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By Marcella Gautê Cavalcante Xavier

As ligas livres de chumbo (Lead-free solder alloys) potencialmente utilizáveis em processos de soldagem branda, tais como as ligas à base de Sn, vêm sendo estudadas como alternativas para substituir as ligas do sistema Sn-Pb. Em vista disto, o presente trabalho, aborda tanto a análise das características microestruturais formadas durante a solidificação transitória das ligas eutética Sn-0,2%Ni e hipereutética Sn-0,5%Ni, quanto a determinação das suas respectivas correlações com os parâmetros térmicos de solidificação: velocidade da isoterma eutética (VE) e taxa de resfriamento (?E). Para tanto, as ligas foram solidificadas unidirecionalmente no sentido vertical ascendente e em regime transiente, e caracterizadas por técnicas de microscopias ótica e eletrônica de varredura. Na liga hipereutética Sn-0,5%Ni, o aumento da quantidade de Ni na liga influenciou tanto o comportamento térmico quanto o espaçamento celular (λC), proporcionando maiores valores de ?E, porém, λC mais grosseiros.O intermetálico NiSn4 formou-se na região eutética de ambas as ligas, enquanto que na liga Sn-0,5%Ni, as fases primárias identificadas por EDS-MEV foram NiSn4 e Ni3Sn4. A transição morfológica celular/dendrítica(?E> 1,2ºC/s) ocorreu apenas para a liga eutética, enquanto que as células regulares da liga hipereutética deram origem as células do tipo placas(?E> 1,4ºC/s).

Oct 30, 2017

By R. C. Timberlake

An understanding of the Florida Phosphate Industry, the mining practices and extraction processes and the historical development of the Industry, is essential to any consideration of reclamation. In the earliest days of the Industry, phosphate rock was produced by screening the phosphate pebble from the matrix. The waste, which consisted of overburden, clay, sand and fine phosphate, and was called "debris", was disposed of onto, either the adjacent surface area, or into mined-out pits. Since the Central Florida area was sparsely settled in those early days, there was no complaint from residents about contamination of streams or the resulting spoil piles - environmental concerns were non-existent. The development of the flotation process in the 1930's and the implementation of the flotation process in the early 1940's was a significant technological breakthrough in the Industry. This technique made possible the extraction of fine phosphate particles, and doubled the recovery of phosphate values from the matrix. However, the implementation of the flotation process produced a new waste disposal problem.

Jan 1, 1978

By Stephen C. Tadolini, Thomas M. Barczak, Paul McKelvey

A new generation of hydraulic mine support prestressing devices has been developed. These thin-walled steel shells are machine-welded and can be inflated with water or any liquid to provide prestressing for a wide variety of roof support products ranging from Can supports to props and cable bolts. With an expansion capability of several inches, depending on the geometry and size of the unit, they can also establish roof contact eliminating the need for wooden wedges or crib blocks that are commonly employed with several standing roof support products. Capable of withstanding pressures from 1,000 to 6,000 psi, these cells are able to transfer roof loading into the support structure without rupturing. A recent development has been the addition of an inexpensive yield valve that provides control of the maximum pressure and load development on the support. This paper examines the performance capabilities of these inflatable prestressing units and the impact they have on the performance of various support systems, including an evaluation of the overall stiffness of the support system and the load control during yielding of the prestressing unit. Recommendations are made regarding the design requirements of the prestressing unit to optimize the support performance. A summary of mine applications using this technology is provided with general comments regarding their impact on ground control.

This report summarizes the work performed under USBM Contract No. H0395041. The primary objective of this work was to extend the noise control technology developed under earlier USBM projects to a wider range of load-haul-dump models to evaluate the general applicability of these techniques. Noise control treatments were designed, fabricated, and installed on three Wagner LHDs (an 5T-2B, ST-2D, and an 5T-8A) selected as demonstration machines for this project. The machines were evaluated either in production mines or at the Bureau's Lake Lynn Mine. The results indicate that it is possible to achieve overall noise reductions of between 4 and 8 dB using these techniques. Engine cooling and seal design were determined to be important design issues in such treatments.

