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By See J. B

The zinc-nickel alloy process, TECHNIGALVA, was developed for the control of the thicknesses of zinc -coatings on reactive silicon-killed steels. These are steels containing between 0.04 and 0.15 per cent silicon which have become more common in recent years as more steel is produced by continuous casting. The introduction to this paper will review the current status of this process in Europe, North America and Australasia. It is well known that the presence of silicon at certain levels in steel can cause sufficient growth of intermetallic phases during galvanising to form a grey coating of excessive thickness. This type of coating is undesirable because it is brittle and has poor adhesion to the steel base. Since the early-1980s a widely accepted practice for suppressing the reactivity of steels containing silicon during general galvanising has been the addition of approximately 0.1 mass per cent nickel to the galvanising bath ie the TECHNIGALVA process. The paper will also discuss metallurgical aspects of the use of nickel in galvanising such as the mechanisms by which nickel suppresses reactivity, the structure and composition of the ternary Zn-Fe-Ni drosses formed when using nickel and the use of nickel in the galvanising bath at a level of about 500 ppm to give thinner, smoother and brighter coatings on steel.

Jan 1, 1993

By C. Cortés

Flotation is a highly interactive process where a change or disturbance in any part of the circuit results in different final grades and recoveries. This high variability of the circuit metallurgical performance complicates the diagnosis of the scavenger stage at the end of the line, as copper losses in the final tailings are erratic and not totally a consequence of problems in the scavenger section. The assessment of the scavenger performance requires a more elaborated procedure than that used for others stages of the circuit. This communication describes the application of an approach that combines results of laboratory flotation tests with those of surveys performed at the plant. The approach is based on running surveys in one of the circuit lines to collect samples for determining grade vs. recovery curves for total mass and size-by-size fractions. Full mineralogical and liberation analyses are also considered on some samples of the feed and tailings streams selected to have a range of feed grades. A separate sample of the feed is used to run laboratory flotation tests to determine optimum flotation time. Two additional pieces of information are the effect of operating variables on recovery, determined through a test program based on design of experiment techniques, and operational data on every cell in the line gathered by visual observation. The application of this approach to one of the scavenger lines at Los Colorados concentrator (Minera Escondida, BHP Billiton) is demonstrated.

Jan 1, 2007

By V. H. Valenzuela

Materials in process or in stocks are quite relevant items in almost every plant, particularly in mining operations, where efficiency in rate of recovering material of interest becomes a key issue when production costs are evaluated. A manager requires information to do an effective use of the resources, especially when raw materials are involved. Losses associated to leaking, efficiency in the transformation process, performance of equipment, and operating conditions are a short list of items which must be properly identified and evaluated. Operations supervisors require information in order to keep key process variables under control. Because of these information needs, it is absolutely necessary to carry on a series of activities related with installation and maintenance of measuring equipment, sampling equipment, sample preparation, chemical analysis, statistical analysis, data handling and reports generation. These pieces of data must be managed on a wise manner in order to get the most of it, keeping always on mind data reliability. Normally, information related with metallurgical balance and even more, the metallurgical balance concept, is handled under an accounting criteria which does not allow dealing with the real world. This situation happens because the criteria utilized do not consider aspects such as bias and uncertainty associated with every measurement that affect the quality of the information and therefore conclusions drawn from it. The purpose of this paper is to give a few rules, necessary to follow, in order to develop an adequate Metallurgical Balance System for an operational point of view. The Gaussian approach for error propagation is used as a basis, allowing one to know the actual uncertainty of the balance and the way how it can be improved. A few real applications of this concept are listed, detailing experiences obtained from practice.

Jan 1, 2007

By J. M. Richardson, A. L. Mular

Metallurgical balances are fundamental to the successful design and operation of concentration and dewatering circuits. With computerized balance techniques gaining prominence in recent years, it is essential that engineers understand the basic principles that underlie the new methods, as well as the various applications for design of new plants and analysis of existing operations. This chapter discusses two important types of metallurgical balance: (1) steady-state design (2) operating data adjustment Application of computerized steady- state design balancing is demonstrated through the example of a typical copper concentrator flowsheet. Operating data adjustment to achieve a consistent balance is demonstrated for a typical concentrator operation.

