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By Daniela Barçante Perasoli

O aço inoxidável duplex (AID) representa uma classe importante de aços inoxidáveis, particularmente para aplicações que exigem alta resistência mecânica e à corrosão. Sendo assim, o estudo das propriedades eletroquímicas dos filmes passivos formados em AID tem sido uma contribuição importante para a compreensão do comportamento protetor contra a corrosão. O objetivo deste trabalho é estudar o filme passivo formado no aço 2205 laminado a morno utilizando espectroscopia de impedância eletroquímica, (EIE), em ambiente de íons de cloreto. Para esse propósito, as chapas como fornecidas de AID foram laminadas a morno a 600°C até 60% e 80% de redução na espessura e submetidas aos testes eletroquímicos. O estudo mostra que o tratamento termomecânico utilizado não favoreceu a formação do filme passivo nessas condições e levou a uma menor resistência à polarização. O AID 2205 como fornecido apresentou uma maior resistência à transferência de carga na comparação com as amostras laminadas a morno.

Oct 30, 2017

By Fernanda de Lima Menezes

O biodiesel, obtido a partir de um éster e um álcool na presença de um catalisador, é produzido pela reação de transesterificação e tem como coproduto a glicerina. A produção de biodiesel da Petrobras Biocombustível tem, em uma de suas etapas, a lavagem dos produtos para remoção do catalisador básico, metilato de sódio, por meio da reação de neutralização com ácido clorídrico. Devido a essa prática, a glicerina obtida é acidificada e contêm resíduos de cloretos, o que leva à corrosão localizada dos aços utilizados em determinados pontos do processo de produção. Dessa forma, o presente trabalho avaliou a resistência à corrosão do aço austenítico 317L e do aço lean duplex 2304, em meio de glicerina acidificada contendo cloretos. Todas as medidas foram conduzidas a 64ºC, visando simular as condições de operação da empresa. Para o estudo em questão, utilizou-se as técnicas de potencial de circuito aberto (OCP), polarização potenciodinâmica e microscopia eletrônica de varredura (MEV). As análises mostraram que o aço AISI 317L obteve menor potencial de pite que o SAF 2304, logo foi menos resistente. Por meio do MEV foi possível confirmar a presença dos pites, sendo que as cavidades presentes no aço AISI 317L foram mais numerosas e profundas que as observadas no aço SAF 2304.

Jan 16, 2018

By Alessandra Souza Martins

O aço inoxidável super duplex vem apresentando um desempenho satisfatório em ambientes de maior agressividade. Esse tipo de aço possui boas propriedades de resistência mecânica, resistência à corrosão e tenacidade ao impacto. Entretanto, mesmo apresentando desempenho satisfatório, esses aços podem apresentar problemas de corrosão quando sofrem algum tratamento térmico, devido à precipitação de uma fase deletéria chamada de alfa linha (?’), a qual precipita em temperaturas entre 300°C e 550°C e pode ocasionar uma diminuição da resistência à corrosão e tenacidade do material. Portanto, o objetivo deste trabalho é avaliar a resistência à corrosão dos aços inoxidáveis super duplex de grau 5A e 6A após sofrerem tratamento térmico a 475oC. A diferença entre os aços de grau 5A e 6A ocorre na presença de cobre e tungstênio na composição química do aço com grau 6A. A resistência à corrosão dos corpos de prova foi avaliada por meio das seguintes técnicas eletroquímicas: polarização anódica, espectroscopia de impedância eletroquímica e temperatura crítica de pite. A resistência mecânica dos corpos de prova foi avaliada por meio da técnica de dureza Brinell. Foi realizada também a caraterização microestrutural e a quantificação das fases do material. Os resultados mostraram um aumento da dureza do material, indicando um aumento da presença da fase ?’ com 10 horas de tratamento térmico apresentaram maior resistência à corrosão.

