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By K. C. Liddell, B. Dou

"In producing multilayer films for magnetic data storage applications, the interfacial roughness must be controlled in order to obtain high quality materials with reproducible properties. The present understanding of the effect of roughness on multilayer properties such as magnetoresistance is sketchy, particularly for electrodeposited films. In this study, quantitative atomic force microscopy was used to characterize surface morphology before and after Ni films of varying thickness were deposited on Cu cathodes. A multinuclear multilayer growth mechanism is supported by both the deposition conditions and the AFM images, and a multinuclear multilayer model gave a satisfactory fit to measurements of the density of peaks on ultrathin Ni films between 0 and 8 nm thick.Alloys consisting of alternating ferro-and paramagnetic layers have begun to replace Permalloy in the sensing elements of magnetic hard drives. The operating principle of the new read heads is giant magnetoresistance (GMR), and they are smaller and more sensitive than previous inductive heads (1). Experimental studies on sputtered multilayers have emphasized the role of layer thickness and interlayer roughness in determining the presence and size of the GMR effect (e.g., 2,3,4,5,6). However, roughness in electrodeposited multilayers has rarely been measured, even though read heads are likely to continue to be made by this process for some time to come. Cu/Ni can be considered a model system for understanding processing-microstructure-property relationships in electrodeposited multilayers and is the most widely investigated of all such systems (e.g., 7,8,9,10,11,12). Nevertheless, the roughness of the interfaces in Cu/Ni electrodeposits has not been systematically characterized by quantitative techniques, and in all studies reported so far, the total deposit thicknesses were considerably greater than the 10 nm needed for most sensor applications (1). The thinnest such films were about 50 nm (7)."

Jan 1, 1998

By Kota Nakashima

Residues from titanium smelting tend to contain scandium. The scandiumis discarded because no suitable process exists for its recovery from the residue. Valuable-metal recovery from discharged residue is critical for environmental conservation and to achieve a sustainable society. Since 2015, JXNippon Mining&Metals has been developing a process for scandium recovery from the residue of a titaniumsmelting process. The process consists of the following steps: scandium concentrating by classification or neutralization, selective scandium leaching, impurity removal by neutralization, solvent extraction of scandium by using D2EHPA, purification, and roasting. We optimized the above steps to achieve an effective process to obtain scandium oxide (Sc2O3). In this paper, we introduce results from the bench-scale test of the scandium recovery flowsheet developed by JX Nippon Mining & Metals.

By R. J. Evans

THE Combined Metals Reduction Co.'s plant is at Bauer, Utah. It was built primarily to treat ore from the Combined Metals mine at Pioche, Nevada. Shortly after its completion, the company acquired the old Honerine mine, and ores from this mine, as well as custom ores from widely scattered districts, are now being treated at the Bauer plant. PIOCHE ORE The Pioche ore, which comprises about 50 per cent. of the mill feed, occurs as a replacement of an impure thin-bedded limestone. The lime beddings are separated by thin layers of micaceous shale containing appreciable quantities of sericite and graphite. The ore is an exceptionally fine-grained, dense mixture of minerals and gangue, assaying approximately 0.03 oz. gold, 7.2 oz. silver, 7 per cent. lead, 15 per cent. zinc, 16 per cent. iron, 29 per cent. insoluble and 1.5 per cent. lime. Of the total lead 7 per cent. is in the form of sulfate and carbonate. Approximately 10 per cent. of the ore consists of chert nodules impregnated with barren pyrite; the nodules average 0.8 mm. in size, and are extremely hard, compared with the other constituents of the ore. Microscopic examination of Pioche ore ground to 80 per cent. minus 150 mesh shows pyrite, sphalerite and galena still attached. EARLY ATTEMPTS AT ORE DRESSING Metallurgists, both professional and those working for private companies, have been more or less familiar with the Pioche ore since 1913; in fact, a total of 35 commercial and plant laboratories experimented with the ore between 1913 and 1921. The work during this period was decidedly negative, it being seemingly impossible to effect a satisfactory separation of the valuable minerals into marketable products. In 1913, it was recognized that fine grinding-that is, about minus 200 mesh-was required to liberate the minerals from one another, and from the gangue, but such fine grinding was not considered practicable at this time.

