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By Ernest Darby

IF the correct balance between fuel and air is maintained in an open-flame furnace,1 little chemical action may be expected between the products of combustion and the metal being melted. Physical changes in the metal are the object of the melting operation, and indirectly, under certain conditions, may be the cause of subsequent chemical actions. If sufficient heat has been introduced into the metal to bring about the change from the solid phase to the liquid phase, and still further from the liquid to the vapor phase, the metal vapor in all probability will be carried from the furnace by the exhaust and rapidly combined with the oxygen of the outside air. The charge being melted in the furnace may contain elements which are chemically inactive at normal temperatures but which will form compounds at the elevated temperatures of the metal bath, or even at a lower degree. Such indirect chemical actions are very confusing and often lead to incorrect conclusions regarding furnace atmospheres. In the open-flame furnaces used in the melting of bronze, the furnace atmosphere is spoken of as being either neutral, oxidizing or reducing in its effect upon the metal. A neutral atmosphere, as mentioned, is generally considered as the atmosphere of the furnace that will produce melted bronze, neither oxidized nor gassed. It is in effect an atmosphere which is not directly the cause of any chemical action. In such an atmosphere absolutely pure metals may be melted and poured without the absorption of gases or the formation of metallic oxide. The metal has undergone a simple, physical change.

Jan 1, 1930

By R. Pérez, James A. Finch, F. Tavera, Cesar O. Gomez

"Gas holdup is a variable which affects the operation of flotation columns. On one hand, gas holdup is a function of bubble size (a function of sparger type, frother characteristics and concentration, and air flowrate), tailings flowrate, solids content, and mixing patterns in the collection zone. On the other, gas holdup defines flotation kinetics and carrying capacity. Therefore, gas holdup is a useful variable to control and diagnose the operation of a flotation column, but the lack of a reliable sensor for on-line gas holdup monitoring has prevented its use in industry.This work describes the principle and the practical difficulties associated with the development of a gas holdup sensor based on the measurement of the electrical conductivity of dispersions. Two different approaches have been devised. These approaches will be described and test results presented of prototypes in laboratory and industrial columns.Background.Several years ago, a research program was initiated at McGill to use electrical conductivity as the basis for developing sensors for process measurements in mineral processing. Electrical conductivity is an intensive property which is a function of the concentration of the different phases present in a dispersion. The initial focus was on the detection of the interface between two dispersions with different characteristics (i.e., that between the collection and froth zones in flotation columns or that between clear water and sedimented solids in thickeners). The technique works in this case by searching for the location at which a sudden change in specific conductivity occurs, as a consequence of different gas holdup or solids content, and absolute values of the specific conductivity of the dispersions involved are not necessary1,2."

Jan 1, 1995

By Rudolph K. Hoagberg

Silica sands, primarily in coarse size ranges, are used to prop open fissures or voids created in the bedrock by hydraulic fracturing. This procedure increases the flow of gas or oil or other fluids through the bedrock. The sands used must meet various specifications relating to their physical and chemical characteristics; these characteristics are in turn related to the geologic provenance of the sand deposit. The Jordan Sandstone, a Cambrian formation which is exposed in Minnesota and Wisconsin, meets the specifications of a proppant sand by virtue of its depositional history and its sedimentary properties.

Jan 1, 1980

By G. S. Rice, J. A. Davis

The Péchelbronn oil field is located in the province of Alsace, in the Rhine Valley, about 30 miles north of Strasbourg. It is approximately 4 miles wide and 12 miles long, extending from the villages of Lobsann on the north to Wintershausen and Ohlungen near Haguenau on the south. (See Fig. 1.) The productive area includes about 44,000 hectares (107,680 acres). The name Péchelbronn signifies "pitch-spring" or "pitch-fountain." The first exploratory galleries were driven in from the hillside in 1735; and in 1745 the first official concession was granted by the French government and the first pit sunk to a depth of about 30 ft. Extraction by drilled wells was begun in 1879, supplementing the mining operations, and during the next 10 years 200 wells were drilled to an average depth of 172 m. (568 ft.). The bringing in of two "gusher" wells, in 1882 and 1888, respectively, was followed by the abandonment of all underground work. Underground mining, with a view to increasing the production of petroleum by recovering the oil left in the sands after drilling wells, was resumed in 1916. This mining operation started by sinking shaft No. 1 to a depth of 150 m. (495 ft.). The underground developments were pushed during 1917 and 1918 and the annual production of the Péchel-bronn field was increased to about 50,000 metric tons or 350,000 bbl. On the signing of the Versailles Treaty the province of Alsace, which had been taken by Germany as the result of the war of 1870, was returned to France, and the proprietary rights were taken over by the French Government. Concessions or leases, which embraced all the known oil-bearing territory of the field, were granted to the present operating company, Mines de Péchelbronn. This company followed both the drilling and the mining methods of the previous company.

