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By G. R. Adams, N. Y. Tang, N. Qiang

"Aluminum is the most important alloy addition to Zn baths for controlling the reaction kinetics between the steel substrate and molten Zn in continuous galvanizing operations. Due to the complexity of the Zn-Fe-Al ternary system, the measurement and control of effective bath Al remains a challenge for modem galvanizers. The successful development of Al sensors has made the real-time measurements of bath Al contents possible. To facilitate their application, a computer interface and a palm-size data logger have been developed by Cominco. Plant applications indicated that the sensor possessed sufficient accuracy for process monitoring and control. The working mechanism of the Al sensors and Cominco's development work is described, and the results of sensor applications are presented.IntroductionControl of bath Al content is critical in modem continuous galvanizing because it has a strong influence on coating structure and properties and the overall product quality. The control of effective bath Al content (Al in liquid solution) is particularly critical for galvannealing where a high bath Al content may lead to incomplete alloying during post annealing, and a low bath Al content may result in other operation problems, such as excessive bottom dross accumulation and difficulties in coating thickness control. The desirable accuracy of the Al control is within ±50 ppm of target levels. In principle, such an accuracy is achievable for modem chemical analysis facilities, such as atomic absorption photospectrometer (AAS) and induction-coupled plasma (ICP). However, a recent study carried out by the International Lead and Zinc Research Organization (ILZRO) indicated that such an accuracy is rarely achieved in the zinc and steel industries.(1)"

Jan 1, 1997

By A. H. Taitt

The original basis for the search for oil in Great Britain was described last year.t During 1937 the exploratory drilling by the D'Arcy Exploration Company, Ltd. has been continued. Three wells have been completed in the south of England and a fourth is nearing completion. In addition, test wells are now being drilled in Scotland and East Yorkshire. Southern England The test well on the Portsdown structure, which at the end of 1936 was drilling in the Lower Lias at 5792 ft., entered the Triassic at 6540 ft. and was completed in that formation at a depth of 6556 ft., without encountering further indications of petroleum. The Henfield well encountered the Lias at a depth of approximately 4090 ft., and after drilling 800 ft. of an argillaceous development of that formation entered a series of marls, breccias and conglomeratic limestones of the Carboniferous. Drilling was suspended at a depth of 5105 ft., in the latter formation. The consistently impermeable nature of the strata encountered in the Portsdown and Henfield test wells focused attention on the desirability of obtaining shore-line conditions of the Jurassic. With this end in view the Kingsclere anticline, a few miles south of Newbury in Berkshire, was selected for a next test. The Kingsclere well has now reached a depth of 5032 ft. in the Lower Lias and has encountered a full development of the Jurassic. With the exception of the Portland sand, which has a slightly greater porosity, and the Corallian, in which relatively great thicknesses of impervious limestone were met, conditions of sedimentation have been found to be comparable with those of the earlier wells. Small traces of petroleum have been found in cuttings and cores, but formation tests carried out at frequent intervals have yielded no flow of oil. In order to test the Corallian, from which series an outcropping oil sand had been found, a test well was drilled in a near-by anticline at Poxwell in Dorset. The Poxwell well started in the Portland beds and entered the Corallian at 995 ft. The sands at the horizon of the out-

Jan 1, 1938

By P. Peczak

A Monte Carlo simulation technique has been used to study dynamic recrystallization in polycrystals. A continuum microstructure of the polycrystal is modeled employing a discrete lattice. The response of the material to hot deformation is simulated by adding stored energy and recrystallization nuclei continuously with time. The experimentally observed nonuniform character of deformation substructures is modeled by employing a phenomenological expression for inhomogeneous distribution of the stored energy. All simulations were performed on HP-Apollo 9000 Series 700 workstations. A program written in FORTRAN with use of PHIGS graphics library calls was used to interactively monitor the current state of the matrix and all relevant parameters: deformation stress, average grain size and effective nucleation rate. Visual analysis of the simulated microstructure allows a better understanding of the data developed by averaging over a number of very long Monte Carlo runs. Since the essential features of dynamic recrystallization are accurately reproduced by the model, it is used to discuss the role of the controlling mechanisms of the dynamic recrystallization in real polycrystal.

