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By E. D. Musin, S. S. Gudkov, A. V. Epiforov, S. V. Balikov

The standard technology for processing of gold-bearing sulfide raw material has many problems associated with the use of cyanide as a gold lixiviant. Therefore, many tests to find alternative gold recovery methods are being undertaken. This paper describes some technological solutions, which can become alternatives to cyanide technology in the future. Pressure oxidation (POX) of refractory gold-bearing sulfide concentrates from five different Russian gold deposits were investigated. Concentrate 1 was gold-copper concentrate. Concentrate 2 was gold-pyrite concentrate. Concentrates 3-5 were pyrite-arsenopyrite double refractory concentrates. The POX tests were at temperatures of 110, 200 and 220 °C and oxygen pressures of 1.5, 2.4 and 3.0 MPa were carried out. Gold lixiviants, such as chloride, thiosulfate, sulfite and thiocyanate were tested. The recovery of gold from sulfide gold-bearing concentrates by non-cyanide methods was 97- 99%, and from double refractory concentrates, 86-93%. The tested reagents are less toxic than cyanide, and their use will reduce of the cost of gold production. These methods make it possible to recover gold in acidic media, and eliminate the washing operation and POX slurry neutralisation. In addition, precious metals recovery from POX cakes using lead reduction smelting was investigated. It was shown that the “POX-pyrometallurgical” technology for double refractory concentrates processing could be used with recoveries of gold and silver of 97 and 96%, respectively. Keywords: Recovery of gold, refractory sulfide gold-bearing concentrates, double refractory concentrates, pressure oxidation, non-cyanide lixiviants of gold, chloride autoclave leaching, thiosulfate leaching, thiocyanate leaching, sulfite leaching, reduction smelting, POX-pyrometallurgical technology

Jan 1, 2020

By P Martin, A Somarin, S Bailey

Field-based research was conducted to investigate the performance of field portable X-ray fluorescence (FPXRF) in the analysis of reverse circulation (RC) drill chips in iron ore exploration. For years, FPXRF has been considered unsuitable for iron ore exploration due to the limitations of the elements it is capable of analysing for, in particular its inability to measure light elements (Mg, Al, Si, P, S). With the advent of the use of silicon drift detectors (SDD) in FPXRF, light elements are now measurable elements. However, doubt over the appropriate use of this new technology still exists due to the absence of reliable comparative field data. These doubts concerned the ability of the FPXRF data to correlate strongly with the laboratory assay of the same samples. It was believed that inconsistent grain size and other variables not being controlled would contribute greatly to this perceived unreliability.We tested RC chip samples on-site in the Pilbara, with the portable Thermo Scientific Niton XL3t X-ray fluorescence (XRF) analyser for a range of elements including Fe, Mn, Al, Si and S and then compared the results with laboratory assay data. A strong correlation indicates that the FPXRF results are reliable. Furthermore, to show the effect of simple sample preparation, we also analysed pulps of the same samples in the same way.The correlations were good for all of the elements of interest for the RC chip samples (R2 values between 0.82 and 0.9), and excellent for the pulps (R2 values between 0.89 and 1). The results also showed a direct correlation between sample preparation and improved quality of results with the FPXRF. This indicates that FPXRF can produce data from unprepared RC chips for Al and Si that, when compared with laboratory assays, is reliable for a field application in drilling and grade control. CITATION:Somarin, A, Martin, P and Bailey, S, 2013. Non-destructive analysis of diamond core for light elements using Niton field portable x-ray fluorescence, in Proceedings Iron Ore 2013 , pp 117-230 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 12, 2013

