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By Howard B. Bradley, Charles F. Weinaug

The phase behavior of a naturally occurring hydrocarbon system whose critical temperature is near the reservoir temperature has been described. The same volume per cent liquid was observed for the firkt time at three different pressures for isotherms immediately below the critical temperature. The shapes of the isothermal equilibrium constant curves necessary to predict this phenomena are discussed and illustrated. INTRODUCTION The phase behavior of a number of hydrocarbon systems has been reported; however, very little data are available on natural occurring hydrocarbon systems whose critical temperature is near the reservoir temperature. This appeared to be the case for the fluid studied here; therefore the pressure-volume-temperature data for this system were determined for preqentation. METHOD The PVT data were obtained with equipment similar to hat described by Weinaug and Katz,1 consisting principally of a two-section, double-windowed gauge mounted in a conktant temperature air bath. The procedure followed was essentially that used by Katz and Kurata5 except that a cathetom-eter, reading direct to 0.01 cm, was used to determine the height of each extreme phase limit. The system studied was formed by recombining -.vapor and liquid samples from the first stage separator of the well. Portions of these samples were displaced with mercury into the cell which had previously been filled with mercury. A predetermined amount of the liquid sample was introduced, while an excess of vapor was admitted. The resulting mixture was brought to equilibrium at the condition of the separator during sampling. By adding mercury to maintain the pressure, enough vapor was displaced to give a gas/oil ratio within the cell equal to that produced by the separator at the time of sampling. The remaining material was then considered to be equivalent to the reservoir fluid. An analysis of material in the cell, computed from analysis of vapor and liquid samples and the separator gas/oil ratio. is given in Table I. Table I — Composition of Hydrocarbon System Component Mole Per Cent Carbon Dioxide 0.13 Nitrogen 0.76 Methane 53.91 Ethane 14.20 Propane 9.64 Iso Butane 1.25 Normal Butane 4.29 Iso Pentane 1.12 Normal Pentane 1.87 Hexane 2.72 Heptanes + 10.11 hloleculal. Weight of Heptanes + 178.50

Jan 1, 1951

Pressure for Better Safety Practices ? Increase Government Regulation ? Safety practices evolve from: ? Increased efficiency and performance ? More knowledgeable workforce ? Focus on decreasing risk to shareholder value In Order to achieve this ? Focus Points: ? Skill Development ? Best practices ? Situation-based decision making ? Enablers: ? Adoption of new technologies ? Transformed miner education ? Delivering on-demand information to the point of work Results: Miners empowered to improve mine safety

Aug 1, 2013

By A. Kraly, M. Complojer, P. Paschen, K. Gamweger, H. Antrekowitsch

Increasing quality of aluminium alloys and continuous optimization of the production process leads to an improvement of the gas purging systems. The application of porous plugs for the treatment of liquid aluminum is nowadays not widely used in the aluminium industry especially in Europe. The Department of Nonferrous Metallurgy and the Christian Doppler Laboratory of Secondary Metallurgy of Nonferrous Metals intensified the research and development of refining and alloying processes by gas treatment during the last years. CFD-modeling supports these experiments, which should lead to lower hydrogen content, lower suspended particles and a better distribution of alloying elements in the melt. Different parameters such as temperature, bubble size, gas amount and which kind of gas is used influence the quality of the products.

Jan 1, 2006

By Reed S. C. Rogers

There is recent evidence that high frequency screening can be a viable alternative to hydrocyclone classification for a wide variety of grinding applications. However, since high frequency screening is a relatively new development, the decision to use screens generally must be based on full scale screening tests of a slurry material of interest. In this paper the authors employ mathematical simulation models as an aid to evaluating the use of screens versus hydrocyclones for closed circuit fine grinding. This approach is validated in a pilot plant study and then demonstrated for the design of full-scale grinding circuit, including classifier cost comparisons. For the case of maximum production rates versus product size, without a constraint on fine product solids densities, results indicate that screening with Derrick sandwich type cloths can give higher grinding circuit production rates with more narrowly sized products than when hydrocyclones are used. These results are explained in terms of the bypass and Sharpness Index of the respective classifier partition curves. Classifier cost comparisons for the full scale circuit show that although the installed cost of screens is substantially higher than equivalent capacity hydrocylone operations, even modest increases in circuit capacity caused by screens; can significantly reduce total grinding costs.

