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By Phyllip Worley, Frank E. Chase, Christopher Mark

The Harris No. 1 Mine, located in Boone County, WV, has been longwalling the Eagle Coalbed for over 30 years. Harris has experienced numerous interactions associated with the extensive room-and-pillar and longwall mining operations which have been conducted in the overlying No. 2 Gas Coalbed. The problems have included roof falls, excessive rib sloughage, and gateroad and bleeder entry closure. A detailed evaluation of the multiple seam experiences at Harris No. 1 Mine was conducted as part of the National Institute for Occupational Safety and Health (NIOSH) nation-wide multiple seam mining case history data base. One observation from the Harris gateroad case histories was that smaller, critically loaded, upper seam pillars seemed to cause more severe ground conditions than did wider pillars. The LaModel program was used to investigate this supposition, and the results confirmed that “critical” sized pillars do transmit the highest amounts of stress to adjacent seams. In addition, the data suggest that the probability of a major multiple seam mining interaction increases when the depth of cover is 1,000 ft or greater and when the Eagle seam pillars have a Analysis of Longwall Pillar stability factor less than 1.50.

By David C. Oyler, Winton J. Gale, Jinsheng Chen, Christopher Mark

A collaborative project between RAG Emerald Mine, NIOSH, and SCT Operations was conducted to investigate ground behaviour, reinforcement performance, and stress redistribution in a coal mine entry subjected to a severe horizontal stress concentration. Field measurements indicated that the stresses applied to the study site nearly doubled during longwall mining, resulting in roof deformations extending to a height of 4.8 m (16 ft) above the entry. This paper focuses on the computer simulation that was undertaken to provide more insight into the roof behaviour and rock bolt interaction during mining. The model’s input rock properties were derived from extensive laboratory testing, and the model itself simulated a broad range of failure mechanisms. The effects of different bolt patterns on roadway behaviour were evaluated. Comparison between the model results and the field measurements indicated that that the model effectively simulated the critical elements of the actual roadway’s behaviour. With the confidence gained, the model was used as a baseline for additional simulations that evaluated the expected performance of alternative roof support systems. The study will also provide a benchmark data set for future applications of numerical modelling to U.S. coal underground mining.

By Marc T. Filigenzi

Two of the major ground control safety issues confronting underground mine operations today are shaft pillar stability and the failure of rock around active mine openings. Failure of a mine shaft can lead to the entrapment of workers. Failure of rock around active underground mine openings can lead to roof falls, which in turn can result in worker injuries and fatalities. Finite-element analysis has proven to be a reliable method for predicting stresses and displacements around underground mine openings. However, this is a complex and time-consuming technique and is not used as often as it could be in mine planning. The purpose of this paper is to demonstrate one technique developed at the Spokane Research Center that allows the user to create a finite-element model of a two-dimensional section of an underground mine in a relatively straightforward manner. This model is then used to calculate stresses, displacements, and safety factors around mine openings. With this information, mine planers can evaluate the stability of mine openings as well as the stability of pillars and mine shafts. This analysis will help develop mining sequences and layouts that minimize stresses in that section of the mine. This, in turn, should minimize the occurrence of shaft failure, roof falls, and other hazards associated with underground mining.

By Harry Dobroski

Communications with moving tracked vehicles in a rail haulage mine pose a difficult problem. These communications take place from dispatcher to vehicles or from vehicle to vehicle via the trolley line, which is a very poor communications line. As a result, deadspots and high-signal areas can occur anywhere along the line, or signal can decrease simply as a function of distance. An analysis is made of the trolley line as a communications line, and methods of improving its characteristics are discussed. Data from inmine experiments are presented, showing actual improvements in communications. Recent Bureau developments in new hardware are also discussed. These include an adaptive speaker control for existing carrier phones and a new generation of improved carrier phones.