Jan 1, 1927

By Hans von Michaelis

The revolution in development of new technology and practices in the gold mining and metallurgy industry continues unabated despite the ups and downs in the gold price. Some of the new cutting edge technologies are listed in Table 1 overleaf. There is room to discuss just a few of these here, but many more are identified and described in RANDOL (1992). Cutting edge advancements in gold recuperation, can be sorted into three categories. The first category includes fundamental advances that offer major improvement with significant economic benefits. Second would include evolutionary developments that offer smaller, but nonetheless commercially valuable improvements. Finally there are those "advances" that are interesting but of trivial or question­able economic benefit to industry. It is essential to adopt a "systems approach" philosophy towards developing and applying new technology. Practical innovation often comes about as a result of having to solve a problem. Innovation for innovation sake is an ego trip. Environmental management has become an important part of the system and the environmental implications of new processes and practices in the mine and mill have to be carefully considered for potential benefits and/or liabilities.

Jan 1, 1993

By G. Hergert

SUMMARY Three gradients have been identified in regard to the average horizontal ground stress increase with depth. [S (0-900 m) = 9.86 MPa + 0.0371 MPa/m SHa (900-2200 m) = 33.41 MPa + 0.0111 MPa/m SHae (extreme)= 12.36 MPa + 0.0586 MPa/m] The extreme stress values are not caused by mining geometry and are of limited extent only. In some cases geological disturbances like faults and rock type boundaries suggest an explanation but in other cases the unusually high stresses cannot be explained readily. It is interesting to note that in the same locations the vertical stress components are very much higher than those derived from overburden weight and that the vertical stress gradient is similar to the gradient obtained from the extreme horizontal stress components. INTRODUCTION Ground stress determinations have been carried out in mines in Ontario and Manitoba, Canada, over more than a decade (Herget, 1980). Most of the sites are located in the Superior and Southern Tectonic Province of the Canadian Shield, which consist of Archaen and Proterozoic rocks comprising volcanics, metamorphosed sediments and granites. The youngest orogenic deformation occurred during the Grenville Orogeny (955 million years ago).

Jan 1, 1982

By Basil B. Zavoico

During 1938 the Russian oil industry, while able to increase its production 4.69 per cent above the preceding year, was not successful in correcting some of its basic difficulties, and the industry's position as it entered 1939 was unsatisfactory. The internal political difficulties of 1937 and 1938 took a toll in the oil industry as they did elsewhere in the U. S. S. R., further complicating the solution of the problems facing it, most important of which still remain: lack of experienced and responsible leadership, able to make quick decisions; undisciplined and migratory labor; and insufficient and often unsatisfactory quality of the various equipment needed by the industry and its ineffective distribution. Recent developments in the U. S. S. R. suggest that during 1939 the management will be granted more latitude and hence somewhat better results may be anticipated from the executive branch, provided, however, the "purges" do not recur. The labor should be better disciplined and should not shift as easily, owing to the introduction, at the close of 1938, of individual labor passports to all workers in the country, the principal purpose of which is to correct those two deficiencies. It is not anticipated, however, that the service of supply will show any appreciable improvement in 1939, partly because of inherent difficulties and partly because the manufacturers of heavy machinery are working primarily and necessarily for munitions. Production Production of crude oil during 1938 is estimated at 224,714,000 bbl., as compared with 212,742,000 bbl. in 1937, an increase of 4.69 per cent but 12.76 per cent below the planned output. While there were no major readjustments in the source of supply of crude oil, both the older districts, Baku and Grozny, were barely able to maintain their 1937 levels of production, the increased output being supplied primarily by the fields of Maikop and Ural Permian Basin districts. While exploration work was outstandingly successful in 1937, in 1938 no discoveries of any