Jan 1, 1993

By D. W. Leyshon

The fluidized solids technique for the calcination of phosphate rock has been well established for over 10 years. This paper is intended to review the recent performance of many of the Dorr-Oliver FluoSolids* calciners. In addition, design features of these three compartment refrac¬tory construction reactors will be described and a comparison made with fuel requirements for single compartment calcination. Also presented will be certain, aspects of the use of the rock including a discussion of non sulfate sulfur in the rock. A system is described for producing a blended mixture of calcined and uncalcined rock.

Jan 1, 1972

By S. B. Patterson, A.R. Amos

Log washers have been used for many years in the washing of clay iron ores, phosphate rock and manganese ores, but not until the past 15 years have they been employed to any extent in the preparation of aggregate materials and fluxing stone. For a machine of such importance where tenacious clay or soft rock must be eliminated, there are few data generally available. The purpose of this paper is to set forth the results obtained from several operations, together with a few suggestions for planning a specific installation. Where the material to be washed out consists of loose surface soil, silt, or small amounts of quickly soluble clay, there is little competition with other forms of washers, because greater power and maintenance are required for the operation of log washers, but where the foreign matter is a stiff clay, such as occurs with high-calcium limestones and in marginal gravel deposits, the ability of other kinds of washers to eliminate completely the hard clay balls is at least uncertain. Then the log washer comes into its own field, for with the breaking and churning action of the logs it will clean out the toughest clay. Even with material from the hydraulic dredge, if it contains tough clay, the log washer is desirable unless the gravel is subjected to a costly soaking and rehandling process. Recently there has been a considerable development in other types of machines to accomplish these results but it is not within the scope of this paper to make comparisons between competitive types, but to present the best obtainable data on log washers only. From the primitive design that gave it its name, a long log hewn from a tree, with paddles forged to shape from strap iron and attached by lag screws, the log washer has gradually been developed to the present all-steel type. As now manufactured, the log washer consists essentially of two built-up logs on which are mounted a series of paddles, carried by shafts fitted at the ends of the logs on bearings fastened outside the enclosing steel box, or trough, which is set at an angle of about 5" to 10" and into which the material is fed. Stuffing boxes at the places where the shafts pass through the box at the lower end are equipped with water-

Jan 1, 1938

By A. R. Amos, S. B. Patterson

Log washers have been used for many years in the washing of clay iron ores, phosphate rock and manganese ores, but not until the past 15 years have they been employed to any extent in the preparation of aggregate materials and fluxing stone. For a machine of such importance where tenacious clay or soft rock must be eliminated, there are few data generally available. The purpose of this paper is to set forth the results obtained from several operations, together with a few suggestions for planning a specific installation. Where the material to be washed out consists of loose surface soil, silt, or small amounts of quickly soluble clay, there is little competition with other forms of washers, because greater power and maintenance are required for the operation of log washers, but where the foreign matter is a stiff clay, such as occurs with high-calcium limestones and in marginal gravel deposits, the ability of other kinds of washers to eliminate completely the hard clay balls is at least uncertain. Then the log washer comes into its own field, for with the breaking and churning action of the logs it will clean out the toughest clay. Even with material from the hydraulic dredge, if it contains tough clay, the log washer is desirable unless the gravel is subjected to a costly soaking and rehandling process. Recently there has been a considerable development in other types of machines to accomplish these results but it is not within the scope of this paper to make comparisons between competitive types, but to present the best obtainable data on log washers only. From the primitive design that gave it its name, a long log hewn from a tree, with paddles forged to shape from strap iron and attached by lag screws, the log washer has gradually been developed to the present all-steel type. As now manufactured, the log washer consists essentially of two built-up logs on which are mounted a series of paddles, carried by shafts fitted at the ends of the logs on bearings fastened outside the enclosing steel box, or trough, which is set at an angle of about 5" to 10" and into which the material is fed. Stuffing boxes at the places where the shafts pass through the box at the lower end are equipped with water-