Jan 1, 1984

By George A. Morrison

A deposit Of limestone Was known to exist at a depth of 2000 ft under the property of the Columbia Chemical Division of the Pittsburgh Plate Glass Co. at Barber-ton, Ohio. A 662-acre site was selected for the projected mine, some two miles northwest of the plant and near the main line of the Erie Railway. An electric railway 8800 ft in length connects the mine and the plant. The deposit is overlain by 18 ft of un-consolidated (sand and gravel), 100 ft of water-bearing sandstone, and finally 2080 ft of shale into which thin layers of sandstone are embedded. The limestone bed itself is 345 ft thick and overlies 200 ft of gypsum. A 300-ton-per-hour capacity mine was decided upon. Two shafts were deemed advisable, one for production and the second for service; and these were sunk 550 ft apart, one to a depth of 2323 ft and the other to 2258 ft. Each is 16 X , ft in the clear and timbered with 6-in. steel H-sets on 8-ft centers, using 3/8 X 4 X 4-in. angles as studdles. Twelve inch I-beams were used at 160 ft intervals as bearers set in deep hitches and concreted to a vertical depth of 8 ft. Wooden sheathing was first employed but sloughing of the shale created a pressure on this lining and finally concrete was deemed necessary. Water was encountered only within the first 315 ft, flowing at 60 gpm and by grouting this was reduced to 15 gpm. Temporary wooden sinking headframes were installed with 300 cu ft capacity storage pockets and with doors automatically controlled by air cylinders by hoistmen. Each shaft was operated on four 6-hr shifts. The usual V-cut was drilled at the center of the shaft and the round consisted of 34 holes- A 40 pet gelatin dynamite was employed with some 60 pet in the cut holes. Drilling crews consisted of four to six men. Shale drilled easily but became more bed in depth and sandstone wore away the gauge Of the bits rapidly. A room-and-pillar mining system was adopted whereby rooms turned off on 80-ft centers, each room 40-ft wide and 50-ft high. Rib pillars between rooms were cut into 100 ft lengths by frequent holes. Ventilation is achieved through the two shafts, the down-draft through the service shaft, and the return through the pr0duction shaft. The hoist has a a Of 300 tons per hour and is equipped with 10-ton balanced skips requiring. a 2-min cycle Or 30 trips Per hour- Hoisting is designed to Operate by automatic loading and no hoistman is required for normal Operation. The 48 X 60 in. jaw primary crusher is underground. It is fed through chute and chain feeders and is flood-oil lubricated and cooled. An inclined belt conveyor returns oversized material to the crusher. Tramming is by Diesel-powered trucks.

Jan 1, 1948

By George A. Morrison

A deposit Of limestone Was known to exist at a depth of 2000 ft under the property of the Columbia Chemical Division of the Pittsburgh Plate Glass Co. at Barber-ton, Ohio. A 662-acre site was selected for the projected mine, some two miles northwest of the plant and near the main line of the Erie Railway. An electric railway 8800 ft in length connects the mine and the plant. The deposit is overlain by 18 ft of un-consolidated (sand and gravel), 100 ft of water-bearing sandstone, and finally 2080 ft of shale into which thin layers of sandstone are embedded. The limestone bed itself is 345 ft thick and overlies 200 ft of gypsum. A 300-ton-per-hour capacity mine was decided upon. Two shafts were deemed advisable, one for production and the second for service; and these were sunk 550 ft apart, one to a depth of 2323 ft and the other to 2258 ft. Each is 16 X , ft in the clear and timbered with 6-in. steel H-sets on 8-ft centers, using 3/8 X 4 X 4-in. angles as studdles. Twelve inch I-beams were used at 160 ft intervals as bearers set in deep hitches and concreted to a vertical depth of 8 ft. Wooden sheathing was first employed but sloughing of the shale created a pressure on this lining and finally concrete was deemed necessary. Water was encountered only within the first 315 ft, flowing at 60 gpm and by grouting this was reduced to 15 gpm. Temporary wooden sinking headframes were installed with 300 cu ft capacity storage pockets and with doors automatically controlled by air cylinders by hoistmen. Each shaft was operated on four 6-hr shifts. The usual V-cut was drilled at the center of the shaft and the round consisted of 34 holes- A 40 pet gelatin dynamite was employed with some 60 pet in the cut holes. Drilling crews consisted of four to six men. Shale drilled easily but became more bed in depth and sandstone wore away the gauge Of the bits rapidly. A room-and-pillar mining system was adopted whereby rooms turned off on 80-ft centers, each room 40-ft wide and 50-ft high. Rib pillars between rooms were cut into 100 ft lengths by frequent holes. Ventilation is achieved through the two shafts, the down-draft through the service shaft, and the return through the pr0duction shaft. The hoist has a a Of 300 tons per hour and is equipped with 10-ton balanced skips requiring. a 2-min cycle Or 30 trips Per hour- Hoisting is designed to Operate by automatic loading and no hoistman is required for normal Operation. The 48 X 60 in. jaw primary crusher is underground. It is fed through chute and chain feeders and is flood-oil lubricated and cooled. An inclined belt conveyor returns oversized material to the crusher. Tramming is by Diesel-powered trucks.

