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By E. C. Perkins

This report describes a ferric chloride trap, based on formation of a low-melting sodium chloride-ferric chloride mixture of near-eutectic composition, and its use in chlorination of impure titaniferous materials. The trap is placed in the hot gas stream between the chlorination reactor and the condenser. Virtually all of the iron is removed by the trap. The condensed titanium tetrachloride is free of suspended solids and contains only a trace of iron. Four examples are given of the use of the ferric chloride trap in chlorination of impure titaniferous materials. INTRODUCTION In the Kroll process, ductile titanium metal is produced by reducing titanium tetrachloride with magnesium metal.4/ In commercial practice, titanium tetrachloride is produced by chlorinating titaniferous materials in the presence of carbon.2/ In 1957 most producers were using rutile, and virtually all plants were designed for its use. About four-fifths of the domestic consumption of rutile was imported from Australia. The Bureau of Mines, under provisions of contract DMP-116 with the General Services Administration, studied electrosmelting of domestic ilmenites and titaniferous magnetites to produce high-titanium slags with pig iron as a byproduct. Under the same contract, chlorination studies also were being made of these slags. Smelting was done at the Northwest Electrodevelopment Experiment Station, Albany, Oreg., and chlorination at the Electrometallurgical Experiment Station, Boulder City, Nev.

Jan 1, 1958

By William O. Vanderburg

Some mines after passing through the prospecting stage and becoming sizable enterprises still adhere to the development program of the prospect, extending their workings without definite plans. In mining operations where definite structural conditions do not exist, a prearranged layout of mine development is not feasible; but where exploration and preliminary development have indicated the extent and probable limits within which the ore is expected, careful planning of development will result in a lowering of mining costs and a consequent increase is profits. A lack of definite plane for laying out mine workings is one of the contributory factors to unnecessarily high costs. Although this paper deals primarily with the influence of level spacing on mining costs, still other phases of mine development, such as the proper spacing of ore chutes and raises, can be analyzed on a cost basis in a similar manner, as shown herein. LEVEL SPACING The problem of establishing a new level or levels in order to exploit steeply dioping ore deposits and prospect the ground at depth recurs at intervals during the active life of mines. Driving levels is largely "dead work" and therefore costly. By the judicious selection of the proper level interval after balancing the opposing factors involved in the problem, a considerable saving in mining costs can be effected. Although much has been written in regard to the various methods employed in ore extraction, mining literature is still incomplete in regard to the factors-influencing level spacing at various mines. Level spacing involves procedures not lending themselves readily to description, and, moreover, it is a phase of mining operations that is apt to escape criticism, because only those in close contact with the operations are equipped with the necessary familiarity with the conditions to pass judgment.

Jan 1, 1932

By M. R. Hosseini

Among all gravity concentration methods, Shaking-table is the most effective one from the metallurgical point of view. In this study, Shaking-table was used for concentrating a manganese ore sample from Ghasem Abad area in Kerman, Iran. Experiments were designed by using L8Taguchi design with five variables and each variable in two levels. The influence of each variable and their interactions on the operation of the device was studied. The variables under investigation were: table slope, table frequency, water flowrate, feed rate, and particle size. The manganese concentrate grade and recovery were used as response variables. It was shown that water flowrate, table slope, feed rate, and particle size are the significant variable on concentrate grade; while, all the variables influence manganese recovery.

Jan 1, 2014

By P. K. Chatterjee, G. D. Just

Sublevel open stoping is a low-cost method that has been successfully employed in many large underground mining operations. Where ore body characteristics are suitable, extensive mechanization and the use of large-scale stoping techniques can considerably reduce operating costs. However, careful long-term planning of mine layouts and large capital commitments in development are required prior to production. Implementing precise mine design procedures and carefully controlling operations can result in considerable benefits. This article describes methods to achieve these objectives based largely on mining operations at Mount Isa, where sublevel open stoping has been used since 1932. Ore won by this method accounted for a very large percentage of the total tonnage produced at Mount Isa. Major costs associated with sublevel open stoping can be classified as drilling, explosives and charging, and LHD costs. In this article, analyses of these costs are made with particular reference to stope design. Parameters such as burden, drill hole diameter, explosive density, specific charge, etc., are considered in establishing the interrelationship of unit operating costs, as well as total costs of sublevel open stoping.