Jan 1, 1938

By Oliver C. Ralston

Fluorescence is of growing interest to the mineral industry because certain minerals may be detected thereby and because, as shown in figure 1,4/ many minerals (natural or synthetic) are needed in tubes and lamps. The use of fluorescent lighting is expanding, and large numbers of lamps of many sizes and shapes are being made and used in works, factories, stores, offices, homes, and in photography. Fluorescent tubes, as distinguished from clear tubes filled with neon, argon, or other rare gases through which a current of electricity passes, fluoresce owing to specially, selected and prepared minerals placed in the tubes. Luminous chemicals and paints also contain special minerals and are used in similar applications; therefore, these also will be considered in this report. Although the quantity of minerals (in tons) that are used for fluorescent purposes is small, and probably will continue to be so, this use is significant because it exemplifies a requirement for "pure" minerals in which a trace of contaminant as" minute" as one part in ten million may distinguish between the acceptance or rejection of a particular material. This extreme purity makes synthetic minerals almost essential, and natural mineral's are now little used.

Jan 1, 1944

By S. Groudev

Acid drainage waters generated in the uranium deposit Curilo, Bulgaria, were treated by means of a pilot-scale passive system consisting of a permeable reactive multibarrier and a constructed wetland connected in a series. The multibarrier had a total volume of 23 m3 and consisted of an alkalizing limestone drain and an anoxic section for microbial dissimilatory sulphate reduction, bio-sorption and additional chemical neutralization. The waters had a pH in the range of about 2.5 ~ 4.0 and contained radionuclides (uranium, radium), heavy metals (copper, zinc, cadmium, lead, nickel, cobalt, iron, manganese), arsenic and sulphates in concentrations usually much higher than the relevant permissible levels for waters intended for use in agriculture and/or industry. The water flow rate through the multibarrier varied in the range of about 1 ~ 17 m3/24 h, reflecting water residence times of about 300 ~ 18 hours. An efficient removal of pollutants was achieved by the multibarrier during different climatic seasons, even during cold winter days at external air and water temperatures close to 0oC. The multibarrier effluents were enriched in dissolved organic compounds and in some cases still contained manganese and iron in concentrations higher than the relevant permissible levels. These pollutants were removed in the constructed wetland as a result of the activity of different heterotrophic microorganisms, including some bacteria able to oxidize the bivalent manganese and iron ions to Mn4+ and Fe3+, respectively.

Jan 1, 2014

ENGINEERS AVAILABLE (Under this heading will be published notes sent to the Secretary of the Institute by members or other persons introduced by members.) Graduate mining engineer, with 10 years' experience, having an office in New York, would like to represent a mining company as selling and purchasing agent, and general supervision if desired. Machinery agency considered. No. 259. Member, technical graduate, with several years' experience as engineer for a pyrites company, and as geologist and engineer for copper, nickel, and silver companies, desires a position as engineer or superintendent of mines. No. 260. Member, technical graduate, aged 29, with experience as draftsman, surveyor, and superintendent of iron and gold mines, and as construction engineer, is open for a position as mine superintendent, or in mine examination or construction. No. 261.

