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By William J. Campbell

These investigations were undertaken as part of a program to determine the optimum X-ray spectral lines to use for analyzing the wide variety of samples received by the X-ray Laboratory. Theoretical calculations and experimental data derived from these investigations show that longer wavelength spectral lines, > 2A, are very useful for many analytical problems. Because of the low fluorescence yield of the elements of atomic numbers 13-22 and the small depth of penetration of their X-ray spectral lines, these elements were originally considered to be insensitive; however, these studies show that the wide dispersion of their spectral lines, coupled with their weak beta lines, permits the use of wide collimation, thus increasing the line intensity. More importantly, the background due to scattered primary radiation is very low in the long-wavelength region.

Jan 1, 1959

By Fabiano Mendes

Processos industriais de carbonização são tecnologias maduras e operam há mais de 7 décadas. Contudo, o sistema integrado de produção de ferro primário e aços a base de biomassa como fonte de energia e termorredutor, mesmo sendo a alternativa ambiental de menor impacto existente, chega a seus limites tecnológicos, ambiental e econômico, ameaçando a sua sustentabilidade. O grupo Vallourec buscou o processo Lambiotte como base tecnológica para desenvolver seu ambicioso projeto de carbonização contínua, em substituição ao processo artesanal de fornos retangulares de batelada, utilizados atualmente. O esforço experimental de mais de meia década, com a adaptação e profunda reengenharia do processo Lambiotte, que é o que melhor representa esta classe de reatores, para que ele atendesse as condições brasileiras e o uso das espécies de madeira da família dos Eucaliptos culminou no desenvolvimento do processo de carbonização continua Carboval, que demonstrou sua plena capacidade, para atender aspectos econômicos, sustentáveis e de qualidade siderúrgica do carvão vegetal produzido.

Aug 17, 2017

By Luís Carlos da Silva

Apresenta-se uma revisão das características e propriedades do nitreto cúbico de boro (cBN) bem como de diferentes tipos de processamento. A influência da adição de ligantes e a formação de compósitos com outras cerâmicas são também revistas. Finalmente, destaca-se a grande importância prática do cBN como cerâmica de elevada dureza na substituição do diamante em ferramentas de corte.

Oct 30, 2017

By M M. Collisson

The Synthetic Rutile (SR) plant operations, North Capel, produce electrostatic precipitator (ESP) fume and kiln scrubber residue. Typically ESP contains about 18 per cent Ti, 13 per cent Fe, 0.5 per cent Mn, eight per cent Si, six per cent Al, 16 per cent C, 0.9 per cent Zn, 0.6 per cent Pb, 300 ppm As, 300 ppm Cr and 5 ppm Cd. These wastes are held in a storage dam together with neutralised acid effluent (AE) liquor. A project was initiated to treat the fume and produce a benign residue that could be delivered to landfill, reducing dam space storage. Plant AE, containing free acid (9 - 14 g/L), Fe (6 - 7 g/L) and Mn (1 g/L), was used to leach ESP. The degree of extraction achieved for various elements include about 20 per cent Zn, almost 50 per cent As, five per cent Al, 0.4 per cent Pb and 15 per cent Cd. Extraction was most effective at pH The residue from AE leaching still contained Pb. TCLP tests of the leach residue produced Pb extraction significantly higher than the 0.1 ppm stipulated by Class 2 landfill guidelines. Other elements (eg As, Cd, Cr) successfully met the limits. Further leaching of the residue with EDTA extracted up to 65 per cent of Pb content. TCLP tests on treated residue showed Pb leaching potential of Lead was removed from the leach circuit as the sulphate by acidification of EDTA leach liquor, allowing EDTA to be recycled. The study showed that one waste stream can be used to treat another and help reduce plant waste.

