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By K. S. McClure, S. B. Chitralekha, R. B. Gopaluni, Chmylek. T., S. L. Shah

This is a tutorial paper on industrially successful approaches for nonlinear process monitoring. Online process monitoring is essential to continuous operation of plants at high efficiency. The problem of process monitoring is one where an impending but undesirable process condition has to be identified and used to alert process engineers. This problem has traditionally been solved by practicing engineers using statistical techniques that detect a change in the underlying correlation structure of process variables. For linear correlation structures, algorithms such as principal components analysis, independent component analysis and partial least squares have been proposed. However, many industrial processes exhibit nonlinear correlation structure between the process variables. In this tutorial we describe various nonlinear monitoring techniques and elaborate on two recently developed methods, namely Support Vector Machine and Local Linear Embedding. The two methods are evaluated by application on two experimental case studies, a SAG mill and a polymer extruder.

Jan 1, 2014

By Alex Heath, Andrew Barycki, Baladron. Javier

"Efficient flocculation is important to thickener performance, affecting the overflow clarity, solids settling flux, underflow density and operability. Many factors affect flocculation; from the material/flocculant type, dilution of the feed and flocculant solution, mixing, to the shear rate and shear history. The flocculant addition point (or points) can be used as a tuning method to alter the effective flocculation time in a feedwell, with addition further up the feed pipe increasing the residence time but making the aggregates more prone to breakup if they experience high shear later in the process. Conversely, adding the flocculant later, eg under the feedwell shelf decreases the mixing time but allows some free (unadsorbed) flocculant to be available at the feedwell exit. An extensive trial has been performed on an operating thickener comparing seven individual different flocculant dosing positions through a Vane feedwell, and some combinations of two dosing points simultaneously. Measurements of the velocity, solids concentration and aggregate size were made throughout the feedwell at the different positions, with the dosing points significantly changing the aggregate size and clarity, and also affecting the solids concentration at some positions. The results are accessed in terms of flocculation kinetics and used as CFD validation data."

Jan 1, 2014

By Stefano Trevisani

Abstract The FIEC Sustainability Vision states that “risks should be identified and allocated in a fair manner across the project team from the early stages of the design phase. A partnering approach, where objectives and timescales are agreed in advance together with all relevant partners in the value chain, offers a useful solution to improve on site efficiency and reduce disputes”. An alliance or collaborative form of contract involving all parties is the best way to ensure fair contract conditions and proper risk allocation in construction projects. Collaborative contracts are particularly useful where there is uncertainty or undefined information or in the event of technical difficulties and other risks difficult to allocate among the parties involved in the project. Owners sometimes require even special output in terms of innovative technical solutions or special performance. In addition, this particular form of cooperation has been construed and developed with the intention of avoiding and mitigating another great risk associated with the construction industry (especially in complex projects): disputes and conflicts, which are often a major cause of delays, increased costs, loss of reputation and opportunities. In contrast, Alliances are a way to increase and strengthen business relationships, technical and economic innovation and effectiveness, in a worldwide global context where the waste of resources must be avoided in order to guarantee future recovery and growth. Of course, the total cost of a project is usually a key factor and the main driver for the Owner and the Contractors in deciding the type of relationship between them as well as the subsequent relationship with subcontractors and lower-tiers. This paper and presentation, will explain the main features and the principle benefits that the use of collaborative contracts can bring to all parties involved in the construction project, including the sustainable financial return that might be achieved if costly and time consuming disputes can be avoided.