Jan 1, 1948

By B. Mishra, A. Staley, D. Kirkpatrick

The major waste product of the alkaline extraction of alumina from bauxite [Bayer Process] is known as red-mud. Approximately, a ton of red-mud is produced for every two tons of bauxite mined. The red-mud produced from Jamaican bauxite is rich in hematite, alumina and titanium oxide. It has been shown that over 90-wt. pct. alumina can be recovered from red-mud by soda-ash sintering and caustic leaching. Hematite can be carbothermically reduced with a degree of metallization of over 94 pct resulting in attempts for magnetic separation. These separations are desirable in the notion that there is no waste product generated from this type of processing and consequently an opportunity for complete utilization of the waste material. Conversely, the pre-separated material could be charged through the tuyeres in an iron blast furnace or smelted to produce pig iron. If smelted, the concentration of titanium oxide in the slag will be significantly high justifying its recovery by established acid-leach process. This paper describes the results of alumina recovery and the plans for titanium oxide recovery from red-mud. In addition, the situation of ongoing efforts in iron extraction, particularly, the method of magnetic separation of the reduced material. The problems associated with the use of reduced red-mud as an alternative to direct-reduced iron [DRI] has also been discussed. Critical assessment of the recovery sequence chosen for the products has been described based on economics.

Jan 1, 2001

By Charles H. Moore

In the study of the properties of rutile pigments it became apparent several years ago that certain physical and optical properties could not be determined on particles of pigmentary size. Since reflected light is the dominant type which reaches the eye from small particles, the true color of pure rutile was not known. Most rutile pig-ments are acicular in habit, elongated parallel to the "c" axis. It was considered important to know the nature and tone of light transmitted, for example, by a basal plate. Further, as shown by spectrophotometric curves, there is a very strong absorption of light of 4000 A as measured on particles with random orientation. It would be interesting to see whether this absorption position varied with predetermined and selected orientations. Also, since the behavior of titanium pigments in a vehicle is important, a knowledge of the surface wettability of single crystals by various media should prove very fruitful. Finally, the optical properties of rutile are such that it should show, in a single pure crystal, greater fire and brilliance than the diamond. Mineralogists had long speculated that this would be the case and curiosity was strong to produce a single crystal large enough to cut. In light of the above, a project was initiated for the formation of single crystals of rutile. Method of Formation of Rutile Single Crystals Fortunately, purification of TiO2 produced from both titanium tetra-chloride and titanyl sulphate solutions had reached the stage where spectro-graphically pure starting material could be made. Spectrographic analysis of the feed material used in the initial experiments is compared with the present feed material in Table 1. It is apparent that the present large scale purification is approximately as good as the original experimental, small scale purification. Verneuil1 produced synthetic ruby and corundum in 1904 by the well-known flame fusion process, which today bears his name. Except for mechanical improvements the present commercial production of synthetics by flame fusion is essentially unchanged from his initial method. His burner consisted of an inner orifice through which was fed the feed material and oxygen. Surrounding this was a larger outer orifice through which was fed hydrogen at lower pressure. This arrangement consists then of a lance of oxygen burning in an atmosphere of hydrogen. The proportions of hydrogen to oxygen usually used in corundum production is about 3:1, providing there is sufficient temperature to reach the 2050.°C required for the fusion of alumina. From work done in the Titanium Division Laboratories2 and from the published work of Erlich3 it was known that rutile appears to lose oxygen near its melting point and that it would not be possible to grow single crystals in a strongly reducing environment. Consequently, in order to determine whether single crystals could be grown at all, an Airco oxygen-acetylene torch with

