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By H. G. Iverson

As a part of the program of investigation of domestic sources of manganese ore, mining engineers of the Bureau of Mines examined and sampled three properties in the vicinity of Winnemucca, Nev. As the ores were too low grade for direct production of ferromanganese, they were tested for their amenability to concentration by ore-dressing methods. Two samples of ore were procured by examining engineers of the Bureau of Mines from several outcrops in the Pollard Canyon area, Pershing County, about 30 miles southeast of Winnemucca. The manganese occurs in relatively small lenticular bodies as secondary replacement deposits in chert and quartzite. The first sample represented average run -of -mine ore as exposed in the Pollard Canyon deposits. Sample 2 was composed of hand-sorted, high-grade ore.

Jan 1, 1954

By R. G. Dressler

The design and operation of the Koppers powdered-coal gasifier and its auxiliaries at Louisiana, Mo., are described. This unit was designed to convert 1 ton of coal per hour with oxygen and superheated steam into synthesis gas - primarily carbon monoxide and hydrogen. The first run was made on May 4, 1949. After this, 44 short runs (less than 8 hours each) and 1 long run (lasting 11 days) were made. Total gasification time was 420 hours. The gasifier was not cooled down during the year when these runs were made. After an initial period of test operations and equipment proving, during which 12 runs were made, the effect of numerous variables on gasifier performance was studied. The long run was made primarily to check the equipment in sustained operation. Detailed data from these runs are presented.

Jan 1, 1954

By B. M. Hamilton

"IntroductionTHE PROCEDURE and technique for drilling holes has probably undergone as great a change during the past ten years as any one of the other operations conducted in hard-rock mining. During this period, we have seen a change from the heavy leyners and drifters to the light jackleg type of drill machine; from steels that were forged and hardened on the bit end to the inserted •carbide-tipped rod, from the necessity of providing special bit-end fabrication and beat treatment of shank steels to the simple grinding or turning of a plain section on a shank with no heat treatment required for bit attachment.When the steel maker was first called upon to manufacture a hollow drill rod, it was required that the steel must not only have sufficient strength and fatigue resistance to cope with the stresses of service, but also must be capable of being heat treated on the bit end to a high hardness for resistance to wear and abrasion . Little was known at that time about alloy steels and the beneficial effects to be gained from additions of chromium, nickel , and molybdenum. So it was that the plain 0.80 per cent carbon analysis was selected, since it had already proven to be a suitable grade for chisels, hammers, and other such shock tools. This grade has long endured the test of time and is still used in considerable tonnage today, particularly by the construction industry.As the metallurgist learned more about the influence of alloying elements, a new hollow drill analysis was placed on the market in the early 'thirties'."

Jan 1, 1954

By H. A. Johansen

Recent advances in the metallurgy of chromium have enabled this metal to begin to take its place among the refractory metals. Considerable work is being done on the development of high-temperature alloys containing high percentages of chromium.1/2/ In spite of the relatively large amount of work done on these alloys, little is known of the properties of the pure metal. Information in the literature concerning the tensile properties of pure chromium metal is quite scant. This deficiency maybe explained by the great difficulty of preparing test specimens from such a brittle material, resulting in many losses in each phase of the specimen preparation and testing procedure.

Jan 1, 1954

By H. M. Thorne

The Union of South Africa has been interested in oil shale for a long time, and deposits of oil shales, torbanites, and similar rocks have been found in many parts of the country. (Fig. 1.) Samples differ markedly in oil yield and in the characteristics of the oil. The strata vary in thickness, and most of the deposits that have been found are in unfavorable locations because of remoteness from markets or absence of transportation facilities. This report deals mainly with the torbanite deposit near Ermelo, Transvaal, in the Union of South Africa, and the operations of the South African Torbanite Mining and Refining Co., Ltd. (hereafter referred to as Satmar), in mining the torbanite, retorting it, and refining the crude oil.

