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By W. D. Ludemann, E. A. Loria, E. A. Rowe

The isothermal recrystallization of electrorefined vanadium has been studied as a function of annealing time , temperature , and prior deformation . Specimens were cold- rolled from 30- to 75 - percent reduction in thickness , then annealed from 700 ° to 1,200 ° C at time periods ranging from 1 minute to 96 hours . The course of recrystallization was followed by means of hardness , metallographic , and X- ray techniques , and a recrystallization diagram was constructed . Interpretation of the data indicated that there was around 50- percent softening due to recovery ( first stage of softening) before recrystallization began . The defining of recrystallization limits with respect to the amount of deformation was precisely established for electrorefined vanadium . More than 30- percent reduction was necessary for recrystallization to occur at 850 ° C. With 60- percent reduction , it was initiated at 750 ° C and completed at 950° C. The activation energy for recrystallization , as derived from the data , was 95,300 cal per mole for 60 - percent reduction and annealing at 750 ° to 900 ° C. Recrystallization by the mechanism of nucleation and growth was the principal process during the second stage of softening . minor part of the second stage of softening took place as strain- induced boundary migration , which was observed in specimens reduced 30 percent , bent in L- shape , and annealed at 950 ° C. Grain size decreased significantly only with the largest reductions and annealing between 750 ° and 950 ° C. Grain growth was expressed by the empirical relation D = KKtt"" ,, the exponent being the same at 60- percent reduction and annealing from 750 ° to 900 ° C. Accordingly , the activation energy for grain growth was 75,000 cal per mole .

Jan 1, 1964

By K. K. Kelley, L. B. Pankratz, W. W. Weller

The heat capacity of columbium (niobium) carbide (CbC ) was measured over the temperature range from 51 ° to 298 ° K, and the entropy at 298.15° K was evaluated . Also , the heat content above 298.15 ° K of columbium carbide was measured to 1,800 ° K. The results were combined with the known heat of formation at 298.15 ° K to obtain values of the heat and free energy of formation over the temperature range from 298.15 ° K to 2,000 ° K.

Jan 1, 1964

By C. D. McMaster, John C. Hartley

Three systems that monitor ventilating fans are described . These electronic monitoring systems automatically perform most of the operations required to conform with the provisions of the Federal Mine Safety Code in the event of fan failure or slowdown .

Jan 1, 1964

By Morgan B. D

Since the mid 1950s, limonite deposits of a new type have been found in the northwest of Western Australia. The deposits consist of extensive fossil valley fillings up to several hundred feet in depth, of medium to high grade limonite, frequently containing limonitized fossil wood, and of Mesozoic or Tertiary age. The distribution of the deposits is closely linked with hilly outcrops of Archaean and Proterozoic jaspilite in the headwaters of the old valleys, from which the iron has been derived by leaching, and presumably re-precipitated by a process not unlike that which operates in forming bog iron deposits. Due to the relative resistance of tlie limonite to erosion, the rejuvenation of streams in the area in recent times has left limonitic remnants as mesas up to· several hundred feet above the levels of the present creeks, the courses of which generally are adjacent to or within a few miles of those of the old limonite filled valleys.The Robe River limonite deposits are the largest of this type known and can be traced for approximately 130 miles along the old stream, over 30 sq. miles of limonite remnants remaining at the present time.The present quantity of limonite in this system alone is probably in excess of 5,000,000,000 tons, and the original quantity must have exceeded four times this tonnage when allowance is made for erosion.Some thousands of millions of tons of this material contain in excess of 54 per cent Fe, with approximately 10 per cent combined water. The chief impurities are SiO2 and Al2O3, and minor elements are not present in objectionable amounts. A portion of these deposits was extensively tested by The Broken Hill Proprietary Company Limited (the B.H.P. Co. Ltd.) during 1962-1964. Most of the data presented in this paper are based on the work done on these deposits which are typical of those discussed. The overall problem of the origin of the limonite is discussed. It is apparent that the limonite originates from the jaspilitesof Archaean and Proterozoic age which form the highlands at the upstream ends of the deposits. The iron oxide has been chemically and/or mechanically derived from these jaspilites and deposited by one or more of the following mechanisms.A.-Chemical-sedimentary mainly by biological agenciesB.-Replacement of fluviatile sediments by iron-charged watersC.-Clastic sedimentary processesD.-Lateritization of fluviatile sediments.These various mechanisms are discussed; the authors favour machanismA.Manuscript received' at The Institute, 14th July, 1964.