Jan 1, 1928

By D. Robert Weir, Verner B. Sefton

The reduction roast-ammonium carbonate leach-hydrogen reduction process for laterites has been under development by Sherritt Gordon for the past 20 years. The process can treat high iron or low iron laterites, with some process modification, and gives extractions of 88-93% Ni or 82-88% Ni, respectively. Five campaigns on a 1 tonne per day Pilot Plant and four campaigns on a 35 t/d Demonstration Plant have been carried out on laterite from three different deposits, and many other laterites have been investigated in the laboratory. The Marinduque Surigao Nickel Refinery in the Philippines was designed on the basis of this work. The process comprises roasting to selectively reduce the nickel and cobalt in the laterite, leaching the calcine in ammonium carbonate to dissolve the metals, recovery of cobalt by precipitation of a mixed metal sulphide, concentration of nickel from the carbonate solution by basic nickel carbonate precipitation and recovery of high purity nickel by hydrogen reduction of nickel from ammonium sulphate solution. Ion exchange has been developed as an alternative to BNC and for recovery of trace nickel from BNC barren liquor. Details of the development of some of the process steps through the laboratory to commercial plant are discussed. The process metallurgy has been confirmed in the commercial plant.

Jan 1, 1979

By C. S. Griffith

Lithium Australia NL (ASX:LIT) and ANSTO Minerals have been working together since 2015 on the development of halide accelerated leaching for the extraction of lithium from lithium-bearing micas, spodumene and clays. This technology has been termed SiLeach® process. The driving force behind development of the SiLeach® process, initially, was to develop a hydrometallurgical process to extract lithium from micas and spodumene without the need for the energy intensive, high temperature processing conventionally applied to lithium extraction. This driving force remains today and continues to hold promise in realising the value of previously under-utilised lithium resources. A comprehensive understanding of the technology and its applicability to the processing of micas and spodumene currently exists, and the flowsheet has been rigorously piloted. Production of battery grade lithium carbonate has been demonstrate

By J. P. Ress

In 1903, seventeen years after mining of the Witwatersrand gold-bearing reefs started, the findings erf the Miners' Phthisis Commission (Transvaal) resulted in the initiation of measures with the object of controlling dust production. The substance of these measures was as follows: Removal of persons from places where they would be exposed to blasting fumes; use of water to suppress dust made in drilling and in other operations; supply and control of air to working-places; filtration of dusty air; and determination of the amount of the dust in the air. Broadly speaking, progress in dust control has followed these four lines with increasing success as the nature of the problem has become better known. Complete success has not, however, been achieved, partly because increasing mechanization of mining has intensified the problem and partly because the application of these measures is not infallible, being subject, in many cases, to human control. A brief summary of the development of these measures will lead to a description of present-day practice.

Jan 1, 1947

By C. H. Bucknam

A review of phase analysis methods used to characterize refractory gold ores is presented. Updating of assay methods using database technology, on-line instrument interfacing and response surface modeling is highlighted. The use of assay results to classify ores for metallurgical purposes is demonstrated.

Jan 1, 1987

By H. Siebert, G. Raitt

With the advent of the Interstate Highway Pro- gram, many problems have been encountered in the application of highway design standards to topography, particularly rock cut design. A rigid application of slope ratios with little respect to rock type, dip, foliation, structure and height of cut face is a problem. Generally a slope ratio of ½ : 1 or 63º for shallow cuts and 1/3: 1 or 71º in deeper cuts are used in Connecticut. The deepest cut face constructed recently was greater than 185 ft. With cuts of this size, rock fall and stability become a problem, and a way to reduce the problem is to construct a stable face initially. A search of the literature indicates that adequate information on the construction of stable rock slopes is not available. A major highway contract was awarded in 1962 to Savin Brothers, Inc., in which line drilling on 6-in. centers was required in many portions of the contract where the cut was greater than 60 ft and one or more benches were to be constructed. From the start of the project many variations were attempted regarding slope hole spacing and distribution of explosives in the holes. Rock ranged from a competent granitic gneiss to an incompetent soft graphitic schist. Generally, the roadway alignment was roughly normal to the strike of the foliation having a dip of ± 60º. An important factor affecting construction of rock slopes was the existence of intersecting joints and faults. The spacing used in less competent rock was about one ft on center. Loading of holes was purposely varied. As competency of the rock increased, hole spacing was also increased. Thus, on a different project in similar rock, spacing was kept at 4 ft.