The President: "It gives me great pleasure to call on Professor Howat to present the paper written jointly with P. R. Jochens and C. W. Wolhuter entitled, 'Utilisation of slags for the manufacture of cement.' After the presentation of the paper the President said: "Thank you, Professor Howat, for so ably introducing the paper prepared by yourself, Dr Jochens and Mr Wolhuter. Once again we are deeply indebted to you for bringing to our attention a new development in the metallurgical field, this time a technique for assessing the suitability of slags for the production of slag cement, and thereby providing a means of turning a waste material into a valuable asset. May we hope that this will lead to an end to unsightly slag dumps and, at the same time, to some conservation of our local limestone resources. Discussion within this Institute on the problems of cement manufacture, has of recent years been all too infrequent, and we thank you for bringing this interesting and important subject again to our notice. We are doubly grateful to you and your co-authors. May I now call on Dr Stutterheim, Deputy Director of the Council for Scientific and Industrial Research, to contribute to your paper, and to tell us something about the Conference on the Chemistry of Cement which he attended in Tokyo towards the end of last year." (Applause.) Dr N. Stutterheim, Mr B. F. van der Merwe and Dr F. S. Fulton then contributed to the paper. (These contributions will appear in a later issue of the Journal.) PAPERS OPEN FOR DISCUSSION The President: "Listed on the agenda are papers open for discussion. I would suggest that anyone wishing to contribute to these papars, submit their contributions to the Secretary in writing." CONCLUSION The President: "I would like to thank everybody for their attendance here tonight, and on your behalf I am sure you would like me to thank the authors and the contributors for the most interesting time that we have had this evening. Thank you very much." The meeting closed at 6.00 p.m. NOTICE SYMPOSIUM ON THE RECOVERY OF PYRITE A symposium on the recovery of pyrite will be held on 12th and 13th June, 1969 at Kelvin House, Johannesburg under the auspices of the Institute and the National Institute for Metallurgy. Notices will be sent to members as soon as more details are available as regards the papers and the programme.

By T. A. Wright

The sampling of waste materials containing copper, lead and tin has taken on a new significance within recent years, and is of increasing importance, on account of the entry of some of the copper refineries into this field and the tendency towards consolidations among the smelters. In the past, such material was sold on the basis either of a rough or grat) sample or of casual inspection of the lot. The two principal sources of this waste are the processes of fabrication and the scrapping of automobile, electrical, plumbing, railroad and other equipment. In both cases rnuch material can bc sorted, salvaged and sold by classification and grade to be melted "as is" or with the addition of new or virgin metal. The increasing care in classifying exercised in the large manufacturing plants tends to incrcase the proportion of this usable scrap; on the contrary, the increasing use of more complex and special non-ferrous alloys tends to makc sorting and grading more difficnlt in turnings, borings, clippings, etc., and conseqllcntly is making sampling of more moment. In tin, lead, alumiinum, and zinc furnace by-products such as ashes, drosses, skimmings, etc., the trade practice of evaluation has not varied much. For instance, tin drosscs, battery lcad, and aluminunl skimmings are ordinarily sold on what is called "metallic button" or "metallic recovery" or "metallic yield." Coppcr and Icad wastcl, howcvcr, is being sold more and more on actual copper and lead contents bascd on sarrlple and chemical analysts. This paper will be dcvotctl chiefly to the sampling of niaterials suitablc only for refining and recovery of one or more of the metals present. The methods described are often bascd on thc fact that but one, metal, such as copper, is to be paid for. The loss of volatile constituents in melting does not appreciably affect thc final copper result, as the "after-melting" assay can be readily calculated to the "bcfore-nltltingl' basis, but if smelter efficiency continues to increase, so that in tiltie zinc, for instance, may be rccovrred on a paying basis, thc method of sampling dirty brass, for example, will have to bc changed also. As a matter of fact, we may cxpect that improved refining proresses will make possible the partial reeovrry of lcad and tin which are now lost