Jan 10, 1981

By Ghislain Bournival, Cagri Emer, Seher Ata

"It is well known among flotation practitioners that the contact angle can be correlated with the amount of material recovered from feed by flotation. The contact angle of solids can easily be modified by the addition of a collector. However, some collectors also have frothing properties thus altering the solid and bubble surface properties simultaneously. To avoid this problem, a technique has previously been used in which silanol groups are attached to the surfaces of the particles, but this method has its own problems. In this work, silica particles with various surface hydrophobicities were prepared using an esterification process. By using alcohols with different hydrocarbon chain lengths, from 4 to 12 carbon atoms, surfaces with a wide range of contact angles could be prepared. The technique was used in the modification of silica particles that were tested in a fluidized bed flotation column, and a laboratory mechanical flotation cell. In parallel experiments, dodecylamine (DDA) was used as a collector. It was found that irrespective of the type of flotation machine and surface preparation method, there was a close correspondence between flotation recovery and the contact angle of the particles. The silanation process has known drawbacks relating to the presence of moisture during the reaction, and the stability of the silane coating after it is been prepared. Esterification does not suffer from these disadvantages. This work has shown that the esterification technique is a robust alternative method for preparing hydrophobic quartz surfaces."

Jan 1, 2014

By C. J. Clayton, A. J. Haynes, D. A. Hickson, B. Thiele

The Meadowbank Gold Project, formerly owned by Cumberland Resources Ltd. and currently owned by Agnico Mines Ltd., is currently being developed approximately 70 km north of Baker Lake, Nunavut, in the eastern Canadian Arctic region. The Meadowbank Gold Project currently consists of a series of gold-bearing deposits within relatively close proximity to one another, which are planned to be mined primarily as a truck-and-shovel open pit operation using conventional gold milling and extraction. The mining plan indicates that approximately 20 million tonnes of ore will be mined over a mine life of eight to ten years. The operation will generate approximately 160 million tonnes of mine waste rock and about 20 million tonnes of tailings. The site is located in an area of continuous permafrost with mean annual average air temperature of -11°C and average annual precipitation in the range of 100 to 200 mm. Lakes cover a large portion of the site, including some of the ore deposits. The location of the site and the physical environment pose challenges to development. This paper presents some of the designs considered to effectively manage and utilize the waste products of mining at the project. Note that volumes, tonnages, construction concepts, and data presented in this paper are accurate for the time of writing and are subject to change and modification as the project progresses, additional modelling is carried out, and additional data are obtained.

Jan 1, 2007

The sampling of a run-of-mine (ROM) ore with the objective of controlling the fundamental variance associated with the sampling step is a poorly understood subject. Finding the effective sampling constant by repetitive sampling to establish the variance between nominally identical subsamples of a given mass of the ore is a laborious, time-consuming and very expensive exercise. In this paper, the run-of-mine ore is modelled using three components: ore, waste, and relatively fine material which shows significant liberation of the mineral phase(s) carrying the target analyte. The expression for the sampling constant of the mixture is developed from first principles. The form of the equation provides insight into the factors that are important in controlling the magnitude of the sampling constant and hence the fundamental uncertainty associated with a given mass of sample. The controlling factors are shown to be the size distribution of the ore/waste mixture, the proportion of waste mixed with the ore and the extent of liberation and the size distribution of the liberated material in the finer fractions.

Jan 1, 2008

By S. A. Ford

A SHORT and accurate method for the estimation of manganese in iron and steel is of great advantage to Bessemer works, and I think it may be of interest to some of the members of the Institute to give in detail the process in use in the laboratory of the Edgar Thomson steel works. The process is based on the reaction first described by Beilstein and Jawein.* The steel, spiegel, or iron is dissolved in strong nitric acid, sp. gr. 1.4. Evaporation to dryness is not necessary, unless the amount of silicon is large, as in the case of certain pig irons. Then, as a clogging of the filter in the subsequent filtra¬tion is apt to follow, dissolve first in a dish in hydrochloric acid, quickly evaporate to dryness, redissolve in the strong nitric acid, boil, and while boiling throw in crystals of chlorate of potash from time to time. Violent action ensues, yellow fumes are given off, and binoxide of manganese is precipitated, since it is insoluble in strong * Berichte der deutschen chemisehen Gesellschaft, vol. xii, page 1528.