Aug 8, 2018

By Luiza Cruz Guimarães

Os fabricantes de instrumentos endodônticos de NiTi têm desenvolvido diferentes estratégias para aumentar a resistência à fadiga e à ruptura torcional desses instrumentos. A tecnologia “Controlled Memory (CM)”, que envolve o emprego de tratamentos térmicos em instrumentos já usinados, é uma dessas novas estratégias. Neste trabalho, dois tipos de instrumentos CM foram avaliados em termos de sua capacidade de recuperação de forma e resistência à fadiga após ciclos de flexão até 45 graus e esterilização em autoclave, simulando o uso clínico. Os resultados obtidos em relação às temperaturas de transformação martensítica e reversa, ao momento de dobramento a 45 graus, à recuperação de forma e à resistência à fadiga após ciclos de flexão/esterilização mostraram que os tratamentos aplicados aos dois tipos de instrumentos, embora referenciados como tecnologia CM, produziram resultados diferentes em termos de microestrutura e propriedades.

Aug 17, 2017

By Janine Feitosa de Deus

Compósitos ambientalmente corretos, fabricados a partir de fibras naturais lignocelulósicas (FNL), estão entre os mais investigados e aplicados atualmente. Dentre as FNL, destacam-se as fibras de Rami (Boehmeria nivea), que surgem como alternativa em sistemas de blindagens multicamadas, para uso em coletes de proteção balística, por serem leves, de baixo custo, resistentes e ambientalmente corretos. No presente trabalho, investigou-se o comportamento mecânico de compósitos de matriz epóxi reforçados com tecido de rami, através de testes de flexão. Compósitos contendo separadamente 0, 10, 20 e 30% em volume de tecido de rami e resina epóxi, foram fabricados em um molde metálico, sob condições de vácuo. Os corpos de prova fraturados foram analisados em MEV e os resultados foram avaliados visando algumas propriedades de flexão com a incorporação do tecido de rami, visando sua posterior aplicação em blindagem balística.

Oct 30, 2017

By Francisco Geraldo Toledo Junior

Os aços inoxidáveis possuem características essenciais para um bom acabamento quando o que se busca é estética e boa resistência à oxidação. Quando se específica um aço inoxidável, o acabamento é um dos aspectos relevantes que devem ser considerados. O acabamento possui uma importante influência em algumas características do material como, por exemplo, na facilidade da limpeza e na resistência à oxidação / corrosão. Há uma grande variedade de acabamentos. Através de ensaios de oxidação a quente, medição de potencial eletroquímico, medição de dureza a baixa carga (microdureza) e medição da tensão residual via difração de raios x foi possível perceber uma diferença entre os acabamentos 2D, 2B, RO, BB, Nº4 e Nº6. A medição de tensão residual mostrou qualitativamente que o aumento de dureza e o forte amarelamento ocorrido no material com determinados acabamentos é função de uma deformação elástica na superfície imposta durante alguns dos processos de fabricação desses aços. Esse mecanismo é relevante e interfere na resistência a oxidação e corrosão nos casos estudados.

Aug 17, 2017

By Caroline Gomes de Oliveira

Nas últimas décadas, as fibras naturais têm sido investigadas como uma alternativa para a utilização de fibras sintéticas, como material de reforço, tais como fibras de vidro. Algumas vantagens das fibras naturais são a menor densidade, biodegradabilidade e o fato de virem de fontes renováveis. Com o intuito de melhorar ainda mais as propriedades de compósitos de fibras naturais, investiga-se o desempenho de compósitos reforçados com tecidos de fibras naturais, uma vez que estes proporcionam um reforço multidirecional e permite a introdução de uma maior fração de volume de tecido. Neste trabalho, investigou-se a resistência à tração dos compósitos com matriz de poliéster reforçados com diferentes frações de volume de tecido de rami, que é uma das mais lignocelulósicas mais resistentes. Os espécimes foram testados em uma máquina universal de ensaios Instron. Os resultados mostraram um aumento na resistência à tração com o aumento da fração de volume de tecido.