Jan 1, 1985

By G. C. Branner

The bauxite diagram presented as figure 1 was developed to clarify, by graphic means, the theoretical chemical constituents of gibbsite-kaolinite-type bauxite for all possible proportions of these two minerals from pure gibbsite to pure kaolinite. The tables in the report reflect the same date. The diagram provides (1) a graphic representation of the relations of constituents with respect to a ill possible percentages of alumina and silica, (2) a basis for verifying the accuracy of analyses of gibbsite-kaolinite bauxite, and (3) a basis for estimating the type and proportion of alumina hydrate and/or silicate minerals that may be present in gibbsite-kaolinite-type bauxite. The diagram, with accompanying interpretations and use formulas, will be useful to those connected with the mining and processing of bauxite.

Jan 1, 1955

By M. W. BERNEWITZ

DURING my recent extended visit to Australia and New Zealand, these notes on oil and gas prospecting in that part of the world were compiled from recent reports-press and government, from conversation with one of the financial leaders in the search for oil, and from personal observation of operations of the principal importers, blenders, and distributors of oil products; also from the astonishing testimony given by them to the Petrol Commission. Australia and New Zealand have practically no petroleum production beyond a few thousand gallons a year from wells in the latter Dominion. Everything is imported, Table 1. showing the quantities for 1929-30 in Australia and for 1930 in New Zealand,

Jan 1, 1934

By Sérgio Fernando Nunes

No presente estudo foi realizada uma investigação da influência do teor de hematita especular, percentual e granulometria da carga circulante do pelotamento nos parâmetros de qualidade física das pelotas cruas e queimadas de minério de ferro da Samarco Mineração. Preliminarmente foram executados testes exploratórios em escalas de laboratório e industrial objetivando avaliar o melhor teor de umidade, área superficial específica do pellet feed e carga circulante do pelotamento. Após essa fase exploratória, foi feito o projeto de experimentos dos ensaios de pelotamento e de queima no pot grate, empregando três fatores em dois níveis com ponto central e réplica. A resistência á compressão a úmido e a seco, diâmetro médio e bulk density, foram os parâmetros de qualidade física avaliados para as pelotas cruas. A resistência á compressão, índice de tamboramento e abrasão, porosidade e bulk density, foram os parâmetros de qualidade física avaliados para as pelotas queimadas. O atributo percentual de pelotas nucleadas queimadas também foi avaliado. Concluiu-se que a mineralogia, granulometria do pellet feed e composição da carga circulante influenciam fortemente na qualidade física das pelotas cruas e queimadas.

Aug 1, 2018

For the first time in its history the Institute will hold a meeting in the State of Arizona. A few years ago Arizona stood third in the copper-producing districts of the United States. Since that time, with the development of porphyry mines, the output has gone up with great rapidity until it not only is the leading district, but its output at the present tune is at the rate of nearly double the Montana output; which now stands second in the list. In connection with this development, most interesting departures have been made in methods of mining, concentration and smelting. Principles of mining and metallurgy of the greatest interest will be covered by papers which will appear in the Bulletin and be presented at Technical Sessions, while ample opportunity 'will ,be- afforded for those who go to the meeting to see all the points of interest to them. In addition, members will be well rewarded by the marvelous natural features to be seen on the trip, including the petrified forests, the cliff dwellings on the Apache Trail and the Grand Canyon of Arizona. It is planned to start the special train from New York, but members and guests may join the special at other points en route as indicated by the following schedule: ITINERARY Thursday; September 14th, Lv New York Grand Central Terminal 5.30 p.m. Dinner in dining car, a la carte