Jan 1, 1964

A mathematical model of a decision is represented by the table in Figure 4. The numbers in the matrix are a measure of the effectiveness of each alternate for an objective. In this case, it is the per cent of desired profit that is satisfied by each alternate for each objective. By adding all of the values in a row, we have a measure of which alternative is best for both objectives. However, if you think that alternate 1 is necessarily better than alternate 2, you are wrong. Why? Because the weight of the objectives may not be equal. It could just be that this plant can sell more than it can produce, so that the loss in profit represented by increased sales is more than twice as important as reductions in costs. (See Figure 5). In that case, let us weigh objective 1 as 30 per cent and objective 2 as 70 per cent. It must also be obvious that the sum of all the "objective weights" must equal 100 per cent. Now, by evaluating our alternates according to their weights. we find that alternate 2 is better than alternate

Jan 1, 1964

By Andrews B. S

The sinter plant at the Sulphide Corporation's Cockle Creek works produces a feed for the company's Imperial Smelting Furnace. The feed contains lead and zinc oxides and all the fluxes necessary for furnace operation. The quality of this feed is a major factor in furnace performance and the considerable flexibility of operation possible at the sinter plant has been used in efforts to achieve optimum operating conditions.Operating data is processed daily and information gathered from this source has led to three of the four improvements described.These improvements have resulted from elimination of gas recirculation, reduction of sinter returns sizing and alteration of ignition conditions and main layer fuel loading.

Jan 1, 1964

By Green A. D M

The establishment of the Imperial Smelting Furnace at Sulphide Coporation Pty. Limited for the smelting of zinc and lead made it necessary to design and install sintering capacity to produce approximately 500 t.p.d. of zinc-lead sinter. The updraught sintering process installed is a recent development and the plant was designed with adequate flexibility and equipment to enable operating staff to investigate the process and achieve maximum production under optimum operating conditions.Sulphur dioxide gases from the sinter machine are passed to a contact acid plant for the manufacture of sulphuric acid.

Jan 1, 1964

By Lionel A. York

This paper outlines the type of water-bearing formations encountered in the Prairie Sediments and describes a method for effectively sealing these zones in order that shaft-sinking operations may be carried out with safety. Details are given of the procedure for carrying probe holes ahead of the shaft bottom. These probe or grout holes are employed for establishing a series of overlapping grout covers around the proposed shaft excavation to safeguard against large inflows of water during sinking. The pattern and length of grout covers cannot be standardized, and each cover needs to be specially designed to suit the varying ground conditions. In order to provide effective protection through the Prairie Sediments, the number of holes in any one cover would not be less than 8, and possibly as many as 64 would be required in certain zones. The length of covers would vary from 100 ft. to 250 ft. Emphasis is placed on the need for obtaining accurate geological and water information from exploratory holes, drilled in the shaft vicinity, in order to effectively plan all grout covers.

Jan 1, 1964

By Donald W. Mitchell, John Nagy

Observations made on coking of coal, deposition of soot, dust transport, flame, violence, and related phenomena following experimental coal-dust explosions are summarized. Data are given on gas explosion pressure, flame length, flame velocity, and variation of these parameters with concentration. Conclusions from these observations are useful in preventing similar occurrences in operating mines and serve as a guide in improving safety.

Dec 1, 1963

By Robert T. Beckman

The results of a preliminary investigation of compressive strength versus length-diameter (L/D) ratios of potash specimens and the statistical treatment of the data are summarized in this report. The purpose of the study was to evaluate a laboratory method for obtaining estimates of the strength of potash pillars during robbing operations. The specific objectives of this preliminary investigation were to test the method and the reliability (confidence limits) of the data, and to determine the number of additional specimens necessary for given confidence limits. The specimens were taken from three sites at two mines in New Mexico. The statistical analyses included the determination of the confidence limits for the data and the number of additional specimens necessary to obtain confidence limits of ±500 and 100 psi. The testing method was found acceptable, and estimates of the comprehensive strength, within 1500 psi, could be obtained by testing about 110 additional specimens from the three sites. The compressive strength of the specimens tested fits an empirical equation of the type

