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By S L. Birch, M D. Raven

X-ray diffraction (XRD) is a well-recognised, invaluable tool to provide detailed mineralogical analysis on a wide range of applications. However, despite the wide use of XRD in many industries, there are currently few recognised standard methods for quantitative XRD analysis and none for the analysis of iron ore materials. An initial step towards preparing a standard method for XRD analysis of iron ores was to assess the current level of precision achievable by practitioners of the technique by organising an international round robin. Six Australian chemically certified iron ore reference materials were distributed to over 100 international participants. A summary of over 120 data sets from more than 80 participants is presented. Results show that a bewildering array of techniques for sample preparation, data collection, phase identification and quantification were used. The reported values for the main components (ie hematite, goethite, quartz and amorphous content) show not only extensive variability between participants but also within participants’ results for those who submitted multiple data sets. The disappointing low level of precision exhibited for a relatively simple mineral phase system indicates a strong requirement for development of a standardised procedure.CITATION:Raven, M D and Birch, S L, 2017. Summary of results of an international X-ray diffraction round robin for mineralogical analysis of iron ores, in Proceedings Iron Ore 2017, pp 599–604 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By Robert T. Chapman

Many of us are privileged in that we have witnessed the transition from mining methods used in the first quarter of the twentieth' century to those practiced today. In the late Twenties, for example, many mines still used hand mucking methods. In the middle Thirties, more than one large metallurgical limestone quarry still used the 4 cubic yard railway steam shovel formerly in use at the Panama Canal. Mules could occasionally still be found underground, where they provided the-main-source of motive power. Within the last decade, and even within the past five years or less, great improvements have been made in blast-hole drilling, ore loading, and ore hauling equipment. Industrial demand for minerals can be expressed in exponential terms as compared to that at the turn of the century. Even marine mineral resources are receiving accelerated attention. One overall result is that larger and lower grade orebodies can be exploited at a profit. This profit must be made despite, for example, a static monetary price for gold, and despite the continual cost escalation involving labor, materials, supplies, and equipment. Accordingly, the application of the necessary degree of knowledge and judgment required to meet production, cost, and profit goals is paramount.

Jan 1, 1966

By I H. Jung, W O. Choe

Gallium (Ga)-containing compounds such as Gallium Arsenide (GaAs) and Gallium Nitride (GaN) are widely used in electronic devices due to their superior electro-optical properties and their usages increase rapidly. For the sustainable supply of Ga to electronic industry, therefore, the recycling of Gallium becomes essential. Pyrometallurgical Ga recycling process involves the complex chemical reactions between slag, matte, liquid metal, gas, refractories, etc. Therefore, the accurate thermodynamic information and phase diagram data for the oxide system containing Ga2O3 is important. In the present study, new phase diagram experiments for binary SiO2-Ga2O3 and ternary CaO-SiO2-Ga2O3 system are carried out using Differential Thermal Analysis (DTA) and quenching experiments followed by Electron Probe Micro-Analyser (EPMA) and X-Ray Diffraction (XRD) phase analysis. Based on new phase diagram data and available literature data, the thermodynamic modelling of the entire CaO-SiO2-Ga2O3 system is performed for the first time.

Jun 19, 2024

By Du Sichen, S. Seetharaman, A. Jakobsson

"In the Present paper, the principles of oxygen potential measurements have been discussed along with the design details for oxygen sensors that are used in copper industry. A description of some of commercial probes is presented along with their salient features. The application of these sensors in flash smelting, converter and casting sections of copper production are discussed along with their implications on process optimization.I. IntroductionThe high temperature galvanic cells have come into prominence on account of their numerous applications in both fundamental as well as applied measurements. Since the inception of the oxygen-ion conducting electrolytes like ZrOrCaO·by Kiukkola and Wagner [1], the oxygen concentration cells have been extensively used in laboratories as well as in industries. In metal-production technology, these cells have been used to monitor the oxygen potentials in metallic, slag as well as gas phases and also to control and styr metallurgical processes. The pioneer among the various industrial users of such cells is the copper industry. To-day, high temperature solid electrolyte cells involving oxygen ion conducting electrolytes have become an integral part of copper pyro-refining and continuous casting. In the present paper some of the applications according to the industrial processes are described including the developments that are going on in the European scene."