Jan 9, 1916

By L. C. Lien

Tower crane layout (TCL) is a typical construction site layout (CSL) problem, which is suitable for a wide range of work assignments and site conditions. Tower crane is one of the key facilities for vertical and horizontal transportation of materials, especially for heavy prefabrication units such as steel beams, ready mixed concrete, prefabricated elements and large panel formwork such as machinery and equipment, and a wide variety of other building materials within a construction site. However, it is a difficult combinatorial optimization problem to determine the locations of tower cranes with materials quantity supply and demand for engineers. Swarm intelligence (SI) was very popular and widely used in many complex optimization problems which was collective behaviour of social systems such as honey bees (bee algorithm, BA) and birds (particle swarm optimization, PSO). This study applied a hybrid swarm algorithm namely particle bee algorithm (PBA) based on a particular intelligent behaviour of honey bee and bird swarms by integrates theirs advantages. This study compares the performance of PBA with BA and PSO for a proposed hypothetical construction engineering of TCL with materials quantity supply and demand problem. Results show that PBA performs better performance than the mentioned algorithms on a proposed hypothetical TCL problem.

Aug 1, 2013

By R. W. Lawrence

A high rate biological reduction technology has been developed to provide low cost hydrogen sulphide for various uses in water treatment and metallurgical processes. Commercial operations produce sulphide safely at a fraction of the cost of chemical sulphide. The biologically produced H2S is used for treatment of acid wastewater and selective metal recovery whereby metals present in wastewater streams are recovered in high grade metal sulphide concentrates that are sold to smelters. The combination of biological H2S production and selective metal recovery is currently marketed under the process name BioSulphide-Thiopaq. The process can be applied on a stand-alone basis or in conjunction with a conventional lime water treatment. Process advantages include: reduced lime treatment costs, reduced volume of waste sludge free of toxic metals leading to reduced long term environmental liabilities, selective recovery of metals and, in some cases, net profit from water treatment achieved through the sale of metal concentrates. Three case studies are presented to provide examples water treatment and metal recovery: the Caribou Mine, New Brunswick; the Phelps Dodge Bisbee operations, Arizona; and Falconbridge?s Raglan nickel mine in Quebec. A fourth case study is presented to highlight environmental control for treatment of ARD in the Leadville mining district of Colorado. Process flowsheets, capital and operating costs are presented for the four case studies