Jan 1, 1881

By S. C. Termes, R. L. Wilfong

As part of an effort to provide basic data on the fundamental scientific and engineering principles of minerals beneficiation, the Bureau of Mines is conducting research on the flocculation of mineral fines. This paper presents results of studies using cross-linked starches containing carboxyl, diethanolamine, iminodiacetic acid, and xanthate groups to flocculate hematite, goethite, chromite, manganite, pyrolusite, cuprite, and cassiterite fines. The carboxyl and xanthate derivatives flocculated all minerals except cassiterite; the latter was flocculated by only the diethanolamine derivative. The imlnodiacetic acid derivative flocculated hematite, goethite, chromite, cuprite, and pyrolusite fines. Zeta potential measurements were made to help define the reaction mechanism responsible for flocculation. These measurements indicate that electrostatic attraction probably is not involved, except possibly in the case of the diethanolamine derivative. The separation of hematite from quartz by selective flocculation with chelating crosslinked starches under two pH conditions and with two dispersing agents is described. Best recoveries and grades were found when either the carboxyl or xanthate derivatives was added at the natural pH of the pulp in the absence of a dispersing agent.

Jan 1, 1984

By N. V. Nayak

Konkan Railway Project is one of the most ambitious railway construction projects in India, involving construction of a 760.km long, Broad Gauge (1676 mm), single track railway line, connecting Roha in Maharashtra State with Mangalore in Kamataka State. The railway line travels along the Western Coast of Indian subcontinent, through states of Maharashtra (382 km), Goa (105 km) and Karnataka (273 km) (Fig.1). The project alignment traverses through one of the most formidable terrains ever encountered, in the history of railway construction in India. In the State of Goa only, railway alignment is crossing 6 major rivers Terekhol, Chapora, Mandovi, Zuari, Sal and Talpona. Zuari Railway Bridge (1305.6 m), Mandovi Railway Bridges (I and II) (1182.7 m) rank as 2nd and 3rd long bridges, (first longest bridge being Sharavati Bridge (2.2 km} at Honavar) which have been constructed on Konkan Railway. All these three bridges have been constructed by M/s.Asia Foundations and Constructions Ltd. (AFCONS). This paper presents, case history of construction of pile/caisson foundations for Zuari and Mandovi Bridges.

Jan 1, 1996

By Harry R. Cedergren

Properly designed drainage systems can be of great benefit to many kinds of Civil Engineering works, including embankments, and often are the most economical way to protect such works from the damaging effects of water. To function properly, drains must be able to remove water without also removing soil or becoming clogged with soil or erodible rocks. The first criterion to be used in designing drainage systems, called the filter criterion, can prevent all such problems (erosion and clogging) when properly fulfilled in design and construction. The second requirement of drains is that they must be capable of removing all of the incoming water without the build-up of large amounts of head that can damage the protected works. To insure this kind of perfomance, the discharge capabilities of drains should always be verified by appropriate hydraulic and seepage calculations. This paper describes these two basic drain design criteria and also gives examples of application of seepage principles to the evaluation of the potential benefits of drains and to the design of drains for mine waste embankments.

Jan 1, 1985

By H. Reginald Hardy, Xiaoqing Sun

Rheological models are widely accepted as a means of describing the mechanical behavior of geologic materials. It has been found, however, that rheological models developed for a specific stress level on the basis of linear visco-elasticity generally are not satisfactory at other stress levels. It has been suggested that the parameters of such models should be functions of stress level (Hardy, 1965; Kim, 1971). In this paper, continuous functions of stress have been utilized to obtain the required variation of Burgers model parameters with stress level. The model developed using these functions provides a constitutive relation which reflects the real time-dependent behavior of rock materials. The new model is capable of predicting the creep behavior over a wide range of stress levels and also predicts mechanical behavior under different loading condition (e.g. constant stress rate). It is also interesting to note that the mechanical behavior of individual elements in the model appear to reflect the different stages of brittle fracture in rocks (Bieniawski, 1967), namely; crack closure, elastic deformation, stable fracture propagation and unstable fracture propagation.