Jan 4, 1966

By Y Zhang, Z Zhao

The green production of the steelmaking process has urgent requirements for fluorine-free fluxes. In this article, a new solid waste-based slagging flux was applied in the external dephosphorisation test of low silicon hot metal to replace the traditional fluorite-lime dephosphorisation slag. The results showed that under laboratory conditions, the new flux was utilised for smelting low-silicon molten iron with a phosphorus content of 0.10~0.13 wt per cent, the temperature of the molten iron was 1350°C and the slag amount was controlled at 2 per cent. Within ten minutes of smelting, the dephosphorisation rate of the molten iron reached more than 50 per cent. When making slag with new flux, the slag melting time was about 40 seconds and the P2O5 content in the final slag was higher than 8 wt per cent. In the industrial test of a 150 t molten iron ladle, under the same molten iron conditions, an out-of-furnace dephosphorisation test was conducted in the Kambara Reactor (KR) process. The flux material consumption per ton of steel was 8~10 kg. Within 15 minutes of smelting, the dephosphorisation rate of the molten iron was about 30 per cent. During flux slag making, the slag melting time was about three minutes and the P2O5 content in the final slag was higher than 6 wt per cent. This new solid waste-based flux has significant cost advantages and outof- furnace dephosphorisation effects and is expected to become the benchmark for a new generation of fluorine-free steelmaking fluxes.

Aug 21, 2024

By Hideaki Kitajima, Ryo Sakamoto, Katsuya Sasaki, Maehata Hidehiko

The Electric Discharge Impulse Crushing System (EDICS) is a technology for carrying out crushing by using electrical power and nitromethane. It is designed for construction tasks such as splitting of concrete and rocks.The EDICS consists of an electric discharge generator that supplies a high-voltage high-current pulse, a cartridge that generates power by using electric discharge energy, and cables that connect the electric discharge generator and the cartridge. The cartridge contains a thin metal wire that evaporates because of the electric discharge energy and a nitromethane that reacts with this evaporated metal wire. The cartridge can be used to generate a high pressure on the order of gigapascals within a time interval of several hundred microseconds, and crushing power equivalent to that generated by explosives is generated during this period. In recent years, the EDICS has been widely used in Japan because of its good performance and favorable characteristics.

Jan 1, 2011

By Beatriz Dogliani, Elisabeth Williams, Maria Berenice Sandobal, Carina Bertino

The environmental management of steel mill slag should be understood as a management philosophy, observing technical, economic and environmental criteria associated with their generation, storage and final destination. The slag can be considered as a synthetic mineral resource and become a very useful co-product in different areas. The Argentinean steel industry prioritizes the efficient environmental management of its waste, thus contributing to its own survival taking into account the sustainable development. In the world, the slag produced by the steel industry has been used as steel aggregate for road bases, railway ballast and filling material among others. Any factor that influences the economy of the country affects all branches of society, mainly public agencies, whose financial resources are increasingly scarce to deal with all public works. It is necessary to join efforts of private and public initiative in the adoption of alternative materials that replace the use of finite natural resources. This presentation aims to show the work done by private companies together with public bodies and universities to obtain a regulatory document for the management of slag as steel aggregates for three different uses, namely: road use, railway use and general use.

Nov 5, 2019

By G M. Volkmann

Pipe umbrella support systems – also called canopy tube systems – have been used successfully for tunnelling in challenging ground conditions since the 1970s. Historically, the drilling unit was the limiting factor for pipe umbrella installations – less attention has been paid to pipe couplings and their influence on labour time and load-bearing capacity.This contribution investigates the influence of the type of pipe connection on the load bearing characteristics of a connected pipe and discusses associated influences on design calculations and installation performance. Standard thread connections reduce the effective cross-section and thereby load-bearing capacity in the connection area. To achieve design parameters, over-dimensioning of the un-weakened pipe section is the only way to overcome this limitation. Recently, two new, alternative connection types were designed and developed for connected pipe umbrella pipes. The first one is the nipple coupling, consisting of fitting with a threaded connection that is pressed and welded into the ends of standard tubes. The second type is the squeezed connection, which mechanically connects non-threaded pipe ends, achieved by force-fitted squeezing from the drill rig. Both coupling types have technical as well as operational advantages compared to the common thread couplings, which are the weakest point in the support system.In the following sections significant technical differences are explained, design values given and a site example presented to illustrate the operational advantages of the newly developed coupling?type.CITATION:Volkmann, G M, 2014. Development of state-of-the-art connection types for pipe umbrella support systems, in Proceedings 15th Australasian Tunnelling Conference 2014 , pp 333–338 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 17, 2014

