S. K. Gilman, P. S. Marcos

There are basic areas of importance within a concentrator or mineral separation plant, which require focus to ensure acceptable recoveries, throughputs remain at an acceptable level and product grades meet specification. Professional and para-professionals within the mineral sands industry are in demand due to the booming resource sector. Added to this, new mineral sands operations are being commissioned straining the industry further. These factors have increased staff turnover and introduced many new people to the industry. It is essential these new entrants are armed with basic plant troubleshooting skills relevant to the minerals sands industry to minimize production lost through poor recoveries. Mineral sands processing does not involve highly technical or sophisticated unit processes. However, success is often slow to arise due to a lack of detailed understanding, as well as managing multiple interrelated unit processes within a plant. Fundamental background physical conditions (such as equipment loading and water quality) must be met for unit processes to be efficient. Technical management of these process plants should always include observation of these background conditions for they often provide the answer to underperformance. Examples are presented with an indication of the possible effects on recovery and product grade.

Jan 1, 2007

Currently the most widely used formula in pillar design is the power formula, which implicitly assumes a volume effect. This assumption is critically examined, and it is proposed .that a limiting strength value, the critical rock mass strength, be used for pillar design instead. A methodology is provided to determine this value. It is suggested that the effects of geometry on pillar strength are well described by a linear function and the power formula, for w/h ratios less than or equal to about 5. This approach together with the use of the critical rock mass strength, removes the volume effect. Various factors that affect pillar strength are examined. The concept of explicitly determining the stability of each component in the pillar system is briefly discussed. It is proposed that pillar design be expanded to a pillar system design procedure that incorporates the interaction of the pillar, roof and floor strata, and the loading system.

Jan 1, 1998

By I T. Tshabalala

In typical conventional narrow vein stoping operations, the use of temporary support components to offer some support to workers, whilst the permanent and generally more elaborate support system gets installed or constructed, still results in injuries to people. The authors wishes to explore the probability and practicality of making use of new generation support products to make the support operations safer as well as enhance productivity in the stope face. This paper will examine the use of Autorock Drills as a means to drill roof support holes and install appropriate support components into these holes, as well as the application of ?Thin Spray Liners?, commonly called TSL?s as an additional means of creating a safer operating environment. The installation of netting as a means of roof protection and other support aspects such as cemented roof-bolts will also be explored. These proposed items are envisaged to improve the safety of our people and reduce production down time and increase production and productivity.

Jan 1, 2008

By R. T. Muller

Contribution to the above paper by R. T. Muller (Visitor) Demands are being made and pressure is being brought to bear on employers in South Africa to narrow or eliminate the wage gap between their White and Black employees. Few thinking people will dispute the fact that a constant improvement in the wages of Black personnel is essential, but this cannot be done merely by a redistribution of income in South Africa.

Jan 7, 1974

By T. O. Hagan

A system for the monitoring of micrcoseismic events. which is designed for use in feasibility studies of rock-burst prediction, has been operating at Western Deep levels Limited since 1977. Analyses have revealed that the presence and Orientation of geological discontinuities ahead of the mine face can be predicted from the data produced by this system.

Jan 1, 1981

By E H. O Meyer, K van Dyk

Fine powders normally exhibit, to a more or lesser extent, some ability to participate in dust explosions. Zinc dust as used in the extractive metallurgy of zinc, is not known to be a reactive powder in the industry. No evidence could be found in the literature where zinc dust was involved in an explosion or explosive type event. On 3 May 2002 an explosive type incident occurred at Zincor in Springs, South Africa, which led to a fatal accident. Given the history of relative benign behaviour of zinc powders under conditions conducive to dust explosions, it was decided to share the information of this incident with industry in an effort to prevent similar incidents. Therefore, the purpose of this paper is to describe the incident that occurred at Zincor, discuss the major findings, report on corrective actions, as well as publish the results of subsequent tests that were performed to determine the conditions under which zinc powder exhibits explosive characteristics.

Jan 1, 2005

By B. W. Wallace

Permitted explosives in South Africa are those explosives approved by the relevant State authority for use in fiery coal mines. The main tests that an explosive must pass for this approval are the gallery tests derived from the Buxton (U.K.) classification. These tests are described briefly. In addition, the safety of permitted explosives is affected by their ability to deflagrate, and to produce a naked flame after blasting, rather than to detonate fully. Tests done on this phenomenon are discussed. A further potential hazard of explosives is after-blast fume. The testing and behaviour of several permitted explosives in this respect are covered, both in the laboratory and in the field. Performance testing of permitted explosives, specifically the double-pipe, underwater, and ballistic mortar tests, and their relationship to field use, are considered in some detail. The application of traditional and new tests to permitted explosives leads to guidelines for the safe and efficient formulation and use of these products.

