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By C. G. Dunn

Nuclei that are formed during the recrystallization of a grain following plastic deformation generally have orientations that differ from the original. This aspect of recrystallization may be described in terms of orientation changes. It was shown previously, in an investigation on recrystallization in silicon ferrite,&apos; that the observed orientation changes were highly improbable on a chance basis, and that some mechanism must be involved. Analysis showed that the data could be satisfactorily classified into the smaller of two subclasses† of the 36 third-order twin transformations. No attempt was made at that time to classify the data within the special class of 12 third-order twin transformations, although results did indicate a greater probability for some of them to occur. A classification of this type would be more valuable, of course, with more data on orientation changes per old deformed grain. The present work fulfills this condition to some degree and also extends the scope of the investigation to include the effects of original orientation and the amount of plastic deformation. The effect of original orientation is of considerable interest because of the known effects of orientation on plastic deformation, particularly with regard to degree of fragmentation and the formation of deformation bands, and because the orientations produced by deformation should influence the orientations obtained through recrystallization. Barrett and Levenson2 reported that single crystals of iron deformed in the range 82 to 97 per cent could be put into three general classes; namely, crystals in class I maintained a reasonably sharp single orientation, those in class 2 transformed into two distinct orientations, and those in class 3 changed into a large number of major and minor orientations. Something similar would be expected for silicon ferrite crystals, and verification of this for a few cases of types class I and class 2 deformation has been reported elsewhere3 for single crystals of silicon ferrite cold-rolled in the range 10 to 20 per cent. As an example of class 2 deformation, it was shown that a crystal of silicon ferrite cold-rolled in a (110) plane in a <100> direction developed two layers, or deformation bands differing in orientation. When this happens it is possible to etch away one band and leave a single structure for use in studying the orientation changes that occur during recrystallization. when preferred crystal orientations are obtained in recrystallization, it is not particularly necessary to evaluate groups of common orientation, as was done previously (ref. I, Table 6); but an

Jan 1, 1947

By Daojin Cao

The chemical components in the saturated aqueous solution of ammonium dimolybdate (ADM) were investigated at room temperature by comparative Raman spectroscopy. In order to explore the further detailed results, a new method of qualitative and half quantitative analyses, based on the main vibrant frequencies and the intensity ratio of the strongest peak to the second strongest peak recorded in Raman spectrum of saturated aqueous solution of ammonium heptamolybdate tetra hydrate (AHM), was put forward and attempted to analyze the chemical components of saturated aqueous solution of ADM. The results showed that there was obvious difference between Raman spectrum of saturated aqueous solution of ADM and that of ADM, but there were good relationships between Raman spectrum of saturated aqueous solution of ADM and Raman spectra of the three samples including AHM, the saturated aqueous solution of AHM and monomolybdate ion in aqueous solution. It was found that aggregated dimolybdate ion ({Mo2O72-}n)did not exist in the saturated aqueous solution, and was changed into heptamolybdate ion (Mo7O246-) and monomolybdate ion (MoO42-), which were in equilibrium each other, but the distribution ratio of heptamolybdate ion was larger than that of monomolybdate ion. In addition, Raman spectral pattern of saturated aqueous solution of ADM was reported.

Jan 1, 2006

The Fortieth Regular Meeting of the Rocky Mountain Coal Mining Institute was called to order in the Hotel Utah, Salt Lake City, Utah, Wednesday, June 10, 1942, at 11:30 a.m., by President, Wetzel, who presented Mr. William A. Fealey who, in turn, introduced Mr. Bracken Lee, Mayor of Price, Utah, who made the address of welcome. President Wetzel then made a few remarks. The Secretary announced with regret that, due to the critical illness of Mr. Sidney Hale, he would be unable to at- tend the meeting. On motion of Charles M. Schloss, duly seconded and carried, the reading of the minutes of the Thirty-ninth Regular Meeting was dispensed with. Mr. Schloss also moved that the Chair appoint the usual committees, which motion was seconded and carried. President Wetzel then announced that the committees would be appointed during the afternoon session. Following routine announcements, the meeting recessed at 12 o&apos;clock noon to reconvene at 1:30 p.m.

