Search Documents

By C. MeCulloch

A NOVEL practice in the bituminous coal industry is the accelerated method of burning coal to ash used in the laboratory of the Fidelity washery of the United Electric Coal Companies, Du Quoin, Ill. Development of this method has supplanted the tedious float-and-sink process for plant control at this plant. In normal operation the plant operators have available within thirty minutes the accurate ash percentage of the coal loaded in the railroad cars and can therefore make adjustments to maintain a practically uniform quality of washed coal, regardless of the variations in washery feed.

Jan 1, 1937

By F. Woodcock, A. R. Laplante

A test to characterize the amount of gravity-recoverable gold (GRG) in an ore is described. Typical GRG results are given and possible uses are discussed. The overall database, which includes 68complete tests, is presented. The ore samples treated had an average GRG content of 63% of the total gold in the sample, with a standard deviation of 20% and a range of 3% to 97%. Both the F8(, of gold and the GRG content at a grind of 100% finer than 850 pm correlate well with the overall GRG content (at 80%finer than 75 pm). The primary use of the test is to determine whether gravity recovery should be used and how. Results can also be used to predict gravity recovery, as many of the ores tested are from plants employing gravity recovery. Gravity-circuit simulation can be used to refine recovery estimates or for optimization studies.

Jan 1, 2000

By Patrick R. Taylor

Glass is used for immobilization of radioactive and hazardous wastes due to its durability and ability to accept a variety of waste constituents into its network structure. Alternative high temperature vitrification techniques have the advantage of increased throughput, increased waste loading and being applicable to variable and heterogeneous waste streams. However, the increased processing temperature places further concerns on the increased volatilization of contaminants, and increased corrosion and erosion of me Iter components. A database of melt properties at higher temperatures, such as partitioning, viscosity, density and electrical conductivity, in the temperature range of 1400-20000 K are being developed.

Jan 1, 2000

By Tang Chaoho

Laboratory research on the reducing and matte smelting of Jamesonite concentrate has been carried out. The influence of the process conditions such as the smelting temperature, the amount of pyrite cinder (the agent of fixed sulfur) and the amount of additives on the smelting process have been studied. Under the optimum condition the direct recovery ratios of antimony and lead are 83.26% and 68.50% respectively. The ratio of fixed sulfur is 98.97% but more than 15% lead and 30% silver remained in the ferrous matte. The key problem to be solved of this new process is how economical and effective is the recovery of silver and lead in ferrous matte.

Jan 1, 2003

By Tang Chaoho

Laboratory research on the reducing and matte smelting of Jamesonite concentrate has been carried out. The influence of the process conditions such as the smelting temperature, the amount of pyrite cinder (the agent of fixed sulfur) and the amount of additives on the smelting process have been studied. Under the optimum condition the direct recovery ratios of antimony and lead are 83.26% and 68.50% respectively. The ratio of fixed sulfur is 98.97% but more than 15% lead and 30% silver remained in the ferrous matte. The key problem to be solved of this new process is how economical and effective is the recovery of silver and lead in ferrous matte.

Jan 1, 2003

By M. Moats, J. Young

Short term laboratory cell electrorefining experiments were performed to examine the impact of electrolyte composition, current density and temperature on deposit structure, roughness, and adhesion to 2B mill finished 316L stainless steel. Copper electrodeposits were produced using synthetic electrolytes with thiourea and the continuous addition of glue. Deposit structures were evaluated using X-ray diffractometry. Surface roughness was measured using profilometry and analyzed using scaling analysis. Finally, an internally developed method was used to measure the force required to remove the electrodeposited copper from stainless steel to determine adhesion strength.