Jan 1, 2001

By P. Bramwell, R. Tremblay

"The Port Radium leaching plant of Eldorado Mining and Refining, Limited, produces 450 t./d. of sulphuric acid leach liquor containing l. 73 g. /I. U 308. After solvent extraction, the waste solution is discarded at 0.002 g./l. U30s for a recovery of 99.8 to 99.9 per cent. The solvent is acidified with weak sulphuric acid, loaded to 4.5 g./l. U80:1 in three-stage extraction, scrubbed with water, and stripped with soda-ash solution in single-stage stripping. Caustic removes the UaOs from the pregnant strip solution as a precipitate. The slurry is filtered, re-pulped with water, and re-filtered. The pressed precipitate at 81 to 82 per cent equivalent U30s is dried and packaged. The carbon-ate filtrate is cooled to remove sodium sulphate build-up and carbonated to convert excess caustic. Reagent consumptions are 4.1, 0.22, and 0.39 pounds per 1,000 gallons of pregnant solution for Diesel oil, amine, and alcohol, respectively. Caustic consumption averages 1.3 to 1.4 pounds per pound U3O8.Extraction and stripping is accomplished in sheet-iron mixer-settlers lined with Phenoline. Piping on both circuits is Schedule 80 polyvinyl chloride. Valves are straightway Buna N lined with American Hycar diaphagms. Extensive instrumentation ensures good metallurgy with a minimum of variations and labour. Mixing in a continuous organic medium and careful acidity control are required to minimize third-phase formations. Heating the precipitate slurry is conducive to good filtering in Perrin presses with neoprene-coated, rolled-steel sectors. Sodium sulphate is crystallized from carbonate filtrate solution by batchwise cooling to 54°F. with lake water."

Jan 1, 1959

By P Luo, J E. Danoczi, P Nakutnyy

Sensor-based sorting methods to remove waste or for upgrading ore prior to downstream metallurgical processing is becoming more prevalent for mining operations. X-ray transmission (XRT) sorters are a popular choice for mineral processing plants since they can sort a wide variety of minerals. XRT sorters pass high intensity X-rays through particles to generate images of varying greyscale, based on their effective atomic density. The ore sorter then mechanically separates the particles using algorithms based on the images. A popular test currently used to evaluate the amenability of the ore to XRT sorting is to pass the particles through the sorter and obtain the greyscale images showing mineralogical differences. This test provides information on the mineralogical heterogeneity between ore particles for their separation. However, it does not provide an understanding of the actual mineralogical composition of the ore or information pertaining to which other minerals may respond in a similar manner, nor does it provide liberation information. This paper describes a test that combines high resolution X-ray micro Computer Tomography (CT) combined with QEMScan to obtain information about amenability of ore to XRT sorting and to obtain valuable information that can streamline metallurgical testwork programs. This test also provides information relating to particle thickness and associated X-ray attenuation coefficients, desired mineral presence and mineralogical information relating to associated minerals and clays to assist with developing sorting algorithms. Combining the CT and QEMScan can address many limitations of the current method to determine whether XRT sorting technology is appropriate for particular ores. Mineralogy information from QEMScan can identify incidences of; mineral encapsulation, problematic clays, detrimental minerals as well as calibrate the greyscale values of CT data. Additional 3D CT imaging carried out on cores provides spatial information of the minerals within the ore and mineral grades.

Nov 10, 2020

By S. D. F. Rocha, A. L. A. SANTOS, E. M. A. BECHELENI, R. M. Papini, P. R. M. Viana, F. P. C. Silvas

The kinetics of atmospheric sulfuric acid leaching from a Brazilian nickel laterite ore was assessed using distinct reducing agents and ore mineralogy. This transitional ore contains 1.63% Ni distributed as 1.27% in coarse size (− 500 + 150 μm), mainly as silicates (lizardite and chlorite—28.6%), and 2.06%in the fines fraction (− 75 μm), mainly as iron oxy-hydroxides (goethite and hematite—49%). The effects of temperature, acid concentration, reducing reagent type, and concentration were evaluated. The − 75 μm fraction limited the leaching efficiency and the use of reducing media with thiosulfate improved leaching and Ni-Fe selectivity. However, at constant Eh of 626–743 mV and a pH range between 0.2 and 1.1, no substantial rise in metals extraction, except for Co and Mn, has been observed. In order to determine the process control at 95 °C, two regions in the extraction curves were used in combination with the shrinking core model. Control by porous diffusion was observed and the kinetic constant was found to be in the order kFe<kNi<kMn<kCo<kMg for atmospheric leaching without Eh control. In reducing media for the first 15 min of leaching, the kinetic constant was found to be kFe<kNi<kMg≅kCo<kMn as derived from Ni disseminated into iron oxides structures.