Jan 1, 1954

By G. Vibert Douglas

"Gold occurs in Nova Scotia in three ways, saddle reefs, fissure veins, and fossil placers. Of these the saddle reefs are the commonest. They have been the source of most of the gold and have also been the subject of most of the literature on the gold occurrences.The Meguma or Gold-bearing series of Nova Scotia is a conformable succession of quartzite's and slates, possibly Precambrian in age, which have been folded into a number of anticlines and synclines that strike (Fig. 1) roughly east and west. This folding has been termed Acadian and is probably a westward continuation of the Caledonian revolution in Britain. It may have started in the Ordovician and continued through the Silurian and into the Lower Devonian. It was followed by the intrusion of the great Devonian granite batholiths. It is thought that the mineralization is connected with the late phases of the cooling of the granite. As the name saddle reef implies, the veins form on the crests and flanks of the anticlines, possibly in the synclinal troughs as well. The beds favoured by the solutions are the slates. The reason for this is apparent when it is realized that in order to fold over 30,000 feet of sediments (the thickness of the Meguma according to E. R. Faribault) through p radians of arc it is necessary to have a differential movement between the top and bottom beds of p times the thickness of the sediments. In the case of the Gold-bearing series, in which strong quartzite beds lie between incompetent slate beds, most of this differential movement was taken up in the slates. The evidence for this is the remarkably fine drag folding and the intense shearing and comminution of some of the beds of slate (Fig. 1). The quartzites exhibit some shearing and faulting, but there is little doubt that the greater permeability lay along the incompetent slate beds. The mineralizing solutions followed these beds and also passed from one slate bed to another through a joint or fault in the intervening bed of quartzite. These joining veins are called angulars in Nova Scotia. Within the veins the gold is in shoots and the real problem is to find out what controls the position and extent of the shoots."

Jan 1, 1954

By J. J. Forbes

This publication is a revision of the first of a series of four Miners' Circulars originally prepared and issued in 19'29 for use in a course of training designed to prepare mine officials to organize men for rescue and recovery operations. These circulars were revised in 1937 and 1938 and again in 1948. This circular (Miners' Circular 33) discusses mine gases and methods for detecting them. The second of this series (Miners' Circular 34) gives instruction in Bureau of Mines methods of sampling and analysis of mine gases; the third (Miners' Circular 35) describes methods and equipment used for protection against mine gases; and the fourth (Miners' Circular 36) explains procedures used in sealing and unsealing mine fires and in recovery operations after mine fires or mine explosions.

Jan 1, 1954

By W. L. Bancroft, Peter Price

"What is now known as the 'Waite section' of the property of Waite Amulet Mines, Limited, was originally the Waite-Ackerman-Montgomery mine. It includes a group of twenty-eight claims lying on either side of the Duprat-Dufresnoy township line, and about 8 miles north-northwest of Noranda, Quebec. ,The original discovery of ore on the property was made by Thomas Montgomery in Block Q, Duprat township, and was staked by him on behalf of himself, I. C. Waite, and C. H. Ackerman, in the summer of 1925. The property was optioned late in 1925 to N. A. Timmins who, after trenching and drilling the deposit, sold his 85 per cent interest to Noranda Mines, Limited. Early in 1927, a company known as Waite-Ackerman-Montgomery Mines, Limited, was formed and shaft sinking and development undertaken. Production commenced in August, 1928, ·and continued tJ May, 1930, when, owing to falling metal prices, shipment of direct smelting ore was stopped. Development of the mine by shaft sinking, drifting, and drilling continued until March, 1932, when owing to the prolonged low price of metals, the property was closed down. In September, 1933, an amalgamation with Amulet Mines, Limited, was effected, the new company being called Waite Amulet Mines, Limited. Early in 1937 operations were resumed, first by direct shipments to the smelter and later by aerial tramway to the Amulet mill. Operations have been continuous up to the present time, reaching an average of 720 tons a day milled for the year 1940. Production during the initial period (1928-1930) amounted to 75,811 tons, having an average grade of 7 .11 per cent copper, 4.47 per cent zinc, and 0.03 oz. gold and 0.65 oz. silver per ton. During the second period (1937 to end of 1946) , 1,060,524 tons, having an average grade of 4.53 per cent copper, 2.97 per cent zinc, and 0.03 oz. gold and 0.65 oz. silver per ton, were produced."

