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US 4,181,520 - Direct reduction of iron oxide ore to sponge iron in a rotary kiln. Ore is fed into the kiln along with coal briquettes and passed through a preheating zone and then a reducing zone countercurrent to the flow of a kiln atmosphere which includes air or other oxygen-containing gas. The agglomerated coal is heated at such a rate that it disintegrates into fine particles in the preheating zone. The coal is largely recovered for reuse, while reduction is effected with a reducing flame rather than the coal. G. Reuter and W. Schnabel, assigned to Metallgesellschaft AG. Jan. 1, 1980. 6 pp. (75-36). Filed- 10-19-78 (952,870). Priority: West Germany, 1-14-75 (2,501,182). Same: British 1,532,969, dated Nov 22, 1978.

Jan 1, 1982

US 4,190,434 - In the thermal production of magnesium metal, a mixture of calcined dolomite, an iron- silicon-aluminum alloy as a reductant, and residual slag from the production of ferrochromium is smelted to evolve magnesium vapor, which is then condensed. The use of bauxite is lessened or eliminated because of the relatively high alumina content of the residual slag. R. Bonfils, A. Mena, C. Payn, and L. Septier, assigned to Ste. Francaise d’Electrometallurgie (SOFREM). Feb. 26, 1980. 6 pp. (75-10R). Filed: 6-14-78 (915,387). Priority: France, 6-24-77 (77/20,227).

Jan 1, 1982

By T. R. Curr, R. T. Jones

Keywords: Pyrometallurgy, Mintek, DC arc furnace, plasma, smelting, chromite, ilmenite, cobalt, slag, zinc fuming, dust, magnesium, laterite, ferronickel, arc modelling, Pyrosim, thermodynamics The Pyrometallurgy discipline at Mintek was initiated in the early 1970s, to support a growing ferroalloy industry in South Africa. In addition to a range of pyrometallurgical options, Mintek specialises in DC arc furnace technology and has pilot plant facilities up to 5.6 MVA, as well as a strong base in process and arc modelling. Industrial processes have been developed for ferrochromium production, ilmenite smelting, and cobalt recovery from slag. Recent work has been done on such processes as the production of ferronickel from laterite ores, the fuming and condensation of magnesium, and the recovery of platinum group metals from 'difficult' feedstocks.

Jan 1, 2006

By U. M. J. Boin, E. V. Verhoef

Pyrometallurgical reactors constitute a key processing component in the total primary and industrial/recycling resource cycle, being involved both in primary smelting, converting and extraction, as well as the reprocessing of scrap, from aluminium cans to end-of-life automobiles. Therefore the pyrometallurgical reactor?s role in achieving sustainability is the central theme discussed in this paper since optimising their operation minimises waste, residue and offgas (NOx, dioxin, CO2) and maximises product quality and therefore efficiency. To effectively control the overall resource cycle, one needs to take a systems modelling approach of the whole cycle, seeking to also understand the dynamic process behaviour of the individual components of the cycle, and then especially the part that contributes most to the chemical conversion, namely the pyrometallurgical reactor. This paper highlights the role of pyrometallurgical thermodynamics in the whole resource cycle and specifically places equilibrium thermochemistry in the context of process dynamics where large, variable inventories are recycled or maintained within the system. This paper will therefore review the semi-empirical dynamic modelling tools, which are used to model complex systems with the specific goal of developing dynamic predictive models, which also include slag-alloy chemistry, towards controlling the recycling in a feed forward manner. To illustrate the primary production of metals, high carbon ferrochrome and Ni-Cu-matte smelting will be presented as a brief case study. Also fundamental studies in blast furnace and waste incineration kilns will be given. It also will show how the distributed nature of the chemistry of melts in the case of primary extraction, and industrial (recycling) materials such as recycled end-of-life vehicles, have a significant impact on the process outcomes and model predictions. It is therefore argued that the fundamental thermodynamics and kinetics in metallurgical reactors play a final crucial role in modelling the closed material cycle, but only when it is used in conjunction with process systems theory based on reconciled data for parameter estimation and model calibration. System models for aluminium and car recycling will be given as well as a dynamical system model that describes the interconnected material flows for Ag, Au, Bi, Cu, Fe, Ni, Pb, PGM, Sn and Zn for a study on lead-free solder.