Oct 7, 2020

By B. P. Martinez

A process for regenerating spent pickle liquor is proposed in which some of the water is evaporated at atmospheric pressure and ferrous sulfate is precipitated as monohydrate crystals..Equilibrium conditions are set for a slurry of crystals in a mother liquor containing 5 percent FeS04 and 45 percent E2S04, by weight, and boiling at about 235° F. The slurry is pumped continuously to a filter, and the mother liquor from the filter is pumped back for reuse in the pickling tanks. The net result of the process is to remove ferrous sulfate in the regeneration plant at the same rate ac it is produced in the pickling tanks. This process is integrated with the steel-pickling operation and controlled by the pickling requirements for particular steels. Spent pickle liquor is removed for regeneration continuously from both batch and continuous picklers at higher acid concentrations than would be dumped to waste because no acid is neutralized or discarded. However, the process is not designed to keep a sulfuric acid concentration stronger than 25 percent in any pickling tank. To retain flexibility in the pickling operation, all acid makeup is added to the pickling tanks. Rinse waters are used as water makeup for the pickling tanks. To further minimize waste of acid in the rinse waters, improvements of rinsing practices are outlined.

Jan 1, 1953

By James P. Bennett

The U.S. Bureau of Mines investigated the role of imported natural flake graphites in dolomite-carbon refractories used in steelmaking processes and evaluated carbon fibers as a potential substitute. Varying quantities (1.5-30 pct) of natural flake graphite and carbon fibers were added to test samples. The effect of the additions on modulus of rupture (75°-2,750° F), deformation under load (2,750° F), and air-slag-metal resistance (3,000° F) was studied. Carbon purity of natural flake graphite additions did not influence hot strength, deformation under load, or air-slag-metal resistance. When the quantity of 90-pct-carbon graphite addition varied between o and 30 wt pct, hot strength was highest, deformation under load lowest, and air-slag-metal wear the least at 10 wt pct. As test temperature increased from 500° to 2,750° F, the hot strength difference became less. Carbon fiber additions were limited to 1.5 pct in dolomite-carbon brick. At this level, physical properties were generally comparable to those obtained with natural flake graphite, but were below values obtained with 10-pet-f1ake graphite additions. Carbon fibers are not considered a satisfactory substitute for natural flake graphite.

Jan 1, 1989

By DIEGO RAFAEL MONTEIRO DINIZ

Os processos de recebimento, armazenamento e distribuição de combustíveis em grandes empresas mineradoras necessitam de um controle robusto e eficaz de todas as operações, uma vez que representam elevado custo por tonelada de minério produzida e expedida. Para tanto, a automatização dos processos que envolvem combustíveis é necessária, capaz de promover redução de custos, aumento de produtividade, confiabilidade e precisão nos dados e melhorias nas condições de trabalho na gestão e operação em combustíveis. Foi aplicada uma análise descritiva de um estudo de caso de um projeto de automação para esta finalidade implantado na empresa VALE S/A. Foi feita uma avaliação sistemática dos recursos, equipamentos e tecnologias necessárias a completa automação e integração dos processos que envolvem combustíveis e os ganhos alcançados após a implantação.

Oct 30, 2017

By A. M. Cameron

THE HOISTING PLANT at the Stobie section of the FroodStobie mine is a two-shaft installation designed to handle a daily production of 18,000 tons of ore at depth. The two vertical shafts are within 100 feet of -each other, an arrangement made to provide the needed capacity and to give flexibility of operation (Figure 1). No. 7 shaft, used for handling men and supplies as well as for hoisting ore, has been sunk to the 3000 level and is served by a manhoist handling two cages and an orehoist with two 14-ton capacity Kimberley skips. No. 8 shaft, so far completed to a depth of 1,900 feet, handles only ore. The hoist is semiautomatic with push-button control and the skips are 15-ton capacity bottom-dump. The ore-loading pocket for first stage hoisting at both shafts is 120 feet below 1,600 lev-el and additional pockets are planned, as the shafts are deepened, at 800 foot intervals down to 4,000 feet.