Jan 1, 1986

By G P. F Chitombo

The dilution of blasted ore with cemented backfill materials has been recognised as a significant factor influencing the economics of some underground metalliferous mining operations. Several mechanisms have been identified as possible causes of fill failures. The purpose of this study was to determine the possibility of damage as the result of one mechanism, that of production blasting adjacent to bodies of cemented hydraulic fill (CHF). A vibration amplitude transfer function has been developed to model the transmission of blast vibrations from the source, through ore, across the ore to CHF interface and into the CHF mass. The model may be applied in the near field. The model has permitted estimation of vibration amplitude at a point in a CHF mass, to which damage criteria may be applied. A number of assumptions and simplifications have been made to render the problem relatively tractable. Ore and CHF material characteristics recorded by a number of authors were utilised to formulate preliminary damage estimations. A simple application of the amplitude transfer model indicated that a zone of plastically deformed CHF would be produced, and would extend to a distance of approximately 0.5 metres from the interface into the CHF. A sensitivity analysis was also conducted, that indicated that the zone of plastic deformation would be more extensive given appropriate conditions. Recommendations for further model development and future laboratory and field investigations have been made.

Jan 1, 1998

By D. Noort, M. Dawborn, D. O. del Castillo

This paper was originally presented at the North American/9th US Ventilation Symposium, June 2002, Kingston, Ontario, Canada. Reprinted with permission of the publishers, A.A. Balkema Publishers, Rotterdam, Netherlands. This paper is a study of the ventilation, cooling and refrigeration system design of the Mindola copper mine in Zambia. The challenges that were addressed varied from the restrictions imposed by an ageing infrastructure to the requirement for increasing the annual production rate, coupled to the introduction of a higher level of mechanization while maintaining acceptable conditions and limiting total ownership costs. A description of how the ventilation, refrigeration and cooling systems were modelled in order to obtain the projected heat loads associated with two different mining methods over the life of the project. The methodology included a number of iterations to optimise the design and include aspects such as the expected inrush of hot fissure water, the operation of diesel machinery at depths in excess of 1500m below surface, developing a cost-efficient cooling strategy and selection of the refrigeration machinery to meet the requirements imposed by the cooling strategy. This paper demonstrates the successful implementation of an integrated design approach.

Jan 1, 2005

By Y. W. Pan, Y. R. Liu

The disturbed natural rock mass tends to equilibrium state accompanying with non-equilibrium evolution process which has significant influence on the long-term stability of engineering structure. The deformation development in the non-equilibrium evolution is determined by two intrinsic processes, trend to equilibrium and damage development, which can be illustrated by evolution of excavated tunnel. Thus the creep and damage must be taken into account in study of non-equilibrium evolution process. Within Rice’s irreversible thermodynamics with internal state variable (ISV), the conjugate force function which equals to zero is a convex surface which divide the stress space into two parts, called equilibrium and nonequilibrium stress space respectively. The concept of effective stress of non-equilibrium has been proposed, in which the stress difference (d - d ) are the effective driving forces of non-equilibrium evolution process with hardening and damage effective. The formulations of inelastic strain rate and energy dissipation rate have been recast in the form of effective stresses. The inelastic complementary energy (ICE) is proposed to measure intensity of non-equilibrium evolution of material system. The specific equations of conjugated forces and kinetic equations of internal state variables are presented. The ICE and rate of energy dissipation are all calculated to be used to evaluate long-term stability of geo-engineering. The results show that rate of energy dissipation may be more convenience and flexible than ICE for internal state variable constitutive equation of rock mass.