Jan 1, 1986

By L. Joncourt, N. Touchard, G. Pochart, C. Perdon

Worldwide, the major Manganese ores can be separated into three different types: ?Oxidized ores (MnO2): in Australia, Gabon, Brazil,?. ?Semi-oxidized ores (Mn2O3): in South-Africa, Australia,?. ?Carbonated ore (MnCO3): in Ghana, South Africa, Kazhakstan?. The other Manganese ores are less rich but can be used locally or in the neighbour countries (China, Ukraina, India?). Since the beginning of the 20th Century, Manganese has played a big role in the steel industry process average usage ratio: 9,5 kg/mt of steel). The recent grow-up of this industry has led to an increase of Manganese ores demand. In parallel, several companies have increased their Manganese ore producing capacity. In this presentation, we explain the link between the main Manganese ores characteristics and the key different factors for an effective and low cost Mn alloys production (HCFeMn and SiMn): ?Chemistry ?Size ?Reactivity Then we will point out the advantages of Comilog ore and Sintec ® usages in various Manganese alloy metallurgical process compared with the other main ores and with the local ores. Some advised formulations for the different kinds of furnaces and alloys will be also discussed.

Jan 1, 2007

By Norbert Patzelt, Johann Knecht, Wolfgang Baum

High pressure roll grinding (HPGR) is a mature but still expanding comminution technology. In the metals mining industry, HPGR is slowly gaining acceptance as a cost-efficient, high-throughput alternative for plant optimization. The increasing need to treat ores with progressively lower grades, complex mineralogies, refractory metal occurrence and variable rock types requires an energy-efficient comminution technology that reduces metallurgical problems inherent in conventional crushing and grinding, while stabilizing leach and flotation circuits and increasing metals extraction. This paper will summarize our latest HPGR pilot test results for gold and copper projects in the United States and South America and their confirmation through the first HPGR operation in copper mining. This paper will also stress the use of the high pressure grinding roll as a metallurgical tool. The application of HPGR for the treatment of heap leach SX-EW ores, semi-refractory gold ores, waste rock material and concentrator feeds will be illustrated.

Jan 1, 1998

By I. Baltov

The Chelopech Mine, located in Central Bulgaria, is one of Europe?s largest underground copper- gold mines, currently mines and processes approximately one million tonnes of ore per year. Copper concentrates containing gold and silver with significant arsenic content are produced and sold on the world markets. The operation was acquired by Dundee Precious Metals in 2003. A modernization program for the Mine and Plant has since been in progress to increase both production and mechanical reliability, and also to optimize metallurgical recoveries. Since then, mine output and plant throughput have doubled, plant availabilities and utilization have increased significantly, and overall metallurgical performance for copper and gold improved. The paper presents the systematic approach for obtaining and analyzing data, communicating it, and making suggestions for changes to the technological parameters and flowsheet in order to maximize metal recoveries. These studies have correlated the ore characteristics (particle size distributions, metal assays, and Cu and Au mineralogical and phase analyses) with the actual plant performance (kinetics, recoveries, and throughput). Cu recovery by size has been calculated from the mineralogical analyses of feed, concentrate and tails, with the most significant losses being identified in terms of fraction and phase recoveries. This has provided the recommendations (some of them tested in plant) for changes in the grinding and flotation circuits.

