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By P. R. Perry

This publication is a compilation of tested methods for the analyses of titanium tetrachloride, titanium sponge, and various intermediate materials and products. They are presented in concise form without the detail usually found in publication of new methods because many of them are modifications of well known procedures. The Electrometallurgical Experiment Station, Boulder City, Nev., has been developing titanium production methods since 1945. Most of this development was on a modified Kroll Process but also included work on sodium reduction and electrolytic methods. During these years a large variety of samples were analyzed. Most of the analytical problems were solved using published methods or modifications of the same. At the start, there were no published procedures for analyzing titanium sponge using spectrochemical methods. A great deal of study was given to testing several of the well known techniques, and some of them, such as direct sparking of the metal, proved to be completely unsatisfactory. Solution-spark techniques were finally tried, and satisfactory procedures were developed for some of the more common impurities. These spectrochemical methods were then put into routine use for several months before their publication.2/ Some new modifications have been made, and techniques have been developed to determine other impurities found in titanium sponge and tetrachloride. All spectrochemical methods used in 1954 are included in this publication.

Jan 1, 1955

Approximately half of all the fuel energy used in the United states is now pro-vided by oil and natural gas. A persistent and rapid growth in energy demand during the last 3 decades has been absorbed largely by the liquid and gaseous rather than solid fuels. In 1948 the energy provided by coal was substantially the same as in 1920. Meanwhile, the use of oil and natural gas each had increased fivefold. On a per capita basis, the change is more significant. Coal consumption has dropped from about 6 tons per person to 4-1/2 tons, while oil has increased from 4-1/3 barrels to 14-1/3, and natural gas from 7,500 cubic feet to about 35,000. These facts would have only academic interest if the United States had unlimited supplies of all fuels. However, while the Nation's reserves of coal are adequate to meet our needs for centuries, those of oil and natural gas appear limited. It is obvious, therefore, that the security of our liquid-fuel position would be greatly enhanced if the supply could be based in an increasing degree on solid fuels, such as coal and oil shale, which make up more than 95 percent of our fuel reserves, instead of natural oil and gas. In addition, this would create new employment and help to stabilize the market for coal, which may be facing comparatively bleak prospects in the near future unless its position with respect to other fuels is improved.

Jan 1, 1950

By Alfred Bellows

The objective of this contract is to design, build and demonstrate a support system to improve roof control in the entries of longwall mines. The objective of this phase has been the detailed design of such a system and the selection of a test site in which to perform the pilot demonstration. The result is a complete set of detail drawings or specifications which define the three major components of the system. The Gate Support is a variation of a face chock which has an extended canopy and additional hydraulic legs to protect the region of the face-entry intersection. The Entry Support is a steel beam and hydraulic prop set which is reusable and serves to support the first 100 or more feet of entry inby the longwall face. The Transporter is a bolter-like vehicle with a crane used for installing and retreating the beam sets. The test site selected is CF&I's Allen Mine in Colorado. They presently use simi¬lar steel beams and expect the FMA support system to be more effective as well as recoverable. It is recommended that the completed drawings be used to build a prototype system and test it first in a remote section of the mine and then in the active longwall tail entry.

Jan 1, 1978

By William K. Cunningham

The investigation described in this report was begun as part of the Bureau of Mines progress to develop acid processes for the extraction of alumina from low-grade bauxite and. clays. A domestic shortage of high-grade bauxite sui table for treatment by the Bayer process became acute as a result of' World War II; an intensive search for a practical acid process using lower-grade alumina-bearing raw materials was therefore warranted. The laboratory development was described in a preceding Bureau of Mines publication wherein the basic theory for the design and erection of a pilot plant maybe found. A 2-ton-per-day continuous pilot plant was constructed and successfully operated at College Park, Md., which demonstrated conclusively the chemical and mechanical feasibility of a solvent purification process for aluminum sulfate. The estimated production cost of $38.64 indicates that under present market conditions the process would not be economically feasible.

Jan 1, 1948

By David S. Brown

What troubles me so often about debates over the environment, which I have heard since I entered government in the late 1960's, is that the issues are so often presented as a false dilemma--the either-or fallacy in logic. The either-or fallacy allows only two possible choices: Either protect the environment or exploit it. In reality, however, there may be a few more options. The diverse, often competing, values that the Earth offers require us to weigh and balance those options through a range of policy options. A quality environment and economic growth and opportunity are not mutually exclusive. First, let me acknowledge that I support a set of resource values recognized in U.S. laws and deemed important down through history for the success of free, progressive, and secure societies: the importance of access to raw materials. Increasingly, however, mineral raw materials have been viewed at best as not particularly relevant to a sophisticated, technologic society, and at worst monstrously destructive of our natural environment. Both perceptions, in my judgment, are wrong.