By Lisa Steiner, Robin Burgess-Limerick

In 2004, underground coal mines in the United States reported 3,405 injuries to the U.S. Mine Safety and Health Administration (MSHA). Of these, 17 percent were associated with the use of bolting machines, 8 percent with continuous miners, and 4 percent each with scoop/load-haul-dump (LHD), shuttle cars and personnel transport. Analysis of the injury narratives identified five hazards that required attention. They are rock falling from supported roof inadvertent or incorrect operation of bolting machine controls, handling continuous miner cable, collisions while driving underground vehicles and driving or traveling in underground vehicles on rough roadways. The rate of lost-time injuries has steadily decreased during the past 10 years (from more than 10 per 100 FTE in 1995, to six in 2004). However, underground coal mining remains a hazardous industry. One of the contributors to this elevated injury risk is working with or near underground coal mining equipment. Roof bolting machines and continuous miners have been consistently identified as high risk equipment. They account for approximately 24 percent of all injuries to underground coal miners (Sanders and Shaw, 1989). LHD's, shuttle cars and personnel transports are also associated with injuries in underground coal mines (Burgess-Limerick, 2005). Conventional analyses of injury statistics typically provide tables detailing the breakdown of injuries by body part nature of injury or mechanism of injury. Such analyses are worthwhile and may be helpful in tracking broad trends over time. Further information is available in the narrative text field completed for each injury reported. The detail contained in these narratives varies. However, they generally provide some insight into the causes of the injury, such as the activity being performed at the tune of

By V. I. Lakshmanan

The demand for elements such as nickel, cobalt, titanium and gold in various applications has increased significantly. Innovation to recover these elements now plays a major role in metallurgical processes as established technologies have challenges in treating the types of ores that are available while meeting the increasingly stricter environmental regulations. Alternative chloride based processes have been developed that can be used to recover the value elements from the available feed stocks with potentially lower environmental impact. Chloride-based hydrometallurgical processes have several advantages, including higher leachability of complex ores/tailings and relative stability of chloro-complexes of the metals. Process Research ORTECH Inc. (PRO) has developed mixed-chloride process flowsheets, where innovative solvent extraction process steps are used for the separation of nickel, cobalt, titanium and gold from their respective chloride solutions. This paper will discuss the potential aqueous chloro-chemistry of these metals and separation reaction mechanisms involved in the solvent extraction process.

By Clara Godoy, Álvaro Dapía, Paulo Couceiro, Håkan Schunnesson, Juan Navarro

This paper applies geostatistical tools in Measure While Drilling (MWD)data to estimate the probability distribution of values in all the points of the studied domain in order to assess the continuity of rock classes between boreholes. The analyses carried out by Ghosh et al.(2018) and Navarro et al.(2019) have been used as starting point of this work to classify the geotechnical rock condition in four classes: solid rock, fractured rock, cave-in rock and cavity. From it, an application for the geotechnical rock condition of ore bodies have been developed, aiming at characterizing the rock before the charging the holes to minimize unexpected rock conditions and to address issues associated with charging and blasting operations. Such problems are closely related with non-optimal rock fragmentation after blasting. The procedure has been applied in the geotechnical block model results obtained from Navarro et al.(2019)’s work in the Luossavaara-Kiirunavaara AB’s (LKAB) Malmberget underground iron ore mine, Sweden. Navarro et al.(2019)’s model was developed based on102 fan-holes from five ore bodies and extrapolated to the full-scale in20 drifts with 5600 fan-holes from two orebodies. A multi-step transformation of the MWD parameters was carried out in order to minimize external influences other than the rock mass. The study shows the calculations of the variogram and kriging estimation in the 3D domain for six ring-blasts, from one of the ore bodies studied in Navarro et al. (2019)’s work to assess the continuity of the rock classes along the six ring-blasts in a 3D mapping model. For that, intermediate rings between the measured ones from the MWD have been estimated. The probability distribution of values in the entire domain of rings with measured samples has been plotted together with the rock classes identified by the blasthole paths. The results show high accuracy in the matching between the kriging and the values given by the MWD data, allowing to visualize smooth trends of different rock classes along the ring. The representation of the 3D mapping model for the six ring-blast shows clear fractured and cave-in zones developed along the drift that correspond to zones with geotechnical problems found, as from internal reports.