Dec 1, 1963

By George J. Carter, George H. Todd, Hal J. Kelly

In July 1956, the Bureau of Mines and the J. R. Simplot Co. participated in evaluating and beneficiating drill-hole samples from the Bovill, Idaho, clay-silica deposit and in tests of the beneficiated products. The geology, mineralogy, beneficiation, and potential uses of the clay and quartz fractions of the Bovill deposit are described. Test work showed that a filler-grade clay having an apparent spectral reflectance of 78 percent can be made by bleaching, and by removing some of the submicron-size particles. A quartz product suitable for the manufacture of glass containers can also be made.

Dec 1, 1963

By N. A. Caspero, W. E. Eckard, W. T. Wertman

A thermal oil-recovery experiment was conducted in the Venango First sand, Goodwill Hill oilfield, Warren County, Pa., about 10 miles northeast of Titusville. The Quaker State Oil Refining Corp., Bradford, Pa., performed the experiment with assistance from Sinclair Research, Inc., Tulsa, Okla., and the Federal Bureau of Mines. The Goodwill Hill field was discovered in 1885. Primary-production oper- ations continued until 1930 when an air-gas injection project, which is still in operation, was started. At the location of the combustion experiment, the reservoir is 400 feet deep and 30 feet thick, with wide permeability and porosity variations. The crude oil is typical Pennsylvania Grade paraffin- base oil with a gravity of 43.9° API and a viscosity of 4.55 cp at 60° F. The well pattern for the experiment consisted of 5 producing wells, enclosing an area of 1.28 acres, and a central ignition-injection well. An air-natural gas mixture was ignited in the ignition well on July 29, 1961. Ignition was followed by injection of air and natural gas at various rates. The experiment was suspended January 5, 1962, when it became evident that economic oil production could not be achieved. There was no conclusive evidence that self-sustained combustion was achieved or that combustion increased oil and water production. A slight increase in liquid production was attributed to stripping action caused by the air-injection rates, which were higher than those normally used during air-gas injection.

Dec 1, 1963

By Wallace R. McCord, William E. Eckard

This report presents a detailed lithologic description of the Big Lime, Keener, Big Injun, Weir, and Berea horizons from a well cored in the Spruce Creek oilfield, Ritchie County, W. Va. Well logs and results of core analysis are also included. The information was obtained during the Bureau of Mines continuing technical evaluation of selected Appalachian area oil reservoirs for increased ultimate recovery. The lithologic study of these important West Virginia oil and gas producing horizons was made on a 4-inch-diameter core. Commercial oil production was obtained by the well owner after the Big Injun horizon was successfully hydraulically fractured.

Dec 1, 1963

By W. E. Lamont, R. E. Perry, I. L. Feld

The Bureau of Mines conducted research to determine the conditions required to sinter a pyrrhotite calcine into a product suitable for iron blast furnace feed . The calcine , a fine - grained iron oxide produced by roasting sulfide flotation concentrate , analyzed about 60 percent iron and 1 percent sulfur . Sintering of the calcine without prior pelletization was not successful whereas firing of preformed calcine charges yielded acceptable sinter products . Batch tests were made to study the effect of the following variables on the sinter quality : Size of green pellets in the charge , quantity and type of internal carbonaceous fuel used , depth of sinter bed , moisture content of the charge , flux additions , and binder additions . The batch and continuous sinter tests showed that minus 1 / 4 - inch pellets prepared from a mixture of the calcine , coke , dolomite , and water gave sinter cakes analyzing 57 to 61 percent iron and 0.05 to 0.02 percent sulfur .

Dec 1, 1963

By Pedro Máximo Ángeles

El presente texto señala el proceso «Strategic-Udy Modificado Angeles» utilizado para la producción de fierro o semiacero en Chimbote, Ancash. En ese sentido, durante la producción de aceros, es opcional el uso de fierros secundarios en la fundición (Scrap). La gran flexibilidad que ofrece el proceso permite producir tan bajo tonelaje sin sacrificar el costo de producción por tonelada de metal. Asimismo, las reparaciones pueden hacerse con gran facilidad, quitando la alimentación, drenando el horno eléctrico y cortando la corriente. Se puede operar el tonelaje deseado en una planta ya instalada con un pequeño descenso en la eficiencia. Por ello, es el método más adecuado en los lugares donde no se dispone de coke, tal es el caso de Chimbote - Perú y en donde se dispone de energía eléctrica barata, y de carbones que requieren procesos caros para su coquificación.