Jan 1, 2015

By Matteo Montesi

Deep foundation elements are often used as discrete elements in externally supported earth retaining structures such as soldier piles and lagging walls, secant/tangent pile walls, anchored walls, etc. These structures can be designed using different approaches such as conventional limit equilibrium methods, finite element/difference analyses, and soil spring (p-y) analyses which are contained in various commercially available computer programs used by engineers worldwide. Although these programs usually undergo various degree of verification and validation, users must be aware of each program’s limitations and conditions in which each design approach should or should not be used. These programs may incur difficulties when non-continuous deep foundation elements are used as part of the retaining system and in cases of non-uniform geometry where closed-form solutions are not available. Design input parameters such as passive arching width, wall-to-soil friction, and p-multipliers (pm) are not always given enough attention which may result in potential design deficiencies. This paper presents the main features of various earth retaining structure design approaches and discusses their advantages/disadvantages. The paper addresses some of the limitations and difficulties that may be faced with when utilizing non-continuous discrete deep foundation elements and identifies key elements that are sources of potential deficiencies and errors. An example comparing the design outcomes using different design approaches is presented. INTRODUCTION Earth retaining structures are used to retain soil and create or maintain a difference in ground elevation between grades in front and behind the retaining structure. Deep foundation elements have been used for decades to support earth retaining structures. Earth retaining structures that are supported by deep foundation elements are typically referred to as externally stabilized system (O’Rourke and Jones, 1990). An externally stabilized system uses an external structural element, in contrast to internally stabilized systems which rely on reinforcements installed within and extending beyond the potential failure mass. The design of externally supported retaining structures can be accomplished using different approaches, which can be challenging under certain conditions. Each approach has been discussed extensively in available literature, and is well summarized in the and Federal Highway Administration (FHWA) guidelines. The objective of this paper is to present the most widely used design approaches and discuss their limitations and difficulties in one concise and brief document, giving the reader a good source for comprehensive understanding of the various design approaches, supported by a technical example. This paper is not intended to be a comprehensive review of all available design methods and formulations available in the literature.

Jan 1, 2018

By I. L. Feld

This Bureau of Mines report describes the development of a simple method of producing low-phosphorus hematite concentrates from certain submarginal southeastern iron ores. The investigation was undertaken to obtain additional information on the Clinton iron ore outcrops at the southwestern extremity of the Birmingham district of Alabama and to assist in the development of operating techniques that would make it profitable to use the marginal ores of this area for blast-furnace feed. Batch and continuous pilot-plant tests demonstrated that a relatively simple wet scrubbing treatment) followed by a desliming operation to reject argillaceous (clayey) gangue, consistently yielded a marketable granular hematite product. Iron losses were relatively high but could be tolerated in view of the low treatment cost.

Jan 1, 1960

By Laura Prati

Gold-on-carbon catalysts resulted very active and selective in liquid phase oxidation [1, 2, 3] and during past studies we established that activity is ruled by two factors: particle dimension and gold exposure on the carbon surface [4]. These two parameters are also connected to the nature of activated carbon where the chemical nature of the surface oxygenated groups probably plays an important role [5]. Our studies, focused on the design of an active gold-on-carbon catalyst for liquid phase application, were aimed, operating a fine tuning of all the parameters involved in determining activity, to optimize gold-on-carbon preparation, keeping in mind that gold particle activity increases with decreasing particle size and increasing gold exposure. Gold sol immobilisation represents a versatile methodology in preparing gold catalysts [6]: throughout this work we used as sol stabilizing agent, the N-dodecil-N,N-dimethyl-3-amino-1-propan sulphonate (SB), that provides both sterical and electrostatic stabilisation, a condition we already demonstrated necessary to preserve particle dimension when carbon is used as the support [6]. We generated different gold sols by varying the relative amount of reagents (HAuCl4, SB, NaBH4), the type of alkali and the temperature of the gold precursor reduction. Moreover, as we had recently evidenced that there is also a carbon effect [5], we employed only one active carbon to immobilize the sols.

Oct 1, 2003

By Jeffrey Mitsopoulos

King County?s (KC) Brightwater Conveyance Project in Seattle, Washington involves the construction of approximately 21 kilometers (13 miles) of bored tunnel, in three contracts, with four TBM?s which produce large amounts of real-time digital mining data. To facilitate the management of TBM data with a single interface and assist in project Quality Assurance, KC?s Construction Manager (Jacobs Engineering) recommended the use of the software TPC (Tunneling Process Control), developed by Babendererde Engineers GmbH. The paper demonstrates how TPC was used for oversight, analysis and QA on a complex tunneling project and how contemporaneous review and management of data results in a better understanding of TBM performance than can be obtained by retrospective analysis of data.

By Wils L. Cooley

This report analyzes electrical accident data in the metal/non-metal mining industry. Accidents are categorized to determine their root causes. Special attention is given to accidents associated with inadequate or defective grounding of mine power systems. Recommendations are made concerning proper grounding practice, especially for dredges and for quarries in hard rock or sand. The costs of instituting the recommended practices are estimated for model mine power systems which are based on field data obtained from 37 mines and several electrical contractors. The expected benefits of various suggested safety practices are also estimated.

Jan 1, 1981