Mar 2, 2022

By Andrew Artzer, Michael Moats, Jack Bender

Antimony and bismuth in copper electrorefining electrolytes can cause cathode contamination, leading to the careful control of their concentrations. This study examined the laboratory scale removal of bismuth and antimony from an electrorefining electrolyte using a solvent extraction mini-pilot plant. The ability of a proprietary phosphonic acid ester extractant (REX-2) in a commercial diluent was studied in a simulated commercial setting. Antimony and bismuth were both extracted effectively from the electrolyte (72% Bi and 70% Sb removed) and Bi was effectively stripped (92% Bi recovered) with 400 g/L sulfuric acid. A final strip solution was obtained from the SX circuit containing 0.36 g/L Bi, 0.043 g/L Sb, 1.3 g/L Cu, and 0.18 g/L As. Unfortunately, most of the extracted Sb remained in the organic phase. Following the pilot study, experiments were performed to examine the precipitation of bismuth from the aqueous strip phase and the removal of antimony loaded on to REX-2. INTRODUCTION For many years, antimony and bismuth have been some of the most problematic impurities in copper electrorefining (ER) (Bardwell & Lapee, 1933). Along with surface roughening, high concentrations of Sb and Bi can contaminate the copper cathode and precipitate at the copper grain boundaries. This drastically reduces the drawing ability of the metal (Bender & Emmerich, 2016). For these reasons, it is necessary to control Sb and Bi concentration in the cathode, which is done by controlling their concentration in the electrolyte. Conventionally, Sb and Bi concentrations are controlled by maintaining a proper As/(Sb+Bi) molar ratio in the anode and arsenic concentration in the electrolyte. Antimony and bismuth are removed during electrolyte purification using liberators (electrowinning cells) and/or ion exchange. Liberators treat an electrolyte bleed stream from the ER circuit and electrodeposit increasingly impure copper as the copper concentration of the solution decreases. Traditionally, first stage liberators reduce the copper concentration from ~45 g/L to ~15 g/L and produce saleable copper. Second stage liberators decrease the copper concentration to ~8 g/L (Biswas & Davenport, 1980) which results in contaminated cathode that is returned to anode production (Biswas & Davenport, 1980; Wang, 2004). Further electrolyte purification is not always required but third stage liberators can be used to reduce copper concentration below 2 g/L which results in significant removal of As, Sb and Bi and very impure deposits which are recycled to a smelter or used for As production. However, liberators do not have very high energy efficiency (Acharya, 2014; Ando & Tsuchida, 1997) and below 0.5 g/L copper, highly toxic arsine gas may form (Biswas & Davenport, 1980).

Jan 1, 2019

By K B. Quast, A Schuurmans

Laboratory batch rod and ball milling tests were conducted on samples of Heavy Medium Separator (HMS) sinks from Renison Limited. The effects of mill rotation speed, rod volume and ball size on the resulting product size distribution were investigated. Between 48 and 69 per cent of critical speed, the product sizing distribution curves remained very similar, with a finer grind resulting from increasing the speed of rotation at constant grind time. Increasing the rod loading from ten to 53 per cent by volume caused the product size to become finer and more closely sized with a transition occurring at approximately 29 per cent. This was interpreted as a change of dominant grinding mechanism from abrasion to impact. No preferential grinding of the cassiterite was observed. The effect of increasing ball size at constant charge weight was to preferentially grind the coarser particles and generate more intermediate sized particles, whereas the product from a mixed ball charge gave a distribution similar to that obtained when a charge containing only smaller balls was used.

Jan 1, 1998

By K B. Quast

Changes in feed size distribution can have significant effects in rod mill grinding. The product sizing resulting from wet batch milling of a tin ore showed little influence on fines production after truncating the feed at either the coarse or fine end. The addition of fine material caused a less amount of fines to be produced and a possible increase in grinding at coarse sizes, although this is complicated by the changing feed size distribution. The changes in feed size distribution caused no tendency for preferential grinding of the cassiterite.

Jan 1, 1998

It is possible to closely simulate the product sizing distribution from an industrial rod mill by the correct choice of parameters in laboratory batch milling. For laboratory batch rod milling, changes in per cent critical speed and per cent rod volume cause the product sizing distributions to move in parallel at a constant slope. For ball milling, larger sized media in batch milling grind more coarse material giving a closer simulation to the industrial rod mill product. Changing the feed size distribution by removal of coarse particles or addition of fine particles changes the product sizing distribution, but would not normally be practiced in laboratory testing. These data should be applicable to many instances where laboratory simulation of an industrial product size distribution is required.

Jan 1, 1998

By P G. Hicks

The influence of feed size and pulp density on the specific rate ofbreakage of quartz was investigated. Plots of log fraction of feedremaining within the feed size interval against grinding time allowed the application of the first order grinding model to be examined. Substantial non-linearities were observed for all feed sizes due to environmental and material factors. For feed sizes above 1.3 mm, the specific rate of quartz breakage was higher with rod milling than ball milling, but below this size the reverse was true. Material that remained in the feed size interval after the initial grinding broke more slowly in subsequent grinding than the original feed material. Grinding media and time as well as feed size influenced the effects of pulp density on grinding. More dilute pulps (eg 50 per cent solids density by weight) were favoured for higher rates of breakage in rod milling but for ball milling, the optimum pulp density appeared to be 60 to 70 per cent solids by weight.