Aug 17, 2017

By Noan Tonini SImonassi

A utilização de compósitos de matriz polimérica reforçados com fibras naturais vem assumindo um papel importante no âmbito da engenharia de materiais. O baixo custo, a biodegradabilidade e a redução do peso especifico torna a utilização desse tipo de compósito bastante atrativa. O objetivo deste trabalho é avaliar o desempenho da fibra de sisal como reforço do policarbonato visando uso utilização militar, especialmente em proteção balística. Antes da confecção dos corpos de prova, foi realizada a redução no tamanho de partícula do policarbonato e da fibra de sisal através de um moinho de facas, posteriormente dos corpos foram submetidos aos ensaios de tração e flexão.

Oct 30, 2017

By David Siu

Many problems were encountered with the mechanical wedge-type splices used for the 15-inch square precast prestressed concrete piles installed at an industrial plant site. Many of the wedges were breaking during installation of the splices and after pile driving resumed following splicing. Dynamic monitoring of the piles and uplift loading tests confirmed that the problems were associated with cracked or damaged wedges. More ductile, annealed wedges were subsequently used, and, while not completely satisfactory, they were found to perform better than the original more brittle wedges. Introduction Long precast prestressed concrete piles were installed to support heavy, settlement-sensitive structures at an industrial plant in Port Alberni, British Columbia, Canada. The piles were driven through soft compressible silts and clays to toe bearing in a dense sand and gravel deposit or on bedrock. Each pile consisted of two or three segments joined with mechanical wedge-type splices trademarked DYN-A-SPLICE. Shortly after construction began, problems arose during pile installation, and these problems were, later, identified to be related to the wedges, or clamps, used to connect the splice plates.

Jan 1, 1991

The following resolution was prepared, by the War Minerals Committee and was submitted by it to the Board of Directors of the American Institute of Mining Engineers, asking that it be passed by the Board and used to the best advantage to secure the end desired. WHEREAS, the steel industry of the United States is almost entirely dependent on the importation of foreign manganese ores, the consumption of which for the year 1918, it is estimated, will exceed 850,000 tons; and WHEREAS, the ships now engaged in transportation, especially from Brazil, are needed with ever increasing urgency for supplying our Army and Navy forces abroad; and WHEREAS, much shipping may be spared from manganese transportation and the domestic sources of manganese may be utilized, provided the steel manufacturers of the United States will cooperate to this end by taking advantage of the possibility, in open-hearth and Bessemer practice, of so called "residual" manganese, and by using spiegeleisen instead of ferromanganese, thereby following the example already set by three large and prominent steel producers; BE IT RESOLVED, that the Board of Directors of the American Institute of Mining Engineers urges the steel manufacturers of America, for patriotic reasons, to give immediate consideration to the development and utilization of domestic manganese ores; to use no ferromanganese, except for the manufacture of grades of steel below 0.15 per cent. carbon, to use domestic ores whenever possible in place of the high-grade imported ores; and to urge their associates and colleagues in this and other possible ways, to vie with one another in releasing ships for importation of any materials that cannot be secured or produced in this country.

Jan 1, 1918

The following resolution was passed by the Military Engineering Committee of New York on April 12, 1917. Copies are being sent to each member of Congress and to each of the five members in every State forming the committee representing, the five National engineering societies which carried on the industrial census under the direction of Howard Coffin. The Committee is urging every man to wire his Congressman and his Senator, asking him to do everything in his power to obtain favorable action by Congress on this resolution: Whereas in any large army to be created for the war, engineer troops will be needed in large numbers, and Whereas they should be officered by skilled engineers only, and Whereas the composition and training of such troops differ so much from the composition and training of non-technical troops that they should be organized under one central authority rather than under many scattered authorities. Now, therefore, be it resolved: That the members of the Senate and House of Representatives be requested to insist that all new units of engineer troops be organized and maintained by the War Department and not by the individual States.