By Stanko Nikolic

The Top Submerged Lance (TSL) technology, developed in the 1970s, is now widely used for the processing of a range of materials. TSL technology for continuous converting was first patented in the 1990s. The process is based on the use of calcium ferrite slag. Although this slag system had been applied elsewhere the phase equilibria had not been thoroughly investigated. This lead to a collaboration between the Process Technology group of Mount Isa Mines, now part of Glencore, and the Pyrometallurgy Innovation Centre (PYROSEARCH) at The University of Queensland. Through multiple research programs this complex system was successfully investigated. The results were then implemented within thermodynamic modelling tools. This combined new knowledge was then applied to the design and industrial implementation of the TSL continuous converting technology, ISACONVERT™. This paper describes the key findings of the research and how this was applied to the industrial implementation of the technology.

By E. D. Peters

It frequently occurs in the establishment of reduction works, in an entirely new and untried mining district, that the metallurgist in charge finds considerable difficulty in determining the process best adapted to the ores which he receives for treatment. At the first glance it would seem easy enough to decide what style of furnace is best adapted for beneficiating any one class of minerals. If the ore possessed a quartzose gangue and was comparatively free from base metals, while salt could be obtained at a reasonable price, one would naturally resort to a chloridizing roasting, and pan or barrel amalgamation for the extraction of its silver contents. If galena or carbonate of lead was the prevailing mineral, and charcoal could be obtained at moderate figures, the blast-furnace would beneficiate the ores most advantageously. But if, as is usually the case in Colorado, the ores consisted of an intimate mixture of galena, zinc-blende, copper-pyrites, and noble silver minerals, associated with an overwhelming mass of siliceous heavy spar, or limestone gangue, the common reverberatory furnace can be used to the greatest advantage ; and, although the product is only a copper matte, I do not hesitate to affirm that it can be treated, and the silver, gold, and copper produced at nearly the same price for which silver and lead can be separated. In Germany, blast-furnaces are frequently used for this same purpose, both for argentiferous and non-argeutiferous copper ores; but any one who will take the trouble to examine the statistics of smelting at Fahlun, the Oberharz, and other Continental works of this description, will see that the expenses are far too great, and the production much too small to think of employing this method in our mining districts, where only the softest and most miserable kind of charcoal is obtainable. I propose in this paper to give an accurate account of the expenses incurred at the Mount Lincoln Smelting Works in treating the same kind of ore, and producing the same end-product in both blast and reverberatory furnaces. I have taken for comparison a favorable campaign of the blast-furnace, and a good average month's running of the reverberatory. In the blast-furnace estimate I have included the calcining and concentration of the matte produced during that campaign, as I always, when possible, concentrated the regulus made

By Vincent Canaguier

Methane is increasingly considered as a promising reductant for metal oxides, including chromite. To assess the possibilities of such reduction route, the gas-solid reactions between Ar–CH4–H2 gas mixtures and synthetic chromites are studied between 950 and 1050 °C. The influence of Mg and Al additions on the reduction-caburization of (Fe,Mg)(Cr,Al)2O4 solid solution is investigated thermodynamically, structurally and kinetically. The product phases are examined by x-ray diffraction (XRD), scanning electron microscopy (SEM), and electron probe microanalysis (EPMA). The reaction rate is derived from real-time exhaust gas measurements and post-reaction product analyses such as oxygen analysis. Kinetic models are proposed based on the product phase morphologies and confronted with the empirical data.

By M. C. Chapman, E. C. Westman, A. T. Iannacchione

Examination of seismic records during the time interval of the Sago Mine disaster in 2006 revealed a small amplitude signal possibly associated with an event in the mine. More needs to be understood about the seismicity from mine explosions in order to properly interpret critical seismic information. A seismic monitoring system located at NIOSH’s Lake Lynn Experimental Mine has monitored experimental gas and dust based explosions and impact tests. The seismic signatures from these different events were analyzed using standard waveform analysis procedures. The magnitude of seismic energy during a gas and dust explosion was found to be more dependent on mine entry geometry and seal behavior rather than on the amount of explosive fuel present. The results suggest a large explosion that’s not restricted can generate potentially the same magnitude as a small explosion that is restricted.