Jan 1, 1998

By H. R. Hardy Jr., E. J. Kimble Jr., H. W. Shen

"The primary objective of this research project is to study the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. Secondary objectives include the investigation of the acoustic emission technique as an indirect method for coal dust characterization and remote bit wear monitoring. The results of the project will be useful in developing efficient coal cutting techniques which significantly reduce the harmful coal dust components, and in providing methods for remote monitoring of bit condition and associated coal dust character. This paper will outline recent experiments carried out on coal under uniaxial compression, linear single-bit cutting, and cutting using a laboratory-scale, single-bit shearer. During the experiments acoustic emission and a variety of other mechanical parameters were monitored. · A commercially available artificial intelligence computer package, namely: JCEPAK (Intelligent Classifier Engineering Package), has been utilized to provide a powerful and objective means for AE waveform analysis. This program is able to evaluate a number of features of each AE event and to make objective comparisons between AE signals associated with different loading or cutting parameters. Finally, the paper will discuss the results obtained from a variety of coal breakage tests.INTRODUCTIONStudies to date clearly indicate that the reduction of the severity, and eventual elimination, of Coal Workers' Pneumoconiosis (CWP) depends on gaining fundamental understanding in a number of major areas. These include dust generation and entrainment, transportation, suppression, medical effects of dust and possible treatment. At present a project is underway by the authors to investigate the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. An important aspect of this on-going project is the development of acoustic emission (AE) criteria which will make it possible to carry out remote monitoring of coal cutting operations. Suitable on-line analysis of monitored AE data would allow engineers to evaluate factors such as shearer bit condition and cutting efficiency, and to quantify the particle size and shape distribution of the generated dust. The on-going AE studies are fundamental in form and were undertaken to evaluate the general feasibility of AE monitoring techniques using simplified coal cutting procedures. This paper will outline recent experiments on coal under uniaxial compression, linear single-bit cutting, and cutting using a laboratory-scale, single-bit shearer. Additional information on these studies are presented elsewhere [4]."

Dec 1, 1996

By William A. Hockings

This report describes the results of laboratory studies on leaching of copper ores.tlf These studies are the first step of a program for the investigation of in situ leaching of tabular, metalliferous ore bodies.(2) The basic steps required in the development of an in situ process are: 1. Leachability - the ability to dissolve the metal values from the ore under in situ conditions must be demonstrated. 2. Ore Preparation - the ore must be prepared so that sufficient contact with the solution can be attained. 3. System Design - integrated in situ systems must be designed and studied for engineering feasibility. 4. Economic Feasibility - the economics of the system must be shown to be economically feasible and competitive. 5. Environmental Feasibility - the loss of reagents into the environment must be investigated. 6. Pilot Scale Testing - the feasibility of the system must be demonstrated on a sufficiently large scale. The studies described in this report were concerned only with the first step of the program, viz., leachability. Native and sulfide copper ores from the Michigan copper district were selected as model ores for these studies. Aqueous amnonia solutions were chosen as the solvents to be investigated. In this study carbonate (CO3, HCO3, H2CO3) was used exclusively as the anion. In keeping with custom it is referred to as carbon dioxide and concentrations are ex- pressed in terms of CO2. When leaching native copper the reaction is

Jan 1, 1976

By Joseph Hirschi, Naga S. Y. Tirumalaraju, Aditya Mishra, Anthony (Sam) J. S. Spearing

"Primary roof support in underground coal mines in the USA consists mostly of fully grouted passive rebar or grouted (partially or fully) tensioned rebar. Research conducted at two room-and pillar coal mines in the Illinois Basin and one longwall mine in Colorado monitored the performance of these passive and active rock bolts under similar geologic and mining conditions and found no significant initial loads in either passive or active rock bolts (Spearing et al., 2011). Active rock bolts showed significant loss of initial pre-load, although the exact reasons for this were not fully investigated. Subsequent laboratory testing has also shown that in weak rock, resin creep occurs, caused by slippage of the mechanical key between resin column and rock interface. These creep tests were studied in the laboratory in an effort to quantifythis phenomenon.INTRODUCTIONResin-grouted rock bolts are the first and main line of defense to counter roof and rib falls in underground coal mines of the United States. Rock bolts are categorized as active or passive. Active bolts are tensioned during installation whilst no (or limited) tension is applied to passive bolts, which need subsequent strata movement to generate reactive loads. During installation of passive bolts, some reactive pre-load may be generated by a significant up-thrust from the rock bolter boom.The selection of active or passive bolts is critical and is mostly dependent on the conditions and properties of the immediate roof (Unrug, 2009). This decision is frequently made based on personal experience, bias, and most recently cost. Active bolts are generally used in cases of highly laminated roof rock. When active bolts are tensioned, they develop compressive forces between these layers forming a beam, which helps to stabilize weak individual layers thereby increasing frictional forces between layers and decreasing effects of horizontal stresses. The fully grouted tensioned rebar system is high in stiffness as compared to mechanical bolts and provides higher surface area of contact along the length of the bolt due to the grout, which permits it to develop a strong anchorage mechanism."