Jan 1, 2003

By Dale A. Vaughan, Oliver M. Stewart, Charles M. Schwartz

Solid-solubility limits at 1500°, l000q and 500°C for carbon, nitrogen, and oxygen in high-purity tantalum were determined by X-ray lattice-parameter methods. For carbon, the solubility was found to be 0.17 at. pct at 1500°C, and less than 0.07 at. pct at 1000°C. A nitrogen solubility of 3.70 at. pct at 1500° C decreases linearly with temperature to 2.75 at. pct at 1000°C, and 1.8 at. pct at 500°C. In the case of oxygen, the solubility was found to be 3.65 at. pct at 1500°C, 2.95 at. pct at 1000°C, and 2.5 at. pct at 500°C. The phases Ta2C, the low-temperature modification of Ta205, and Ta,N of unknown composition but which has a superlattice structure based upon the original bcc tantalum lattice have been identified as the initial precipitates in the respective systems. Metallographic methods were employed to verify the X-ray analyses. The etching behavior of Ta is discussed in terms of lattice i?rzperfections and precipitate phases. The excellent fabricability, high melting point, and nuclear properties of tantalum are responsible for interest in this refractory metal. Data on the solid solubility of the interstitial elements (oxygen, nitrogen, and carbon) in tantalum and on the precipitate phases are somewhat limited. The significant contributions are discussed below. Because the purity of electron-beam melted tantalum (only recently available) is considerably higher than that used in previous studies, the present investigation was initiated. Gebhardt et all-3 have investigated the tantalum-oxygen and tantalum-nitrogen systems with particular reference to the changes in physical properties and to the rates of reaction between these gases and the metal. The solubility of oxygen in tantalum was reported2 to be 3.7 at. pet at 1500°, 2.3 at. pet at 100O°C, and 1.4 at. pct at 750°C. Schonberg4 reported that several oxide phases (Ta40, Ta,O, TaO and Ta,05) exist while X-ray studies by Gebhardtl showed only two oxides, Ta,05 and an unidentified phase which was associated with a platelet-type precipitate. La-gergren and Magneli,' however, questioned the existence of compounds other than the two allotropic modifications of Ta,05 for the tantalum-oxygen system. In the case of nitrogen, the solubility was estab- lished by Gebhardt3 to be of the order of 7 at. pct at 1800°c. The solubility was reported to decrease rapidly with temperature, and, although no limits were established, a precipitate phase was observed by Gebhardt except when the high-nitrogen specimens were cooled very rapidly from the reaction temperature of 1800c. He reported the initial precipitate phase to be a tetragonal distortion of the bcc tantalum lattice while Schonberg6 reported the phase lowest in nitrogen Jo be a cubic super-lattice with a cell size of 10.11 A. Two other nitride phases, Ta,N and TaN, were reported; these appear to be isomor-phous with the carbides of tantalum. The tantalum-carbon system was investigated by Ellinger7 and by Lesser and Braurer. Two compounds, Ta,C and TaC, were reported to exist, each with a range of composition. The solubility of carbon in tantalum was found to be practically nil at all temperatures. Thus, of the interstitial elements which are present in small amounts in high-purity tantalum, carbon might be expected to form precipitates. The present investigation was initiated to obtain additional data on the solid-solubility limits of these interstitials at 1500°, 1000°, and 500' with particular emphasis on the distribution and the identification of the precipitate phases. EXPERIMENTAL WORK AND RESULTS In the present investigations of the solid solubility and of the precipitate phases in the systems tantalum-nitrogen, -oxygen, and -carbon, high-purity tantalum was reacted with high-purity gases, homogenized at 1800°c, and annealed at and quenched from 1500°, 1000,