Nov 1, 1963

By W. E. Young, D. T. Delicate

This study was made to present the mining methods and costs of a uranium mine typical of other mines in the highly productive Westwater Canyon member of the Morrison formation in New Mexico. Four mining methods have been used at the Section 23 mine: the retreat- room-and-pillar method, a sublevel-slicing method (also called top-slicing), the horizontal-cut-and-fill method, and a modification of the ring-drill method. The application of the methods at this mine and at other mines in the area should be of benefit to operators with similar problems. Ore bodies in the Section 23 mine are irregularly shaped and vary in size, in rock strength, in moisture content, and in uranium concentrations; different mining methods are required and mining costs are not constant. A 6-month period of operation at the Section 23 mine was analyzed and mining costs, not including amortization, depreciation, or Federal taxes, averaged about $6.80 per ton.

Nov 1, 1963

By Max Arias Shreiber

El presente texto establece de forma general los aciertos y deficiencias más importantes del Código de Minería de 1950. Para elllo, se revisa las características de la industria minera, productividad, nivel de inversión, sistema de propiedad eminente del Estado sobre los yacimientos mineros, establecido por la Constitución y repetido por los Códigos Civil y Minero.

Sep 1, 1963

By D. A. Sutch

En 1958 se instalaron dos hornos Tysland-Hole en la planta Siderúrgica de Chimbote, construído por Elektrokmisk A.S, cuya sede social se encuentra en Oslo, Noruega. En ese sentido, el presente texto describe el funcionamiento de dichas hornos para la reducción de minerales de fierro en Chimbote. Para el revestimiento del horno se emplean materiales aislantes diversos y tres tipos de mezclas refractarias que se colocan mediante apisonado. Asimismo, estas mezclas retractarias son apisonadas contra moldes metálicos que permanecen "insitu", es decir, que reciben la primera carga del horno.

Sep 1, 1963

By Víctor T. Mejía Campos

El presente texto describe el proceso de remolienda efectuado en el circuito de flotación de bulk en la concentradora Casapalca. Dicho estudio se basa en dos proyectos anteriores, donde se buscó mejorar la molienda inicial con la instalación de un molino de bolas Marcy - 64-1/2 y el uso cuatro ciclones tipo Krebs de lú11 (3 en trabajo permanente y uno de repuesto) y un clasificador tipo Dorr Duplex de 71 x 28-1/2' de 19 rastrilladas por minuto. Dado el éxito obtenido en el primer proyecto, se prosiguió con el segundo. Finalmente, el 6 de octubre entró en operación normal el nuevo circuito de remolienda de las partículas gruesas en el circuito de flotación de bulk donse se comparó los promedios de los resultados metalúrgicos obtenidos en el año 1960, contra los resultados obtenidos en el año 1962 y se evidenció que este proceso mejoró la recuperación, produciendo más toneladas adicionales de concentrados.

Aug 20, 1963

By Luis A. Maradiegue

El presente estudio refiere el diagnóstico correcto de la silicosis a través de una revisión de la historia ocupacional, historia clínica y el ambiente del trabajo del trabajador. El control del trabajador y del ambiente de trabajo, lo deben realizar los médicos e ingenieros, para evitar o retardar la progresión de la silicosis o enfermedades respiratorias y facilitar el cambio de lugar de ocupación del trabajador, controlando el medio ambiente, respectivamente. Asimismo, en la evaluación del riesgo silicógeno en una industria extractiva, el ingeniero utiliza el instrumento Midget Iapinger, el muestreo, y los métodos de "campo brillante" para la cuenta de particulas, y la dispensación de la muestra en aceite de inmersión para la medición de partículas. El análisis de sílice libre comprende los métodos petrográficos, difracción de rayos X y el de fusión. Finalmente se hace una interpretación de resultados y se presenta un informe detallado de la condición de salubridad del trabajador.

Aug 20, 1963