Jan 1, 2014

By Kilian Neubert, Hermann Wotruba, Henning Knapp

Sensor-based sorting has been integrated into more and more applications in mineral processing over the past decades. Various sensor types, such as line scan cameras, near infrared sensors and X-ray transmission sensors, allow the separation of a vast variety of raw materials. Sensor-based sorting has several economic benefits which can make the difference between an uneconomic operation and a profitable mine. Sensor-based sorters can be applied to fulfill various sorting tasks, such as waste rejection, product quality improvement and ore type diversion, and have a significant impact on the layout of the processing plant. Therefore, it is important to include sensor-based sorting into the planning of a processing plant at an early stage. To evaluate the applicability of sensor-based sorting for any specific ore type, it is currently necessary to provide several hundred kilograms of material for subsequent bulk tests. In exploration, ore samples are usually rare and only available in form of drill cores. The acquisition of drill cores is time-consuming and expensive especially for deposits in great depth. Hence, it is unfavorable to spoil valuable drill cores for bulk tests. This paper describes a methodology to evaluate the applicability of sensor-based sorting based on drill core analysis. That methodology offers the possibility to calculate the achievable performances of different sensor types for various grain sizes without comminution of drill cores. The general methodology is shown on basis of an exemplary test work on drill cores from a currently conducted exploration.

Jan 1, 2014

"Chairman: Mr. K. F. LaneRapporteur: Mr C. T. ShawPapers:Design of crushing plant flow sheets by simulation by T. GurunThe impact of transportation networks upon the potential supply of base and precious metals from Sonora, Mexico by P. de V. Harris and D. E. EurestyProfitability sensitivity analysis of a mining venture by C. A. Beasley and E. P. PfleiderTechnological innovation and its potential effect on the opening of new gold mines in South Africa by N. C. JoughinMr Turgay Gurun, in presenting his paper, indicated that this simulator was no purely theoretical exercise, but that the model had been used in the design of crushing plants of capacities ranging from 3 000 tons per day to 66 000 tons per day, and that recently the design of a plant of capacity of 99 000 tons per day had been studied.The crushing plant simulator was an independent portion of a much more comprehensive simulator for the design of a. complete recovery plant. It would be possible to use each section of this simulator on its own, and simulators would be designed to cover flotation concentrates, cash flow analyses of the entire project, and so on.Each simulator would be backed by a comprehensive data bank. For example, the crushing plant simulator was backed by such a data bank which included the performance and cost data from five manufacturers for an average of 30 items of process and materials handling equipment each. This meant that data preparation involved generally less work than would be required for a manual calculation. On average, data preparation for one run took 30 minutes and three minutes of computer time on an IBM 360/40 completed the run. The model could be valuable as a design tool in that it allowed the designers an opportunity to make a thorough examination of many alternative designs. It was also of value to plant operators as it could be used to predict the consequences of operating decisions.This paper generated much interest and there were numerous questions and contributions, so many, in fact, that the discussion had to be cut short.It was pointed out by Mr K. F. Lane that crushing plants represented a very large capital investment. A plant designed for 40 000 tons per day at 98 per cent efficiency might well in practice be run at 50 000 tons per day at, say, 83 per cent efficiency. He asked how, therefore, their design could be investigated without building economic criteria into the model? The author conceded that this was a tender point. He would have liked to have given facilities for more variability of the metallurgical information. He pointed out, however, that while there was no overdesign for conservatism built into his system, some overdesign was inevitable as the performance characteristics given by the manufacturers were generally conservative. Also, in his system, if lower recovery was allowed for, the system would nut through more tonnage."

Jan 1, 2014

By Crasta Jeason, T. Sreenivas, M. Narasimha

The subtle nature of the flow inside the hydrocyclone has encouraged development of mathematical models for predicting its performance, which are widely used in simulation of comminution circuits. But most of the models available are based on single average feed density. But the feed to hydrocyclone classifier is generally mixture of particles of different densities. This effect of varying density of feed particles on performance of hydrocyclone has been reported in literature. Further investigation of the effect of multi component feed on the performance of hydrocyclone is the objective of this work. This work involves experimental work to study multicomponent behaviour in various size cyclones. The performance of hydrocyclone for feed mixture of magnetite and quartz has been studied. The effect of presence of magnetite, a high density material on efficiency of separation of quartz has been analysed. It was observed that the effect of component interaction increases with feed solids concentration leading to an increased cut-size for a given optimum cyclone conditions. Based on the multi-component exiperiments available in literature, a concept for modeling the performance of hydrocyclones is proposed. A set of semi-empirical model equations for cut-size, sharpness of separation are presented. An attempt to validate the new hydrocyclone model on multi-component behaviour is made.