Jan 1, 2003

By Norman E. Lehman

INTRODUCTION The Washington Camp - Duquesne mining district is located on the east flank of the Patagonia Mountains, 98 kilometers south of Tucson and within 5 kilometers of the International border (Figure 1). Since the development of high-grade silver and copper ores by settlers in 1862, the Washington Camp - Duquesne district has yielded an estimated 450,000 metric tons of ore. The mined ores averaged 8% zinc, 2% copper, 3% lead and 124 grams of silver. REGIONAL GEOLOGY The Patagonia batholith, of Laramide age, crops out in the core of the Patagonia Mountains intruding Precambrian granite, Paleozoic sediments and Mesozoic igneous, volcanic and clastic rocks. This granodioritic batholith lies in a northwest-trending zone of Laramide plutonic rocks, which can be traced for a distance of 320 kilometers from the Nacozari district in Sonora, Mexico to the Silver Bell Mountains west of Tucson, Arizona. Several major porphyry copper systems occur within this plutonic belt including the Red Mountain deposit found at the northern end of the Patagonia Mountains. Data from more than 80 mineral deposits within the Patagonia Mountains show metal zoning symmetrical to the Patagonia granodiorite (Graybeal, 1975). Disseminated copper-molybdenum deposits occur within the batholith. Pyrometa-somatic, limestone replacement and vein deposits of copper, lead, zinc and silver occur in the wallrocks adjacent to the. granodiorite and epithermal manganese-silver deposits occur at the outer periphery of economic mineralization. GEOLOGY OF THE WASHINGTON CAMP - DUQUESNE DISTRICT Stratigraphy Nearly 900 meters of miogeosynclinal Permian and Pennsylvanian sediments are exposed in the district (Figure 2). In addition, 700 meters of older Paleozoic rocks crop out 6 kilometers north of the district. The Paleozoic rocks occur in fault contact with a sequence of Triassic-Jurassic pyroclastic and flow rocks, ranging in composition from latite to rhyolite.

Jan 1, 1977

By Norman E. Lehman

Pyrometasomalic mineralization occurs within meta-morphosed Paleozoic carbonates intruded by Laramide granodiorites. Two types of alteration developed shams in the district. The dominant type is post-magmatic which developed an early hydrous endoskarn phase, and intermediate anhydrous exoskarn phase, and a late hydrous phase affecting both sham types. A rare, second type is magmatic in age, lacks the hydrous phases, and developed a mineralogically-zoned endoskarn. Garnet exoskarns lacking associated plutonic rocks are stratigraphically controlled and contain an early anhydrous phase, an intermediate hydroxyl-bearing phase, and a late hydrous phase associated with base metal deposition.

Jan 1, 1981

By R. W. Newcomb

THE constancy of calibration, and to a great extent the life, of a thermoelement is dependent on the suitability of the primary protecting tube in which the wires are mounted, particularly when used at high temperatures. An ideal thermocouple protecting tube would be com-posed of materials that would not contaminate the thermoelement wires contained in it-one that would remain absolutely gas-tight ,it all temperatures of usage, that will not be attacked by gases, or other surrounding agencies, that is not destroyed by heat, that withstands sudden and extreme temperature changes, that affords a high degree of mechanical protection and does not deform at high temperatures, that is a good heat conductor and obtainable in small diameters so as to keep down lag factors. It has not yet been possible to produce tubes of any known mate-rials that will meet all of these conditions. In selecting protecting tubes, therefore, one should be chosen the characteristics of which best fit it to the particular conditions of usage. Frequently conditions are such that two tubes have to be used, a primary gas-tight protecting tube inside of a secondary protecting tube, because certain agencies will attack the primary gas-tight tube unless it is guarded by the outside tube.