By Vishwajeet Ahuja, Benoit Jones

"INTRODUCTION Shotcrete lining forms an integral part of conventional tunneling and is widely applied for underground excavations. Early strength gain of the shotcrete is a crucial aspect for ground support and safety of operatives. Strength requirements are dependent on various factors such as lining thickness, ground type, excavation size and tunnel depth. The early strength gain is typically monitored using destructive tests, such as needle penetration, stud driving or coring samples for uniaxial compressive strength testing in the laboratory. Being destructive, these tests cannot be directly performed onto the lining without causing damage that must be repaired, which is a particular problem for permanent linings. For this reason and to avoid the need for operatives to work near to exposed ground and/or fresh shotcrete, these destructive tests are often performed on panels, which are sprayed at the same time as the tunnel lining. All current testing methods are also very local, testing only a small part of the lining or a panel, which may not be representative because the temperature history could be significantly different. Therefore, these tests do not provide an accurate or complete picture of the lining strength gain. New testing methods that are non-destructive and can scan the whole lining remotely would be extremely desirable. This paper describes a new method, using thermal imaging techniques, that achieves these aims. It also discusses the real-time on-site application of the method, providing insight into the experience gained and conclusions derived. Shotcrete Shotcrete used for tunnel linings requires immediate strength development. The strength development is a direct result of the hydration reaction of cementitious materials present in it. A progressive sequence of the hydration reaction changes it from a solid suspension (typically referred to as fresh concrete) to a solid skeleton with a porous network and thereafter, into a solid with predominantly discontinuous pores (Byfors 1980). In the case of shotcrete, early strength is needed to support the self-weight and then continuing early age strength gain is required to begin to support ground loads. These strength requirements, along with other workability needs, are met by careful concrete mix design, the use of admixtures, such as accelerator and superplasticizer (BS EN 934-5 2007), and supplementary cementitious materials, such as silica fume."

Jan 1, 2016

By J. R. Tickner

"Gold is conventionally analyzed using fire-assay or other destructive chemical methods that impose significant sample preparation, OH&S, and skilled labour requirements. Developed over the past 15 years by the CSIRO, PhotonAssay provides a new approach. A high intensity, high-energy x-ray source is used to activate atoms of gold and other elements in bulk mineral samples. The resulting activity is counted to automatically, accurately and rapidly determine metal grade. Samples weighing 0.5–1.0 kg can be measured in a few minutes with minimal preparation. As the method is matrix-agnostic, traditionally hard-to-assay materials such as highly refractory ores, carbon pulps and copper concentrates require no special treatment. We present the status of commercial PhotonAssay systems being developed by Chrysos Corporation. The first unit with a throughput of up to 80 samples per hour is to be deployed in an Australian assay laboratory in late 2017; smaller systems suitable for providing real-time assay directly at the mine-site will be progressively rolled out from mid-2018. Performance results from extensive testing using both mine-sourced and standard reference materials are presented, demonstrating the sensitivity and accuracy of the method. Implications for replacing conventional gold assay in exploration, mining and processing operations are discussed.INTRODUCTION Accurate methods for assaying ore grade are essential throughout the exploration, mining and mineral processing value chain. The discovery and evaluation of new ore deposits, reserve and resource definition, mine operations planning, ore processing, metal accounting and product quality evaluation all rely on accurate measurement of the valuable metal content of bulk materials. The analysis of gold presents particular challenges, stemming from the very low concentrations at which commercial operations run (often part-per-million (ppm), or equivalently one gram-per-tonne levels or below), and the highly heterogeneous nature of many gold deposits. These challenges mean that any analytical method must have high sensitivity and be capable of measuring large-mass samples. The most widely used quantitative analytical method for gold is fire-assay (Hoffman, Clark and Yeager 1998). An initial ore sample typically weighing several kilograms is dried, crushed and pulverized to allow a small sub-sample (10–50 g is common) to be representatively drawn. The sub-sample is mixed with flux, litharge (lead oxide), a reducing compound and other reagents. The mixture is fired at a temperature of 1000–1200°C until molten. After cooling, the slag is removed and the lead button containing any gold present in the sample is remelted in a porous cupel. The lead is absorbed into the cupel, leaving a gold prill which is either weighed directly, or dissolved in acid and analysed via atomic absorption spectroscopy (AAS) or inductively coupled plasma spectroscopy (ICP or ICP/MS)."