By Rafael Abreu Fraga, Carlos Noberto Paula da Silva, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Since 2016 Gerdau Ouro Branco has been producing steel plates of various qualities and grades. However, it was not until 2018 that the first plates produced by accelerated cooling process were made available for external testing, in this case for large diameter UOE pipes manufacturing. Recent line pipe and OCTG specifications are showing that the oil and gas market still consumes regular API grades, such as X60, X65 and X70, however with increasing wall thicknesses, reaching values up to 1.5 inches. These specifications also demand longitudinal and transverse tensile guarantees and drop weight tear tests in temperatures as low as -40°C. Projects with these types of mechanical properties present process requirements as challenging as those necessary for higher API grades in lower thicknesses. This paper shows the steel design concepts and rolling routes for achieving the necessary properties for X70 steel plates in 28.15 mm. The microstructural features were also investigated and associated with the production process and the tensile and toughness results. Finally, challenges such as tensile anisotropy and DWTT abnormal fracture are presented.

Oct 1, 2019

By N. S. Tanious

The need to provide better mine roof support and control in longwall tailgate entries prompted the Bureau of mines to search for a replacement product for wood cribs. Their search isolated steel-fiber-reinforced concrete (SFC) as the most effective replacement. Through successful laboratory and underground mine tests, handmade SFC cribs proved to be a viable and more effective roof support system. However, to ensure wider usage, U. S. Steel Mining Co. initiated a joint development and evaluation program with Burrell Construction Company in order to mass produce SFC blocks of reasonable dimension, weight, and cost. Small specimens and full-size cribs were evaluated during this program to determine their compressive strength and post failure characteristics. After considerable testing and adjusting of various concrete mixtures, a final formulation for the SFC crib blocks was selected. That formulation permitted the construction of SFC cribs possessing a nominal crib strength of 3200 psi (22.1 x 106 Pa) and a nominal modulus of elasticity of 1.0 x 106 psi (6894.76 x 106 Pa). These SFC cribs can support from 3.5 to 14.5 times as much load as a wood crib, depending on the size of the wood crib being replaced. Both laboratory and limited mine tests, conducted by U. S. Steel Mining Co. have shown the SFC crib to be an economical and effective means of roof control.

Jan 1, 1984

By C. Alexander

Stillwater Mining Company is developing a second underground palladium and platinum mine approximately 21 km (13 miles) west of their existing Nye operation in south central Montana. A 5650 meter (18,550-foot) tunnel is required to gain access to the ore bearing horizon (J-M Reef). Access and primary mine development can be accelerated through the use of two 4.6 meter (15-foot) diameter tunnel boring machines (TBM). One TBM was purchased new while the other was purchased used. Machine specifications, site support facilities, portal/launch chamber construction, TBM assembly, startup and operation are discussed in this paper.

Jan 1, 1999

By A. Halim, A. Martikainen, S. GYAMFI

This paper outlines a unique case of the development of strategies to reduce ventilation and heating costs in Konsuln iron ore mine in northern Sweden. The mine, located just south of Luossavaara-Kiirunavaara Aktiebolag’s Kiruna iron ore mine, was developed as a test mine from 2018-2020 for the Sustainable Underground Mining (SUM) project. Besides functioning as a test mine, Konsuln also contributes to ore production. The existing mine ventilation system was designed for the current production rate of 0.8 million tons per annum (Mtpa). There is a plan to increase this rate to between 1.8 and 2.0 Mtpa.