Jan 9, 1919

A. 0. ASHMAN, Palmerton, Pa. (written discussion *.).-Mr. Newcomb's paper has interested me greatly, as I have had numerous experiences along this line. I do not think enough emphasis can be put on his warn-ing to keep platinum couples free from contact with quartz tubes, as silica shows a tendency to alloy with platinum to a surprising degree even at low temperatures. I have frequently had evidence of silica contamination in a perfectly good tube, in which there was seemingly no possibility of a reducing atmosphere. This is rather important as it seems to be common practice to insulate, as well as protect, the wires by means of- capillary silica tubing, thus allowing the entire wire to be in contact with the silica. The best way to mount a couple in a silica protecting tube is by means of double-bore porcelain insulating tubes, the protecting tube being slightly longer than the couple so as to leave a space between the couple and the end of the tube. In this way there is no possibility of contamination from silica. In no case should silica capillary tubes be used to insulate platinum wires. Mr. Newcomb states that there is still much to be desired in pyro-meter protecting tubes; this is in keeping with my experience. From a practical standpoint there is not a satisfactory pyrometer tube on the market for high temperatures; with all clue respect to the many improve-ments and good work recently done in this line. I believe that the whole future development of pyrometry is dependent on the development of suitable refractories. With suitable refractories, for example, Darling's1 work with liquid couples could be developed to a practical basis, making possible the use of base-metal couples to replace platinum.

Jan 12, 1919

By F. A. Harvey

DURING the last few years, there has been a constant tendency toward increasingly high temperatures in many lines of industry. The necessity for increased production of coke gave a 16-hr. coking period where we used to have 24 or even 30-hr. periods. Mechanical stokers have increased the temperatures in boiler furnaces. The use of a chain-grate stoker with coke-breeze fuel necessitates a low arch in the furnace and temperatures run much higher than firebrick were formerly called upon to stand. These higher temperatures have necessitated more rigid tests and the separation of even high-grade firebrick into separate classes. More severe tests mean higher temperatures and closer control, and this, in turn, means better pyrometer tubes. Platinum couples do not have a very long life when used at temperatures exceeding, say, 1200° C., but the proper selection of a high-grade brick to be used in a-boiler setting will save the cost of several couples; and with freight rates continually increasing it becomes increasingly important to know where brick may be bought, nearest the job, that will prove satisfactory. Couples that will stand continuous use at higher temperatures, of tungsten, molybdenum, or other metal, will doubtless be forthcoming as soon as the need becomes sufficiently urgent. There are on the market several tubes that are entirely satisfactory for temperatures up to 1300° C., if properly protected from heat shock. The Semet-Solvay Co. makes a practice, however, of testing silica and clay firebricks at 1450° C. for 72 hr., and so far we have been unable to find a tube that- is entirely satisfactory for this purpose. A graphic record of the temperature during the entire test is extremely desirable and hence we have been trying out anything that gave promise of success. Several years ago we were using insulating tubes, made purely for electrical work, of vitrified porcelain. These tubes stood up under any temperature we were able to reach and were apparently impervious to gases. When this stock gave out, due to mechanical breakage, we tried other insulation tubes only to have them melt down like glass. Marquardt Masse tubes were tried next under a statement from the distributors

Jan 9, 1919

By Otis Hutchins

IT is intended to discuss in this paper the protection appliances used for high-temperature pyrometer installations involving the use of platinum couples and describe some of the characteristics of a new carborundum protection tube. Of all the components that go to make a complete pyrometer installation, the one given the least attention and the one about which there is the least exact information is the outer protection tube. This condition is unfortunate as much, and in some cases even the success of the equipment as a whole, depends on the proper type of protection. In the majority of cases, the installation is allowed to operate without attention until some part of the apparatus breaks clown. The outer tube is the component that usually fails and, more often than not, the failure causes breakage of the porcelain protection and ruin of the couple. This condition should be recognized and studied as it has a very important bearing upon the upkeep cost of pyrometer equipment. The cost of the outer protection tube is small compared with the cost of the platinum couple and procelain protection and it would well repay users of this type of equipment to replace their outer protection tubes at certain definite periods, which experience shows is necessary to prevent destruction of the platinum. Speaking generally, platinum thermocouple equipment is used for measuring temperatures over 2000° F. (1094° C.), and is used extensively for the control of brick and pipe kilns, glass pot furnaces, glass tank furnaces, heat-treating furnaces, open-hearth furnaces, and forge furnaces. A satisfactory protection tube must be sufficiently refractory not to soften at the maximum temperature within the furnace. It must be resistant to cracking clue to temperature changes, should be as nearly gas-tight as possible, and should be made of a material with a high thermal conductivity and great resistance toward erosion by the furnace atmosphere.