Jan 1, 1997

By P. C. Pistorius, M. P. Maphutha, J. D. Steenkamp

Advanced high-strength steels (AHSS) are sophisticated materials being developed by the steel industry to mitigate challenges related to the performance of motor vehicles. To meet the requirements of AHSS, the ferromanganese alloys (FeMn) utilized in the production of the steel are required to contain acceptable levels of unwanted impurities, i.e. P, S, N, H, and C. The focus of the current study was to investigate dephosphorization of ferromanganese to produce a low-P alloy that could be effectively utilized in the production of AHSS. The study involved conducting laboratory-scale testwork to study the efficiency of CaO-based slag systems to dephosphorize FeMn alloys. The addition of Na2O, CaF2, and BaO to MnO-CaO-SiO2 slag was considered. The test work was carried out in a 25 kW induction furnace at temperatures of 1350°C, 1400°C, and 1450°C. The P partition coefficient (Lp) remained small at <1, which is an indication that dephosphorization had not been achieved. The baseline slag, comprising 40%CaO-40%SiO2-20%MnO, reported higher Lp values. Addition of Na2O and CaF2 did not show any further benefit. Substituting half of the CaO by BaO, resulted in similar Lp values to those of the baseline slag under conditions of 1350°C and 1450°C at 30 minutes. In summary, based on the Lp values obtained, the conditions investigated with the CaO-based slags appeared to have been unfavourable for dephosphorization of FeMn alloys, as most of this impurity element remained in the alloy.

Sep 1, 2021

By C. Gu

Flow field design is critical for PEM fuel cells. The flow field design can affect reactant distribution to the catalyst surface, water management, thermal management and current collection. Therefore, it has tremendous impacts on the fuel cell performance and durability as well as reliability and operational flexibility. In this paper, an optical method is used to study the reactant distribution in the flow field channels of two commonly used flow field designs, straight channel design and serpentine channel design. Images of the flow patterns are shown followed by discussions of the flow patterns.

Jan 1, 2005

By C. Kunze

ABSTRACT Although closure sureties cover works that are carried out during the existence of a mining company, certain liabilities are not known when the surety is established and become apparent only in a late stage of the closure phase, or even after the site has been relinquished. This paper supports the concept that these financial risks lend themselves to insurance solutions. Making insurance for unknown liabilities mandatory while defining unambiguous legal conditions could create a viable market for insurance products, provide a sufficient statistical basis for the calculation of premiums, and reduce costs.

Jan 1, 2013

By C. G. Carlström

The total iron ore production in Sweden in 1969 was 33.3 million metric tons. 31.7 million tons were exported mainly to Western European countries. 27.8 million tons (87 per cent) originated from the mines at Kiruna, Svappavaara and Malmberget, located just north of the Arctic Circle in Sweden. Planned production for 1970 is 25 million tons during 10 months, due to a strike at the beginning of the year. Present production plans for the next five years expect an annual export capacity around 33 million tons in 1975, including 5.7 million tons of pellets. The mining and shipping at the loading terminals of Narvik on the Atlantic coast and Luleå at the Gulf of Bothnia are managed by LKAB - a 96 per cent state-owned company. 4 per cent of the share capital is owned by the private Grängesberg Company. The railway - 106 miles from Kiruna to Narvik and 130 miles from Malmberget to Luleå - is operated by the State Railways in Sweden and Norway. Comprehensive expansion of the Narvik ore port will be carried through during the next five years to increase the annual shipping capacity to at least 35 million tons and meet the development of rapidly growing ship sizes.