Jan 1, 2014

By C. Stollberg

The recovery of valuable materials from electronic waste is of growing importance for the re-source management not only in the industrialized nations. Being a significant step in an innovative automated process for recycling of metals and plastics from used electric and electronic equipment, the results of the work introduced below, prove the applicability of microbial leaching of metals from printed circuit boards (PCBs) at industrial scale. Within the first project step, which started in March 2005, experiments in shaking flasks with a mixed culture of chemolitotrophic bacteria (mainly Acidithiobacillus ferrooxidans and Leptospirillum ferrooxidans) were carried out to study the solubilization of non-ferrous metals present in the electronic waste. It was found that the best results were achieved by means of a two-stage process in which leaching of these metals was carried out by acidified ferric sulphate solutions generated as a result of the prior bacterial oxidation of ferrous ions to the ferric state. Special reactor systems for bacterial generation of such solutions and for the subsequent leaching of non-ferrous metals from the waste were developed, constructed and tested under laboratory and pilot scale conditions. The optimum technological parameters such as concentration of iron ions, pH-value, temperature and presence of nutrients were established for both reactor systems. Parameters such as particle size, pulp density and flow rate of the suspensions being leached were established for the leaching process carried out under continuous-flow conditions. The complex flow sheet reflects a highly efficient technology on the basis of metal recovery, environmental effect and economical acceptance. The process was successfully implemented into an industrial demonstration unit.

Jan 1, 2014

By Steve Kral

"The Rapid Excavation & Tunneling Conference (RETC) is a world-renowned event that attracts some of the best minds in the global underground construction and tunneling industry. The experts gather at this conference to impart new technologies, discuss challenges to their projects and learn about new technologies that have become available to them.The 2015 RETC will be held June 7-10 at the Sheraton New Orleans, in New Orleans, LA. This biennial conference, of which SME is a sponsor, is expected to attract about 1,400 attendees from around the world. These professionals represent all parts of the global tunneling and underground construction industries - contractors, engineers, owners, consultants and equipment suppliers.More than 110 technical papers in 21 sessions will be presented over two-and-a-half days. Paid attendees will receive a proceedings volume of the conference. The proceedings will also be available from SME. In addition to the technical programming, the accompanying exhibit will include 155 exhibitors occupying 175 booths, providing RETC attendees the opportunity to get a look at the latest in equipment and service technology. Three short courses will be held on the Sunday preceding the start of the show. And there will be plenty of opportunities for attendees to meet and chat during several social activities that are scheduled throughout the conference."

Jan 1, 2014

By Mahdi Shevrini, Hamed Haghi

"In this research, the operation of screen classifying in silica processing circuits was investigated and modified by replacement of available trommel screens with teetered bed separator (TBS). In addition the effect of the mentioned replacement and addition of attrition scrubber on quality of final product, impurities removal, recovery and production rate were inspected. Considering screen efficiency problems to achieve certain particle size distribution, hydraulic classifying system was selected instead of trommel screens. Application of suggested plan improved quality and particle size distribution of produced silica significantly. Optimization of size classification in process circuit resulted in increase in production rate up to 21% (from 67% to 81%), silica recovery (from 68.35% up to 83.11%) and relative enhancement in removal of impurities such as Fe2O3 and TiO2. After optimization and stabilization of grinding and size classification section, industrial attrition scrubbing tests were carried out and the best solid percent and retention time were determined i.e. 70% and 6 minutes, respectively. Using sodium carbonate during attrition scrubbing, has major effect on removal of surface coating and staining especially sharp increase in clay removal; therefore 2 kg/t of sodium carbonate can be optimistic point of industrial procedure for this silica processing plant. It should be mentioned that application of attrition scrubbing which is followed by screw classifier for de-sliming were useful for better cumulating of particles in the range of appropriate liberation degree (+106-300µm) and efficient removal of metallic (iron and titanium oxides) and non-metallic (clays and feldspars) impurities."