Jan 1, 1956

By Jaeheon Lee, Jai‑Won Byeon, Junmo Ahn, Jun‑Jae Lee, Eun‑Woo Kim, Yoo‑Jin Kim, Jiajia Wu, Jae‑Yeon Kim

Growing demand for valuable battery materials and environmental issues from battery disposal make the recycling of spent lithium-ion batteries (LIBs) essential. Specifically, the green approaches using organic reagents have garnered many attentions for battery recycling. In this study, a synergetic organic leaching system using methanesulfonic acid (MSA) of strong organic acid and citric acid (CA) with good chelating ability was investigated to extract valuable metals from LiCoO2. Hydrogen peroxide was used as a reducing agent to enhance leaching kinetics. Cobalt extraction of 98% and lithium extraction of 97 % were achieved in the optimized condition; 2.4M MSA, 1.6M CA, 1.0 vol% H2O2, S/L ratio 80 g/L, 85 °C, and 1 h. The optimal leaching condition of the MSA-CA mixed leaching system exhibited good applicability to various cathode scraps, such as LiCoO2, LiNixMnyCo1- x-yO2, and LiNixCoyO2. The dissolved Co and Li ions in the MSA-CA leachate were selectively recovered with high recovery efficiencies of 99 % and 97 % as Co3O4 and Li3PO4, respectively. The recovered Co3O4 and Li3PO4 were utilized to regenerate cathode materials. LiCoO2 and LiFePO4 were also synthesized through a solid-state reaction and hydrothermal method. The recycling process based on the MSA-CA-H2O2 synergetic leaching system was proposed, and it might be applied as a green and economical organic leaching system for the recycling of various types of spent LIBs.

Sep 20, 2023

By Richard A. Walker

This report describes the development and performance of a multi-level, multi-function Calibration Light Source designed for field-calibration of a group of specific photometers. The Calibration Source is capable of providing ±35% accuracy calibrations at all of the following levels: 0. 05 foot-Lamberts, 6 foot-Lamberts, 6 foot-candles and 20 foot-candles. The Source was found to provide constant light output to within 1% over 50 hours of lamp operation and for line voltage variations of ±25%. It is compact and light-weight (11 pounds), and can be easily transported and used by one man in normal office environments (without requiring a darkroom).

Jan 1, 1976

By K. Bachmann, M. Rudolph, U. A. Peuker, H. H. Duong, T. Heinig, T. Leißner, H. Schubert, Helmholtz-Institute Freiberg for Resource Technology, Technische Universität Bergakademie Freiberg

"Minerals can be liberated by random fracture of particles into smaller fragments or by detachment along phase boundaries. These two mechanisms represent borderline cases. When ores get comminuted the liberation of minerals is achieved to some extent by both mechanisms. This article describes a method to determine the extent of transgranular and intergranular fracture on surface exposure of minerals based on 2-dimensional liberation analysis.The approach uses the non-biased surface information like phase specific surface area (PSSA), phase specific free surface (PSFS) and phase specific locked surface (PSLS) of minerals and their change with comminution. The amount of transgranular and intergranular fracture on surface exposure can be calculated using the phase specific surface parameters.A sedimentary rock (apatite ore), an igneous rock (nepheline-syenite) and an artificial material (copper slags) were ground to different fineness. Based on the mineral liberation analysis (MLA) of feed and products, the extent of phase boundary fracture on the surface exposure of the minerals is studied.INTRODUCTIONMinerals can be liberated ether by comminution or by detachment (Gaudin, 1939). Liberation by comminution is a random fracture mechanism, which is not being influenced by ore texture, grain boundaries and mineral features (transgranular fracture). Liberation by detachment represents a fracture along grain boundaries (intergranular fracture). Random fracture often is named as the dominating mechanism for the liberation of ore minerals. This has been the basis to simplify models for liberation modelling (Barbery, 1991; King, 1979; Meloy, 1984) assuming that the probability of cracks moving along grain boundaries is zero. Thus, no interfacial area is lost during comminution."

Jan 1, 2016

By T. M. Korzekwa, R. L. Cavanagh

Following considerable experience with the beneficiation of Wabana iron ore by standard methods, a study was made of the benefits to be obtained by semi-reduction. The basis of the laboratory program was an extensive mineralogical and liberation investigation which guided subsequent work. Partial reduction and beneficiation on a laboratory scale was carried out on lump ore and fines. The reduced ore was magnetically concentrated and the concentrated fines were briquetted. Data are presented on reducibility, sizing vs reduction rate, magnetic cobbing and separation, and the elimination of phosphorus. Past work is reviewed briefly and comments are made on the relation of laboratory to pilot-scale tests.