Jan 1, 1942

By William G. Gruzenaky

The separation of yttrium and the individual rare-earth elements (lanthanons) from mixtures in which they occur has been a difficult problem through-out the years. Because of the increased interest in the various uses of these metals, the economy of their production may become of great importance. Studies relative to this problem, undertaken at the Federal Bureau of Mines Albany Metallurgy Research Center, resulted in the development of a solvent extraction method by which yttrium can be separated from the rare-earth metals. A separation factor of 10.93 was obtained between yttrium and cerium from a single-stage extraction, and a factor of 1.78 was obtained between yttrium and erbium from a multistage system. The valuable metals were extracted from euxenite by caustic soda fusion or by chlorination, and several separation methods were investigated. Partial separation of the yttrium and rare-earth element fraction was made by chemical methods and by solvent extraction. Thermal decomposition of aqueous rare-earth nitrates or selective ignition of yttrium and rare-earth oxalates yielded a fraction enriched in cerium. A fraction enriched in the light rare-earth elements resulted from a double sulfate precipitation, whereas a potassium ferrocyanide pr cipitation yielded a fraction enriched in yttrium. Precipitation with dimethyl phosphate yielded a fraction enriched in yttrium and heavy rare-earth elements. Enriched fractions were obtained with several solvent extraction systems. A system consisting of rare-earth nitrates, nitric acid, and tri-n-butylamine-3 methyl-2-butanone favored the separation of yttrium from the heavy as well as from the light rare-earth elements.

Jan 1, 1961

By N. Brown, J. Washburn, E. R. Parker

MOST previous quantitative work on creep of single crystals has been concerned primarily with developing empirical equations for the creep curve. Although the equations used by Cottrell and Aytekin¹ and Tyndall² represented the data quite well, it was often necessary to use different values of the constants for different specimens even though they were apparently tested under identical conditions. In the course of previous work on the effect of surface coatings on creep of zinc single crystals," it was found that equal resolved shear stress frequently did not produce equal creep rates in different specimens. The work of Chalmers&apos; in the very

Jan 1, 1954

By Shulin Nie

The detonability of a chemically gassed emulsion explosive has been studied in recent tests, after the study of three micro-balloon sensitized emulsion explosives. Blasting experiments in steel pipes and computer simulation have been carried out. This study showed that the gassed emulsion explosive and the micro-balloon sensitized emulsion explosives have different desensitization features. Namely, the gassed emulsion explosive can recover its detonability very rapidly after the pressure vanishes, in contrary to the micro-balloon sensitized explosives.

Jan 1, 1997

Prior to 1972, Peko Mines Limited at Tennant Creek used a central mill at Peko, which consisted of a gravity circuit, flotation and cyanidation of tailings, to treat their gold ore from surrounding mines. The Warrego concentrator, 60km to the west, was built to handle the Warrego and Gecko copper orebodies, which were being developed concurrently with the concentrator construction The Warrego concentrator consisted of a flotation circuit, using autogenous grinding at 100 - 120 tph, compared to the more elaborate Peko circuit employing rod mill - ball mill grinding capable of treating only 18 - 26 tph. During development of the Warrego copper mine a gold rich ore pod was located, because of which the mining plans were adjusted to allow simultaneous, separate extraction of the copper and gold ores. However, the plans for the concentrator were not affected as the gold ore could be carted 60km to the Peko central mill for processing.

Jan 1, 1978

By N. B. Devi

The extraction of Cu(II) from HCl media using Cyanex 923 in kerosene was investigated. The effect of shaking time, aqueous phase acid concentration, extractant concentration, chloride ion concentration, various metal ions (Mn2+, Mg2+, Fe2+, and Ni2+), and temperature on the extraction were studied. Using 0.1 M Cyanex 923 the extraction of Cu(II) was 6.7 per cent from 3 M HCl, which increased up to 78.5 per cent with 6.5 M HCl and then decreased due to acid extraction by the extractant. The maximum extraction (97.5 per cent) was obtained with 1 M Cyanex 923 from 5 M HCl solution. A mathematical model has been developed to describe solvent extraction equllibria over wide ranges of concentration of extractant, acid, and chloride ions. The composition of the extracted species has been predicted on the basis of slope analysis results and extraction equilibrium modelling. The negative values of enthalpy change and entropy change confirm the exothermic formation of the extracted complex.

Jan 1, 2012

The genesis of the Bulong Laterite Ni/Co deposit spans some 60 per cent of earth history: from development of the parent rocks in the Archaean to lateritic weathering in the Cainozoic. In a man&apos;s term, the discovery and evaluation history of the deposits has also been protracted and, at any given time, the perceived value of the deposits has depended upon the available technology and world markets.

Jan 1, 1996

By John Kosek

The electrochemistry of carbon monoxide, nitric oxide and nitrogen dioxide was investigated at a variety of electrode materials in different supporting electrolytes. A portable detector for carbon monoxide was developed using a porous gold anode in perchloric acid supporting electrolyte. This detector has two full scale ranges, 0-100 ppm and 0-500 ppm. A portable detector for mixtures of nitric oxide and nitrogen dioxide was developed using a porous silver cathode in sulfuric acid supporting electrolyte. Nitrogen dioxide was determined in the gas stream by electroreduction. The nitric oxide in the gas stream was oxidized to nitrogen dioxide by passing it over Cr(VI) on firebrick. Electroreduction gave the sum of NO + N02. Analog circuitry was used to display the amounts of NO and N02 separately. Two ranges were available for each gas. They were 0-10 and 0-50 ppm for NO and 0-2 and 0-10 ppm for N02.