Jan 6, 1917

The resolution drafted by J. W. Richards, J. V. N. Dorr, and Allen H. Rogers on the death of J. E. Johnson, Jr., and adopted by the Board of Directors, is as follows: "The Boards of Directors of the American Institute of Mining and Metallurgical Engineers wishes to place on record its great personal loss in the sudden death of Mr. J. E. Johnson, Jr., our fellow Director of the activities of the Institute, a member our Executive Committee, Chairman of the Institute's Committee on Admissions, and Vice-chairman of its Iron and Steel Committee. "A mere recital of these positions of trust and responsibility, which he filled with conscientious efficiency and marked ability, shows how greatly the Institute has lost by his death. No one else of the Institute's officers could have been so illy spared. We, his colleagues, take up his tasks with a sense of our inability to discharge them as well as he, and this with a doubled sense of our loss. "Others have written and spoken of the blow which his death has been to the furtherance of the metallurgy of iron and steel. His pre-eminence in this line is one of the facts of which the Institute is justly proud. Here his personality, originality, courageousness in advocating new principles, clearness of writing and forcible presentation of facts, are irreplaceable. His two great treatises on the blast furnace are his literary and scientific memorial.

Jan 7, 1919

At their last meeting, the Directors of the Institute passed the following resolution regarding Robert W. Hunt, who was president of the Institute in 1883 and 1906. This resolution was engrossed and presented to Captain Hunt at a dinner given to him in Chicago, December 9, on the occasion of his eightieth birthday. Resolution At that time it was announced that $5000 had been guaranteed as the nucleous of a fund, the income of which will be used for prizes to be awarded each year, under the supervision of the American Institute of Mining Engineers, for the best papers on iron and steel subjects. The Board of Directors of the American Institute of Mining Engineers extend to their distinguished colleague, Robert W. Hunt, a hearty greeting upon his eightieth birthday anniversary. They congratulate him upon his notable achievements as a pioneer in ,the manufacture of iron and steel, and his long and admirable service both as a practical director and as a wise critic and counselor in that art. They remember with gratitude his successful administration, for two separate periods, of the Presidency of the Institute, and they recall with pride the honor conferred upon it through the award to him of the John Fritz Gold Medal. Not least is their satisfaction in the retrospect of forty-four years of his membership in the Institute, with its unbroken record of loyal friendship acid delightful companionship; and they pray, that this record may be continued for happy years to come. In witness whereof, they have ordered this minute to be entered upon the records of the Board, and a copy duly attested to be sent to Captain Hunt.

Jan 1, 1919

By Randall Wheeler

In early 2008 we were asked by a quarry to become involved in a conflict with a pipeline company concerning blasting near one of their underground high pressure gas lines. The pipeline company, without the quarry’s knowledge, had sought and obtained a temporary restraining order against the quarry forbidding them from blasting near the pipeline.

Jan 1, 2011

At a meeting of the Board of Directors, held Jan. 21, 1916, the following resolution was adopted: Resolved, that this Board has learned with indignation and sorrow of the unprovoked and brutal murder of 18 American citizens on January 10, in the State of Chihuahua, Mexico, and laments especially the death of Messrs. C. R. Watson, C. A. Pringle, H. C. Hase, and W. J. Wallace, who were members of the American Institute of Mining Engineers. As these men and their companies were engaged, in the lawful prosecution of their work, we trust that nothing will be allowed to prevent or delay appropriate action by our Government concerning the outrage by which they lost their lives;