Jan 1, 1967

By Jack L. Woodward

The evolution of surface mining equipment has resulted in larger, faster haulage units, loaders, etc., resulting in increased demands on steering technology. Careful analysis of these systems was warranted to determine if steering-related safety problems have been introduced. The objectives of this program were to: 1. Define the generic types of steering systems being used on mobile mining equipment used in surface mining operations. 2. Gather information on steering-related accidents in mining operations. 3. Assess the need for initiating government-sponsored research into steering system technology. A comprehensive literature survey was conducted concurrent with extensive contacts with mining operations, mining equipment manufacturers, steering system component manufacturers, and government agencies. A Technical Evaluation Group composed of representatives from the above organizations was formed to review the data gathered. It was concluded that the steering systems in use on surface mining equipment are reliable and do not present a safety problem. The Society of Automotive Engineers, Inc. is active in pre-paring voluntary consensus standards to assure that the minimum levels of performance are defined for industry.

Jan 1, 1979

By J. A. Organiscak

Enclosed cabs are a primary means of reducing the silica dust exposure of equipment operators at surface mines. The National Institute for Occupational Safety and Health (NIOSH) has investigated various factor effects on enclosed cab air filtration system performance. Factors experimen­tally investigated were intake filter efficiency, intake air leakage, intake filter loading (filter flow resistance), recirculation filter use and wind velocity effects on cab penetra­tion (inside to outside cab concentration ratio). Adding an intake pressurizer fan to the filtration system was also investigated. Results indicate that the intake filter efficiency and recirculation filter were the two most influential factors on cab penetration. Use of a recirculation filter significantly reduced cab penetration over the intake air filter by itself due to the multiplicable filtration of the cab interior air. Cab penetration was also affected to a lesser extent by intake filter loading and air leakage. Adding an intake pressurizer fan notably increased intake airflow and cab pressure while providing only minor changes to cab penetration.

Jan 1, 2008

By Dirk van Zyl

Pad construction costs can impact the overall economics of heap leach projects. Pad construction costs for single-and double-lined pads, using various designs, are listed for a typical small and large project. Double-lined pads are now more often required by regulatory agencies. Unless such designs reduce the risk of site specific contamination significantly, the extra costs cannot be justified from an economical viewpoint. Specific attention is given to the short project life (typically five years) of heap leach projects. A few numerical examples are presented to demonstrate the overall economic impacts of these costs on economic parameters.

Jan 1, 1990

By Mike Wongkaew, Brandon Kluzniak, Per Vilhelmsson

Rail access to Ontario International Airport (ONT) has long been a goal of San Bernardino County Transportation Authority (SBCTA) to increase public transit options to ONT and provide incoming ONT passengers improved access to San Bernardino County and the greater Southern California region. This paper describes the planning for the Design-Build-Operate-Maintain (DBOM) delivery of an emerging technology tunnel connection between the Rancho Cucamonga Metrolink station and ONT. The paper discusses key technical considerations, challenges, and opportunities; conceptual configuration development; and construction planning and establishment of the footprint for the underground connection.

Dec 1, 2022

By Hans Jahncke G

El petróleo se forma por rocas porosas, que al producirse se llaman los "reservorios de petróleo". Por lo cual este debe poseer intersticios entre las partículas sólidas, que acumulen ciertos fluidos. Empero este no es el único fluido encontrado, sino que pueden contener aguas, gas, en tanto solución del petróleo libre. En este sentido, el objetivo del texto es señalar el funcionamiento del laboratorio de reservorio, en tanto determine estas propiedades, las cuales son básicas en todos los cálculos de reservorios, determinación de reservas, desarrollo de la producción y las posibilidades futuras de recuperación secundaria. Las funciones del Laboratorio de Reservorios de la International Petroleum Company se dividen en dos partes: El primero refiere el trabajo de campo, que incluye obtención de registros de presión, temperatura y determinación de niveles de fluido en los pozos y el segundo, los trabajos de laboratorio propiamente dichos como la determinación de las propiedades físicas de las rocas del reservorio y de los fluidos que contiene. Estos a su vez comprenden la saturación y permeabilidad. En cuanto a los trabajos de muestras de petróleo del subsuelo, encontramos factores como la presión de saturación, relacion de gas-petróleo, volumen de formación y viscocidad. Asimismo los análisis de trabajos de muestras de gas se realizan mediante el desplazamiento de fluídos por inyección de agua.

Jul 20, 1956