Jan 1, 1954

The Black Hills Mineral Atlas briefly summarizes all pertinent date available on the mines and mineral deposits in the Black Hills that have been explored, developed, mined, or located. The purpose of the atlas is threefold: First, from available date the general potentialities of the Black Hills region can be determined, although it is not possible to calculate actual ore reserves; second, it will provide the necessary basic information regarding a given property or commodity for further detailed study; and third, the compilation is a comprehensive directory of Black Hills deposits.

Jan 1, 1954

By V. A. Nieberlein

The purpose of this investigation is to determine the reserves of columbium (niobium) minerals in Arkansas and to develop metallurgical methods for concentrating the minerals and extracting the metal. The columbium resources of central Arkansas were explored by drilling and trenching, and a number of samples were taken. On the basis of this exploration the known reserves of the metal were estimated to be over 78,000,000 pounds. The reserves could possibly be extended by additional exploration to 150,000,000 pounds.

Jan 1, 1954

By J. S. Scott

"The Quemont property comprises 640 acres lying directly north of and adjoining the Noranda (Horne) mine. During 1926 to 1928, United Verde Extension Mining Corporation sank a shaft 235 feet and did 3,000 feet of development work on the 215-foot level. Between 1929 and 1930, Quemonr Mining Corporation deepened the shaft to 926 feet, and did further lateral work and drilling on the 500- and 900-foot levels. This work was confined to an area close to the south boundary and met with little encouragement.Following a period of idleness a magnetic survey was made in the winter of 1944, followed in the summer of the same year by some 6,000 feet of drilling. The first successful hole was drilled in February, 1945, from the ice of Osisko lake.To the time of writing, 131,000 feet of drilling, surface and underground,have indicated a large tonnage of gold-silver-copper-zinc ore, and although some knowledge of the geology and structure is emerging, it is too early to draw definite conclusions. The following brief description deals only with those structural features that are reasonably well indicated."

Jan 1, 1954

By J. P. Martin, A. H. Geisler, J. H. Crede, E. Both

The investigation of a 50 pct Co alloy was undertaken to determine whether there was any direct correlation between the structure and properties of Co-Fe alloys which were given various magnetic heat treatments. The magnetic anisotropy and texture of the 0.002-in. cold-reduced 98 pct material tend to decrease and change in nature with increasing temperature of the recrystallization anneal. Annealing samples in a magnetic field had little effect on either the magnetic properties or texture. However, cooling them in a magnetic field greatly improved their magnetic properties. THE beneficial influence of a magnetic field applied during the heat treatment of certain soft magnetic materials has been known for a long time. Early work showed that the presence of a magnetic field of a few oersteds during the heat treatment of Fe-Ni alloys will cause a large increase in maximum permeability. A pronounced increase in the residual induction which is produced by the magnetic anneal causes the hysteresis loop to approach the shape of a rectangle. Such results are beneficial since the desired properties are high permeability, high induction at maximum permeability, high residual induction, and low coercive force. More recently Libsch and coworkers1 studied the effect of magnetic annealing on the hysteresis properties of a series of Co-Fe alloys prepared from powders. They observed good response for the 35 and 50 pct Co alloys but little response for the 42 pct Co alloy. They pointed out that this was somewhat surprising since the 42 pct alloy has a high linear magnetostriction and zero crystal anisotropy and similar conditions in Fe-Ni alloys give excellent response to magnetic annealing. They found optimum properties to be at the 50 pct composition with residual induction, Br = 19,000 gauss and coercive force, Hc = 0.68 oersteds after the magnetic anneal. Before the magnetic anneal these values were B, = 12,600 gauss and Hc = 1.15 oersteds. The optimum treatment consisted of cooling from above the y-a transformation temperature to 900°C in a field of 20 oersteds, holding 11/2 hr at 900°C, then cooling at a rate of 20° to 25°C per min in the field to below 230°C. Cooling rate mainly affected coercive force with the value decreasing from 1.09 to 0.88 oersteds as the rate was increased from 3° to 48°C per min. Cooling from 1020" to 900°C in a field followed by further cooling to 230°C without the field gave properties decidedly inferior to those for samples annealed with the field applied throughout the cooling. They concluded that to get the best properties the samples must be cooled in a field to a threshold temperature above which the alloy is plastic enough to be affected by magnetostriction. In this respect the holding temperature must be high enough so that the alloy exhibits good plasticity to permit the optimum orienting of magnetic domains by relaxation of magnetostriction. In contrast, the holding time was of less significance for there was little improvement when the time exceeded 1/2 hr. The improvement in properties effected by magnetic annealing has usually been attributed to the establishment of a domain texture caused by the "freezing in" of magnetic strains. On the other hand, Smoluchowski and Turner2,3 apparently found that a magnetic field applied during recrystallization could alter the crystal texture. If this effect is real, improved properties would also be expected when