Jan 1, 2014

By D. R. Nagaraj, Raymond Farinato

Water constitutes one of the most valuable resources employed in mineral recovery and processing. Identifying potential problems encountered in mineral processing in waters unusable for drinking or agriculture (including seawater and even hypersaline waters), understanding chemical factor interactions, and optimization of flotation reagents will greatly expand our ability to create more sustainable beneficiation technologies. The current paucity of our knowledgebase regarding high salinity effects on flotation clearly signals a need for a significant research effort. We report here results of a study designed to probe effects of pulp chemistry on metallurgical performance in the flotation of Cu and Cu-Mo ores in saline waters. The results clearly demonstrate that pH (more correctly dosage of pH modifier to target a pH set point) has the most significant effect on Mo recovery when using seawater. This is linked to the formation/precipitation of Mg(OH)2 when pH = 10.3 (in seawater). The type of pH modifier used, NaOH or Ca(OH)2, had no impact on Cu or Mo recovery, indicating that Ca2+ ions were not involved in any reduction in Mo recovery in the pH range of 9-11. Our results in tap water spiked with either Ca2+ or Mg2+ ions in the same pH range (controlled by NaOH), confirmed that Ca2+ ions had no effect on Cu or Mo recovery, but that addition of Mg2+ ions had a severe adverse effect on Mo recovery at pH = 9.5, and to a lesser extent on Cu recovery. The onset of Mg(OH)2 precipitation occurred at a higher pH, and the adverse impact of Mg(OH)2 on Cu recovery (and perhaps Mo recovery as well) was less, in sea water than in tap water spiked with Mg2+. These effects are attributed to the mitigating role of the high electrolyte concentration, notably NaCl.

Jan 1, 2014

By K. Saberyan

In this study the extraction of zirconium and hafnium has been investigated by solvent extraction using Cyanex 302 in various media such as nitric, sulfuric and hydrochloric acid has been investigated. Effect of various parameters such as type and acid concentration, extractant concentration, type of diluent, equilibrium time, various foreign ions and finally type and concentration of strip-ping agent have been studied. The results showed that nitric acid was optimum media for extraction of zirconium and hafnium. The extraction of zirconium and hafnium occurred quantitatively in the concentration of higher than 4 M nitric acid but in hydrochloric acid media, quantitative extraction obtains over 8 M HCl. In sulfuric acid media, extraction of zirconium and hafnium is negligible. Stripping studies showed that the optimum reagent for stripping was 0.5M sulfuric acid.

Jan 1, 2014

By B. Rai

Processing of dolomitic phosphate ores remains one of the most challenging problems in phosphate ore beneficiation. The beneficiation plant at Jhamarkotra in Rajasthan, India for example is currently using a conventional double stage flotation process which involves first a fatty acids flotation to produce a combined dolomite-apatite concentrate (bulk concentrate) from associated silicate gangue. Dolomite is then separated from this bulk concentrate by flotation with fatty acids collectors and depressing apatite with phosphoric acid and sulphuric acid. This process requires addition of large dosages of reagents (H3PO4 and H2SO4) to depress apatite and to maintain highly acidic pH during flotation. Furthermore several cleaning and scavenging stages are needed to obtain the product of desired quality. We have developed and employed a molecular modelling based methodology of designing selective reagents for apatite-dolomite separation. We have been able to take into ac-count the differences in the distribution of calcium cations on these two surfaces in our design and hence develop novel phosphonic acid based depressants for apatite-dolomite separation with con-ventional fatty acids as flotation collectors. We have demonstrated the utility and power of molecular modelling based reagents design approach through this work on beneficiation of Jhamarkotra dolomitic phosphate ore using our novel phosphonic acids based depressants at pH?s close to natural pH. It was possible to reduce the MgO content of the ore from as high as 13.3 % to 1.5% in a single stage flotation. Our flotation separation results on Jhamarkotra ore with these new phosphonic acids based tailor-made depressants for apatite-dolomite flotation separation are discussed in this paper along with results of corresponding molecular modelling computations on the same system.