Jan 11, 1915

By E Niva

The IsaMillÖ is challenging the way that plants are designed and operated. This paper challenges existing designs of concentrator flow sheets, particularly focusing on magnetite circuits.   From what has started out as a small scale ultra fine grinding mill in the pharmaceutical and pigment industries, it has been redesigned and improved upon for mineral processing, and has been the mainstay of fine grinding applications for over ten years. These applications have required energy efficient grinding to succeed, and have been predominately in the base metals industry.   Further development of the IsaMillÖ has now resulted in the machines being able to treat larger tonnages, with higher capacity motors. This development, along with the introduction of purpose designed ceramic media, has allowed the mill to treat courser feed sizes. At the same time, the mill still offers highly efficient grinding, and has enabled it to be operated in coarser tertiary and secondary grinding applications.   The acceptance of the mill in coarser applications, predominately in base metals and PGM applications, has enabled the IsaMillÖ to be a serious contender for beneficiation in other minerals. One such application is the potential for IsaMillsÖ to be part of magnetite flow sheets, which are being considered in Australia to meet the growing iron demand of China. The high energy efficiency of the IsaMillÖ compared to conventional technologies, as well as the smaller infrastructure requirements, provides a great opportunity to reduce the power intensity of magnetite circuits.   This paper will examine the use of IsaMillÖ technology in conventional grinding applications, including recent testwork in a primary grinding base metal circuit, as well as testwork on magnetite ore comparing a lab scale IsaMillÖ with a lab scale Tower Mill.   The growing demand for minerals over the next decade, coupled with higher energy cost, will result in energy efficient technology, such as the IsaMillÖ, being included in standard circuit design.

Jan 1, 2008

By P. Condori

In spite of the importance of the slurry transport and discharge in autogenous and semiautogen-ous (AG/SAG) mills, it is evident that a more comprehensive and useful model is still required. Semi-empirical models used up to now have many limitations and cannot be used beyond the ranges in which they were developed. The breakage of particles as they are transported along a mill com-plicates the experimental analysis and the modelling of the transport process within the mill. The interaction of the grate discharge and the pulp lifters, with the added issue of backflow from the pulp chamber into the mill, makes the discharge modelling process difficult. In order to overcome these difficulties, a mechanistic approach has been applied. The general transport and discharge model was subdivided into four independent models: Flow through the charge, flow through the grate, flow in the pulp lifter, and flow-back. This paper gives an overall description of the modelling approach and discusses in particular the modelling of transport of fluids through the charge. In order to evaluate and calibrate the model, experimental work was carried out. To evaluate the gradient pressure under different conditions of charge packing and flow rate, a specialised experimental rig with a highly sensitive pressure gauge was used. Preliminary results identify the differences of the charge and grate on the restriction of flow. The existence of a dynamic voidage in our particular system was more evident and as a result, a semi-empirical correlation for the voidage was developed. In general, results show that the me-chanistic model derived from Ergun?s equation for flow through a packed bed can be satisfactorily adapted.

Jan 1, 2014

By John R. Hayes, Kebbi A. Hughes, John Rowson, Peter E. R. Blanchard, Jeremiah C. Beam, Andrew P. Grosvenor, Arthur Situm

Uranium ore bodies contain elements within mineral phases that need to be disposed of responsibly. Solid waste can be placed in a tailings management facility (TMF) to contain the waste elements and limit interactions with the environment. It is important to understand how the chemistry of the tailings evolves throughout the lifetime of the operations that feed the TMF and after the site has been decommissioned. The objective of our collaboration with Orano Canada was to study how the tailings from the TMF located at McClean Lake, Saskatchewan change over time. This manuscript discusses our use of X-ray absorption spectroscopy (XAS) and X-ray microprobe to study the fate of Mo and Ca in the tailings. Mo is considered an element of concern (EOC) and it is necessary to determine if a stable solid Mo-bearing species forms. Thermodynamic modeling suggested that aqueous Mo would precipitate over time as powellite (CaMoO4). Comparing Mo K-edge XAS spectra from the solid tailings to the aqueous Mo concentration in the pore water showed that powellite did form and that this did result in a decrease in the aqueous Mo concentration over time. Further, it has been proposed that Ca2+(aq) can react with bicarbonate ions in the pore water and precipitate as calcium carbonate (e.g., CaCO3). This reaction would limit the aqueous bicarbonate present in the tailings that could react with uranyl ions to form soluble uranyl-carbonate complexes. We have identified several trace Ca-bearing species, including carbonates, in the tailings using XAS and X-ray microprobe.