Jan 1, 1989

By Flavelle IV

A survey is made of changes in the technical status of a number of western world copper extraction and refining operations over the past 20 years. Specific developments in pyro- and hydro-metallurgy and refining practices are identified together with factors in the changing environment of the industry which has influenced their adoption. Nickel extraction and refining is similarly discussed.The replacement of traditional technology by more attractive alternatives has occurred in a considerable number of operations. The develop-ment and status of new continuous smelting processes, advances in hydrometallurgy and refining innovations which emerged during the 1960s and early 1970s is discussed. The varying experience in commercial acceptance of these new technologies is noted.Finally some possible future directions are canvassed for both operators and the research and development institutions.

Jan 1, 1985

By Kristian E. Waters, Hao Ma, Haibei Wang

Over the past few decades, ELM based separation processes have become an attractive and efficient way to remove toxic metal ions from the various aqueous waste effluent streams. This paper provides a comprehensive review of the generation, characterization, and applications of emulsion liquid membrane (ELM) from the more than 280 papers and books published so far. First, the ELM formation and the transport mechanism are introduced. Then the ELM stability and emulsion splitting methods are discussed in detail, followed by the latest research and findings of the extraction of copper and nickel using the ELM technique during the past few decades, including a thorough discussion of ELM operating parameters that impact ELM stability and extraction. In addition, the kinetics study and industrial application of this technique for the removal of coppers/nickel solutes are also presented and discussed.

Jan 6, 2023

By C. H. Schack

Extractive metallurgy techniques currently employed to recover silver from primary ores and secondary scrap were reviewed and evaluated to identify and delineate metallurgical problems whose resolution would increase the supply of silver from domestic materials. The survey revealed that practically all primary silver is recovered by froth flotation concentration of various types of ores, followed by smelting and refining of the separate lead, copper, and zinc concentrates. Silver losses during the complex processing are, with rare exception, inconsequential. Furthermore, any silver production gain from base metal ores, which contribute about two-thirds of the total primary silver, is directly dependent in improvement in the market for the base metals. Statistical data on new and old silver scrap are wholly inadequate to make reliable conclusions about scrap processing problems and the possibility of increasing the recovery of silver from the many forms of secondary silver- bearing materials. The available information indicates (1) that efficient silver reclamation practices are employed by the larger users of silver, and (2) that recovery of additional secondary silver involves solution of problems of collection rather than of processing. Several possibilities exist for limited increases in silver production from primary ores by improvement in metallurgical practices. Specifically, research is needed to (1) solve the problem of recovering silver from the copper ores of the Copper Range district, Michigan; and (2) devise economically feasible methods for recovery of silver from presently marginal or submarginal ores that because of grade, location, and frequently complex nature cannot presently be exploited by conventional techniques.

Jan 1, 1965

By V. Bredykhin

The efficiency of scrap processing depends firstly on reliability of information about its chemical composition. The paper presents the results of the investigation and development regarding solid copper alloy scrap in the range of lump size 40÷300 mm. Nowadays the sorting of lump scrap is done by two methods: 1. Sorting according to metals and alloys is done at places of scrap generation, and further till metallurgical processing each lot has its "certificate"; 2. Hand sorting of scrap is done according to the marks on solid items in special shops using proximate analyzers or manually by experienced workers. This sorting process is labor - consuming low efficient and involves mistakes. The informational method is a promising trend in the copper scrap sorting. The method is direct, i.e. as a result of sorting the chemical composition of each scrap lump or main elements is determined, and assured data of qualitative and quantitative composition are received.

Jan 1, 2006

By A. Yousefpour, M. Hojjati, M. Simard, M. Laramée, M-A. Octeau

The need for effective and reliable joining methods grows as the use of advanced thermoplastic composites becomes widespread in aerospace industry. An experimental investigation of resistance welding of APC-2/AS4 thermoplastic composite laminates is presented. In this method, a heating element is placed between the bond-surfaces then the interface is heated by passing electrical current through the heating element. The polymer at the weld interface is melted due to resistance heating, then diffuses and consolidates under applied pressure, resulting in a weld. APC-2/AS4 prepreg, APC-2/AS4 commingled, and different grades of metal mesh heating elements were considered. A custom made resistance welding rig was designed and developed to perform lap-shear welds. The mechanical performance of the welds was quantified using single lap shear tests. The effects of different heating elements on the mechanical performance of the resistance-welded parts were investigated. Also, quality of the welds was examined under optical microscopy.