Jan 1, 1954

By J. E. Hawley, R. C. Hart

"The Preston East Dome gold mine is in the southeastern part of Porcupine district, Ontario, 5 miles southeast of Timmins, and immediately south of the property of Dome Mines, Limited.The claims now owned by this Company were originally staked in 1909. After the property had remained dormant for many years, the present Company was organized in 1936 to resume development operations. Two shafts had been sunk: at the time of the early work on the claims, but lateral work from these failed to reach the ore deposits. A successful diamond drilling campaign undertaken under the direction of D. G. H. Wright, however, was followed by the sinking of a five-compartment shaft arid the erection of a mill. From the start of operations to the end of 1944, 1,292,000 tons of ore averaging $11.60 in gold a ton have been mined.An outstanding feature in this mine is the occurrence of the major gold deposits in quartz porphyry intrusives, though minor deposits are also found in the adjacent Keewatin volcanics. Most of the ore occurs in fractures, but the filling was accompanied by varying degrees of replacement of schistose wall-rocks. The ore deposits may be classified as:"

Jan 1, 1954

By K. K. Kelley

Despite the wide interest in titanium and its compounds, no heat and free-energy-of-formation values for titanates (that is, compounds formed from titania and other metal oxides) have been available heretofore except for ilmenite (FeTi03). Such data are needed for understanding and developing processes for producing titania and titanium tetrachloride from ores (and possibly slags) and in connection with ceramic usage of titania. This paper reports experimental measurements of the heats of formation at ordinary temperature of 11 titanates-ilmenite, perovskite, barium metatinate, strontium metatitanate, barium-strontium metatitanate, barium orthotitanate, strontium orthotitanate, barium-strontium othotitanate, geikielite, magnesium-titanium spinel, and magnesium dititanate. The experimental method was solution calorimetry. The solution calorimeter was operated at 73.7°C. and used a strong hydrofluoric-hydrochloric acid mixture as the calorimetric fluid and reaction medium.

Jan 1, 1954

By H. Clare Horwood

"Three types of structures, the main shear zone, the north shear zone, and a series of hanging-wall fractures, contain all the orebodies so far discovered at the McKenzie Red Lake mine. Lenses and veins of quartz in these zones and fractures are the sources of the ore. The ore-bearing structures are unusual in that they are in a complex intrusive mass known as the McKenzie-Gold Eagle stock. They are believed to have been produced by compressive stresses from the south andsouthwest.The mine is on the northeast side of McKenzie island, in Dome township in the central part of the Red Lake area. The original discovery, the main shear zone, was made in 1928, about 3 years after the property was staked, by M. L. Bouzan who was in charge of prospecting and development work on the property. Subsequent diamond drilling and underground exploration led to the installation of a mill, which came into production early in 1935. The hanging-wall fractures were found branching out from the main shear zone during development work on the 350-foot level. The north shear zone was discovered in 1940.From 1935 when the mill began operation until the end of 1946 total production from the mine was approximately 269,349 oz. gold and 69,317 oz. silver, having a value of $9,679,739, recovered from 823,527 tons of ore.GENERAL GEOLOGYThe McKenzie-Gold Eagle stock has a total length of approximately 1 ½ miles and a width of about ½ mile. It was intruded into a complex synclinal fold in Timiskaming sediments. The sediments, which have been cut in only one place in the underground workings, are principally wellbedded greywackes. The stock is composed of large masses of diorite and granodiorite, a small mass of hornblende pyroxenite, and basic dykes of two ages. The diorite occurs as irregular masses in large measure surrounded by the granodiorite that it intrudes. It contains tabular crystals of andesine, having a maximum length of3/4 inch. The hornblende pyroxenite is an elongated lens or dyke in the diorite. The granodiorite masses occupy about two-thirds of the stock. Along its eastern side the main mass tends to become darker and more dioritic toward the diorite contact.Basic dykes of pre-vein and post-vein age are the youngest intrusive rocks at the mine."