Jan 1, 2017

By A. M. Venter

"SynopsisThe availability of advanced characterization techniques is integral to the development of advanced materials, not only during development phases, but in the manufactured components as well. At Necsa, two modern neutron diffractometers equipped with in-situ sample environments, as well as complementary X-ray diffraction instruments, are now available as User Facilities within the National System of Innovation in support of the South African research and industrial communities. Neutrons and X-rays, owing to their different interaction mechanisms with matter, offer complementary techniques for probing crystalline materials. Both techniques enable nondestructive investigation of phenomena such as chemical phase composition, residual stress, and texture (preferred crystallite orientation). More specifically, the superior penetration capabilities of thermal neutrons into most materials allows for the analysis of bulk or localized depth-resolved properties in a wide variety of materials and components. Materials that can be investigated include metals, alloys, composites, ceramics, and coated systems. In particular, depth-resolved analyses using neutron diffraction complements surface investigations using laboratory X-rays in many scientific and engineering topics. The diffraction techniques can add significant downstream value to the anticipated nuclear industry development activities.IntroductionMaterials characterization is central in understanding the relationship between the structure, properties, and performance in order to engineer materials that fit the performance criteria for specific applications. This is conveniently represented in the form of a tetrahedron, generally known as the material science paradigm (Figure 1).The availability of advanced characterization techniques is integral to the development of advanced metals, not only during development phases, but in the form of manufactured components. At Necsa (South African Nuclear Energy Corporation), modern X-ray and neutron diffraction instruments are now accessible to the South African research and industrial communities. These facilities enable nondestructive investigations of materials and components that could add significant downstream value to the anticipated nuclear industry development activities."

Jan 1, 2015

For the last few years, a new and innovative technique has been successfully used to determine refractory and castable thickness in various metallurgical vessels. The acousto ultrasonic-echo (AU-E) technique uses stress waves to detect metal penetration and delaminations within refractory linings. In addition, it is capable of measuring the thickness of refractory layers and build-up material. The inspection and measurements can be carried out while the furnace is in full operation. The present paper discusses the principles of the AU-E technique, and its advantages and limitations. A number of case studies are presented to demonstrate various capabilities of this new Non-Destructive Testing (NDT) technique.

Jan 1, 2005

By Harold N. Miller

Lost time and services caused by electrical equipment breakdown or cable faults can often be substantially reduced by the use of direct-current high-voltage testing as a maintenance tool. This paper discusses the relative merits of alternating-current versus direct-current testing, pointing out the advantages in size and cost of equipment and more definitive results achieved through the use of D.C. General principles of direct-current high-volt-age testing, types of testing, methods of performing the actual test and interpreting the results are explained. ?The value of insulation resistance measurements and their relationship to high-voltage testing is discussed. Pinpointing the physical location of a cable defect using a fault locator or thumper is described. Reference is made to several organizations that have effected considerable savings with high-voltage test programs. Introduction T HE past decades have seen great advances in the field of electrical power distribution and application. Motor generators, power-operated equipment, cables, etc., have all gone through various stages of improvement both in efficiency and reliability. Un-fortunately, however, power failures and equipment breakdown still occur -frequently with disastrous effects in loss of time,

Jan 1, 1965

By Houquan Zhang, Yu Wu, Yanlong Chen, Zhenfu Luo, Aihong Lu

"A non-destructive detection scheme for bolt installation quality was designed by adopting the method of non-destructive detection on bolt installation quality. Based on the field measurements, a random non-destructive detection method for determining the characteristic length including anchoring length, free segment length and initial axial load of bolt was discussed, and the characteristics of increasing bolt axial load in the initial stable stage was obtained. The results show that the bolt axial load and deformation of surrounding rocks correlate each other. Compared with the traditional detection technique for bolt installation quality, the non-destructive detection method has obvious advantages such as random, accuracy, and economic. The method provides a reliable basis for bolt support optimization and stability control of surrounding rocks.INTRODUCTIONBolt support in roadway can make the surrounding rocks and bolt form a structure in the early stage of roadway development through the bolt pre-tension, which can maximize the self-bearing capacity of surrounding rocks. Thus it is a form of active support (Kang, 2007). In order to make the bolt play an active supporting role, it needs to ensure the installation quality of bolting. Thus the bolts can supply a high initial anchoring force and control the deformation of surrounding rocks (Shan, 2009; Wei, 2012). Moreover, bolt supporting is a concealed work. Once installation quality problems appear; it will be difficult for effective detection and screening (Xie, 2008).THE PROBLEMS OF BOLT INSTALLATION QUALITY IN COAL MINE AND ITS DETECTIONThe Problems of the In Situ Bolt InstallationDue to the problems in installation environment, machine, and technique, and workers proficiency (Li, 2003), there are many problems exist in bolt installation. If the borehole depth is too long, the anchoring agent will accumulate at the bottom of the bore, which reduces the anchoring length. Furthermore, if the borehole depth is short due to the poor geological condition, the exposed part of the bolt will be too Jong and the pallet cannot cling to the rock face, which prevent the pre-tension from being applied. The pre-tension is very important for bolt installation. If pre-tension is insufficient the rock bolt cannot control the deformation of surrounding rock efficiently and the bolt anchoring force will decrease considerably. The bolt length is another important parameter for anchoring quality, which will affect the control area of bolt supporting. In addition, the cleanness of drill hole has a great influence on the effective anchorage length of bolt. If the drill hole cleaning is not enough, it will directly affect the anchoring agent and the contact area of surrounding rocks, which will decrease the effective anchorage length and initial anchor-force."