Jan 1, 1950

By G. E. Joe

"This is a panel discussion on the milling experience with large volume flotation machines in Canada. Over the past ten years, the Canadian milling industry has been characterized by treatment of ever increasing tonnages of lower grade ores. In order to treat these ores efficiently, mineral processors have been employing increasingly larger volume flotation machines. In older established mills, standard flotation cells have been replaced by the larger volume models with very apparent savings in mill floor space as noted in the Opemiska copper mill.We are pleased to hear from four mill operators with extensive experience on large volume flotation machines. They are:1. I. E. Wahn, metallurgist with Falconbridge-Manibridge, who will describe their mill experiences with the Tank cell and the Maxwell cell.2. G. M. Hughes, mill superintendent of Sherritt Gordon-Ruttan, will detail recent experience with the Agitair cell.3. J. R. Maxwell, mill superintendent of Opemiska Copper, will report on their Maxwell cell installation and operation.4. A. H. Winckers, superintendent of Development and Technical Control, Sullivan Mill, will present a paper written by H. J. Chalmers describing Cominco's past experiences with large volume flotation machine installations including Denvers, Wemcos and Maxwells."

Jan 1, 1974

By Serge Vézina

Environmental issues have evolved considerably over the last two decades. The main contributing factors, to name a few, have been the changing values of our modern societies, the globalization of trade and its linkage to environment, evolution and accessibility of information/communication technologies, better educated populations, climate change, long range transport of toxics and the increasing influence of NGOs and multistakeholders. As well, environmental management of mining operations had to be realigned in order to meet these new realities and to respond to more elaborated regulations oriented towards sustainability. Environmental Management Systems (EMSs) have emerged and have been introduced to meet not only the assurance of conformance to regulations but also to prevent pollution and to apply the continuous improvement of mining processes. EMS models have been developed and certification to international standards (e.g. ISO-14 001) is a common practice. Globalization has imposed challenges and additional requirements to environmental management. Developing a mine in emerging countries implies dealing with international agencies, local communities and a variety of government infrastructures to obtain a ?licence to operate?. This paper presents the structure of our EMS and how we have adapted its implementation to our operations in South America.

May 1, 2003

By Nicholas J. Grant, Ulf Kalling, John Chipman

D. E. Babcock (Republic Steel Corp., Youngstown, Ohio)—I would like to know what evidence you have to prove the MnO was pure MnO. I would also like to know whether you might not explain it on the basis of a temperature reversion; and, was it due to the oxidizing power of MnO? N. J. Grant (authors' reply)—Briefly, we have no proof that pure MnO was used. The manganese oxide was added as chemically pure MnO,. MnO is assumed as the oxide in the reacted slag following standard molecular slag theories, especially under the reducing conditions of these experiments. The noted sulphur reversion cannot by any means be explained on the basis of a temperature reversion since the temperature effect is shown in this paper to be very small. Until a more logical explanation can be offered, backed I hope by some experimental proof, we propose to explain this sulphur reversion as stated in the paper, namely, that it is due to the oxidizing effect of the added manganese oxide. Member—How did the oxygen in the slag give you a reversion of sulphur? What was the mechanism there?

Jan 1, 1952

By Walter Morley

This paper is a record of the first of a series of tests on sulfide minerals to be made by the metallurgical department f the University of California. The purpose of the tests here recorded is to determine the action of standard oils, oil mixtures, and addition agents on the flotation of pyrites. The question of the commercial value of pyrite was not considered. Of the many factors affecting flotation, only two-the oil and the other agent used-were made variable. The flotation agents used are given in the accompanying table. PENSACOLA TAR AND TURPENTINE CO. (PENTARCO) NON-POL., SP. Dis. REF. PER No. KIND GR. POINTS INDEX ?VISC. CENT. 200 Refined wood creosote oil 0.965 105-275 1.5096 1.7 7-8 350 Crude pine wood oil 1.019 70-345 1.525 2.9 4 75 Crude wood turpentine 0.887 65-217 1.456 0.9 10-12 80 Crude pine oil 0.911 70-232 1.4894 1.1 8 750 Heavy pine tar oil 1.063 165-350 1.557 41.0 400 Wood creosote oil 1.025 190-360 1.4977 2.9