Jan 1, 1970

By H. Breuer

Mineral processing is characterized by a constant adaptation to changing raw materials and market conditions. It is the link between the mined raw material and a marketable product. As a lot of high grade reserves are exploited, a steady deterioration of raw material quality can be observed. At the same time, the customers´ requirements for product purity and consistent quality increase. Indian iron ores are characteristically friable in nature that results in generation of sizeable quantity of fines (0-10mm) every year during various stages of mining and processing in the country with grade varying from 50-60% Fe(T) and are high in silica/alumina (Al2O3 5-8%). The fines generated cannot be directly used for iron making (blast furnace/DRI units) in the country due its physical and chemical properties; therefore, large portion of it gets exported or dumped. Value addition to iron ore fines through various activities such as beneficiation & palletization is the need of the hour, which will not only be economically beneficial to the mining sector in the long run but also generate value addition & employment opportunities. Incentives may be given for adopting latest technologies for direct use of fines in iron making by agglomeration of fines in the form of Pellets and Sinters, as fines forms considerable part of iron ore resources. Due to selective mining, although the iron content of the ore is high but the alumina(Al2O3) content in iron ore is also significantly high which demands for beneficiation as high alumina will create problem during iron making like higher fuel consumption, poor quality of slag produced, reduced productivity of B.F. all mineral has been engaged in hematite iron ore beneficiation with its gravity and magnetic separators since the mid-nineties. The delivery of jigs started for the upgrading of iron ore for its utilization in a Direct Reduction Plant in Australia. Since then, various other installations with jigs for lumps and fines as well as upstream separators for fines are in operation in Brazil, Australia, India and South Africa. Low grade run of mine and/or dump ores are being processed with alljig®-, allflux®- and gaustec®-WHIMS as the core equipment. The article describes the technology in use, the characteristics of various iron ores and the product qualities achieved. The data presented shows the specific advantages of jig application on iron ore upgrading due to the possible high gravity cuts and the easy and low cost operation. The allflux®- technology provides the big advantage of high capacities and a two-step process, both in a single unit. The gaustec®-wet high intensity magnetic separators offer high capacity in combination with unsurpassed process flexibility. Keywords: iron ore, gravity separation, jig, upstream classifier, wet high intensity magnetic separation (whims), pelletization, sinteringMineral processing is characterized by a constant adaptation to changing raw materials and market conditions. It is the link between the mined raw material and a marketable product. As a lot of high grade reserves are exploited, a steady deterioration of raw material quality can be observed. At the same time, the customers´ requirements for product purity and consistent quality increase. Indian iron ores are characteristically friable in nature that results in generation of sizeable quantity of fines (0-10mm) every year during various stages of mining and processing in the country with grade varying from 50-60% Fe(T) and are high in silica/alumina (Al2O3 5-8%). The fines generated cannot be directly used for iron making (blast furnace/DRI units) in the country due its physical and chemical properties; therefore, large portion of it gets exported or dumped. Value addition to iron ore fines through various activities such as beneficiation & palletization is the need of the hour, which will not only be economically beneficial to the mining sector in the long run but also generate value addition & employment opportunities. Incentives may be given for adopting latest technologies for direct use of fines in iron making by agglomeration of fines in the form of Pellets and Sinters, as fines forms considerable part of iron ore resources. Due to selective mining, although the iron content of the ore is high but the alumina(Al2O3) content in iron ore is also significantly high which demands for beneficiation as high alumina will create problem during iron making like higher fuel consumption, poor quality of slag produced, reduced productivity of B.F. all mineral has been engaged in hematite iron ore beneficiation with its gravity and magnetic separators since the mid-nineties. The delivery of jigs started for the upgrading of iron ore for its utilization in a Direct Reduction Plant in Australia. Since then, various other installations with jigs for lumps and fines as well as upstream separators for fines are in operation in Brazil, Australia, India and South Africa. Low grade run of mine and/or dump ores are being processed with alljig®-, allflux®- and gaustec®-WHIMS as the core equipment. The article describes the technology in use, the characteristics of various iron ores and the product qualities achieved. The data presented shows the specific advantages of jig application on iron ore upgrading due to the possible high gravity cuts and the easy and low cost operation. The allflux®- technology provides the big advantage of high capacities and a two-step process, both in a single unit. The gaustec®-wet high intensity magnetic separators offer high capacity in combination with unsurpassed process flexibility. Keywords: iron ore, gravity separation, jig, upstream classifier, wet high intensity magnetic separation (whims), pelletization, sintering