Jan 3, 1916

By D. J. Kennedy, A. W. Stokes, W. G. Klinowski

Sulphur hexafluoride (SF6) has become an accepted standard in the field of mine ventilation tracer gas studies. It has a wide variety of uses for defining mine ventilation flows that cannot be adequately described using conventional instruments such as anemometers and smoke tubes. The Cape Breton Coal Research Laboratory (CBCRL), Energy, Mines and Resources Canada, has been using SF for the past 4 years and has developed numerous release and sampling systems to increase its versatility. The CBCRL has also completed a successful field trial of an automated rapid sequential SF6 analyzer (which gives a pseudo real-time readout) that can be used underground. In doing this work, the authors recognised the potential of being able to use more than one tracer gas simultaneously in an underground study. Two alternative tracer gases (Freon-13B1 and Freon-12) have already been used by CBCRL in some of their underground work. These gases can be measured by gas chromatography utilising an electron capture detector in a similar manner to SF6. A description of these gases, the methods for 6' their handling, release and sampling are given in this paper together with a brief outline of the analytical system used to measure them. Their suitability to mining applications is compared with SF6. A study in which these three gases were used together is discussed and the results and conclusions given. Some of the additional uses for multiple tracer gases to assist the mine ventilation engineer in resolving problems and improving his day-to-day monitoring are discussed. Finally, a brief analysis of developments which can be expected in the near future is outlined.

Jan 1, 1987

By J-S. Marois, F. Cappucitti, Y. Dodier, D. Downey, G. Matton

"The flotation processes of the Niobec Mine have been affected by a seasonal loss of recovery and a significant increase in reagent consumption over the past few winters. This paper discusses the problem-solving methodology that was used to identify the root causes, to develop solutions and to implement changes that resolved the problem to restore the process to summer-like conditions year-round. Mainly, it was found that the process water was contaminated by phosphates ions, which adversely affected the carbonate pre-flotation, and caused detrimental effects on the subsequent niobium flotation. The phosphate ions were being generated by the process itself, but were consumed by algae in summer conditions. It was determined in laboratory studies that concentrations as low as 5 ppm were enough to affect the circuit and that the multiple additions of process water throughout the circuit was worsening the effect. Also, temperature was found to have an impact on the reagent performance. The performance of the plant was restored by implementing a natural treatment of our process water with a simple cost-free rearrangement of our circuit streams. In addition to that, our extensive geometallurgical program was used to provide ore to the plant restricting phosphate generation in the process. Also, a modification of the collector was developed and introduced in the carbonate pre-flotation that provided improved performance during the periods of low pulp temperature.INTRODUCTION Niobec is one the three major global producers of niobium presently in operation. Situated in the Saguenay-Lac-St-Jean region of Quebec and in operation since 1976, the site produces ferroniobium (FeNb) to be used mainly in High Strength Low Alloy (HSLA) steel, which is known to have better mechanical properties than carbon steel. The Niobec operation consists of an underground mine, a concentrator and a converter plant. The concentrator concentrates niobium-bearing minerals, mainly pyrochlore and columbite, to produce a high-content Nb2O5 concentrate which is then converted to FeNb in the converter plant by an aluminothermic reaction. The Niobec concentrator flowsheet, which has gone through many expansions and optimisation over the years, consists of grinding, desliming, flotation and leaching steps. The flotation steps are numerous, sensitive and difficult to operate due to the non-selective nature of oxide mineral collectors. Thus, the pyrochlore concentration process at Niobec still faces many challenges and is constantly going through periods of continuous improvement."

Jan 1, 2018

By Martin P. Schroeder

"Challenges have emerged as subway systems age and as new tunnels are bored in congested corridors or in high-risk environments. To help public transportation agencies address tunneling challenges, the American Public Transportation Association has convened numerous independent industry peer reviews composed of top experts in their fields to come together and provide recommendations and solutions. This paper provides case histories of peer reviews that include topics such as boring through toxic soils, boring underneath existing tunnels, retrofit of tunnel ventilation systems, and mitigation of water intrusion. Peer reviews are applicable to all tunnel projects worldwide. The paper will highlight the conditions of these challenges, peer review recommendations, steps taken to reach agreement, and the successes that resulted, which led to major changes, new legislation and reduction of risk. INTRODUCTION Public transit agencies face many challenges in maintaining and expanding safe transit operations, especially as systems age, ridership expands, and budgets remain flat. The development of new industry standards and federal safety regulations places further demands on transit systems, with compliance often taxing in-house resources. Studies of the state-of-good-repair across US public transit systems indicate a current backlog of $84 billion in maintenance projects, which will require an investment of $18.2 billion per year to eliminate the backlog by 2030[1]. Systems not in a state-of-good-repair may not operate efficiently, may not be available to meet the growing ridership demands, and may not meet required safety goals or reduction of risk. Innovation is another clear need transit agencies have for improving system performance and lowering operating costs.To meet these challenges, transit agencies often turn to industry peer reviews for guidance and recommendations as part of their overall strategy to maintain and grow the safe operation of their systems. As a service to its members, the American Public Transportation System (APTA) has developed an industry peer review program designed to give agencies opportunities to learn from each other and help them address challenges in operations, engineering design, and construction of their systems. Over the past 20 years, APTA has performed hundreds of peer reviews covering all aspects of transit system operations from fare collection to agency organization, project delivery methods to safety culture, and engineering design including tunneling and tunnel fire ventilation. As rail transit systems expand to meet increased ridership, it is often necessary to bore new tunnels for alignments in congested areas where surface rights-of-way are lacking. Such proposed alignments can pose significant challenges for transit agencies, as they contend with various tunneling problems."