Jan 1, 2016

By George Piscsalko

There are numerous methods currently available to assess the integrity of drilled shaft and ACIP piles. Each method has its advantages and limitations. This paper will compare the various available methods as well as introduce a new method for assessing integrity of drilled shafts and ACIP piles. This new method, known as Thermal Integrity Profiling, determines the integrity of the shaft both inside and outside the reinforcing cage by measuring the hydration temperature of the concrete along the length of the shaft. These temperature measurements can be made by either passing a thermal probe through a standard Cross Hole access tube, or from embedding thermal wires within the shaft. This Thermal Integrity Profile method will be described in detail and one case history will be presented. Additional testing methods which will be compared include low strain Pile Integrity Testing and Cross Hole Sonic Logging. Advantages and limitations for each method will be discussed.

Jan 1, 2011

By George Piscsalko

"Quality control of drilled shafts and ACIP piles is greatly dependent upon the practices of the site personnel. In many applications it is difficult to properly inspect the shaft prior to concreting, such as when the shaft is drilled under slurry. In other cases, such as ACIP piles, it is impossible to inspect the shaft in any manner prior to concreting. There are numerous methods currently available to assess the integrity of drilled shafts and ACIP piles. Each method has its advantages and limitations. This paper will compare the various available methods as well as introduce a new method for assessing integrity in drilled shafts and ACIP piles. This new method, known as Thermal Integrity Profiling, determines the integrity over 100% of the shaft both inside and outside the reinforcing cage by measuring the hydration temperature of the concrete along the length of the shaft. These temperature measurements can be made by either passing a thermal probe through a standard Cross Hole access tube typically 12 to 48 hours after concrete placement, or from embedding thermal wires within the shaft prior to concrete placement and monitoring them with unattended data collectors for 12 to 48 hours after concrete placement. This Thermal Integrity Profile method will be described in detail and several case histories will be presented. Additional testing methods which will be compared include low strain Pile Integrity Testing, and Cross Hole Sonic Logging. Advantages and limitations for each method will be discussed.IntroductionDrilled shafts and Augered Cast-in-Place (ACIP) piles have been increasingly used over the past several years due to several reasons including the reduced noise and vibration, speed of installation for ACIP piles, and the large axial and lateral capacities which are attainable for very large drilled shafts. ACIP piles are drilled and cast without any visual inspection. Drilled shafts can be cast in a dry hole which allows for inspection of the hole prior to casting, but the casting process is very difficult to nearly impossible to inspect with any accuracy. Drilled shafts are frequently cast under slurry as a means to stabilize the surrounding soils during the construction process. When casting a drilled shaft under slurry, it is very difficult to accurately inspect the hole prior to casting and it is equally difficult to inspect the shaft during the casting process. Many of the above mentioned processes are blind to inspection and therefore the chances increase for having defects present in the completed elements."