Jan 1, 2004

By H Leonard Mangum, Victor C. Bryan, Dan McCutchen

Recently there has been an unprecedented marketing effort to promote the advantages of various non-electric initiation systems. This activity has probably been influenced by a major manufacturer's decision to discontinue electric detonator production. Subsequently, distributors of explosive materials, rather than introducing new electric detonator brands, are emphasizing the use of existing non-electric systems. In many cases, such methods fill the need of explosive users in the quarry industry. However, the use of any initiation system should be based on performance, rather than the bent of the market or convenience to the supplier. This analysis is an evaluation of the performance of non-electric systems with emphasis on double trunk line and loop (redundant), as compared to precise electric detonators in use by Martin Marietta. Redundant non-electric detonators, even though more costly, offer the most reliable method of non-electric initiation. However, state-of-the-art precise electric detonators give the best overall performance, except in an environment involving extraneous electricity.

Jan 1, 1990

By P. J. Tarkoy

To successfully bid a tunneling contract by machine, a contractor must have a reliable estimate of expected penetration rates and cutter costs. Preferably, these predictions should be independent of those supplied by machine and cutter manufacturers. Therefore, a series of rock index tests have been developed and incorporated in routine Rock Mechanics testing for the purpose of predicting rock boreability. Index properties were evaluated empirically by using rock samples and pertinent construction records from recently machined tunnels. Samples were taken from the completed tunnel walls, tested parallel to machine penetration, and results were compared to localized rates of penetration. Indices are based on two measures of rebound hardness and two measures of abrasive properties. The Shore (C-2 type) Scleroscope and Schmidt (L-type) Hammer were utilized to measure rebound hardness and a Taber Abraser was modified to measure rock abrasiveness and abradeability. Results indicate that rock hardness index properties investigated in this study can be used successfully to predict TBM penetration rates.

Jan 1, 1974

The data about production in this county are exceedingly meager, and there are few reliable data about shipments. It is probable that consid¬erable amounts of coal from here moved north to Erie by both the Beaver and Erie. Canal and the Erie and Pittsburgh Railroad, and if so, they are included with Mercer County. The data in the early state reports are very inaccurate and are always much too low. Much of this coal was used in local furnaces and iron plants and not handled by railroads. There was some production in this county on the line of the Pittsburgh, Fort Wayne and Chicago Railroad, of which no record can be found. The estimated production is based on the number of mines reported as operating in the county at various dates and their probable output, as suggested occasionally in county histories. It is believed that these figures are below, rather than above, the actual figures, which can now never be obtained.

Jan 1, 1942

By Anne Lemnitzer

Experimental data are the cornerstone of scientific research, providing empirical evidence to validate hypotheses, test theories, inform decision-making and help develop innovative design and analysis methods. However, beyond traditional empirical validations, experimental data have also become the most crucial component of AI algorithms, measuring the algorithms' effectiveness, and allowing engineers to ensure their reliability and applicability. The DFI "Rock Socket Project," awarded in the spring of 2018 allowed for the indispensable, experimental data-based validation of structural shear magnitudes, which have been hypothesized and discussed for years within the deep foundations community and cautiously approached by many design engineers. The fundamental project idea, i.e., the investi- gation of pile shear magnitudes through experimental research, was sparked during a heated discussion in the October 2016 Drilled Shaft Committee meeting in New York. Should we design for amplified shear at the rock socket of a drilled shaft or is this merely an artifact of the p-y design approach? Data were needed to provide consensus.

Nov 1, 2023

Australia had been enjoying a market boom led by the mining sector and West Australian mines were leading the way to satisfy the massive demand for our natural resources, especially from China. However, the Apache gas explosion on Varanus Island, 97 km off the west coast, has clearly demonstrated how the unexpected can suddenly impact on profitability and investor confidence for the mining industry. Risk management with contingency planning can provide the most cost-effective solution to help ensure mining projects are successful. For this discussion we will focus primarily on contingency planning, CP for mining projects à and how to plan for the unexpected. The Apache gas explosion will be our example æUnexpected EventÆ. Insurance may provide financial compensation but it will not protect your reputation as a reliable supplier or prevent damage to investor confidence and future mine projects. However, contingency planning can provide real protection for mining projects à to survive the unexpected.