Jan 1, 2015

By H S. Ellis

Flow studies have been conducted on nickel-water suspensions in a 1in.-diam., 42-ft.-long transparent lab-oratory pipeline at concentrations of up to 25 per cent, by volume, and slurry velocities of up to 15 ft/sec. The average size of the nickel powder was approximately 150 mesh (106J.L). Three flow regime were noted. At the highest velocities, i.e., above 10 ft/;sec., where the concentration distribution through the vertical diameter was most uniform, pressure gradients could be correlated with the Durand-Condolios equation (7,8). An intermediate region, i.e., from 7 ft/sec. to10 ft/sec., could be distinguished, the lower velocity limit being that at which nickel particles began to deposit. This region was also marked by decreasing pressure gradients, for a given concentration, as the velocity was reduced. The upper velocity limit in this region was also uniquely defined in that the friction factor for any nickel concentration was the same as that for water. In the third regime, below about 7 ft/sec

Jan 1, 1963

By Jr. Hardy, H. Warren Shen

"A study is presently underway by the authors to investigate the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. An important aspect of this on-going project is the development of acoustic emission (AE) criteria which would make it possible to carry out remote monitoring of coal cutting operations. The on-going AE studies are fundamental in form and were undertaken to evaluate the general feasibility of AE monitoring techniques using simplified coal breakage and cutting procedures. The present paper will focus on the test facilities, experimental techniques, and results associated with linear, single-bit cutting. An AE-transducer, attached directly to the bit, detected AE signals during the cutting process.Experiments have been carried out on seven specimens of coal obtained from the USBM experimental mine at Bruceton, Pennsylvania. Three separate cuts were made for each of two bit angles (10 and 45 degrees) and two bit velocities (0.085 and 0.169 cm/sec), for a total of 12 separate cuts. Data associated with resulting particle size distribution and AE characteristics (major dominant frequency components) will be discussed. Data analysis has also been underway using a computer-based pattern recognition system known as ICEPAK (Intelligent Classifier Engineering Package). This program is able to evaluate over 100 features of an AE event and to make objective comparisons between AE signals associated with different loading or cutting parameters. The results to date show that AE generated during some of the test conditions can be recognized by ICEPAK with a recognition rate of 90% and higher while other conditions cannot at present be separated with a suitable recognition rate. Further analysis of the experimental data is presently underway.The reduction of the severity, and eventual elimination, of Coal Workers' Pneumoconiosis (CWP) depends on gaining fundamental understanding in a number of major areas. These include dust generation and entrainment, transportation, suppression, medical effects of dust, and possible treatment. At present a project is underway by the authors to investigate the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. An important aspect of this on-going project is the development of acoustic emission (AE) criteria which would make it possible to carry out remote monitoring of coal cutting operations. Suitable on-line analysis of monitored AE data would allow engineers to evaluate factors such as shearer bit conditions and cutting efficiency, and to quantify the particle size and shape distribution of the generateddust. The on-going AE studies are fundamental in form and were undertaken to evaluate the general feasibility of AE monitoring techniques using simplified coal cutting procedures. To date experiments have been carried out on coal under uniaxial compression, linear single-bit cutting, and cutting using a laboratory-scale, single-bit shearer. A brief outline of the overall study has been presented in an earlier paper (Hardy, Shen and Kimble, 1995). This paper will consider the linear single-bit cutting studies in more detail.It is generally accepted today that most solids emit low-level seismic signals when they are stressed or deformed. In this paper this phenomenon will be referred to as acoustic emission (Hardy 1972, 1981, 1989). In essence, the measurement of AE activity in a field or laboratory structure is relatively simple. A suitable transducer is attached to the structure, the output of the transducer is connected to an associated monitoring system, and the AE signals occurring in the structure, due to internal or external stress, deformation, and failure are suitably acquired, pre¬processed and recorded."

Jan 1, 1998

By S. L. de Moraes

This study aimed to identify a way to reduce the use of bentonite in the pelletization of magnetite. With this goal, different combinations of binders were compared to bentonite by examining the quality of pellets obtained by balling drum agglomeration. Pellets were subjected to routine tests that included simple compression of the wet and dry 105°C pellets, dropping wet pellets to determine their ability to survive handling and submitting pellets to thermal shock to determine how they tolerate drying and preheating. The best results use sodium silicate (1.5%) as a binder and show that it is possible to pelletize iron ore without using bentonite.