Jan 1, 1939

By Basil B. Zavoico

During 1938 the Russian oil industry, while able to increase its production 4.69 per cent above the preceding year, was not successful in correcting some of its basic difficulties, and the industry's position as it entered 1939 was unsatisfactory. The internal political difficulties of 1937 and 1938 took a toll in the oil industry as they did elsewhere in the U. S. S. R., further complicating the solution of the problems facing it, most important of which still remain: lack of experienced and responsible leadership, able to make quick decisions; undisciplined and migratory labor; and insufficient and often unsatisfactory quality of the various equipment needed by the industry and its ineffective distribution. Recent developments in the U. S. S. R. suggest that during 1939 the management will be granted more latitude and hence somewhat better results may be anticipated from the executive branch, provided, however, the "purges" do not recur. The labor should be better disciplined and should not shift as easily, owing to the introduction, at the close of 1938, of individual labor passports to all workers in the country, the principal purpose of which is to correct those two deficiencies. It is not anticipated, however, that the service of supply will show any appreciable improvement in 1939, partly because of inherent difficulties and partly because the manufacturers of heavy machinery are working primarily and necessarily for munitions. Production Production of crude oil during 1938 is estimated at 224,714,000 bbl., as compared with 212,742,000 bbl. in 1937, an increase of 4.69 per cent but 12.76 per cent below the planned output. While there were no major readjustments in the source of supply of crude oil, both the older districts, Baku and Grozny, were barely able to maintain their 1937 levels of production, the increased output being supplied primarily by the fields of Maikop and Ural Permian Basin districts. While exploration work was outstandingly successful in 1937, in 1938 no discoveries of any

Jan 1, 1939

By Albert Walcott

THE success of various operations in the manufacture of optical glass depends, in a large measure, on the ability to maintain proper heat control. A good pyrometer system is, therefore, a very necessary part of the equipment needed. Men of long experience in dealing with high temperatures, who have acquired through constant practice the ability of judging approximate temperatures by means of color, are undoubtedly valuable, but even the most competent are not as reliable as a good pyrometer system. They admit that their ability to judge accurately varies from day to day and that their judgment is affected considerably by the condition of the sky, whether it is clear or cloudy. Besides, where it is a matter of only a few weeks to train a man to operate a pyrometer system, it takes about as many years to train him to judge temperatures by the state of incandescence. The pyrometer outfit in use in the glass plant of the Bausch & Lomb Optical Co. consists of the following: Platinum elements, optical pyrometers; base-metal elements, indicators, potentiometers, and recording pyrometers. Platinum Elements and Optical Pyrometers.-Temperature control in - the melting operation is of such great importance that it is very desirable to know the exact temperatures, relative temperatures being of little value. The use of the platinum element is to determine the rate of heating or cooling of the furnace. The platinum couple is installed in either the crown or the wall of the furnace. It is placed first in a porcelain protecting tube and this is placed in a permanently fixed fireclay tube projecting from 1 1/2 to 2 in. into the fire-chamber. It has been found impractical to use the platinum couple for determining exact temperatures of the melting furnace, for the platinum element deteriorates rather rapidly at the high temperatures used, 2500° to 2700° F. (1371° to 1482° C.). When protected and installed as described, though,

Jan 9, 1919

By Edwin H. Bentzen, Immo H. Redeker

Important industrial minerals are separated and concentrated by froth flotation by industry today. The following descriptions are presented as an overview of the methods employed to separate and recover a few of these industrial minerals. The minerals described in this section of the book are not, by any means, the only important minerals treated by froth flotation. Other minerals, such as calcite, kaolin, wollastonite, rare earths and vermiculite were not included, primarily due to the confidential nature of the information held by the Minerals Research Laboratory and the Colorado School of Mines Research Institute. Flotation of nonmetallic minerals is sometimes viewed as alchemy. However, the art is, in reality, based on sound chemistry, experience and a little luck in the treatment of new ores. In the flotation of nonmetallic minerals, as opposed to base metal sulfides, highly specific treatment conditions are required to accomplish separations. The presentation of the treatment of each of the minerals described was outlined as follows: DEPOSITS PROCESSING SPECIFICATIONS FLOWSHEETS (in some cases) A presentation of the factors, often critical, which must be carefully investigated to accomplish successful flotation of nonmetallic minerals is presented in the section on Sulfonate Collectors, elsewhere in this volume.