Jan 1, 2009

(Under this heading will be published notes sent to the Secretary of the Institute by members or other persons introduced by members.) Member, graduate Columbia School of Mines, age 35, married, best of health, dependable, desires position as manager or scout for reliable interests. Experience covers responsible positions incident to the mining and milling of gold-silver, copper, lead, and zinc ores, and the examination of base and rare-metal deposits in United States and Mexico. Salary $3600. Available April 1. No. 453. Member, mining engineer, technical training, age 32, assayer, engineer and superintendent of porphyry copper development, churn drilling and shaft sinking. Examination of prospects and development of gold prospects. Considerable flotation experience. No. 454. Young Columbia graduate, conscientious worker, with experience in inorganic analysis, surveying, draughting, and wit. post-graduate training in geology, desires position wt. prospects. Minimum salary considered, $130 in U. S. and $150 in Mexico. At present employed. Draft exempt. No. 455.

Jan 5, 1918

In-seam drilling is conducted mainly to drain coal of gas and/or water prior to development or extraction. The requirements of inseam drilling for gas drainage have mainly surpassed the technical limits of rotary drilling and are mainly being addressed by guided down hole motor drilling, albeit at a higher cost. There is an increasing application of in-seam drilling to detect geological structures or other hazards or their absence in advance of mining to reduce the risks of underground mining. Close collaboration between miners, drillers, geologists, researchers and suppliers over the last four years has seen many advances made to improve the accuracy and reliability of inseam drilling. With such developments will come closer control over the ventilation and safety of future mining under deep gassy conditions, but not without costs. The paper summarises the current applications of inseam drilling, recent technological advances and the next generation survey and geophysical sensing tools which are currently being developed

Jan 1, 1998

By Siemag Transplan GmbH

At the Hansa Mine in Dortmund, Germany, coarse run-of-mine coal, up to 60 mm in particle size, has been brought to the surface hydraulically from a depth of 850 m since November 1977. Hoisting is done by a three-chamber pipefeeder, by means of which up to 400 t/h can be lifted. The pipefeeder operates without problems, and has so far shown itself to be efficient and reliable. Vertical hoisting can be carried out by water supplied from the surface, from underground, or from a surface water supply in combination with minewater from underground. Water that flows into the mine, which would in any event have to be pumped to the surface, can be utilized for hoisting operations. The energy costs per ton of coal for a lifting height of 850 m vary between 41 and 62 South African cents, and therefore lie within the range of costs that apply to conventional hoisting.

Jan 1, 1980

ENGINEERS AVAILABLE (Under this heading will be published notes sent to the Secretary of the Institute by members or other persons introduced by members.) Member, technical graduate, five years' experience as mining engineer and chemist. Actual experience in underground work, surveying, mapping, foreman, etc. Will accept very moderate salary to start with reliable company. Willing to go anywhere. No. 184. Member, technical graduate, with experience as engineer and metallurgist for various copper companies, is open for similar positions. No. 185. Member, specializing in cyanide treatment and cyanide plant construction, with 10 years' experience in Mexico and in the West, desires position. No. 186. Member, technical graduate, first in mining engineering and then in chemistry and metallurgy, Lafayette College; Fellow, School of Mines, Columbia University; special work Royal School of Mines, Freiberg, Saxony, Germany; ten years' experience teaching mining, chemistry, assaying, and metallurgy, desires position as Director of School of Mines or Professor of Metallurgy. No. 187.

Jan 2, 1915

By A R. Butcher

Gold deportment and ore characterisation studies are key tools in gaining an appropriate understanding of complex gold ores for process development and optimisation. These studies have historically involved imprecise chemical methods with slow and costly optical microscopy for gold identification. The traditional approach requires highly skilled petrographers, is prone to human error, and is not scalable, reducing the usefulness in practical analysis. The proposed methodology utilises a decision tree and knowledge base in a staged approach to gold ore characterisation, building up progressively more detailed information about the sample mineralogy, gold deportment and key mineral properties, as the process is followed. Whilst the automated QEMSCAN« system is used for mineral and gold identification, interactive and focused data analyses are used to give more efficient and accurate results. This is complemented by smart sample preparation and chemical methods to enhance and validate the data, making the staged approach methodology reliable, scalable and therefore practical and economical.

Jan 1, 2007