Jan 1, 2014

By Vink L, Johnson N. W, Mackenzie J, Young M. F, Johnston M, Landmark V

The influence of ore textures on metallurgical behaviour is poorly understood for most ores. An alternative method for characterising ore textures and for determining the resulting implications on ore processing has been developed for the Geor

Jan 1, 1998

By J. Alexis, G. Ye, E. Burström

Over the past twenty years the 3 MW DC arc furnace at MEFOS has been frequently used for development of new processes. These processes include recovery of valuable metals from slag, sludge and dust from steel and other metallurgical industry, treatment of ashes from power plant and incinerators, smelting reduction of minerals and zinc recovery from EAF dust. The process characteristics of the DC arc furnace operation in terms of: ? selective reduction, ? total reduction, ? process stability and flexibility, ? dust carry-over, ? thermodynamic conditions provided in the hot spot area, ? precision in composing slag products These are analysed and described in this paper based on technical results from selected test campaigns over the years and thermodynamic considerations. The electromagnetic properties of DC arcs beneath the electrode have been studied by CFD simulation. The calculated result enables us to understand some interesting technical phenomena observed. The heat balance has also been considered based on data obtained from test campaigns and heat balance calculation.

Jan 1, 2004

By F. Henríquez, V. Iriarte, L. Vinnett, J. Yianatos, F. Díaz

Metallurgical characterizations of the collective (Cu/Mo) and selective flotation plants were carried out in Minera Los Pelambres, Chile. The selective plant allows the valuable minerals of Cu and Mo to be separated. The evaluation involved two surveys consisting of metallurgical sampling as well as residence time distribution (RTD) measurements to determine load distribution. The RTD data were obtained in real-time by means of the radioactive tracer technique. In addition, metallurgical data was reconciled and supported by effective residence times. In the collective plant, a performance comparison of parallel rougher circuits was carried out, which included a bank of six mechanical cells of 250 m3 and banks of nine mechanical cells of 130 m3. In the selective plant, the Cu and Mo evolution along the plant was evaluated. The results in the selective plant allowed for performance evaluation of mechanical and pneumatic cells in primary flotation. In both plants, mineral losses were evaluated and their relationship with circuit configuration (cell types and circuit layout) was determined. The metallurgical characterization was a powerful tool to evaluate circuit performance and to detect improvement opportunities at industrial scale.

Jan 1, 2015

By C. Carreno, A. D. Gonzalez Escarcega, M. A. Neri, A. Martinez –Villafane, O. Cobarrubias-Alvarado

"Waspaloy is a superalloy used to manufacture some aeronautical parts subjected to high temperatures and stresses. During thermo-mechanical processing cracks are generated, causing some parts to be rejected. In order to determine the causes of these cracks, this alloy was characterized using techniques such as chemical analysis, optical microscopy, scanning electron microscopy, and EDX analysis. Heterogeneous grain sizes in the microstructure cause a non-uniform strain distribution in these parts, creating cracks in zones with different grain sizes.IntroductionNickel-base superalloys are important materials for high-temperature service applications. The manufacture of components from these materials is typically based on solidification or powder-metallurgy processes [1]. Solidification techniques comprise either the direct casting of parts or the casting of ingots which subsequently undergo a series of thermo-mechanical-processing steps to refine the microstructure. During solidification, microsegregation is usually unavoidable. The primary solidification product is a disordered nickel solid solution with an fee crystal structure (?). In many alloys, the material which solidifies last is a mixture of ã and an ordered fee phase (? '). In prototypical nickel-base superalloys, the ?'-phase is Ni3(Al,Ti) [2-3].Waspaloy is a superalloy that is used in demanding high-temperature environments in which good creep and fatigue resistance are required. One of the most common applications of Waspaloy is for turbine engine rings. To ensure the required mechanical properties, the rings are usually forged and heat treated (Figure 1). Two distinct types of microstructures are usually found to be attractive for such applications: a) A microstructure with a grain size of ASTM 10 to 14 for tensile strength, ductility, and resistance to crack nucleation in low-cycle fatigue; or b) A microstructure with a grain size of ASTM 4 to 8 required for creep strength and resistance to crack propagation [4]. Because it is impossible to refine the grain size through heat treatment, a skillfully designed forging process is crucial for the control of the grain size and, hence the properties of the forged ring [5-6]."