By E. W. Hough, G. L. Stegemeier

Empirical equations for surface tension of propane and normal butane as functions of reduced temperature are obtained from experimental data. Another correlation relating surface tension to enthalpy of vaporization is given for these two compounds. In addition, new paracbor numbers are calculated for the normal paraffin hydrocarbons. These numbers are utilized for the calculation of interfacial tension of two-component systems as functions of pressure and temperature, using a modified form of Weinaug-Katz equation. The experimental data for two binary systems are approximated by the correlation. From these results it is found that the interfacial tension in the high-pressure region remains extremely low at large pressure decrements below the critical pressure. Thus, it appears that condensate systems may have flow characteristics almost like single-phase conditions even though the pressure is within the two-phase region. Experimental data have shown that interfacial tension divided by density difference approaches zero as the critical pressure is approached. A calculation of wetting-phase saturations indicates that the saturation gradient at the two-phase contact becomes increasingly abrupt as the critical pressure is approached. DISCUSSION Prediction of the surface and interfacial tension of the light hydrocarbons and of two-component hydrocarbon mixtures at various temperatures and pressures may be made if other physical properties are known. Extensive experimental work on single-component and binary systemsl is the basis for the correlations outlined in this paper. Interfacial tension is defined as the specific surface-free energy between two phases of unlike fractional composition, while surface tension is defined as the specific surface-free energy between two phase:; of the same fractional composition. The usual definitions relating interfacial tension to a liquid-liquid interface and surface tension to a gas-liquid interface are not clearly defined when the critical region is included, and there is no sharp distinction between a gas and a liquid phase. Interfacial tension is probably the most important single force that makes one-half to one-third of the total oil actually in place in a reservoir rock unrecoverable by conventional gas-drive or waterflood methods. A rough estimate of this figure for the United States is 100 billion bbl. Interfacial tension presently is used by petroleum engineers in the estimation of saturation gradients at the gas-oil contact and at the oil-water contact. The data in this paper should prove useful for estimates of reserves involving gas-oil contacts. Relative permeability undoubtedly is influenced by interfacial tension, for sufficiently small values. These data should be useful in determining how small the values are In addition, these data should eventually add to our fundamental knowledge of surfaces. At the critical point, all surface excesses approach zero and the thickness becomes very large. SINGLE-COMPONENT SYSTEMS It has been observed1 that the following relationships are good approximations to the physical properties of propane and n-butane.

By Robert W. Hunt

The memorable features of American history have been making fast during the last century, and notably so since 1860; and they are by no means confined to political or to any one branch of scientific development. Of all the industrial arts, none show a greater change or 'a mightier progress than the Bessemer manufacture. And this year, while we are celebrating the first centennial of our national life, we can also celebrate the first decennial of American Bessemer practice. While not forgetting or undervaluing what has been done in other countries, I have thought that a brief history of the introduction and development of the Pneumatic or Bessemer process in America would be of interest. In 1863 the Kelly Pneumatic Process Company was formed and an arrangement entered into with William Kelly, who had taken out letters-patent of the United States, Nos. 16,444; 17,628, reissued as 505; 18,910, dated January loth, 1857; June 23d, 1857; November 36, 1857; and December 22d, 1867, respectively. This association mas composed of the Cambria Iron Company, E. B. Ward, Park Brothers & Co., Lyon, Shorb & Co., Z. S. Durfee, and, later, Chouteau, Harrison & Valle joined the combination. Not satisfied with possessing the control of the Kelly patent, they sent Mr. 2. S. Durfee to England, to secure for this country Mushet's patent on recarburization, No. 17,389, dated May 26th, 1857, the same having been taken out in England on September 22d, 1856. In this Mr. Durfee was successful. Previous to the application of William Kelly for a patent, Henry Bessemer, of England, had taken out patents dated February 12th, 1856, and August 25th, 1856, in this country. Kelly claimed priority in the discovery of the principles of the process, and the Patent-office allowed his claim by granting him his patents. In the autumn of 1862 Mr. Alexander L. Holley, while in England, was impressed with the importance of Mr. Bessemer's invention, and so fully foresaw its future, that, upon his return to the United States, he induced Messrs. John A. Griswold and John F. Winslow, of Troy, New York, to join him in endeavoring to possess Bessemer's American patents. Mr. Holley returned to England in