Jan 1, 2014

Optimising flotation designs and innovations is a complex process involving many parameters, one of which is ensuring sufficient testwork is carried out at plant level before these innovations are launched in the marketplace. This paper will describe how modern design tools are utilized, what are testwork phases at various plants and how results and observations have helped to validate and optimise flotation design innovations. Scale-up of equipment has long been the prevalent trend, but how long can it continue? Are there other means for pushing the boundaries of present technology? Some present challenges and future directions are given in the light of theoretical criteria for scale-up and how it has been applied in practice. Very large flotation cells of 300 m3 size have been installed in New Zealand, and relevant results from the metallurgical and mechanical aspects are presented and discussed. Utilization of the cell volume is also important. New innovations in the hydrodynamic domain are presented and discussed. Means to enhance flotation of coarse and fine particles are shown with results from plant testwork. Accurate control of large flotation cells is vital to optimize yields and grades. Froth image analysis and intelligent level control are presented ? again - with relevant plant results.

Jan 1, 2014

By Chee Theng

"So many talks, so little time.One of the toughest challenges associated with attending the SME Annual Conference and Expo is deciding how to allocate one’s resources. After accounting for keynote and plenary sessions, committee meetings, networking events, luncheons and exhibits, attending even one of the 109 technical sessions and more than 600 technical paper presentations can be a labor of love. Many, however, managed to make it to many of the sessions, including the mineral and metallurgical processing technical session on solvent extraction, ion exchange and electrowinning.At one point, that room was seated to near capacity, with a considerable number of the audience members standing by the walls at the back. Brittany Valera of Freeport-McMoRan Inc. was one who came early and enjoyed the session in its entirety. "Everything was pretty exciting," she said. "I really liked the modular plants. I think the future of mining, just like what we talked about in there, lies in thinking about things like remote locations, lifetimes of plants, anything that would be reusable and sustainable; and lower-cost and user-friendly would be really beneficial."Michael Moats, associate professor of metallurgical engineering at Missouri University of Science and Technology, started off the session by presenting on behalf of post-doctoral student Alex Luyima, who, like many before him, had been snapped up by industry and is now working for a secondary-metals refining company in Texas. Their team studied the nucleation and growth mechanism of copper on stainless steel from synthetic acidified copper sulfate in the absence and presence of chloride ions and three commercial organic additives: Hydrostar 4208, DXG-F7 and Cyquest N-900. Currenttime data were analyzed using known models, with reference to scanning electron microscope images. Good agreement was achieved between the models and SEM micrographs of deposits at a commercially relevant current density of 30 mA/ cm2. The addition of 20 mg/L chloride was found to increase the size and reduce the number of nuclei. The addition of 2.5 mg/L of each additive did not change the mechanism, but all three reduced the size and increased the number of nuclei, leading to more uniform coverage of the substrate with smoother deposits produced in twohour electrowinning experiments. N-900 had the best deposition coverage while DXG-7 was the easiest to dissolve."

Jan 1, 2014

By Z. M. Dai

Microorganisms in AMD (Acid Mine Drainage) were enriched in 9K culture medium. The enrichment was applied to leach copper pyrite after the microbial community structure and metabolism was stable. Before and after bioleaching, the microbial DNA was extracted and applied to RFLP (restricted fragment length polymorphism) analysis to demonstrate the relationship between the leaching efficiency and the change of microbial community. Atomic absorption spectrometry results showed that when concentration of the pulp was 10% and pH were 1.5, 2.0 and 2.5, the leaching rate were 56%, 57% and 34% on the 18th day respectively. These results indicated that the rise of pH resulted in the decrease of leaching rate. In lower pH condition, the growth of microbe was faster: when pH was 1.5, the microbial cell number reached to 1.4×107cells/mL on the 9th day; while pH was 2.5, the microbial cell number decreased to 4×106cells/mL. The analysis of microbial community structure showed that Acidithiobacillus ferrooxidans and Leptospirillum ferrooxidans were dominant species before bioleaching (account for 43% and 32% respectively). And after bioleaching, these two species were still dominant when the initial bioleaching pH were1.5 and 2.0. While the initial bioleaching pH was 2.5, the proportion of these two species decreased. These results demonstrated that the initial bioleaching pH would affect the microbial community structure in bioleaching system at room temperature, and this affect could lead to different copper pyrites bioleaching efficiency.