Jan 9, 1919

By W. M. Clark

OUR interest in the matter of pyrometers and pyrometry is primarily that of a user of considerable quantities of heat-measuring equipment; and while we play be somewhat critical on the subject we have aimed to make the nature of these comments constructive. The glass industry in America dates back to 1609, when Capt. John Smith started a small glass plant near Jamestown, Va., with a few Italian workmen, to manufacture glass beads for trading with the Indians. While the industry has expanded until it has reached a volume of over $200,000,000 per annum, the means of heat determination in Colonial days was the human eye, and in much of the industry the same means is used today. About 15 yr. ago the largest glass-house supply dealers began to sell platinum pyrometers, but as nearly all of these proved un-satisfactory, pyrometers met a temporary rebuff from the old-time glass manufacturers. As their ruggedness of construction, reliability, and stability have been improved, however, pyrometers have gradually won their way into more and more extensive use throughout the glass trade. But there are still many applications where pyrometers are not used, largely because of cost and upkeep considerations. There are two distinct fields in glass works for pyrometry. The first calls for accurate temperature measurement and the second only demands knowledge of relative comparative fluctuations of temperature, to know whether the work is becoming hotter or colder. For example, in a lehr for annealing glassware and removing strain we want accurate temperatures to know that the ware is heated to the critical temperature for rapid removal of strain. On the other hand, in a glass pot furnace nearly 120 ft. (36 m.) in circumference, where the pyrometer couples only project inside the furnace wall for less than 2 in. (50 mm.), it is inconceivable that these few inches represent the accurate temperature at every point of the 120-ft. circumference but the relative readings as to whether the pyrometer shows schedule temperature fluctuations are valuable indications for control. The glass melting in the pots is,

Jan 8, 1919

By J. R. Wynnyckyj, R. Marr

Continuous measurement based on radiation pyrometry has often met with difficulties whose causes have been obscure. In this paper the experience gained with on-line pyrometry in utility and Kraft recovery boilers in the range 800-l400oC will be reported. It is shown that the inherent problems are best resolved by using a spectral pyrometer not sensitive to gas radiation. The radiation from the suspended particles thus provides the signal. It is further shown that the principle cause of difficulties is signal calibration drift caused by heat fluxes originating from surrounding surfaces and reflected by the particles to the pyrometer. Several examples are given how such problems may be resolved using process information and/or additional measurements, fed to and processed by and on-line microcomputer.

Jan 1, 1989

By A. H. Miller

TEMPERATURE considerations are of prime importance in the manufacture of steel products-front the time the metal is produced in the melting furnace, where the chemical reactions have a direct dependence on the temperatures of the bath, to the final machining of work on which the expansion due to the rise in temperature of the forgings during machining must be allowed for. Methods employed and difficulties encountered in some of the more important steps are here outlined. These methods are the result of years of experience, with many methods of temperature determination, and have been successful in routine works practice in the manufacture of high-quality steels. In the operations of melting, forging, and heat treatment, if the product is to be of the best quality each operation must be carefully followed through. A high-quality product cannot be obtained even with the best heat treatment if the steel is poorly melted, and, conversely, the best steel ever made may he spoiled by inefficient heat treatment. To perform the best work in any of these operations, temperatures must be accurately regulated.

Jan 8, 1919

By R. L. Frink

I FEAR that my treatment of this subject may not, in all instances, meet the approval of those who read my opinion as to the utility and efficiency of pyrometers in the making of glass, or bottle-glass. It may be superfluous for me to add that this opening statement is based on over 15 years' experience in an endeavor to successfully apply pyrometers, or heat-measuring instruments, to glass-melting furnaces, particularly the type known as tank-furnaces, and that such endeavors have proved more or less futile. It is my desire, therefore, to herein set forth the problems encountered, hoping thereby to stimulate further effort in the successful application of pyrometers. It is my desire, also, to invite criticism of the methods used and suggestions from those who may have a wider experience, or who may have better methods. Fin. 1.-GLASS TANK FURNACE. In general, I believe that the inefficient application of pyrometry to the melting of glass in tank furnaces is not due as much to the instruments as to the conditions under which they must be used and the character of the medium in which they must reside. Most of those present no doubt, are familiar, at least in a general way, with the methods and apparatus used in the melting and making of bottle-glass, or glass that is formed into containers of various shapes and designs. Most of this glass is made in what is known as a tank furnace, these furnaces vary widely in design and construction. In general, they consist of a rectangular tank-like form, built up of fireclay blocks, and range from 2 by 4 ft. (0.6 by 1.2 m.) to 24 by 140 ft. (7.3 by 42.6 m.) with a depth of glass from 2 to 5 ft.; or a capacity of from approximately. 2 to 700 tons. Fig. 1 shows the general