Dec 23, 2021

By A. Martikainen, S. GYAMFI

Luossavaara-Kiirunavaara Aktiebolag’s (LKAB) Konsuln iron ore mine, located just south of the famous Kiruna iron ore mine in Malmfälten in northern Sweden inside the Arctic Circle, was developed as a test mine between 2018 and 2020 for the Sustainable Underground Mining (SUM) project [1]. Besides functioning as a test mine, Konsuln also contributes to ore production. The existing mine ventilation system was designed for the current production rate of 0.8 Mtpa using conventional diesel machines. The design was created by Kiruna mine ventilation team, Stina Klemo and Joakim Jonasson, in cooperation with a consultant, Tomas Bolsöy from EOL Vent Mining AB. There is a plan to increase this rate to between 1.8 and 3 Mtpa in the future, and this requires the primary fans to be upgraded. Therefore, a study was carried out to determine whether using ventilation on demand (VOD) could avoid this fan upgrade and reduce Konsuln’s ventilation and heating power costs in the future. The study also investigated whether using battery electric vehicles (BEVs) along with VOD or as a standalone strategy could further reduce these power costs. In addition, the study analyzed the suitability of heating power reduction strategies presently or previously used in Nordic countries and Canada to investigate potential additional strategies to reduce heating power cost, the largest portion of Konsuln’s ventilation and heating power costs.

By H. J. Thevik, A. K. Dahle

"A mathematical model that calculates the stress development in a coherent and stationary dendritic network due to interdendritic flow is proposed. The fluid flow is assumed to be related to the solidification shrinkage, and under the assumption of no porosity formation and unidirectional solidification, the shrinkage-induced flow within the mushy zone is calculated analytically. The interdendritic melt flow exerts a force on the solid network and an analytical expression for the stress build-up in the network is developed. Parameter studies illustrating the influence of cooling conditions, mushy zone length, dendrite coherency, fraction solid, volume fraction of eutectic, and solidification shrinkage upon the stress development within the solid network are presented. Comparing the magnitude of the calculated stresses to measurements of the strength in equiaxed mushy zones shows that it is possible for the stresses to exceed the strength, thereby resulting in reorientation or collapse of the dendritic network.IntroductionInterdendritic fluid flow is at present regarded as a very important mechanism for feeding of shrinkage during solidification of metal alloys. Solidification of many alloys is often characterised by heterogeneous nucleation of the primary phase on substrates in the melt with subsequent evolution of equiaxed dendrites. These equiaxed dendrites can initially grow freely, but impinge on each other and form a continuous dendritic network, ie. dendrite coherency, quite early in the solidification process. Measurements of the dendrite coherency point have shown that the dendritic network is established at solid fractions ranging between 0.1 and 0.5, and most often around about 0.2 [l]. Depending on the alloy composition this means that as much as 70 to 80% of the volumetric shrinkage has to be compensated by flow of liquid through the interdendritic network. Interdendritic flow occurs with a much larger resistance compared to free flow of the liquid and flow of a liquid with dispersed crystals. The pressure drop associated with the interdendritic flow increases rapidly with decreasing fraction ofliquid."

Jan 1, 1999

By D. K. Dysinger

The U.S. Bureau of Mines investigated leaching of chalcopyrite with sulfuric acid-oxygen under conditions anticipated during in situ leaching. A central composite experimental design was chosen to study oxygen pressures of 150, 300, and 450 psi, leach temperatures of 35?, 65°, and 95° C, oxygen-to-chalcopyrite mass ratios of 0.5, 1.0, and 1.5, leach times of 8, 16, and 24 hours, initial acid strengths of 0.6, 1.2, and 1.8 g H2SO4/g chalcopyrite and pyrite to chalcopyrite mass ratios of 0, 1, and 2. The leaching kinetics were consistent with the shrinking core model. A quadratic response surface model was used to determine linear and interaction effects of the design factors on rate constants from Arrhenius correlations.

Jan 1, 1993

By Yasumasa Hattori

An extensive study including fluid dynamic calculations, cold model tests, pilot plant tests as well as measurements in a commercial flash furnace was carried out in order to develop a new Sumitomo flash smelting concentrate burner. The pressure measurements in the commercial burner indicated that the premixing of the concentrate and reaction air in a burner was insufficient. Pilot plant tests showed that enhancement of the premixing of the concentrate and reaction air is very effective for improving the burner performance. Using the additional pressure drop of the reaction air as an indicator of the premixing, a new type Sumitomo premixed concentrate burner was developed.

Jan 1, 2003