Jan 1, 2020

By W. D. Smith

It has been 5 years since the writer left the Philippine Islands and while in that country his chief work did not lie in this field, though he has visited all but one of the localities mentioned in this article. The principal field studies relating to oil were M de by his colleague, Mr. Wallace E. Pratt. The writer's investigations ealt with the general stratigraphy and paleontology of the Philippines. with the exception of the investigations made by Mr. Pratt and the writer very little information on this subject is available. A number of geologists in the employ of large oil companies have visited the Islands from time to time but, following the general rule, the public has scarcely ever been permitted to learn anything of the results. The writer is indebted to the Bureau of Insular Affairs, Washington, for late information regarding recent legislation in the Islands relating to petroleum. All the known oil seeps, petroleum residues, such as ozocerite, and natural-gas emanations are associated with Tertiary sediments. The chief seeps and most promising prospects are located as follows: 1. Bondoc Peninsula (lower end), Tayabas Province, Southeast Luzon. 2. The west coast of the island of Cebü from Alegria north to, and perhaps beyond, Toledo. 3. Central Mindanao not far from Lake Lanao. 4. The ozocerite veins on the Island of Leyte in the northwestern part in the vicinity of the town of Villaba. 5. Natural gas from some deep wells in Tertiary shale formations on the eastern flank of the Cordillera and extending out under the plain on the island of Panay. The first mention in geological literature, to the writer's knowledge, of gas or petroleum in the Philippines is found in the description of the Island of Panay by the Spanish geologist, Abella, in the year 1890. In 1898, an oil well was being dug on the estate of Smith Bell & Co., an English concern, near the town of Toledo on the west coast of Cebu. In

Jan 1, 1921

By N. N. Moebs

The atmosphere in part of an air-sealed coal mine was monitored continuously through a drill hole for oxygen content to determine the effectiveness of sealing a mine against the entrance of air and the major force that caused the phenomenon of mine breathing through the overburden. The differential pressure across the seal and the barometric pressure on the outside also were recorded. A general correlation, obtained between the oxygen level, differential pressure, and barometric pressure, indicates that changes in air pressure are the cause for periodic replenishment of the oxygen in the mine. Mine effluent quality was determined by conditions in many sections of the mine and could not be related to the oxygen level at the drill hole.

Jan 1, 1972

By V.K. Zworykin

Throughout its development the science of electronics, like so many other branches of science and industry, has been indebted to the metallurgist. Metallurgy has provided the electronic engineer with conductors to furnish passage for electrons outside of his evacuated tubes: it has developed tungsten and tantalum wires for emitting electrons and various refractory metals and alloys suitable for electrodes, which receive them and guide them within the tube; finally it has supplied ferromagnetic materials both for shielding electronic apparatus from magnetic fields and for forming highly concentrated fields for deflecting electron . Today I hope to show you that electronics has not been altogether ungrateful for this assistance. More specifically, I wish to indicate the role that the electron microscope, a relatively recent product of electronic engineering, is playing even now in the study of metals. Every metallographer is aware that his standard metallographic microscope will not reveal structural detail involving separations smaller than a certain fraction —at the very best a tenth—of a micron. This limitation, he knows, is a consequence of the fact that the wave length of the light employed for forming the image has this order of magnitude. It is, thus, a property of all light microscopes. TO overcome it, a different imaging medium must be employed, The existence of such a medium became evident when it was demonstrated1 that electrons were affected by magnetic and electric fields with axial symmetry just as light is affected by glass lenses; these fields, or "electron lenses," curve the paths of electrons reaching them from an object located on the axis of symmetry in such a manner that, at some distance from the lens, a true image of the object is formed. Furthermore, although a wave length may . be ascribed to electron beams just as to light, this wave length is much shorter; for electrons accelerated through a difference of potential of 50 kilovolts, the wave length is only about one hundred-thousandth of that of visible light. Actually, the elcctron microscopes of today resolve detail one hundred times as fine as light microscopes; if the maximum useful magnification of the latter is taken to be a thousand, that of electron microscopes is one hundred thousand. The Electron Microscope Since electrons are readily scattered and absorbed by matter, specimens to be observed in the electron microscope must be prepared to be less than one micron in thickness; furthermore, the interior of the microscope must be carefully evacuated to prevent collisions between the clectrons and the molecules of the air. Finally, as already mentioned, the lenses are formed by axially symmetric magnetic or electric fields, and not by any material medium such as glass. Apart from these basic differences, the electron microscope closely