Jan 9, 1919

By Carl Keuffel

THE manufacture of optical glass is a new industry in this country. In 1914, after the war started, the supply of optical glass from Europe was cut off, but as there was a fairly large stock of glass on hand, it was not until the end of 1915 that the optical instrument makers made serious efforts to produce their own glass. These early attempts were generally made by practical glass men and, due primarily to the fact that very little scientific help was used, the first attempts were unsuccessful. It was not until the whole problem was attacked by technically trained men who used advanced methods of research that good results were obtained. These researches proved that the accurate control of the temperature was a most important factor in the manufacture of optical glass. The early glass maker judged temperatures with his eyes; later, Seger cones were introduced into the furnace at various stages of the melt. Then radiation, indicating and recording pyrometers with rare-metal thermocouples were introduced. Now, in addition to these, an optical pyrometer every hour or so is sighted right into the pot and on the molten glass. Figs. 1 and 2 show how pyrometers are used to control the melt. InFig. 2, Y is the clay pot in which the batch is melted to glass within the furnace X. The rare-metal thermocouple S, protected by a clay tube, extends through the wall and about 4 in. into the furnace. This couple is connected to an indicator T and a recorder U so that a complete record of the furnace temperatures is obtained. The section of the curve ABCD, Fig. 1, shows how gradually and carefully the clay pot must be heated to get rid of moisture AB and during the calcining at CD. The stem of an expansion pyrometer R is extended through a hole in the door Z of the furnace and into the pot in order to more closely follow the temperatures of the clay pot itself during the burning process, that is from A to D. After the pot is calcined, the temperature can be rapidly raised to E (about 1430° C.); from E to F this temperature is much higher

Jan 9, 1919

By Robert B. Sosman

THE relative temperature distribution within a coke oven and among the ovens in a battery can be obtained automatically for the operator's guidance by sighting a total-radiation pyrometer on the face of the coke as it is pushed out, and recording the surface temperature. Keeping the instrument clean and keeping its view of the coke unobstructed by smoke and dust are the principal problems. Typical records from three plants are presented in this paper, showing that the temperature patterns are reproducible. DEVELOPMENT OF METHOD The method of coke pyrometry described in this paper was introduced in 1936 by E. A. Lee, then Assistant Superintendent, now Superintendent, of the Coke Plant at Lorain Works, National Tube Co., Lorain, Ohio. At the request of the Coke Committee of the United States Steel Corporation, the Research Laboratory of the Corporation undertook to adapt the method to the somewhat different conditions met with at the Gary Works of the Carnegie-Illinois Steel Corporation, Gary, Ind., and at the Clairton Works of the same Corporation at Clairton, Pa. This work was done in cooperation with the Leeds and Northrup Co. of Philadelphia and later with the Brown Instrument Co. Division of Minneapolis-Honeywell Regulator Co., Philadelphia. We of the Research Laboratory wish to express our appreciation of the courtesies extended by Mr. Lee, by A. N. Cole, Superintendent of the Gary coke plant, and by D. P. Finney, Assistant General Superintendent in charge of coke-plant operations at Clairton. We are also indebted to the instrument companies for the loan of a part of the equipment. At Gary and Clairton the instruments were installed and various experiments were made by J. W. Bain, of the Research Laboratory of the United States Steel Corporation. PYROMETRY OF COKE The coke inside a by-product oven is almost completely inaccessible to pyrometric instruments. The temperature in the walls can conceivably be measured with thermocouples, but the atmosphere is usually strongly reducing, a condition well known to be destructive to the accuracy of the customary high-temperature couples. In some plants, periodic readings are taken with an optical pyrometer sighted into the top of the combustion flues. This is a useful measure for safety and general control, as it tends to prevent the damage that would result from overheating of the ovens. It does not, however, tell much about the temperature of the coke itself, because of the continually changing gradient in the wall between the coke and the combustion chamber. The best indication of the temperature of the coke itself must therefore be obtained by observation of the product as it is pushed out of the oven. The human eye is very sensitive to variations in brightness of a surface, and particularly to differences in brightness over a continuous hot surface.