Jan 1, 1979

By Frank E. Chase

Sacrificial entries, roof slotting, and other tactics have been used to combat high horizontal stresses during roadway development in U.S. coal mines. In Australia, the "pillar extraction on the advance" mining method has been successfully employed as a horizontal stress control technique. The concept of advancing and relieving mine workings through pillar extraction developed from observations that some mines experience difficult ground conditions when advancing and retreating the first panel in a new reserve. However, conditions dramatically improve in subsequent panels. Apparently, the creation of a gob area stress relieves the adjacent panel workings. After much debate and close scrutiny, the first U.S. roof control plan to advance and relieve was approved in 1998, for the Sargent Hollow Mine in Wise County, VA. The major concern was that this mining practice places section personnel inby of the gob. The tentative approval permitted barrier pillar slabbing and removal of the adjacent development pillar during panel development. The intent of the plan was to provide a "stress shadow" for the advancing faces and outby workings to reduce the excessive number of roof falls. Sargent Hollow successfully extracted their first panel by pillaring on advance and retreat mining using posts. Mobile roof supports were employed to extract pillars while advancing the second panel. This paper summarizes Sargent Hollow Mine&apos;s experiences with the advance and relieve mining method.

Jan 1, 1999

By Conny Postupack, Jim Petrunyak, John Hope

The authors discuss the concepts, engineering considerations, and cost relationships involved in the use of drilling and blasting to accomplish backfilling and reclamation with minimum use of mechanical equipment. The four xchods o f reclsnacisn now in use are reviewed, and their advantages and disadvanrages a r e nocea. Guidelines for seleccrng a particular method are offered in terms of applicability under varying geologic, economic, and technological condirions.

Jan 1, 1989

By Ali Bouafia

Five full-scale horizontal loading tests of piles carried out by the LCPC in France are interpreted in order to analyse P-Y load-transfer curves. The experimental piles are either bored or jacked into quite homogenous sandy soils and instrumented by strain gauges for measuring bending moments along the pile. Successive differentiation and integration of bending moment profiles have led to derive respectively lateral soil reaction and displacements then to construct the load-transfer P-Y curves. The initial horizontal lateral reaction modulus was derived from these curves and shows linear variation with depth in accordance with Gibson soils profiles. P-Y curves are validated by back-computation of the pile on the basis de these curves and the horizontal reaction modulus was compared to the recommendations frequently used in pile design practice.

Jan 1, 2002

By E. A. H. Tays

As I promised, in a former paper on the Bryan Mill,* to give further data regarding the plates from four battery-aprons, I now submit the following: These aprons were 4.5 feet wide by 16 feet long; the first two plates of each apron were 4.5 by 4.5 feet, and the remainder of varying sizes, as can be seen by their relative weights, as shown in the table; but all were 54 inches wide. They were in use 4 years and 9 months, and about 15,265 tons of ore passed over each. The ore was quartz, carrying about the same weight in silver as in gold; showing some copper, and highly impregnated with ferric oxide. The tailings show about 0.6 per cent., and the bullion about 10 per cent., of copper. The silver was present mostly as sulphide; and the copper was also present as sulphide, with some carbonate. The ore treated ill 1898 was a fair average of the whole run; so I take it as an example from which to make a few deductions.

Jan 1, 1901

The underwater test method for the determination of energy content of explosives is a very useful method. It’s also the only one which can separate shock and gas heave energies from each other. The total energy can be determined as a sum of these partial energies. Because of this special feature, the test method can be used to develop the energy content of explosives for different purposes; the military high explosives should contain more shock energy whereas the gas heave energy is a very important feature for the blasting explosives. The goal of this study was to find out the effects of aluminium and sodium perchlorate increments to the shock, gas heave and total energy values of an emulsion explosive and detect the particle size effects of two different aluminium powders to the total and partial energies as well. Both partial energies as well as the total energy were observed to increase linearly as a function of aluminium (A-80) concentration. The fine aluminium powder (A-100) (6%) also seemed to increase the shock energy of the explosive slightly whereas the gas heave energy was observed to remain unchanged to compared to the normally aluminazed (A-80) (6%) emulsion explosive. Therefore the fine aluminium powder also increased the total energy, but only very silightly. The fine aluminium powder can probably take apart to the chemical reactions more easily during the detonation. (3%) of sodium perchlorate (NaClO4) mixed with (6%) of (A-80) aluminium powdered emulsion explosive was observed to effect to the gas heave energy content of the explosive, but only very slightly. The shock energy was observed to remain unchanged.