Jan 1, 2017

By George Piscsalko

Quality control of drilled shafts and ACIP piles is greatly dependent upon the practices of the site personnel. In many applications it is difficult to properly inspect the shaft prior to concreting, such as when the shaft is drilled under slurry. In other cases, such as ACIP piles, it is impossible to inspect the shaft in any manner prior to concreting. There are numerous methods currently available to assess the integrity of drilled shafts and ACIP piles. Each method has its advantages and limitations. This paper will compare the various available methods as well as introduce a new method for assessing integrity in drilled shafts and ACIP piles. This new method, known as Thermal Integrity Profiling, determines the integrity over 100% of the shaft both inside and outside the reinforcing cage by measuring the hydration temperature of the concrete along the length of the shaft. These temperature measurements can be made by either passing a thermal probe through a standard Cross Hole access tube typically 12 to 48 hours after concrete placement, or from embedding thermal wires within the shaft prior to concrete placement and monitoring them with unattended data collectors for 12 to 48 hours after concrete placement. This Thermal Integrity Profile method will be described in detail and several case histories will be presented. Additional testing methods which will be compared include low strain Pile Integrity Testing, and Cross Hole Sonic Logging. Advantages and limitations for each method will be discussed.

By Edmund J. Cardoza

WELCOME TO THE DEEP FOUNDATIONS INSTITUTE 26TH ANNUAL CONFERENCE AND WELCOME ESPECIALLY TO THIS SEMINAR ON NON-DESTRUCTIVE TESTING OF DRILLED SHAFTS, PRESENTED BY MEMBERS OF THE DFI DRILLED SHAFT COMMITTEE. MY NAME IS ED CARDOZA; I AM A VICE PRESIDENT WITH THE MILLGARD CORPORATION, A DRILLED SHAFT CONSTRUCTOR FOCUSING PRIMARLY IN THE EASTERN HALF OF THE UNITED STATES.

Jan 1, 2001

By C Harwood, EáWestman, K Luxbacher

Testing of in situ seals in underground coal mines is critical to determine seal integrity and to provide safe working conditions. In the wake of the 2006 Sago Mine explosion, the United States of America (USA) promulgated the Mine Improvement and New Emergency Response (MINER) Act (USDOL, 2006) which required mines to install 827 kPa (120 psi) rated seals or monitor and maintain the atmosphere behind existing 345 kPa (50 psi) seals. The purpose of developing the regulations was to prevent the breaching of seals in the event of an explosion in the sealed area.While seal design and construction is carefully regulated in practice, the construction of seals is difficult to monitor, as many are constructed under various mine conditions and the methods rely on prescribed placement of the seal material. Further examination of installed seals is limited to two-dimensional visual inspection and atmospheric and convergence measuring devices. These methods do not accurately reflect the integrity of the seal and cannot detect changes, deterioration, or defects within the seal.If detection of defects, deterioration and damage is not possible, unexpected communication between the active and sealed areas may result. Additionally, the ability of the seal to withstand explosions may be compromised. Non-destructive testing (NDT) of underground mine seals is necessary to investigate if the seal properties have been altered and if the seal remains functional as a barrier between active areas and sealed areas of the mine. This paper gives a preliminary assessment of proposed NDT methods for seal evaluation using radio frequency (RF) technologies and tracer gas methods.CITATION:Harwood, C, Luxbacher, K and Westman, E, 2013. Non-destructive testing of in situ underground mine seals - Initial technology assessment, in Proceedings The Australian Mine Ventilation Conference , pp 299-306 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 1, 2013

Numerous underground coal mine ventilation seals have been installed in the United States of America prior to 2006 and after implementation of the Mine Improvement and New Emergency Response (MINER) Act. Seal engineering, design, placement, and construction is regulated in industry, but post-construction monitoring of seals is limited to visual inspection of the outby face and seal perimeter, convergence measurement, and atmospheric monitoring. To monitor seal integrity and to provide safe working conditions, a form of non-destructive testing (NDT) is necessary to accurately reflect the health of the seal by detecting post-construction changes, deterioration, or defects within in-situ seals in underground coal mines. Previous research from the National Institute of Safety and Health (NIOSH) has indicated the potential for utilizing ground penetrating radar (GPR) for assessing in-situ mine seals. This paper provides an update to the assessment of proposed NDT methods for seal evaluation using commercially available GPR technologies and systems. Full-scale free-standing seals and large-scale seal specimens were analyzed with an array of GPR units from various manufactures using multiple frequencies.