Jan 7, 1921

After reviewing the many excellent papers being delivered here, it is apparent that we are all concerned with the same general subjects of commodity agreements, international cartels, and anti-trust problems as well as the impact of governments on resource management and minerals pricing. Accordingly, as a relative newcomer to the mining business, I feel that my most meaningful contribution can be made by taking a more philosophical look at the future of our system of democratic capitalism. Unfortunately, governments the world over seem intent on jeopardizing the high standards of living resulting from the Industrial Revolution and furthered by the emergence of its by-product, capitalism. This tendency is particularly germane to the basic natural resource field, since government regulations, controls, and intervention in mining far exceed even the constraints normally imposed on hard-pressed consumer-oriented businesses. Increasingly, many governments seem to feel that natural resources no longer belong to private individuals but rather are the property of the state to be developed in a regulated manner and usually in a way directly contrary to the functioning of the free market system.

Jan 1, 1978

Resident Instruction: The character of an institution, the varying demands made upon it, its geographical location, its own internal organization, all are factors that predispose against rigid standards, curriculum-making, research programs, and extension services. Mineral industries educators must keep in mind that the under- graduate is the core of the college, a philosophy that implies a set of inviolable principles.1 They will want to turn out graduates with overwhelming talent in their field, together with incorruptible ethics, prepared to deal with people, as well as with theories and things. Curriculum-making is a popular educational pastime. No course makes or breaks a curriculum. The particular qualifications and interests of individual students must find expression. However, selection must be made under guidance so that the student's individual needs are realized. In this way, specialization can be introduced into curricula previously conceived to be of general science or engineering nature only. In its essence, formal education is society's endeavor to put old heads on young shoulders, to implant the experience of centuries in the youthful generation. Seen in this light, it is evident that isolated facts have little

Jan 1, 1950

By A. J. Weinig

THE Liberty Bell cyanide precipitate is unique in that it is apt to vary widely in composition in the course of very short, periods of time, and a method of refining and melting that would prove highly satisfactory at one cleanup would yield almost an hopeless "mess" it a second. Table I gives a general conception of the wide range in grade and composition of those raw precipitates. It is evident that no one standard flux could be expected to produce a high-grade bullion with such a widely variable precipitate, and that any method of treatment with acid requires most careful consideration. Refining by Acids Naturally, our first efforts to improve our precipitates were directed along the lines of acid treatment. Table II embodies the results of careful sampling and analysis of one cleanup at the time when wet refining reached its maximum development at this mill. We have now discarded all methods of wet refining, successfully replacing them by amore scientific method of flux calculation described herein, but it is believed that a general description of this wet refining is warranted as it throws some interesting side lights on acid refining in general.

Jan 3, 1916

By Yu. P. Astafyev

The, control of drilling and blasting is a complicated dynamic system whose aim is to ensure safety and prepare rock of required grade and the standard level of broken material reserves Unlike other processes drilling and blasting, as an object have the following features: -a large variety of drilling and blasting methods due to specific conditions of blasting, various types of drilling equipment, schemes-of blasting, types of explosives and others; -relative continuity of drilling, the character of mammoth blasts being discrete; -increased requirements to the safety of blasting;; -a great. number of control parameters, some of them having a qualitative characteristic but not a quantitative one; -availability of feedforward and feedback with other mining processes in terms of time and space. These features predetermine the hierarchical structure of an automated system of planning and control of drilling and blasting (fig.1). The system is implemented on the basis of unity of the data base and in interre lation with other problems of controlling mining operations. An automated system of this kind makes it possible to take optimal decisions actually on all the levels and stages of operations, with rock having been blasted before extraction.

Jan 1, 1986

By Northcutt Ely

This volume summarizes mining and petroleum legislation in 22 jurisdictions of the Near East and South Asia. Within these jurisdictions, primary attention is given to requirements that must be met in each country for acquisition of rights to permit development of mineral resources. Coverage includes : First, identification of the controlling laws or statutes governing minerals acquisition and reference to the administrative authority; second, analysis of the laws governing mines and quarries and their products; and third, analysis of laws applicable to natural gas, petroleum, and related materials. Where pertinent, sections dealing with historical background or administration have been added. In countries where minerals are subject to control of states or provinces, those areas are considered separately from the central government.