Jan 1, 2012

By J. S. Wozek

In metallurgical applications, coal fulfills dual roles as a chemical feed stock and as a fuel source. These applications range from cokemaking, ironrnaking (including pulverized coal injection), foundry, basic oxygen furnace / electric arc furnace coal additions, direct ironrnaking, Corex, and the futuristic direct steelmaking. In all steelmaking related processes, chemical reactions are simultaneously temperature and chemical dependent. Therefore, coals used in these processes must consistently comply with specific quality parameters in order to promote efficient operations. This paper limits discussion of Metallurgical Coal Quality to cokemaking and ironmaking applications. Its purpose is to present the customer's perspective on the control of critical coal and coke properties.

Jan 1, 1994

By A. D. Fisher

This paper describes the future position of metallurgical coal, particularly as applied to Canadian reserves. Quality coking coal is declining in availability, but preheating practices may alleviate this situation to some extent. Two new processes are discussed in the paper - formed coke and direct reduction - and their coal specifications are outlined.

Jan 1, 1972

By E. J. Burrough

Coal Reserves The Crowsnest Pass coal fields form part of a greater area which comprises the Inner Foothills belt of the Alberta coal fields and the southeastern coal fields of British Columbia. The most valuable and most extensive reserves of the bituminous coals of Canada are concentrated in this?area, of which the Crowsnest Pass fields form an important part. The extent of these coal reserves together with those of the rest of Canada were recently studied by the Geological Survey of Canada for the Royal Commission on Coal of 1946 (1). Quotin from the report, it is of interest to note that, prior to this work, the most widely known, and in fact the only Canadian-wide estimates of, coal reserves of Canada available to the Commission were those prepared by Dr. Dowling in 1913 (2). At that time it was estimated that Canada's reserves of coal were over twelve hundred billion tons. The more recent estimates of mineable coal for the whole of Canada are of the order of 10 per cent of that figure and are reported. as 99 billion tons, which is further reduced to 40 billion tons on the basis of the estimation of recoverable coal. This considerable divergence in estimated reserves is explained in part by the big difference in the bases of measurements. For example, in the original report, seams of one foot occurring at a depth of 4,000 feet were included in the estimates.

Jan 1, 1951

By E. J. Burrough

MR. J. J. McIntyre (International Coal & Coke Company, Ltd., and McGi1livray Creek Coal & Coke Company, Ltd., Coleman, Alta): Mr. Burrough's excellent paper, Metallurgical Coals of the Crowsnest Area, seems especially timely now, when the need for developing iron industries in the west, as well as in the east, is receiving so much attention. His -thorough review of the 'coking' industry is an especially valuable contribution, along with which the following brief remarks on coking in the Crowsnest Pass area of British Columbia and Alberta may be in order. When the Crowsnest Pass line of the Canadian Pacific railway was built there were great expectations for the non-ferrous metal industry; quite a number of smelter's were al-ready in operation in British Columbia and the northwestern United States, and further expansion was confidently expected. The suitability of the medium-volatile coking coals of the Pass for making metallurgical coke had been recognized from the time the fields were first explored. By the time the mines were fairly well developed there was already a market to war-rant the building of coking plants, and a common belief that expansion of the market would require a large coking industry. The first coke production was from plants built by the Crowsnest Pass Coal Company, Ltd., at Fernie, B.C. in 1903, and the International Coal and Coke Company, Ltd., at Coleman, Alberta. These plants were followed by others built by the Crowsnest Pass Coal Company, at Michel, B.C., by West Canadian Collieries, Ltd., at Lille, Alberta, and by Leitch Collieries, Ltd., at Passburg Alberta, and by a plant at Hosmer, B.C.