Sep 1, 2012

By Gabriel Gonzalez, Paulo Couceiro, Luis Manriquez, Alejandro Gutierrez, Juan Navarro

A high-stakes blasting campaign was successfully executed at a major open pit copper mine in northern Chile. This operation posed a significant technical challenge due to its immediate proximity to the tailings dam - a critical infrastructure whose structural integrity depends on strict control of blast-induced seismic vibrations. The geological complexity of the area, characterized by upper andesite interbedded with caliche (carbonate), further complicated the operation. This lithological composition, known for its high tenacity and cohesion, posed additional challenges for achieving effective fragmentation, necessitating a highly customized blast design and loading strategy. The campaign included four production blasts and one secondary blast, all executed under the constraint of not exceeding the Peak Ground Acceleration (PGA) threshold of 0.64g, as defined by the Maximum Credible Earthquake (MCE) scenario. To ensure compliance, geophones were strategically installed at three monitoring points (P1, P2, and P3) on the dam to capture real-time acceleration data. The use of specialized blast patterns, precise stemming control, and electronically sequenced detonations ensured that all recorded accelerations remained well below the critical threshold. A total of 496,163 tonnes of material were safely blasted, with 8,452 meters drilled and powder factors ranging from 419 to 594 g/ton. Therefore, this case study exemplifies operational excellence in controlled blasting, demonstrating the feasibility of safe mining near geotechnically sensitive zones through predictive modeling, rigorous QA/QC, and post-blast analysis.

Jan 26, 2026

By R. E. Fanning

"IntroductionThe Aluminum industry is one of many materials industries which strive to make their material the preferred choice for large volume products. In some applications one material has a natural advantage over others, but more frequently several materials compete with one another, each providing one or more advantages and some trade-offs. Customers may design their product with several objectives such as minimum system cost, maximum customer appeal or maximum manufacturing flexibility, choosing materials which best combine cost and performance. In such markets it may become necessary for a material supplier to enhance the attractive features of the particular material to outweigh its disadvantages.It is difficult, if not impossible, to predict how various materials will evolve. Technological breakthrough, government regulations, material availability or sociological issues may redefine the balance between competing materials. In spite of some uncertainty regarding the competitive position of competing materials, there is little doubt that unrelenting pursuit of product quality improvement and cost reduction are essential to future viability of the aluminum industry. It is the intent of this paper to identify some areas where technological improvement would be beneficial. Thus this paper is a collection of briefly described problems that will hopefully stimulate the thoughts and research required for knowledge based solutions. Rolling ProcessA particular example is the beverage can industry where aluminum, steel, glass and plastics vie for a share of the m.arket. The high cost of aluminum relative to steel or glass requires minimizing the amount of metal per can. The high intrinsic value of aluminum has led to extensive recycling of cans although net metal cost is still higher than that of the competing materials. Intensive engineering of the beverage can led to improved design and better understanding of material requirements. These improvements permitted substantial reduction in sheet thickness over the past decade. The downward trend in metal thickness for beverage can sheet is shown in Figure 1."

Jan 1, 1988

By Guy A. Johnson

This Bureau of Mines report summarizes the results of efforts to develop reasonably priced, reliable mine shaft fire and smoke protection hardware for metal and nonmetal mines. The hardware was incorporated into a viable prototype system that would minimize fire and smoke hazards. The design of the system had to be sufficiently flexible to be utilized in a wide variety of metal and nonmetal mine shaft and shaft station configurations. As a result of long-term, rugged field tests, an improved (second generation) system was developed. The hardware is now commercially available.