Jan 1, 1986

By F. L. D. Cloete

he above article by E. Barnea, which appeared in the January 1978 issue of the Journal (vol. 78, no. 6, pp. 143-145), calls for comment in view of the author's claims for the novelty of his proof. He states in his article that its main purpose is to give a mathematically acceptable proof by induction of the 'recently proposed' equation

Jan 1, 1978

By F. L. D. Cloete, A. K. Haines, T. D. Sampson, T. H. Tunley, W. A. M. te Riele

The recovery of zinc from pickle liquors by ion exchange A. K. HAINES. Ph.D. (Visitor) T. H. TUNLEY. B.Sc;.(Chem.Eng.)(Visitor), W. A. M. TE RIELE. pr, Eng.. Ph. D. (Visitor), F. L. D. CLOETE. M.Sc. (Chem..Eng.)(Visitor), and T. P. SAMPSON. Pr. Eng.. BSc, (Chem.Eng,). B. Econ. (Visitor) Picklers and galvanizers in and around Johannesburg are encountering an ever-increasing problem in disposing of spent liquors from their hydrochloric acid pickling baths. Particularly troublesome is the zinc-contaminated liquor that is produced as a result of the clean-up of rejects from the galvanizing operation. Because of the volatility of zinc chloride. this liquor presents difficulties when processed in a conventional pyrohydrolysis acid-recovery unit. The paper describes the Metsep Process. developed by the National Institute for Metallurgy and Woodall-Duckham S.A. (Pty) Ltd. which involves the use of continuous ion exchange for the separation of the zinc from the pickle liquor. and the use of liquid-liquid extraction for the conversion of zinc chloride eluate to salable zinc sulphate. A description of laboratory and pilot-plant tests is given. and the approach used in the design of a full-scale continuous- ionexchange plant is outlined.

Jan 11, 1973

By D. W. Nel

Nanofiltration (NF) has attracted much attention over the past few years due to the reduced energy consumption compared to reverse osmosis (RO) and better separation performance compared to ultrafiltration (UF). Although research has been done in the area of NF of nickel ions, sodium ions, and acid separation, not much attention has been given to the separation of high nickel concen¬trations from sulphuric acid streams. The use of NF for the separation of nickel and acid from a spent nickel electrolyte is an innovative process alternative for future industrial application within a base metal refinery. In this study, the separation performance of a composite polyamide NF membrane on a spent nickel electrolyte was investigated by varying the sodium sulphate concentration in the feed (50-150 g/l), the trans-membrane pressure (35-55 bar), and cross-flow velocity (1.5-3.5 m/s), and measuring quantities such as total permeate flux, acid rejection, nickel rejection, and sodium rejection. The nickel and acid concentration in the feed were kept constant with variations between 40-60 g/l and 25-40 g/l respectively, while the temperature of the experiments was kept constant at 50°C. The membrane was found to be very selective for nickel ions, with the rejection of nickel ions varying between 54.4% and 98.2%. The rejection of acid ions varied between -5.9% and 21.8%. The rejection of sodium ions varied between 16.6% and 72.4% at a cross-flow velocity of 2.5 m/s and sodium sulphate concentration of 50 g/l in the feed solution. An increase in trans-membrane pressure increased the rejection of nickel, sodium, and acid ions, while an increase in sodium sulphate concentration decreased the rejection of nickel and acid ions. The total permeate flux was found to increase with an increase in trans-membrane pressure and decrease with an increase in sodium sulphate concentration. The cross-flow velocity had an insignificant effect on the total permeate flux and the rejection of nickel, sodium and acid ions.

Jan 1, 2013

By G. Iabichino, M. Cravero, F. Nacci, L. Rinaldi, L. Vigliero

ABSTRACT: The proposed paper is aimed at analysing the failure of a steep cliff slope that, in the past, was exploited for open pit mining operations. A volume of over 400,000m3 of gneissic aplitic rock was involved in the slope failure. An evaluation of possible failure mechanisms is given, based on a structural description of the rock mass, a mechanical characterisation and on computation methods. The block theory and limit equilibrium techniques for sliding and block toppling were applied and a comparison is given with the result obtained by using DEM models. RESUME: Le document proposé vise l’analyse des mécanismes de rupture d’une falaise qui a été intéressée dans le passé par une mine à ciel ouvert. Un volume supérieur à 400.000 m3 de aplite-gneiss a été concerné par la rupture de la falaise. Le document fournit une évaluation des possibles mécanismes de rupture, basée sur une description structurale de l’amas rocheu, une caractérisation mécanique et des méthodes de calcul numérique. L’analyse a été développée à l’aide de la théorie des blocs et de la technique de l’équilibre limite, soit pour le glissement que pour le basculement des blocs, et une comparaison avec le résultat obtenu par application des modèles DEM a été effectuée. ZUSAMMENFASSUNG: Die vorgeschlagene Arbeit zielt darauf ab, den Einsturz einer steilen Felswand zu analysieren, an der in der Vergangenheit eine Mine im Übertageabbau betrieben wurde. Der Einsturz betraf ein Volumen von über 400000 m3 an Gneis und Aplit. In der Arbeit ist eine Einschätzung des möglichen Mechanismus angegeben, der zum Bruch geführt hat, und sie basiert auf einer strukturellen Beschreibung der Felsmasse, einer mechanischen Charakterisierung sowie auf der Anwendung von Berechnungsmethoden. Angewandt wurden die Blocktheorie und die Methode der Gleichgewichtsgrenze für das Abrutschen und Kippen von Blöcken. Darüber hinaus wird ein Vergleich mit den Ergebnissen angestellt, die unter Verwendung von DEM-Modellen erzielt wurden.