Jan 1, 1954

By W. Rostoker, R. P. Elliott, B. W. Levincer

Phase equilibria in the Ti-Cr-Mo system have been investigated for alloys containing 100 to 40 pct Ti in the temperature range 550° to 1300°C. Five experimental isothermal sections and a surface of incipient melting are presented in addition to a summary projection of the space. Seven vertical sections have been constructed from the isothermal sections. A STUDY of the system Ti-Cr-Mo was undertaken as part of a program sponsored by Watertown Arsenal toward the development of titanium-base phase equilibrium diagrams of potential technical importance to alloy development. The scope of the investigation included the composition range contained by the titanium corner and the line of 64 pct Ti (all compositions are by weight) and the temperature range 550" to 1100°C. A surface of incipient melting was constructed from measurements on a large number of alloys. The system Ti-Cr has been established.&apos;-? The phase diagram is characterized by a wide miscibility field of the solid solution at elevated temperatures and a eutectoid reaction of the type: (15 pct Cr) + TiCr, (685C). The a solid solution has a very limited capacity for solution of chromium (< 0.5 pct Cr). The intermediate phase TiCr2 has at best a very narrow composition range. It has been shown that two allotropic modifications of this phase exist. However, this behavior does not appear to be perceptibly reflected in the form of phase boundaries of the type + TiCr,. In the system Ti-Mo,9-10 the phase is stabilized to successively lower temperatures with increasing molybdenum content. There are no known intermediate phases. The a solid solution is limited to less than 0.5 pct Mo. Because of the very extensive range of the phase, the ternary system was ideally suited to the determination of the phase boundaries by the parametric method of Andersen and Jette." A parametric surface was constructed to provide the necessary basis for the application of this method. Preparation and Treatment of Alloys More than 60 alloy compositions were prepared for the study of this system. Alloy buttons of 10 grams were arc-melted in a nonconsumable electrode furnace using inert atmosphere protection and a water-cooled copper crucible. The construction and operation of this type of melting unit have been adequately described elsewhere.&apos;&apos; To insure complete solution of alloy additions, the buttons were remelted alternately on top or bottom as many as five times. This was accomplished by a suitable mechanism for "flipping" over the ingots. Iodide titanium (99.97 pct Ti) was used as the alloy base. An especially high quality chromium (99.9 pct Cr) was obtained from the National Research Corp. Molybdenum sheet (0.005 in.) of 99.9 pct purity was used.

Jan 1, 1954

By M. E. Wilson, A. C. Lee

"The property owned by Senator-Rouyn Mines, Limited, is in Rouyn township about 17'2 miles southwest of the town of Rouyn. It adjoins the Chadbourne claims of Noranda Mines, Limited, on the south and the Bagamac property on the ·west. It includes seven claims-block 44, blocks 80 to 83 and blocks 96 and 97; the mine is wholly in blocks 44 and 82.Late in 1936 gold was discovered in an outcrop of rusty weathering carbonate rock near the north end of block 44, and the following year the present Company was organized to proceed with the development of the property. During 1937-38, 17,000 feet of diamond drill core were bored to determine the extent of the ore deposit at depth. From October 15th, 1940, to April 15th, 1941, the ore was hauled to the mill at the Arntfield mine for treatment. The mill on the Senator-Rouyn property started on April 25th, 1941, and has been in practically continuous operation since than time. To the end of 1946, 574,874 tons of ore, from which gold having a value of $3,836,450 was recovered, were treated in the mill.GEOLOGYThe rocks exposed at the Senator-Rouyn mine, except in the southern part of the property, are almost wholly quartz diorite, part of an irregular mass that extends west from the town of Rouyn along the north shore of Noranda lake and thence southwest across the Senator-Rouyn claims. In the northern part of the propertyt inclusions of rhyolite occur here and there in the diorite. In the southern part the predominant rock is dacite and in the east-central part of block 44 claim andesite. Dykes of andesite, quartz syenite, and later diabase also occur on the property.The andesite of the Abitibi volcanics is not exposed on the property, but has been intersected in three diamond drill holes, one on the eastern boundary of block 44 and two farther west within the block. This andesite is probably the western end of a band of pillowed andesite well exposed in the Larose claim to the east."