Jan 1, 1951

By Wm. Snow, J. R. Wallace, E. P. Duchemin

"GeneralA NOT INCONSIDERABLE proportion of the Canadian economy is dependent on the coal mining industry. This is particularly true of the eastern portion of Canada and especially so of the ( authors') province of Nova Scotia. Much has been said about the trying economic straits of the coal industry in Nova Scotia ( 1), faced, as it is, with difficult mining problems, with considerable distance from large markets, and with •competition from other (and usually foreign) fuels. It is of particular interest, at this time, therefore, to discuss one of the larger outlets for coal -that of the production of metallurgical coke.Scope of PaperWhile the title of this paper indicates that it deals with Metallurgical Coke in Canada, the authors beg leave to treat the Canadian industry very briefly and to deal specifically with coal, •coke, and smelting problems with which they are familiar, namely, the operation of the Dominion Steel and Coal Corporation in the Sydney, N.S., area. No mention is made of metallurgical coke for use in the •many foundries in Canada or in the non-ferrons metallurgical industries.Coal and Coke StatisticsA few statistics of the total output of .Canadian coal, production of metallurgical coke, and similar figures for the Dosco holdings (Sydney area only) are shown in Table I."

Jan 1, 1955

By B. Ignasiak

Laboratory studies suggest that improvements of coke strength brought about by pre-heating caking coals before carbonization accrue from inadvertent oxidation rather than from other low-temperature changes in the coal mass. Controlled oxidation of highly caking coal, followed by laboratory carbonization, produces cokes which, in terms of a laboratory scale tumble test index, are equivalent to those obtained from prime metallurgical blends. Appropriately formulated blends of exhaustively oxidized and fresh caking coal similarly yield cokes with strength indices comparable to those of cokes made from the same coal after oxidation under optimum conditions.

Jan 1, 1979

By Jack S. McPartland, Gene E. McClelland

It is advisable, for any heap leach project, to develop an historical metallurgical data base to predict production heap performance before ore is mined and placed onto the heap. A data base would include results from: interval assays, cyanide solubility tests, and bottle roll tests on exploration drill cuttings samples; and those results plus column leach test data on diamond drill core or bulk ore composites. Subsequent larger scale heap leach test data can then be compared to the historical data base, to blast hole composite data during mining, and eventually to production data. This paper does not discuss metallurgical comparisons between assays, cyanide solubility tests, and bottle roll tests on exploration drill cuttings samples, but does discuss metallurgical comparisons from bottle roll tests, laboratory scale column leach tests, and pilot scale heap leach tests on core and bulk ore samples with operating data for three U.S. commercially producing heap leach operations. Provided that representative core or bulk samples are used for evaluation, heap leach test results accurately predict or understate the success of the commercial operation and remove most of the uncertainty from the investment decision.

Jan 1, 1990

By Fumito Tanaka

The Mitsubishi Process is the sole pyrometallurgical process for the continuous production of blister copper from copper concentrates. Continuous converting originates from the application of the proven technology of a lime-ferrite slag (CaO-FeOX-Cu2O) on the Converting Furnace (C-furnace). Recent improvements on the C-furnace operation have included increasing the processing of recycled materials and the investigation of alternative fluxing agents. However, some minor oxides adversely affect C-furnace operation, with respect to magnetite behavior of the slag, with the most significant impact having been observed with the silica content of the slag. This paper will quantify the impact of silica on the lime-based slag, and discusses the controls that have been identified to sustain continuous converting operation.

Jan 1, 2005

By H. E. Cross

Metallurgical considerations in the automation of gold-recovery plants By H. E. CROSS. Pr. Eng., B.Sc. (Eng.) Hons. (Fellow) The advantages of the automation of gold-recovery plants are examined. The various sections of a gold-recovery plant are analysed, and the extent to which instrumentation can usefully be employed is described. INTRODUCTION The scope of this paper is restricted to the ore-treatment and recovery plants on Witwatersrand gold mines. To extend the field to plants that process base metals and industrial minerals would result in a paper that would be too lengthy. However, the subject matter of this paper is applicable to most mineraldressing and recovery plants and will, it is hoped, be a foundation on which to build somewhat more sophisticated control systems required in the base-metals field.