Jan 1, 1978

By D. Harrington, M. W. Von Bernewitz

Sections 120 and 121 of Article XI. Fire Control, of a proposed Mine Safety Law in preparation, to be used as desired and when approved by any State, contains these provisions: After the adoption of these regulations, no mine operator shall erect any nonfireproof structure within 50 feet of any mine entrance. or airway. Every operating mine having nonfireproof structures within 50 feet of any mine entrance or airway, except headframes necessary for hoisting, shall have such structures fireproofed or removed and replaced with fireproof structures within six months of the adoption of these regulations. Before reopening, mines idle at the time of the adoption of these regulations shall have all non- fireproof structures fireproofed, removed, or replaced with fire- proof structures as required by the foregoing sentence. Upon receipt of the written statement of a mine operator that the fireproofing of existing structures is impracticable, the chief mining engineer (of the State commission) shall satisfy himself as to the abouracy of the statement. If he concurs that fireproofing is impracticable, and if at the same time he holds the opinion that adequate protection can be provided otherwise by such procedure, he shall have authority to issue a written permit for the substitution of fireproof door at or near portals of mine openings and collars: of shafts. Such doors shall fit as nearly gas-tight as possible. and shall be installed in such a way that the mouths of mine open- ings can be closed readily from outside of structures. The effec- tiveness of such permit may be made contingent upon the operator's continued compliance with any additional precautions which are necessary in the chief mining engineer's opinion to protect the lives of miners.

Mar 1, 1932

By Thomas Niehoff

"Oxyfuel combustion systems are state of the art for many melting operations. Airfuel systems have been stepwise modified to oxygen enrichment, oxygen lancing and oxyfuel. Every change of the melting process will have consequences with regards to emissions and energy usage. The uniqueness of many operations requires unique skills to resolve potential issues. This paper will give some examples of how airfuel systems can successfully be converted to oxyfuel.IntroductionOxyfuel technology – meaning the combustion of fossil fuels such as natural gas, oil or coal with technical oxygen instead of air for industrial melting or heating processes is widely used in many industries these days. Even though oxygen production, storage and handling has been state of the art for decades other opinions exist. Often oxyfuel is regarded with fear and potential hazards like: “Oxygen makes the process too hot.”, “Oxygen will melt away the refractory.”, Liquid oxygen is dangerous.”, “Oxygen will cause explosions.”, ……etc.Typically a more detailed discussion about a specific industrial process and how oxygen can be applied in a safe and economic way the seeming issues go away."

Jan 1, 2010

By P. D. Nolan

Smelters operating under pollution control orders have become increasingly dependent upon the reliable operation of sulphuric acid plants and no factor affects the long term reliability of those plants more than efficient gas cleaning. The sources and characteristics of contaminants in smelter of fgases and the conventional approaches to removing these contaminants to accepted levels are discussed. New technology is described which offers advantages of lower capital cost, lower operating cost and reduced space requirements over the conventional approaches. This new technology has been developed by LAB s.a. and is licensed for metallurgical gas applications by Chemetics International Company.

Jan 1, 1983

By A. Whillier

Note: Hydraulic rock drills and their effect on the underground environment by A. WHILLIER, Pr. Eng Se. D., (M.tT.) (Fellow) In any situation where hydraulic rockdrills are used underground, it is evident that an amount of heat equivalent to the total electric input to the power pack would enter the ventilation air. Book review Australian Mineral Industry 1972 Review. Australia, Department of Minerals and Energy. NIM report Report no. 1691 The determination of zirconium and aluminium by 14MeV neutronactivation analysis. Automation in Mining, Mineral, and Metal Processing The International Federation of Automatic Control (IF AC) is to hold its second symposium on the above subject in Johannesburg on 13th to 17th September, 1976. V Simposio de Mineracao A symposium is being arranged for 6th to 9th August, 1975, in Ouro Preto, Brazil. ACHEMA 1976 The 18th Chcmical Engineering Exhibition-Congress and European Meeting of Chemical Engineering will be held in Frankfurt from 20th to 26th June, 1976, and thc Chemical Engineering World Congress Sixth Underwater Mining Institute The above Institute will be held on the main campus of the University of Wisconsin in Madison, U.S.A., on 2nd and 3rd October, 1975.