Jan 1, 1986

By F. Julius Fohs

As an industry approaches stabilization, greater and greater stress must be laid on its technologic progress, which becomes a prime aid in improving its condition. The oil industry is tending toward this stage and hence its engineers must be pressed into greater service to prevent stabilization and stagnation from becoming synonymous, and to supply, either by improvements in processes or by new machinery, a means of obtaining savings in raw and finished products. Thus profits can be assured warranting continued investment. It may be repeated, technology must apply a slight improvement here, a change there, or a complete renovation, to eliminate inefficiencies and make each dollar invested yield greater results. The profits of ycstcrday were made of rich strikes, of monopolized patents or processes, of control of prices and of markets. Sixty-five years of growth, of large investment, of healthful competition, and of expanding markets, have put the oil industry in the foremost rank of world industries. .Just as the railroads passed a similar period of expansion and growth, and arc being stabilized with reasonable profits, so the oil industry must take advantage of the efforts of its engineers and experts to promote its healthful growth and a better service to the people. Herein is attempted a review of recent progress in which is presented the advances in exploration, production engineering, transportation, refining and greater efficiency in uses of petroleum, with a view not only to stressing important new processes and methods, but also the problems that press for solution. This review can only touch outstanding developments of recent years, but the several Petroleum Division symposiums of our program will present details worthy of attention. Exploration Geology offers directly little new in the technique of oil-finding— major stress being laid on improvement in subsurface correlation by means of foraminifera1 studies, additions to the knowledge of which are being made, slowly but surely, and by means of mineral, and especially heavy mineral, determinations in well samples. The general application

Jan 1, 1927

By S. W. Poole, J. A. Rosa

THE object of this investigation was to determine the distribution of chemical elements within a large, killed alloy-steel ingot, by sulphur printing and quantitative chemical analysis. With regard to segregation in steel ingots, the factors of melting practice, pouring temperatures, mold design, etc., and the mechanics of solidification and its attendant functions, have been the subject of intensive study over a period of years by many investigators. Notable among these is the Sub-Committee of the No. 5 Committee of the British Iron and Steel Institute. For an exposition 0f the many problems awaiting the researcher on the heterogeneity of steel ingots, the methods of attacking these problems, together with some of the answers, the reader is referred to the nine reports and numerous papers of that committee and its membership. STEELMAKING DATA Melt.-The heat was made in a 70-ton direct arc-type basic electric furnace. Furnace charge consisted of nickel-chromium-molybdenum steel, most of it in the form of heavy mill scrap. All of the scrap was charged cold. The standard double-slag method was employed, the heat being finished under a strong carbide slag. Aluminum was used as the deoxidizing agent. Tapping temperature, as observed with an optical pyrometer, was 3000°F. Detail of Mold and Ingot Size.-Details of the ingot mold and the ingot itself are given in Fig. I. Teeming.-Teeming temperature of the subject ingot as observed with an optical pyrometer was 2830°F. The ingot was top-poured directly through a 1 ½ in. nozzle and required 7 min., 44 sec. to fill up to the hot top. An additional 2 min., 30 sec. were required to fill the hot top. The ingot was stripped hot and charged with the remainder of the heat into an annealing furnace. There it was given the standard annealing cycle used for these ingots. Subsequent heat-treatments are described elsewhere in this paper. SECTIONING AND PREPARATION FOR SULPHUR PRINTING Because of previous favorable experience in sectioning ingots up to 21 ½ in. square with an oxyacetylene torch, it was decided to use this method to section the subject ingot. The ingot was preheated to 900°F. for 12 hr. It was then placed on a steel bed in a horizontal position so that the longitudinal axis was level and parallel to the track of the motor-driven torch carrier. Two cuts were made, one 2 in. above the longitudinal axis and the other 2 in. below. The time required to make each cut was approximately 75 min. The cutting operation is shown in Figs. z and 3. The 4-in. thick slab was mmediately charged into a furnace standing at 1200°F.