Jan 1, 1962

By S. A. Mersol, C. T. Lynch, F. W. Vahldiek

The microhardness of single crystals of tungsten disilicide has been investigated by the Knoop method. The average random room-temperature hardness of the WSi, matrix was 1350 kg per sq mm. Hardness crnisotropy was noted with respect to plane and indenter orientation as determined by single-crq.stal X-rny studies. Annealing at 1600" and 1800°C decreased the average hardness to 1310 and 1230 kg per sq tnm, respectively, and produced a second phase identified by X-ray diffraction and electron-microprobe analysis to be wSio.7. Ball-impact experiwzents produced rosettes at 850°C. Optical and electron microscopy showed evidence of slip and cross slip and twinning produced by microhardness indentations. Prismatic (100), [001] slip was found and cor~elated with hardness data. THE present study was undertaken to investigate the hardness anisotropy of as-grown and annealed single crystals of tungsten disilicide. The existence of the silicide WSiz in the W-Si system has been well-established and its structure thoroughly investigated zachariasen2 found WSi, to have a tetragonal C type of structure, similar to that of MoSi, with lattice parameters a = 3.212A, Kieffer et al. studied the W-Si system and measured the density and microhardness (at a 100-g load) of both polycrystalline WSi, and WSi,.,. The values found were 9.25 g per cu cm and 1090 kg per sq mm for WSi,, and 12.21 per cu cm and 770 kg per sq mm for WSi0.7, respectively. According to Samsonov et a1.5 the microhardness of polycrystalline WSi2 is 1430 kg per sq mm (at a 120-g load). EXPERIMENTAL The WSi, single-crystal boules investigated in this paper were grown by a Verneuil-type process using an electric arc by the Linde Division of the Union Carbide Corp.6 The largest specimens were 8 mm in diameter by 16 mm long. The crystals had an average density of 9.01 g per cu cm with a tungsten • silicon content of 99.9 wt pct. The major impurities were: 87 ppm O, 41 ppm N. 54 pprn C, 500 ppm Zr, 50 ppm Na, and 50 ppm Mn. The crystals were silicon-poor, the average silicon content being 22.20 pct (stoichiometric value is 23.40 pct), and tungsten-rich, the average tungsten content being 77.70 pct (stoichiometric value is 76.60 pct). As-received single crystals were ground and analyzed by powder X-ray diffraction technique using Cu Ka radiation. Laue and layer line rotation patterns were obtained on cleaved sections of WSi, single crystals. Electron-microprobe traverses of representative crystals were done using a Phillips-AMR electron microanalyzer. Carbon replicas were used to prepare electron micrographs. This work was done with a JEM-6A electron microscope. Prior to the metallographic examination, the specimens were mounted in Lucite and then polished for short times on polishing wheels using 9-, 3-, and 1-p diamond-grade pastes. Finally they were fine-polished with Linde A powder for 24 hr on a Syntron vibratory polisher. The samples were etched with 4H 2 O:1HF:2HNO3, which is a medium fast-acting etchant. The combination 1HF:2HNO3:5 lactic acid is also a satisfactory etchant. Annealing runs for selected specimens were made at 1600" and 1800°C for 3 hr at 1.0 to 3.0 x 10-5 mm Hg. A Brew tantalum resistance furnace with WSi2 powder for setters was used. The WSi2 powder was the same as that used for the crystal growth. Temperatures were measured with a calibrated W, W-26 pct Re thermocouple and a microoptical pyrometer. Powder X-ray diffraction, emission spectrographic, and electron-microprobe analyses were done after the annealing runs. For microhardness measurements a Tukon Microhardness Tester Type FB with a Knoop indenter was used. Although measurements were taken at loads ranging from 25 to 1000 g, the 100-g load was chosen as the standard load. All measurements were taken at room temperature. Only indentations of cracking classes 1 and 2 were considered.' DISCUSSION OF RESULTS Powder X-ray diffraction analysis showed the as-received crystals to be single-phase WSi2. Laue and layer line rotation patterns obtained on cleaved sections of WSi2 single crystals proved them to be tetragonal WS 2 2 The results also indicated that the c axis of the crystal was oriented parallel to the boule or growth axis. Electron-microprobe traverses across the matrix of the as-grown crystals showed them to be homogeneous WSi,. Optical and electron microscopy of etched crystals, however, revealed that they contained minute amounts of the "golden" and the "blue" second phases as opposed to the "white" or WSi2 phase. These two second phases were concentrated in inclusion and etch-pit

Jan 1, 1965

By Yuan Zeping

This paper describes the distribution and removal of the main impurities in the pyrometallurgical process ?at the Guixi Smelter. The paper discusses in detail our converting schedule?of3S-SB and injecting deeply a mixture ofNa2CO) and CaO flux into the converters to enhance impurity removal.

Jan 1, 1998

By R Ahola, M D. Henschel, M A. McParland

With the introduction in recent years of third-generation interferometric synthetic aperture radar (InSAR) techniques, monitoring of mine slopes, benches and surrounding areas has benefitted from increased accuracy and coverage. Fundamental research into point and distributed scattering techniques has pushed the use of InSAR to provide higher spatial and height resolution. In this paper we discuss the operationalisation of third-generation InSAR techniques and show its application to active mining operations.This paper will discuss the use of multiple independent measurements of ground movement obtained from operationally-derived InSAR products over a wide variety of deformation areas within an active open pit mining operation (ie pit slopes, dewatering depressions, tailings containment and waste dumps). A technique that shortens the time between observations (increased observation frequency) and provides ongoing estimates of measurement accuracy will be described. The methodology exploits available satellite data by using multiple satellites and multiple beams. The paper will also examine factors in the design of a mine survey with third-generation InSAR and illustrate some of the necessary engineering trade-offs to efficiently monitor a mine from space.Overall, this paper aims to demonstrate the capabilities and advantages of operational third-generation InSAR techniques for ground movement monitoring of mining operations and provide a framework for proper design of a mine InSAR survey.CITATION:Henschel, M D, Sato, S, Ahola, R and McParland, M A, 2014. Designing interferometric synthetic aperture radar surveys for mine monitoring with accuracy assessment, in Proceedings AusRock 2014: Third Australasian Ground Control in Mining Conference , pp 233–238 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Nov 5, 2014