Jan 1, 2010

By Jamal Rostami, Wei Hu

Efficient performance of EPB TBMs in clayey ground is primarily dominated by the flow capability of the excavated muck in the cutterhead and screw conveyor. Currently, Consistency Index approach is used to evaluate clay clogging potential, but it does not include the effects of surcharge pressure on clay behavior. In this paper, a macro-scale soil rheometer is introduced to assess the clogging potential under various water content and surcharge loading conditions. The results show that, in addition to water content, surcharge pressure has clear impact on clay clogging too. In practice, Consistency Index chart can be refined to incorporate the impact of face pressure to better simulate the EPB tunneling conditions.

Jun 13, 2021

By J. Desroches, J. Burghardt, N. Whitney, B. Lecampion, A. Surdi, M. Houston, S. Stanchits

There is accepted evidence that multistage fracturing of horizontal wells in shale reservoirs results in significant production variation from perforation cluster to perforation cluster. In fact, only a fraction of the perforation clusters seem to contribute to production in many shale gas and shale oil plays. In many cases, the orientation of the lateral section of these wells is determined by lease boundaries rather than principal stress directions, and these often do not coincide. When horizontal wells are misaligned from the far-field principal stress directions, the fracture must reorient from the near-wellbore principal stress directions, which are aligned with the wellbore, to the far-field principal stress directions. The primary objective of this study is to learn how various completion designs influence the near-wellbore fracture geometry when such a misalignment exists. A secondary objective is to understand the influence of rock fabric features, such as mineralized natural fractures, on this reorientation process. To understand these effects, eight laboratory hydraulic fracturing tests were conducted using a true triaxial vessel with 914 mm × 762 mm × 762 mm samples of Niobrara shale. Several different completion designs were studied, including the use of fracture initiation slots with several different orientations and the use of perforations selectively located to encourage a smooth transition from the near- to far-wellbore region. The tests were carefully scaled as accurately as possible to provide insight into the field near-wellbore phenomena. Pressure and fluid flux at the wellbore, deformation of the block, acoustic velocity, and induced acoustic emissions were acquired during the tests. Additionally, sized particles were also injected to gauge the fracture width away from the wellbore. After the test, the blocks were dismantled, and the fracture geometry was mapped in 3D. These measurements allow one to clearly differentiate the fracture initiation and the breakdown—meaning the peak pressure—to be clearly differentiated; the fracture was already well developed when the maximum pressure was reached. The study reveals non-negligible tortuosity and aperture restriction in the near-wellbore region. In the field, this would translate to high treating pressures, uneven proppant distribution, and possibly near-wellbore screenouts. The test results show that, of the configurations tested, the best approach is to use deep slots that are aligned with the far-field principal stress directions. The oriented perforation design did not achieve the simple, smooth transition that was hoped for, and instead produced multiple competing near-wellbore fractures and considerable tortuosity. The study also demonstrated that the presence of planes of weakness, such as mineralized natural fractures, near the slot tip can result in poor near-wellbore fracture geometries, even for the best completion configuration. We conclude from these tests that the misalignment of the well with a principal stress direction creates near-wellbore complexity that, in turn, creates uncertainty in proppant distribution and, therefore, production; proppant might avoid up to a half of the created fracture. Regardless of the wellbore orientation, this uncertainty is further increased by the presence of mineralized features in the rock fabric that can strongly alter or stop the growth of the hydraulic fracture. Preventing those effects by changing the completion alone proves difficult, and new strategies are required to ensure a reliable stimulation of shales.

Jan 1, 2015

The effect of long term exposure of full size bolts to corrosive environments is presented. A special test rig was used to test four bolts under different loading conditions. Four, X-grade identical profile bolts, each of 21.7 mm core diameters (23.7 mm full diameter) were subjected to prolonged corrosion testing using acid sulphate water. The pH value of the circulated water varied between 3.4 and 4.3. The corrosion exposure test period lasted three and half years. Two bolts were axially loaded to 10 and 20 tonnes force respectively, the third bolt was subjected to a 360 Nm torsion load and the fourth bolt was left unstressed to act as a reference bolt. After the test period ended, the bolts were stripped of their corroded coatings and weighted for weight loss. The diameter of each bolt was subsequently measured, and the loaded bolt samples were first tested non-destructively for tensile cracks and then tested for tensile failure. No cracks were found on post corrosion bolts tested non-destructively. The failure strength reduction on all four post-corroded bolts was significant, varying between 21% and 39%. The onset of corrosion was not confined to the targeted mid-section length of the bolt, however, the severest corrosion occurred at the anchored ends of the bolts.

Aug 1, 2013