Jan 1, 2005

The meeting of the Institute of Metals Division was held in Phila-delphia from Sept. 30 to Oct. 2, inclusive. On Monday evening preceding the meeting, a dinner was held at the Ritz-Carlton Hotel at which many of the former officers of the Division and of the present officers and execu-tive committee were present. The subject of a membership committee was discussed and a motion to appoint such a committee with powers to go over the membership list for the selection of divisional members and to institute plans for additional members was passed. Mr. H. E. Howe and Dr. Johnston of the National Research Council attended the meeting and presented their plans for an Alloys Research Association. Many opinions were voiced as to the practicability of such a scheme and Mr. Howe expressed himself in appreciation of the cooperative thought and efforts given him. On Tuesday morning the Institute of Metals Division joined sessions with the American Foundrymen&apos;s Association and listened to the opening addresses. In the afternoon a boat ride was taken on the Delaware River, visiting the plants of the Cramp Ship and Engine Building Co. and the shipyard of the Emergency Fleet Corpn. at Hog Island. The launching of the boat christened "Afoundria" at 5 p.m. was witnessed by members of the party. The opening technical session was held on Tuesday evening at the Ritz-Carlton Hotel at 8 o&apos;clock. The next session was held at the Ritz-Carlton at 10 o&apos;clock on Wednesday morning and the final session at the same time and place on Thursday morning. The sessions were well attended and the discussion was good. The highly technical nature of some of the papers on the program was of special note. Taken as a whole the meeting was one of the most successful ever held. The follow-ing papers were presented:

Jan 11, 1919

By Robert Marchand

_ North-western Quebec _ Bousquet mining district _ 21 M oz mining camp _ 100,000 t/yr (400 t/d) _ Shrinkage : 52 % _ Longhole : 40% _ Development : 8% _ 5 days/week _ 120 employees _Discovered in 1936. _12 changes of ownership. _Exploration & development : 1987 _Commercial production : 1990 _Shaft deepening : 1995 _Internal shaft : 1999

Oct 1, 2001

By Dennis A. Beiter, Kenneth G. Fields, Richard T. Stoltz

Section 56.5001 Title 30, [Code of Federal Regulations1], establishes requirements for respirable dust exposure in Metal and Nonmetal Mines based on the Threshold Limit Values (TLV&apos;s) adopted by the American Conference of Governmental Industrial Hygienists. Respirable dust samples collected by Mine Safety and Health Administration (MSHA) inspectors at a sandstone quarry showed certain workers were exposed to excessive concentrations during development of a "coyote tunnel" that was ventilated with a blowing system. Because exhausting face ventilation systems are known to control dust more effectively than blowing face systems, a change was proposed to improve worker respirable dust exposures. This paper describes the evaluation of the proposed exhausting ventilation system in the quarry&apos;s "coyote tunnel" and compares the respirable dust exposures with those measured by the MSHA inspectors with the blowing system. Results showed the proposed exhausting ventilation system reduced respirable dust exposures to less than 20 percent of those measured by MSHA inspectors when the blowing system was used.

Jan 1, 1993

By Malcolm Roberts

Extensive personal experience in the USA and Australia has shown that Australians working in suitable work environments are capable of world class performance. To build such work environments, mining leaders need to ditch two common management approaches that have not succeeded. Firstly, stop relying on traditional methods of trying to change people's behaviour simply by using communication alone to change attitudes and then change behaviour. Analysis of human behaviour explains why this approach fails in all industries. Secondly, stop trying to improve productivity by just running harder and increasing capital investment. Understanding work processes explains why this approach has limited success. These two approaches underlie problems commonly mentioned by many Australian mining executives: • negative or inadequate attitudes prevailing among Australian miners and managers including the lack of ownership of business goals among people at many levels • inadequate development of managers and accountability • lack of a competitive advantage in an industry in which labour costs are around 50% of mine site cash costs at many mines, and, • logical, emotional and physical barriers to change.

Jan 1, 1995

By Kamran Esmaeili, MINGLIANG TANG

An understanding of the spatial and temporal variations of surface moisture content over a heap leach pad is essential for leaching production and to achieve a high ore recovery. The current leach-pad monitoring and data-collection practice remains highly labor intensive and exposes technical staff to cyanide solution, a hazardous material. To address these challenges, we propose using unmanned aerial vehicles (UAVs) equipped with thermal imaging sensors to remotely obtain image data with high temporal and spatial resolution for monitoring the surface moisture distribution over heap leach pads. A field study was conducted over a sprinkler-irrigated heap leach pad at El Gallo gold mine in Sinaloa, Mexico, and the acquired data were used to generate moisture distribution maps of the heap leach pad’s surface. The created moisture maps provide direct visualizations of surface moisture variation over the surveyed area. Such graphical results are effective tools for inspecting heap-leaching operations.