By J. Loredo

In some rural regions of Peru, artisanal gold mining is currently an essential activity as it provides an important source of income. In the Huanca region (Ayacucho Department) gold deposits are not attractive for mining companies due to their reduced size, but they have enough interest for artisanal mining because of the ease and low cost of mining operations. Artisanal gold mining represents an important damage for the environment, because operations related to amalgamation processes using Hg result in special environmental problems besides the typical ones commonly associated to all mining activities. A preliminary sampling has been made in soils, materials from tailing ponds and surface water of the Acarí River, at the site of the Huanca village, according to networks specially designed for the particular conditions of the area. Studies accomplished revealed high mercury concentrations in soils and tailings. Chemical analyses of soils directly collected in the area of the active or abandoned ?quimbaletes? show mercury concentrations ranging from 15.3 mg?kg-1 to 44.2 mg.kg-1. Mercury concentrations in soils decrease as a function of distance from the before mentioned sources. Water quality of the Acarí River that flows through the area does not present important changes as a consequence of the mining and processing operations.

Jan 1, 2006

By José Carlos Abreu

This work presents a kinetics study covering the effects of temperature over the reduction rates of a carbon composite briquette, aiming its use as burden in some of the new alternate ironmaking technologies, such as the Tecnored process. It is reported that increases in the temperature increases the reaction rate. Additionally, the morphology of the iron phase generated during the reduction of these briquettes is presented. It was possible to verify that three types of iron morphology occurred during the process: an external, dense and continuous iron layer, the presence of iron globules at the center of the briquettes and whiskers at the briquette's core. The measurement of the carbon content on the globules and the external iron layer is also presented.

Jan 1, 2003

By N. Naudé

The theory on particles displacement subjected to upwards and settling movements in water, using a water pulse, is described in literature, but very little experimental data is available to verify these theoretical ideas. The aim of this research work was to visualize the displacement of solid particles in a mixture of water and solid particles created with the aid of water pulses in the Mineral Density Separator. From the literature it is known that lighter particles are subjected to higher levels of displacement than heavier particles, and when the particles then settled down, layers of material are formed ac-cording to the densities of the material. By removing the individual material layers, the materials can then be separated according to their densities. During this study the individual material layers were investigated regarding the density and size distribution in that specific density layer. It is important for this project to have a statistical prediction of the ?real? flow of the particles with different density and size distribution, inside the Mineral Density Separator. The information gathered during this study will be used to show the correlation between a two dimensional model of the particle flow and that of the real three dimensional flow inside the Mineral Density Separator.

Jan 1, 2014

By Richard DePew, Robert J. Auber

The Westerly Storage Tunnel is a 25-foot diameter segmentally lined storage tunnel that is a major component of the Northeast Ohio Regional Sewer District's Project Clean Lake that is designed to capture 39 million gallons of untreated CSO overflows from entering Lake Erie. During the final stages of the project completion, a large-scale rock fallout incident occurred during the final lining installation operations at the down-stream end of the tunnel that extended beyond the designed primary support system. This paper outlines the level of coordination and collaboration between the Owner, Designer and Contractor to remediate the situation safely, quickly and effectively.

Jun 23, 2024

By M. Schwartz

Mining in Argentina is diverse in terms of the number of minerals extracted from the country, but also in terms of the varied approaches and attitudes of mining investors and their trust in the country's individual provinces. Laws are discussed, investment attractiveness and taxation.

Jun 1, 2015

By E. J. Wasp, T. L. Thompson, T. C. Aude

The paper will deal with some of the more important technical aspects of slurry pipelines as they apply to the mineral field. In addition, the use of these technical concepts in arriving at realistic economic figures will be discussed.

Jan 1, 1970