Jan 4, 1975

By A. T. Harris

Ground quartzite, known in the industry as amorphous silica, is produced from a quartzite deposit near Honey Brook, Pa., by George F. Pettinos, Inc., of Bala-Cynwyd, Pa. The quartzite is mined by the open pit method and processed in a mill at the mine. The operation regularly produces five standard grades of sand and one grade of crushed stone; however, the company accepts special orders and will produce material to meet the customer&apos;s specifications. Beneficiation (chiefly crushing and screening) is controlled by laboratory screen tests on samples taken during preparation of the sand. The chief uses of the sand are for foundry operations, furnace lining, concrete aggregate, and other specialized uses. The quartzite in this deposit is of uniform composition and does not require control by chemical analysis. However, for special purposes, analysis will be furnished.

Jan 1, 1965

By A. T. Harris

Ground quartzite, known in the industry as amorphous silica, is produced from a quartzite deposit near Honey Brook, Pa., by George F. Pettinos, Inc., of Bala-Cynwyd, Pa. The quartzite is mined by the open pit method and processed in a mill at the mine. The operation regularly produces five standard grades of sand and one grade of crushed stone; however, the company accepts special orders and will produce material to meet the customer&apos;s specifications. Beneficiation (chiefly crushing and screening) is controlled by laboratory screen tests on samples taken during preparation of the sand. The chief uses of the sand are for foundry operations, furnace lining, concrete aggregate, and Other specialized uses. The quartzite in this deposit is of uniform composition and does not require control by chemical analysis. However, for special purposes, analysis will be furnished.

Jan 1, 1965

By H. R. Babitzke, H. Kato, M. D. Carver

A number of columbium and tantalum alloys were investigated to determine their suitability for use at elevated temperatures . Columbium-vanadium , tantalum-vanadium , and tantalum-hafnium alloys , and also columbium- 10 wt pct titanium alloys modified with additions of 0.1 to 2 mole pct ZrO2 , TiO2 , ZrB₂ , TiB , ZrC, or TiC were prepared and examined . Workability , tensile properties , and oxidation resistance were tested . Of the columbium alloys studied , the columbium- 12 at . pct vanadium exhibited the best properties ; it compared closely with the columbium- 10 at . pct vanadium alloy studied in a previous investigation.

Jan 1, 1964

By J. W. Meier, J. O. Edwards, R. C. Bell

"IntroductionTHE DIE CASTING industry .as we know it today is the direct result of the invention and development of die casting machines during the nineteenth century and of reliable alloys in the twentieth. The early machines were designed to cast low melting point metals such as lead .and tin, and their alloys.It was inevitable that, as these die castings were put into service, the demand should arise for stronger materials. Zinc alloys, often containing lead, tin, copper, and aluminum as major constituents, were relatively easy to cast and stronger than the lead and tin alloys. However, it became apparent after a number of years that these zinc alloys tended to become brittle, distort, and corrode, particularly if kept in warm, humid atmospheres. Thus, considerable quantities of zinc-base .alloys were in use before the trouble was realized and effective measures could .be taken to determine the cause of the instability.The deleterious effect of certain metallic impurities on the properties of zinc •die casting .alloys has now been known for about thirty years. Brauer .and Peirce, and, later, other research workers of the New Jersey Zinc Company such as Anderson and Werley, discovered the pronouned effect of lead, cadmium, and tin on the stability of zinc-alloys."

Jan 1, 1952