Feb 23, 2014

By Heman Manchanda, Jyoti Agarwal

Several infrastructure projects are under construction in India; many of them involves construction of deep foundations like reinforced concrete and steel piles to support super structures. As most of the piles being constructed in India are reinforced concrete bored piles, there are always uncertainties relating to the quality of construction, and in this case non-destructive methods to ascertain quality of piles becomes very crucial to success of any project. Non-destructive pile testing is becoming more and more popular with growing technologies wherein geophysical techniques and wave propagation theories are being used for pile quality and length analysis. Low-strain pulse echo method and cross-hole sonic logging testing are two pile integrity testing techniques being currently practiced in India which are cost effective and provides reliable near accurate results if analyzed properly. Paper presents current practices being adopted in India for conducting these two tests, highlighting the critical site considerations and analysis techniques. The paper also discusses various execution and interpretation challenges faced by practicing engineers and recommends a way forward.

Sep 1, 2022

By Chetan D. Savani, Mike K. Muchard

The necessity to evaluate undocumented foundation lengths is essential in assessing the useable life, need for scour protection, retrofitting, or full reuse of existing bridge foundations. For this purpose, Parallel Seismic Testing (PST) has the best accuracy and is applicable to the widest range of foundation configurations used in bridge construction of any test method. Although not limited to bridges, PST case studies are presented involving two bridges. To preface the case study discussions, an overview of the PST method is given along with its results and analysis thereof. In one of the cases, we were afforded the rare opportunity to see the existing piles being extracted long after the PST testing program was completed. The resulting Class A prediction reaffirms the accuracy of the method. Versatility of the PST method is also exemplified in the two cases presented, where unique situations from complex foundation systems were overcome by analysis to provide successful results.

By Dieter Wittenberg

The use of thc ultrasound technique for monitoring rockbolt support has at last provided support engineers with a measunng system capable of pinpointing fracture failuns in fully-grouted rockbolts. The measurement data are based on the operatmg characteristics of the bolt type, which are determined both under test-bench conditions (DIN 21521) as well as in underground trials. Practical experience acquired to date suggests that this new measuring system is both effective and reliable.

Jan 1, 2001

By L. Lacerda, C. Rose, E. Zellers

Approximately six hundred air sample measurements were taken at several U.S. underground metal/nonmetal mines in 1998 and 1999. This air sampling effort was organized by the Nevada Mining Association to evaluate mining conditions and to evaluate the Mine Safety and Health Administration’s (MSHA) Proposed Rule on Diesel Particulate Matter Exposure of Underground Metal and Non-metal Miners. MSHA’s proposed air sampling method, NIOSH Method 5040, was tested under controlled conditions and under normal mining conditions. Unfortunately, NvMA sampling results have indicated that carbonaceous rock dust, oil mists and even cigarette smoking create severe sampling interference problems for NIOSH 5040.The main conclusion was that NIOSH 5040 did not distinguish between DPM and other airborne carbon particulate. Thus, it is not a reliable method of accurately and unequivocally measuring DPM in underground metal/nonmetal mines.

Jan 1, 2000

By John Watson, Tom Treleaven

This guide presents nur-nerous patterns that provide 8 millisecond separations between initiated charges. The guide is tabulated in seven sections to provide Quick reference by number of decks or bunch blasting. The pattern IS presented in the section where the highe!$ number of decks works. It should be noted that patterns applicable to multipledackshwtings are alsoapplicsblefor fewer decks.

Jan 1, 1995

By R. Patrick

As a unique South African organisation, CSIR: Division of Mining Technology (Miningtek) strives to support the mining industry by improving health, safety and productivity through developing, adapting and transferring technology. Considerable effort is currently directed towards the development of potential non-explosive mining methods with the potential to allow continuous mining in narrow reef conditions. Besides improving productivity, continuous mining results in concentrated mining which has a significant impact on reducing infrastructural costs. Impact Ripping and Water Pulse Rock Breaking have been tried on gold mines, whereas Activation, Mini-Disc? cutting and the Plasma Holemaker are currently being tested on platinum mines. The organisation?s many years of experience in novel rockbreaking, together with its world-wide collaborator network, has placed it in a unique position to assist the mining industry and manufacturers in developing and/or adapting existing technologies for application underground. Currently a range of technologies are being investigated, which have reached different stages of maturity. The main technologies under investigation are; - Impact ripper system - Water pulse rock breaking - Activated undercutting rollers - Mini disc cutters - Electric rock breaking

Oct 1, 2001