Jan 1, 1944

By Norman Pilling

The micrographic analysis of silicon steels is possible if a dilute solution of nitric acid and methyl alcohol in nitrobenzol is used. The action of this reagent differs from that of sodium picrate in that there is no persistent deep-seated staining and the solution is used cold. THE technical difficulties hampering the metallographic analysis of silicon steels are chiefly the result of the extreme corrodibility of these alloys. The addition of silicon to iron in increasing quantities, up to about 6 per cent., rapidly increases the susceptibility of the alloy to chemical attack, not only in acid solution, but in water. This renders the preparation of metallographic sections very difficult, because of a non-selective attack upon the finely polished surface by the water used as a lubricant in polishing. This water attack masks the true structural details revealed by suitable etching reagents. It is thus necessary to use alcohol as a polishing lubricant in the last stages of preparation and to avoid all etching reagents having an aqueous base. A specific reagent for the identification of iron carbide in ferrous alloys, and the one hitherto used almost exclusively by metallurgists, is an alkaline aqueous solution of sodium picrate, which stains this constituent selectively. Its application to silicon steels has not proved successful, as its distinctive selective action is more or less completely hidden by the general attack of the aqueous solvent on the silico-ferrite, greatly accentuated by the fact that this reagent must be used at its boiling temperature (105° C.). Thus, a powerful metallographic aid to the study of the higher silicon alloys, such as transformer steels, is lost. A new reagent has been developed for the purpose of overcoming this difficulty. It is with some hesitation that the list of etching reagents, already overburdened, is increased, but the properties of this new reagent are advantageous in several ways and a definite field for it may be found in the metallography of ferrous alloys.

Jan 1, 1924

By McKenzie C. K, Stewart R. S, Simpson J

Blast control in small scale underground mining leads to improved fragmentation control, improved control over overbreak and dilution, and the optimisation of drilling and charging operations. Greatly improved control can be achieved through blast monitoring, to confirm proper implementation of blast designs and blasthole charging. Further improvements can be achieved through simple modelling, enabling blastholes to be placed in the correct locations and charged with the correct weight and strength of explosive. Improved design can be shown to significantly reduce overbreak and dilution, and even ground support costs. In one mine in Quebec, open stopes of widths varying from 2.5 metres to four metres and dipping at 36¦ to 38¦ were designed to achieve zero dilution using open sloping blasting practices. The first stope designed in this manner was monitored in detail and achieved its objective.A method for contouring damage around blastholes is presented as a basis for selection of drilling patterns, with particular application to the control of overbreak and dilution. Contouring can be used to provide reliable estimates of either overbreak or damage (where rock is broken het reynainc in nlarr)

Jan 1, 1993

By Michel Garon

"Several years ago computer control of the flotation process was successfully implemented at the Matagami concentrator of Noranda Mines Inc. At that time this was the first computer application being installed at this operation. The last few years have seen an extensive use of programmable controllers in areas such as the copper and zinc dewatering circuits and the lime preparation system. With the aid of such instruments, these areas have attained a high level of automation and as a result, a high degree of efficiency. The controllers have proven to be very dependable and easy to use.IntroductionThe Matagarni Division of Noranda Mines Inc. operates two mines in the Matagami District of northwestern Quebec which is located about 650 km northwest of Montreal. The mines ship ores to a central concentrator whose throughput averages 95,000 tonnes of ore per month. Metal contents of the mill feed average 0.9 per cent copper and 5.0 per cent zinc. Concentrate outputs are approximately 3,200 tonnes of copper and 8,200 tonnes of zinc per month.The concentrator commenced operation in 1963. An on-stream X-ray analyzer was installed in 1968, providing analyses of several samples in the flotation circuit without the aid of a computer. In 1974, control of the circuit by computer was added to the system. As a result, zinc flotation efficiency improved considerably and reagent costs decreased through the reduction of copper sulphate consumption.In the past few years it was realized that significant improvements could also be made in other parts of the operation . Copper and zinc dewatering circuits and the lime preparation system were identified as major areas that could drastically benefit from automation. In 1982, programmable controllers were seriously considered as an attractive alternative for achieving the company 's goal. Because of their relative lowcost and their high degree of flexibility, they were selected for implementing automation and, for improving the efficiency in each of these areas."

Jan 1, 1985

By S. Webster, M. Karmis, C. Haycocks

Mining any seam can seriously affect subsequent operations in coal seams both above and below the one being mined. The effect is often detrimental to the recovery, cost and safety of mining the subsequent seams. This paper describes the ground control mechanisms involved in mining through a passive subsided zone or all actively subsiding trough. Data were extracted from case studies, primarily from the Appalachia region, for construction of empirical models to predict interaction problems that can occur in overlying seams. Inner-burden thickness, innerburden lithology, percentage extraction, lower seam height, time and overburden were analyzed to determine their effect on upper seam damage. Magnitude of upper seam subsidence was incorporated, together with a broad classification of rock types, to predict the type and range of damage that can occur in the upper seam. Results are summarized in graphically and nomogram form for use in. engineering design.