Jan 1, 2003

By M. M. Valenta

A number of challenges face platinum concentrator plant operators. These challenges include the increase in operating costs, the increase in smelter cost for the processing of concentrate, the shortage and cost of power, and the tightening of specifications on concentrate quality by the toll-smelting operations. Over the years the focus has moved from extracting the platinum group metals (PGM) from the Merensky Reef to the UG2 reef. This has a number of advantages, including the higher ?basket price? for UG2 concentrate, reduced mining cost per unit volume as a result of the higher density of UG2, and the reduction in overall concentrate tonnage to be smelted. In many cases the Merensky ore has been fully exploited and it makes sense for the focus to shift to the UG2 ore that can be accessed through the Merensky shaft infrastructure. The presence of relatively high levels of chromite in UG2 concentrate is, however, a major disadvantage due to the problems associated with smelting such a concentrate in conventional submerged arc furnaces. In addition to increasing the specification on the minimum PGM grade of concentrates, smelters have had to impose strict specifications on the levels of chromite in the concentrate. The threat of high penalties has forced concentrators to change their modus operandi, often resulting in a significant loss in recovery. The final concentrate grades and PGM recoveries are shown to vary significantly throughout the industry. The reasons for this include varying ore mineralogy and different operating philosophies. This would therefore imply that the opportunity exists to optimize the operations by considering fundamental aspects such as the PGM mineralogy and the application of appropriate technologies. By returning to the fundamentals of flotation and applying the findings of detailed process reviews, it has been possible to increase the concentrate PGM grade, reduce the concentrate chromite grade, and in some cases increase the recovery of PGM to concentrate. This paper presents case studies where this approach has been used to successfully optimize concentrator performance, resulting in lower operating cost and higher PGM production. Keywords Process optimization, platinum concentrator, milling, flotation, grade, recovery

Jan 1, 2011

By B. Steyn

AngloGold Ashanti?s Obuasi Mine, in Ashanti Province, Ghana, operates a plant utilizing bacterial oxidation technology. The mineralization consists predominately of arsenopyrite with gold associated in the sulphides. The plant was commissioned in 1994, at that time was the largest BIOX® plant in the world, and has been operated by AngloGold Ashanti since 2004. The constraints identified in the plantwere the flotation capacity, BIOX® feed size and disruptions to the BIOX® process. This paper focuses on the practical steps that were followed in order to increase the recovery of the plant. The original plant design was based on a head grade of 10 g/t and an overall recovery of 86.5%. In 2007 the plant was operating at an overall recovery of 79.2% at a head grade of 5.6 g/t and this has improved to 80.6% at a head grade of 5.8 g/t during the last quarter of 2008. Additional improvement to 81.5% are expected by the end of April 2009. Improvements that have been implemented include: ?Replacement of the regrind mill ?Installation of additional float capacity ?Installation of a scavenging circuit ?Installation of a complete water treatment plant. In addition we have focused on the effect of the water circuit on the BIOX® process and the steps involved in correcting this problem. The water circuit was originally designed as an open circuit and through environmental considerations the circuit was closed towards the end of 2007. The bacteria in the BIOX® are particularly sensitive to cyanide and cannot tolerate levels above 0.05ppm (free cyanide), this required extensive modifications to the water circuit. The plant improvement project is ongoing and the current scope of work should be complete by the end of April 2009. Further research and development work is being planned, which includes a ?white rot bacteria? that can consume the preg-robbing carbon and oxidize the sulphide in a single pass.

Jan 1, 2009

Results are presented on the elution of gold cyanide and base-metal cyanide complexes from strongand weakbase resins. It is shown that thiocyanate anions, zinc cyanide anions, and thiourea in acid solution are effective eluants of strong-base resins, but that it is generally necessary for electrowinning to be incorporated in the elution cycle if fast rates of elution are to be achieved. Weakbase resins are eluted with sodium hydroxide solution, which is shown to be far simpler and far more effective than the elution of strong-base resins. The effects of parameters such as concentration of the eluant, temperature, and electrowinning efficiency on the rate of elution of the resins are examined.

Jan 1, 1984