Jan 1, 1972

Reduce the noise levels to which operators of double-drum longwall shearers are exposed without compromising the operational effectiveness of the shearer. The Problem Noise produced by double-drum longwall shearers can be harmful to machine operators. Typical noise levels at the lead-drum operator position range from 100 to 105 dBA, and Federal noise regulations allow only one to two hours of exposure per shift at these levels. Noise radiated by the shearer cutting drum is the primary contributor to the overall noise level. However, test of a noise-controlled cutting drum developed by the Bureau of Mines reduced the operator noise level to 95 dBA, thereby increasing the allowable operating time to four hours per shift. Approach The key design aspect of the noise-controlled shearer drum is its reduced vibration-al response to coal-cutting forces. Laboratory studies have shown that these forces are concentrated in the low-frequency region (500 Hz and below). Since the cylindrical core and the cantilevered I plate-like helix of the standard shearer drum are easily excited by these forces (natural vibration frequencies be-

Jan 1, 1985

By O. W. Ellis

THE writer has dealt with the effect of various methods of melting copper upon the gas content of the metal.1 The copper referred to in his in his earlier paper was melted in the foundry both in the oil furnace and the electric furnace. As the metal, did not measure up to conductivity FIG. L -INGOT OF OVERPOLEP COPPER. standard, the term "casting copper" was applied to the material in the title of the paper. It was thought that some information in regard to the gases in a sample of overpoled copper might also be of interest, and through the courtesy of C. R. Stevens, superintendent of the copper mill of the Westinghouse Elec. & Mfg. Co., such a sample was obtained. The metal was chill-cast in the form of an ingot about 7 in. long, 2 ½ in. deep (from the base to the raised surface of the ingot) and from 1 3/8 to 1 7/8 in. wide. A photograph of part of the ingot is shown in Fig. 1. The effect of overpoling on the surface of the metal is here quite clearly shown.

Jan 1, 1929

Detailed mineralogical investigation of a tailing sample from the Juno plant circuit at Tennant Creek was carried out to determine the nature of the unrecovered bismuth and whether any possibility existed for improving bismuth recovery. The investigation showed that the Ibismuth was present in a complex mixture of Bi-Pb-Ou-Se-S minerals (termed "bismuthinite"), of which about 74 per cent was locked (mainly with magnetite) and 26 per cent was liberated (18 per cent in the minus 7 µm slime). The results suggested that attention should be directed to both finer grinding and improved flotation of slime "bismuthinite", and testwork carried out by Peko Mines N.L. on the basis of these recommendations led to a significant improvement in bismuth recovery.Detailed mineralogical investigation of two Juno concentrates was carried out to determine the nature of the selenium present and whether any possibility existed for improving the selenium grade. The investigation indicated that virtqally all the bismuth, selenium, and lead was present in "bismuthinite", which showed a composition range of 32-82 per cent Bi, 0-42 per cent Pb, 0-24 per cent Se, and 5-18 per cent S. Differences in the Bi/Se ratios of the two concentrates could be attributed to different average Bi/Se ratios of the constituent "bismuthinite", and the relatively low selenium grade of the "bismuthinite" precluded the possibility of obtaining a high grade selenium concentrate with high selenium recovery.However, differential flotation and/or low intensity magnetic separation to remove chakopyrite, and magnetite, the main diluents of the concentrate, could be expected to upgrade the selenium content byup to 80 per cent (relative) and .festwork carried out by Peko Mines N.L. on the basis of the recommendations of the mineralogical investigation confirmed that depression of chalcopyrite in the flotation circuit could produce significantly improved selenium grades.These investigations illustrate the application of mineralogy to the practical problems of improving plant performance. Mineralogy has an important role to play in providing quantitative data on which the metallurgist can evaluate plant performance and base a programme of metallurgical testwork, and early mineralogical investigation of feeds, concentrates, middlings, and tailings can lead to the avoidance of much abortive and expensive metallurgical testwork.

Jan 1, 1974