Jan 1, 1942

By P. H. Royster

For a number of years the Bureau of Mines has been investigating certain problems relating to the blast furnace. In the course of these investigations it was desirable to measure, with the optical pyrometer, the temperatures occurring in the hearth of the furnace. Since no systematic measurements of these temperatures have been published a statement of the results may be of interest. The data given in this paper were obtained it thirty-two blast furnaces operated by seventeen companies; twenty of these furnaces were making iron, eight ferromanganese, and five spiegeleisen. The collection of this information was made possible by the cooperation of the American Manganese Co., Bethlehem Steel Corpn., Brier Hill Steel Co., Buffalo Union Furnace Co., Clinton Iron & Steel Co., Donner Steel Co., John B. Guernsey & Co., Jones & Laughlin Steel Co., E. E. Marshall, the McKinney Steel Co., National Tube Co., New Jersey Zinc Co., Republic Iron & Steel Co., Seaboard Steel & Manganese Corpn., Southeastern Iron Corpn., the Youngstown Sheet & Tube Co., and the Wharton Steel Co.

Jan 9, 1919

A. L. FIELD, Cleveland, Ohio (written discussion*.-)In equation 2, B is used to denote the ratio of bases (lime plus magnesia ) to acids (alumina plus silica) it being stated that this ratio gives more concordant results than the ratio either of bases to silica, or of lime to silica. I find, however, that, by making use of the ratio between true CaO (CaO by analysis minus sulfur calculated to CaS) to acids, equation 2 may he modified to agree with the observed facts within an average error of 0.0041 per cent. sulfur instead of 0.0045 per cent. The revised equation is s = 0.072 + 0.01835 - 0.00061 (t - 1400) - 0.0403B where B is the ratio of true CaO to Al2O3 Plus Si02, and the other symbols have the same significance as before. I would not appear to stress too much this slightly better agreement of the revised equation with the observed sulfur. Yet I believe that the use of this ratio of true CaO to acids is to be preferred, if for no other reason than the fact that it is more in harmony with the previous findings of the Bureau of Mines with regard to the effect of magnesia and other impurities on slag viscosity.1

Jan 12, 1919

By Leo Dana

As a part of an investigation conducted by the Cement Section of the Bureau of Standards, at the plant of the Security Cement & Lime Co., Security, Md., the High-temperature Measurements Section was called upon to measure temperatures in a dry-process, coal-burning kiln. Although the measurements were made only under the conditions existing in one plant, the methods employed and the conclusions drawn apply, in a general way, to those existing in most plants. As far as we have been able to learn, no sufficiently thorough methods of making accurate pyrometric measurements in the sintering zone and in the rear end of rotary cement kilns have been described. It is believed that in this investigation, data were obtained that can serve as a foundation for further study of the problems of pyrometry in cement kilns. IMPORTANCE OF TEMPERATURE MEASUREMENTS IN ROTARY CEMENT KILNS The manufacture of Portland cement is today fairly well standardized. The various steps in the manufacture have been developed to such an extent that the process is almost automatic. In spite of these strides the efficiency of utilization of heat in the kiln is very low and an undue proportion is wasted; for example, about 50 per cent; ordinarily goes up the stack. In order to prevent these losses, not only should means be provided to utilize the waste heat but instruments, such as pyrometers, should be installed to study and control the operation with the view of minimizing the losses. At the same time, such control will produce a more uniform product. The saving in-fuel that may be effected by the proper use of pyrometers would be much more than their cost. Where these pyrometers should be installed and what they can show are very briefly indicated in the following paragraphs and discussed in greater detail later.

Jan 9, 1919

FRANCIS T. OMENS, ? Watsontown, Pa. (written discussion§).-In the second paragraph, Dr. Thwing mentions the various stages through which clay ware. must pass but he does not analyze the third stage, oxidation, suffficiently. There are two elements to dispose of in a great many, of the shales that must he burned; these elements are carbon and sulfur. Dr. Thwing speaks' of the carbon, but intimates that it is safe to have a temperature of -800° C., which we find to be rather dangerous on a great tiffany shales. With. one shale that we handle, we cannot go above 535° C. until we have passed this particular stage. At 800° C. the sulfur will begin-to pass off and it is very necessary that plenty of air be ad-

Jan 11, 1919