By Evgueni Jak

Recent advances in analytical, experimental techniques, and computer-based theoretical modelling of fundamental properties and elemental processes, provide new opportunities to develop the next level of whole-of-reactor pyrometallurgical furnace models. These models have the potential to significantly improve the prediction of, and adding value to, industrial operations. In non-ferrous smelting, the starting point of these models is the development of multicomponent thermodynamic databases for gas-slag-matte-speiss-metal-solids phases supported by systematic experimental research. The whole-of-reactor-models additionally should take into account kinetic processes taking place at micro- and macro- scales, and other key factors. Examples of applications of the latest research tools and modelling approaches to analysis of industrial flash and top submerged lance (TSL) sulphide smelting processes are presented. Different levels of industrial modelling are discussed from elemental local reactions, through general and more detailed whole-of-reactor-models, to plant sections and further to whole plant operation models. Some principles for development of pyrometallurgical reactor models are discussed.

By D. Majuste

This paper describes an experimental approach to evaluate the effect of organic impurities or even additives on metal electrowinning and product quality. In addition to electrowinning tests and electrochemical measurements, the approach includes organic analysis by Fourier Transform Infrared spectroscopy and gas chromatography; video monitoring of the reaction interface; and product characterization by using scanning electron microscopy, crystallographic texture and bending tests. The mechanical behavior of metal cathodes was assessed with a customized bending device that is able to bend the cathodes up to angles similar to that of the stripping machine. In this work, the effect of a potential organic impurity, lubricating oil, on the production of electrolytic zinc is taken as a case study. The findings of the investigation allowed a better understanding on the role of this organic on energy consumption and product quality and a qualitative prediction for the behavior of Zn cathodes during the stripping operation. Simple control and optimization procedures resulted in significant energy savings.

By Stephen C. Tadolini, Thomas E. Marshall, Cecil Banta, L. J. Prosser, Anthony T. Iannacchione

The Pittsburgh Research Laboratory of the National Institute for Occupational Safety and Health (NIOSH) endeavors to provide national and world leadership in the prevention of work-related illness, injury, and death. This is accomplished by using a scientific approach to gather information, assemble and create knowledge, then translate the knowledge and results into products and services. These products and services are then delivered to all personnel who can effect prevention. Obviously, the development and use of instruments to monitor mine roof conditions provides an opportunity to execute that mission. In the late 1990’s, based on observations at a number of underground limestone mines, only a few used roof monitors. Subsequently, NIOSH introduced the Roof Monitoring Safety System (RMSS) as an aid to roof inspection beyond traditional visual and sounding techniques. Initial expectations were that by gaining roof movement information, ultimately roof sag rates could provide indications of eventual failure. During this investigation, RMSSs were installed in 13 underground limestone mines in six states and this paper analyzes the data obtained at three of these mines. This paper also provides an overview of the system, data, analysis, and applications relevant to the RMSS.

By William H. Schiffbauer, Ph. D. Mowrey

Proximity warning devices can improve workplace safety by alerting workers when they are in a hazardous area near moving equipment. Industrial work sites often present extreme challenges to safety-based proximity warning devices. Many commercially available types of proximity warning sensors and systems can be rendered useless when covered with mud, ice, snow, ore, rock, and other material. The list includes radar, ultrasonic, capacitive, and visual types of sensors and systems. Addressing these shortcomings, NIOSH personnel have developed a patented active proximity warning system called HASARD (Hazardous Area Signaling and Ranging Device) which employs lowfrequency, low-power magnetic fields which are quite impervious to severe environmental conditions. A shapeable wire loop antenna which provides the marker of dangerous work areas, has been mounted on a continuous mining machine and was mounted inside 1.3-cm thick angle iron. This loop antenna was exposed to more than six months of active underground coal production, which included being covered by and scraped over with tons of rock, sprayed by a continuous stream of water, and immersed in thick mud. After six months the loop antenna showed signs of wear, but was still capable of performing its intended function. The HASARD system is now being applied to other industrial applications and is showing much promise, especially in harsh environments. This paper details the system, describes the tests that have been done, and mentions other areas where it can benefit the safety of industrial workers.