Jan 1, 1954

By A. M. Bell

"Hallnor mine is in the township of Whitney, Porcupine district. To date, its production of gold has been second largest in the east Porcupine field. Ore was discovered in the property in 1936 by diamond drilling in overburdened country. This drilling was undertaken by Noranda Mines following the discovery of ore in conglomerate at Pamour 1 mile to the east.Milling commenced at the Hallnor in June 1938, and to the end of 1945 432,000 oz. gold had been produced from 889,000 tons of ore, giving an average recovery of 0.49 oz. a ton.The West mine of Pamour, the Broulan orebody, and the veins on the Hallnor and Bonetal are all parts of a mile long vein system that has been separated into three sections by cross faulting. In consequence, they could well have been described in one paper. In treating them individually the viewpoint obtained from each may lead to conflicting opinions, and any conclusions advanced in this paper on the general structure should be modified by the conclusions advanced in papers on the neighbouring properties.GENERAL GEOLOGYRock FormationsThe Hallnor orebodies occur within 400 feet of the contact between lavas and sediments, and may lie in either lavas or sediments. The lavas near the ore consist of flows of pillowed andesite and one flow of more acid and less sheared and chloritized lava locally named trachyte. These flows strike east-west and dip steeply. At the surface on the east side of the property the volcanics have been intensely altered to a massive carbonate rock having a north-south thickness in excess of 1,000 feet . This carbonate body extends west across the property with a plunge of 45° (Fig. 1)."

Jan 1, 1954

By H. G. Ames

"The property of Perron Gold Mines, Limited, lies in the southwest corner of Pascalis township, northwestern Quebec. It is approximately 12 miles northeast of the town of Val d'Or.This ground was originally staked by Jack Mathews of Amos in the spring of 1931. Shortly after staking, a quartz vein containing visible gold was uncovered on the south boundary of the property, about 400 feet south of the present shaft. With further prospecting, another spectacular goldbearing vein was found 3,000 feet northwest of the original showing. Subsequently, several programmes of exploration were carried out in search of the main ore zone. By 1933 sufficient ore was outlined to warrant sinking a shaft. The first ore was milled in 1934.Total production from the Perron mine from commencement in 1935 to 1944 has been 317,900 oz. gold having a value of $11,935,106. The average recovery a ton for 1944 was $9.01."

Jan 1, 1954

By H. C. Young

This paper deals with roof bolting in Alabama coal mines and iron-ore mines from the time it was introduced in early May 1948 to May 1, 1953, a 5-year period. The Tennessee Coal & Iron Division of the United States Steel Corp. began systematic roof bolting in early May 1948 in a coal mine and in an iron-ore mine, which had some of the poorest roof conditions in the Alabama mines. After the efficiency of roof bolting had been proved by the Tennessee Co. it was gradually adopted by other companies throughout the State, until in May 1953 approximately 53 percent of Alabama&apos;s total coal production and 100 percent of Alabama&apos;s total iron-ore production, mined underground, was being produced from roof-bolted areas. Statistics in this report will show the advancement made in roof bolting in the 5 years and also the amount of roof bolting that was being done as of May 1, 1953. Significant progress has been made in the coal and iron-ore mines of Alabama in reducing the roof-fall fatality rates during the past several years by adopting systematic roof bolting. The groundwork was laid through successful experiments early in 1948 by the Tennessee Coal & Iron Division of the United States Steel Corp. in cooperation with the Federal Bureau of Mines. This experimental work was based upon the previous experience of the St. Joseph Lead Co.2/ in its Southeastern Missouri mines.

Jan 1, 1954