Jan 1, 1984

By J. B. Newsom

IN the Indiana limestone district, some 50 or 60 per, cent of the merchantable stone in a quarry opening is waste, and only about 40 or 50 per cent of the stone from the opening is finally sold. So long as the present system of quarrying is used, the wastes measured and reported in this paper will continue. Comprehensive development of an entirely different method of quarrying, using wire saws for cutting, promises great improvement. Some of the savings to be expected are pointed out in the following pages. No attempt has been made to measure losses due to variations and natural flaws in the stone, since these vary greatly in different quarries, and accurate measurement would be difficult. The wastes that have been measured account for about 30 per cent of the total ledge, which leaves 20 or 30 per cent chargeable to unmeasured sources of loss.

Jan 1, 1932

By Hughes CA

The need to recover metals from low grade deposits, old tailings, etc., combined with improvements in equipment design and the development of new extractants, has resulted in solvent extraction (SX) metal recovery reaching new importance (Webster & Ferron, 1993). The basic principle of solvent extraction is the use of an equilibrium system in which a metal ion is transferred from an aqueous phase into an organic phase, (Equation 1), (Ritcey, 1984). M + E ME . (1) The organic extractant (E) is usually specific for a certain metal ion (M) and forms a metal complex in the organic phase, leaving the impurities behind in the aqueous phase. To recover the metal, the equilibrium is reversed and the metal ion is transferred back from the organic to another aqueous phase in a process called stripping. The metal is then recovered from the aqueous strip solution, usually by electrowinning.

Jan 1, 1990

By Norman O. Lotter, André R. Laplante

"The pursuit of concentrator surveying for purposes of metal accounting or process optimization has not yet connected with the well-published realm of geostatistics. The reality of lognormality in time has seldom been discussed. One publication by Krige, 1962, examined such effects for a gold concentrator in South Africa, towards an information system that would provide feedback to the mining and surveying teams on grade control of ore mined.During present studies which are designing and testing a new survey model, called statistical benchmark surveying, it was found that the distributions of feed, concentrate and tailings bear significant residual signs of the parent lognormality in space. The multiple hosting of paymetals in different mineral species complicates the understanding of these distributions. These features have to be recognized and treated in order to perform appropriate quality control on the diagnostic sampling performed in the pursuit of statistical benchmark surveying.It is shown in this paper that the above two features can actually be used to advantage in the diagnosis of continuous periods of operations data ahead of such surveying, including the estimation of recoverable paymetals in flotation tailings from a graphical method.INTRODUCTIONAssessment of Concentrator PerformanceMilling and flotation, sometimes accompanied by gravity separation, are well-established unit processes, which have traditionally been used to treat ore that has been mined. This is because these processes liberate, then separate, the valuable minerals, which contain paymetals, from host gangue. This is often done by a combination of crushing and grinding processes, or autogenous grinding, to liberate the paymetal minerals, followed by gravity separation and/or flotation, to separate these valuable minerals into a concentrate, or several concentrates. These concentrate(s) have a lower bulk than the parent ore from which they are derived. Further, they contain a high percentage of the valuable minerals. Accordingly, they are more economically treated in subsequent beneficiation processes than the ore from which they were produced."

Jan 1, 2005

The paper relates to the laboratory and pilot plant studies that have been carried out by Sherritt Gordon Mines Ltd., Metallurgical Research Div., in developing the ammonia pressure leach process for extracting Cu, Ni, Co, and S from high grade Ni concentrate produced from Lynn Lake ores and describes in some detail the chemistry of the process. In the leaching stage air, ammonia, and sulphide minerals react in a sequence of inter-related steps to produce soluble amines of Ni, Cu, and Co in a solution containing sulphate, thiosulphate, polythionate, and sulphamate ions and a controlled amount of free ammonia, the iron and other components of the concentrate remaining as an insoluble residue which is separated from the leach solution by filtration. The pregnant solution produced in leaching is further treated by boiling to precipitate and remove Cu as cuprous sulphide, leaving a copper-free solution with a composition suitable for subsequent precipitation of Ni and Cu by H,

Jan 3, 1955