Jan 1, 1943

By V. K. Zworykin

Throughout its development the science of electronics, like so many other branches of science and industry, has been indebted to the metallurgist. Metallurgy has provided the electronic engineer with conductors to furnish passage for electrons outside of his evacuated tubes: it has developed tungsten and tantalum wires for emitting electrons and various refractory metals and alloys suitable for electrodes, which receive them and guide them within the tube; finally it has supplied ferromagnetic materials both for shielding electronic apparatus from magnetic fields and for forming highly concentrated fields for deflecting electron . Today I hope to show you that electronics has not been altogether ungrateful for this assistance. More specifically, I wish to indicate the role that the electron microscope, a relatively recent product of electronic engineering, is playing even now in the study of metals. Every metallographer is aware that his standard metallographic microscope will not reveal structural detail involving separations smaller than a certain fraction —at the very best a tenth—of a micron. This limitation, he knows, is a consequence of the fact that the wave length of the light employed for forming the image has this order of magnitude. It is, thus, a property of all light microscopes. TO overcome it, a different imaging medium must be employed, The existence of such a medium became evident when it was demonstrated1 that electrons were affected by magnetic and electric fields with axial symmetry just as light is affected by glass lenses; these fields, or "electron lenses," curve the paths of electrons reaching them from an object located on the axis of symmetry in such a manner that, at some distance from the lens, a true image of the object is formed. Furthermore, although a wave length may . be ascribed to electron beams just as to light, this wave length is much shorter; for electrons accelerated through a difference of potential of 50 kilovolts, the wave length is only about one hundred-thousandth of that of visible light. Actually, the elcctron microscopes of today resolve detail one hundred times as fine as light microscopes; if the maximum useful magnification of the latter is taken to be a thousand, that of electron microscopes is one hundred thousand. The Electron Microscope Since electrons are readily scattered and absorbed by matter, specimens to be observed in the electron microscope must be prepared to be less than one micron in thickness; furthermore, the interior of the microscope must be carefully evacuated to prevent collisions between the clectrons and the molecules of the air. Finally, as already mentioned, the lenses are formed by axially symmetric magnetic or electric fields, and not by any material medium such as glass. Apart from these basic differences, the electron microscope closely

Jan 1, 1943

"IntroductionThe Chairman, in his speech to this body last year in Montreal, stated that the Dominion Coal Board looked to and depended upon the Bureau of Statistics for statistical material, and the Bureau does collect and publish monthly and annual data on coal. It may therefore be asked why an officer of the Dominion Coal Board should prepare and give a talk on statistics.I would explain that it has been our experience in the Board that, since the supply and consumption of coal in Canada is subject to a seasonal ebb and flow, it can be more profitably studied on the basis of a twelve-month period ending on March 31st than of a calendar year, since the end of March does represent a fairly stable end point in this ebb and flow. The figures are not prepared or published by the Bureau on that basis and it has therefore been thought that a presentation on this fiscal-year period would be of interest. The Bureau of Statistics has agreed that this may be valuable and all the data here presented are based on the reports secured from various sources by the Mining, Metallurgical and Chemical Division, Dominion Bureau of Statistics. The only contribution by either myself or the staff of the Dominion Coal Board has been the tabulation in a different twelve month period, and the comments upon the picture presented.It should be noted that the data for the month of March, 1950, are not available in all cases and consequently the figures for that year contain an estimate for this month."