Jan 1, 2016

By Mark Johnson, Mathew Janes

"The Resonator RD 260 Resonant Pile Driver delivers ground disturbance free, high production pile driving. The Resonator has recently been used on numerous production pile driving sites in the Netherlands and Melbourne, Australia to drive piles in sensitive areas where conventional pile drivers could not be used. Two case histories are provide in this paper which demonstrate the features and benefits of Resonant pile installation.. In the Netherlands the Resonator RD 260 was used at the Vopak Oil Storage facility in the Port of Rotterdam to install pipe and sheet pile within an active pumping gallery. The site demanded vibration free pile installation to construct a cofferdam within sensitive, highly valued assets. Access was an issue and schedule demands were stringent as shutdown windows were narrow. The RD 260 provided ground disturbance free piling immediately adjacent to fragile structures. At Vopak the only site access was using a large crane positioned over 40 m from the location of pile driving. Driving was conducted amongst 900 mm dia pipes carrying heated crude oil.In Melbourne the RD 260 was used to drive GU 18 sheet piling adjacent to light rail easements. The project was the first of many grade separations being constructed within Melbourne urban areas to lower the light rail and provide quieter rapid transit. The original trial used an RGT MR105 series vibrator but noise and vibration criteria were exceeded. The RD 260 was brought in for a trial and performed with high production and produced negligible ground vibration. Up to 17 sheet piles 14 m in length were driven in a 2.5 hour window during the trial.IntroductionThe Resonant Pile Driving method is gaining acceptance around the world as a new method to rapidly drive piles free of ground borne vibrations. The high frequency vibrator resonates the pile, essentially turning the pile into a spring, to excite the toe of the pile with high accelerations and low amplitude. High acceleration with low amplitude generates high penetration rates but the high frequency stress waves are quickly dissipated in the soil. Typically ground borne vibrations are measured at below 1 mm/sec within 1 to 5 m of the pile. The Resonant method can drive a pile next to a glass of wine, without spilling, as has been demonstrated on numerous piling sites.How Does Resonance Work?The Resonant method uses a hydraulic piston - cylinder geometry to generate high magnitude, high frequency oscillating force. This is a very different mechanism than the eccentric mass technology used in conventional and variable moment vibrators.A unique valve geometry achieves the high frequency flow switching necessary to oscillate the hydraulic piston at up to 180 Hz (10800 VPM). The valve is controlled electronically for maximum accuracy of the desired frequency. The volume of hydraulic oil delivered through the valve to the piston (flow rate) determines the amplitude while the hydraulic pressure determines the peak force."

Jan 1, 1900

By Y. Z. Xu

This paper presents a new dynamic method called Resonant Pile Test (HPT) for evaluating bearing capacity of pile. The basic conception of RPT is given in brief and the measuring system is also introduced. In addition, the influences of the magnitude of exciting force and of the mass of pile cap on test results are discussed. Finally, comparisons between values of bearing capacity given by RPT and by static load tests for a variety of pile types are listed.

Jan 1, 2010