Jan 1, 2014

By S. Martins

The aim of this work is to compare three different results of charge motion in a modified 5ft diameter lab mill and to identify differences and similarities in these results. The lab mill is modified from tumbling a ball charge to tumbling a charge of disks. This modification replicates 2D motion. This 2D condition is measured using an instrumented disk (iDisk) and analysed using a video imaging system. The iDisk is equipped with a 3D accelerometer array and rotation rate sensors. With the help of a video system, some measured quantities are also determined externally. The results of these three predictions or measurements are presented. A discussion is included.

Jan 1, 2014

By H. L. Liu

With the exploitation of mineral resources, valuable minerals are more and more finer and poorer. Priority reclaiming liberation grind particle under rough grinding, will help to pervert loss of melts, raise dewatering efficiency of concentrate, reduce consumption of reagent. And it is propitious to reduce energy consumption and raise the utilization rate of resources. With the feature of coarse particle?s desorption and deposition, CLF flotation machine has special pulp circulating way, which is not only apply to treat coarse particle but also normal size particle. The paper advanced the history, the design principle, the structure feature and the application of CLF flotation machine.

Jan 1, 2014

By Abdolreza (Reza) Osouli

Determining the roof stability condition of underground coal mines in the Illinois Basin is sometimes very challenging. The roof stability of Illinois mines are mostly affected by two types of shales: Anna Shale and Energy Shale. These layers are sometimes weak in parallel bedding when subjected to horizontal stresses. The roof rocks in the Illinois Basin are are typically more moisture sensitive than the other coal fields. In this study the geotechnical properties of some of the shale units as well as limestone layers will be presented. The geotechnical properties of roof rocks consist of moisture content, unconfined compressive strength, slake durability, indirect tensile strength, and point load tests (Axial and Diametral). The correlation of indirect tensile strength versus diametral point load strength as well as unconfined compressive strength versus axial point load test are explored and discussed. These correlations will help in identifying the roof mass index and planning appropriate roof control measures. This study also evaluates the application of CMRR rock mass index for an Illinois coal mine.

Jan 1, 2014

By Braulio Fernández, Gonzalo Montes-Atenas

The mechanisms taking place during the leaching of chalcopyrite when it is in contact with other sulphide minerals, particularly pyrite, is still a matter not fully solved. The GalvanoxTM process has been suggested as a technical solution to extract copper from chalcopyrite at commercial level inhibiting passivation phenomena widely reported in the field of hydrometallurgy. Although there are some rules of thumb to implement the process in fully flooded stirred conditions such as the optimum pyrite/chalcopyrite mass ratio should range between 2 and 4, among others; not many research studies have been focused on studying the effect of the surface contact area between chalcopyrite and pyrite to reach best copper extraction conditions. The aim of this research work is to determine the effect of the mass and surface area ratio between the minerals and the surface area of each of the mineral species effectively exposed to the leaching solution. Different particle size distributions of pure pyrite and chalcopyrite were contacted in a small column and subjected to leach tests using sulphuric acid in concentrations close those used in industrial leaching processes. The mass and surface area ratios which optimize the extraction of copper were obtained. It was found the best leaching conditions were attained when reducing the particle size distribution of pyrite regardless the particle size distribution of chalcopyrite. Further analysis concerning the impact of this conclusions on large scale operations is presented and discussed.

Jan 1, 2014

By M. Hawker, M. Kreuh

The mining and metallurgy industry is known to be of cyclical nature associated with price volatility. As such, some years are quite lucrative and other years require mining companies to tighten their belts. The field is a mix of junior, mid-tier, and major mining companies. One thing that is common to all of them is the time required and the cost to develop a flowsheet in accordance with best practices. Although a long list of factors can impact flowsheet development, this paper will include the impacts of: experienced metallurgical engineers and laboratories, representative samples for high quality and valuable testwork results, and following engineering development stages. The paper also provides typical time frames to complete selected engineering flowsheet development steps.

Jan 1, 2014