Jan 1, 1950

By Jon G. Baird

The suggestion of the use of measurements of trace amounts of mercury as a guide to the location of sulphide ore deposits was first made by the Russian, A. A. Saukov (1), in 1.946. Since Saukov's original work, many others have studied the abundance of mercury in nature, the association of mercury with sulphide ores and methods by which very minute quantities of mercury can be measured in air, soil, rocks, water and plants. The most abundant of the mercury bearing minerals is cinnabar (HgS). Native mercury is also found and sulpha-salts like tetrahedrite are known to have important mercury contents. Other sulphides of base metal deposits contain mercury in amounts ranging from parts per million to as much as one or two percent. (2) The mercury content of sulphide-free rocks is usually less than a few hundred parts per billion (1 ppb - 10-9), Soils usually contain less than 100 ppb and water less than 1 ppb of mercury. Normal atmospheric air contains about 1 nanogram (10-9 grams) of Hg per cubic metre although higher concentrations can be observed near mercury occurrences, sulphide deposits and volcanic exhalations.

Jan 1, 1973

By H. J. Bogert

Shallow, gently dipping quartz veins at the Mineral Hill Mine are mined in room and pillar stopes. Ore zones are severely folded and fractured, thus actual pillar strength and physical properties of the rock mass deviate significantly from conventional laboratory tests and pillar theory. Laboratory specimens large enough to include pre-existing fractures proved to be representative of actual pillar strength. Further adjustment for specific pillars was based on RQD. Deformation and stress were measured in several pillars during pillar recovery. Stress data and finite element modeling were used to estimate absolute pillar stress at failure. The stress/strain relation provided an excellent indicator of pillar behavior. Good agreement between lab data and underground data was found.

Jan 1, 1995

By Steven Bradshaw, Edson Charikinya

The application of high power microwave energy to secondary crusher products has been shown to induce micro fractures and cracks in the ore. This suggests that heap leaching could benefit from microwave-induced fractures, as the extent and kinetics of heap leaching processes depend on the accessibility of grains to lixiviants, which can potentially be improved through microwave treatment. The density and pattern of microwave induced cracks and how these cracks subsequently affect heap leaching recovery has not yet been investigated. The objective of this study was to apply X-ray micro computed tomography (X-ray CT) to investigate microwave induced cracks in large cone and HPGR crushed sphalerite particles within 3D space. The ore particles were microwave treated in a single mode microwave applicator coupled to a switched mode power supply and a water cooled microwave transmission sub system operating at 2.45 GHz. The ore particles were treated at specific absorbed microwave heating energies of between 2 and 3kWh/t by treating at 6 kW of forward power for treatment times of 1 s. X-ray tomography analysis was conducted on fine (-5+4.75) mm, medium (-16+9.5) mm, and large (-25+19) mm sphalerite particles before and after microwave treatment at voxel resolutions of 5 µm, 15 µm and 25 µm respectively. Image segmentation, thresholding and spatial registration techniques were used to study crack patterns in 3D images of HPGR and cone crushed particles. Analysis of the X-ray CT images after microwave treatment shows considerable micro crack formation within the Cone and HPGR crushed particles. The cracks pattern showed interphase cracks propagating across all phases, with no evidence of preferential cracking. A greater density of microwave induced cracks was observed on fine (-5+4.75) mm particles compared to the medium (-16+9.5) mm and (-25+19) mm large particles. The results showed overall increased particle porosity following microwave treatment.

Jan 1, 2014