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By C. H. North, L. E. Lynd, W. W. Anderson, H. Sigurdson

CONSIDERABLE uncertainty is revealed in the literature regarding the nature of the titanium minerals which make up the bulk of the heavy, opaque fractions of numerous beach sand deposits of the world. An investigation was made, therefore, of beach sand concentrates of North Carolina, Florida, Brazil, and India. Magnetic concentration, X-ray, and microscope data were obtained which show that these concentrates consist essentially of ilmenite and its alteration products. The alteration, brought about by oxidation and leaching of iron values, has resulted in upgrading the ores to a range of 56 to 64 pct TiO2, as compared with 52.7 pct in ilmenite of theoretical composition. Conclusions drawn regarding the nature of the dominant titanium-bearing mineral in beach sand deposits have been based mainly on chemical composition, specific gravity, and petrography. This material has usually been referred to as ilmenite or weathered ilmenite. It has also been referred to as arizonite because in chemical composition it resembles an occurrence in Arizona which was described by Palmer1 in 1909.

Jan 8, 1954

By Hsun Hu

The microstructural changes during rolling and at various stages of recrystallization in (111)[112] oriented single crystals of Si-Fe have been studied by transmission electron microscopy. At very low deformation, the dislocation structure consists of jogged dislocation lines, edge dislocation dipoles, and numerous dislocation loops, which may be interpreted by the jog-formation mechanism in moving screw dislocations. Up to 70 pct rolling reduction, no sharply defined cells are formed. Subgrain forma- tion takes place somewhat earlier in the annealing process than in a similarly processed (110)[001] crystal. This may be partly responsible for the reported difference in the rate of recrystallization between (111)[112] and (110)[001] crystals. Evidence indicates that the formation of recrystallization nuclei occurs largely by the coalescence of sub -grains. This is consistent with previous observations on other Si-Fe crystals. AVAILABLE data in the literature indicate that the main features of rolling and annealing textures in (111)[112] and (110)[001] crystals are essentially similar. A (111)[112] or (111)[112] crystal can be rolled 70 pct without changing its initial orienta-

Jan 1, 1964

By R. J. Woody

Design of the most economic continuous counter-current decantation (CCD) circuit is based on selection of the number of stages and the wash volume that will give the minimum summation of the following items: 1) Capital and operating costs of the CCD circuit. 2) Capital and operating costs of the precipitation circuit. 3) Value of the dissolved product lost.

Jan 1, 1959

Book review Pearson, J. S. Ocean floor mining. Park Ridge (New Jersey), Noyes Data Corporation, 1975. 201 pp. NIM reports Report no. 308 A mineralogical study of gold particles in pulp residues from the Bracken Gold Mine. (7th Mar.,1968. Re-issued Oct. 1975.) Report no. 377 Examination of pulp samples, treated with cyanide, for coated gold.(7th Aug., 1968. Reissued Oct.1975.) Report no. 385 The determination of the nature of coatings on gold particles. (2nd Aug., 1968. Reissued Oct. 1975.) Report no. 452 The Purlex Process - a description of the pilot plant leading to the use of the process in South Africa. (13th Jan., 1969. Re-issued Oct. 1975.) Report no. 482 Review of work on the treatment of pegmatites. (9th Apr., 1969. Reissued Sep. 1975.) Report no. 1443 Gravity concentration tests on four samples from Tantalite Valley,S. W.A. (5th Jul., 1972. Re-issued Sep. 1975.) Report no. 1489 The breakage of S oderberg electrodes. (10th Nov., 1972. Re-issued Nov. 1975.) Report no. 1545 A mineralogical investigation of leach residues from the Blyvooruitzicht Gold Mine. (22nd May, 1973. Re-issued Nov. 1975.) Report no. 1583 Preliminary tests on winnowing for the recovery of mica. (12th Nov., 1973. Re-issued Sep. 1975.) Report no. 1652 The identification of diamonds from Premier, Finsch, and Jagersfontein Mines by statistical analysis of data obtained from instrumental neutron-activation analysis. Report no. 1723 The determination of zirconium and aluminium in zirconiumaluminium alloys. Report no. 1739 The determination of trace amounts of noble metals in sulphate media. Report no. 1771 The determination of silver, selenium, tellurium, antimony, tin, lead, and arsenic in anode sludges. Report no. 1772 A study of copper recovery by lime roasting and leaching. Corrigendum The Special Issue of Volume 76 of the Journal ('Recent Advances in Mineral Dressing, October 1975) should be corrected as follows. The South African Institute Of Mining And Metallurgy - Information On Membershlp The Institute was founded in 1894 as the Chemical and Metallurgical Society of South Africa. In 1904 it was reconstituted as the Chemical, Metallurgical and Mining Society of South Africa and in 1956 it became the South African Institute of Mining and Metallurgy. Die Suid-Afrikaanse Instituut vir Mynbou en Metallurgie - Inligting Oor Lidmaatskap Die Instituut is in 1894 gestig as die Chemiese en MIetallurgiese Vereniging van ::!nid-Afrika. In 190-1is dit omvorm tot die Chemiese Metallurgiese en Mynbouvereniging van Sllid-Afrika en in 1956 het dit die Suid-Afrikaanse Instituut vir Mynbou en l\Ietallurgie geword.

Jan 2, 1976

By A. A. Collins

OF widespread interest to all lead metallurgists is a dross smelting process that will consistently give mattes and speiss of low lead and high copper contents. It is a problem that has intrigued operators through the years. In the past few years, with increased amounts of copper and overcrowded metallurgical furnaces, it has been almost imperative to evolve some method. Experience at El Paso has shown that high copper-to-lead ratios can be consistently attained by use of the new soda process. † Older Methods Three older methods, i.e., 1. Dross plus siliceous ore and limestone. 2. Dross plus one fourth blast-furnace speiss and siliceous ore, 3. Dross plus sulphides and siliceous ore and scrap iron, do not give consistent results and the products are higher in lead and lower in copper than those produced with the soda process. Any radical changes in the blast-furnace drosses will throw any of these older methods into a tailspin. For almost ten years, El Paso used the third method, with varying results. It was noted that as the arsenic and anti- mony contents of the dross increased, the speiss and matte steadily increased in lead and decreased in copper. A dross containing four parts of copper to one part of arsenic was considered to be ideal. At times this balance of copper to arsenic was almost impossible to obtain, especially when handling copper Cottrell dusts, which vary so greatly in copper and arsenic. Custom smelters like El Paso, handling a great variety of dusts, concentrates and ores, are apt to have anywhere from I to 15 pct copper on charge, with a variable in arsenic of from 0.5 to 2 pct. With such conditions, and drosses varying from 12 to 40 pct copper, an operator using the older dross reverberatory practices would find it just about impossible to control the reverberatory operations and to produce a good product low in lead and high in copper. These conditions prevailed at El Paso from the year 1940 to the present. In May 1942 it was decided to experiment with the soda process. The Soda Process After considerable work the soda method was finally evolved to the present state. It has never failed to produce a good product even under the most adverse conditions. It might be well to remember that many men of thought in the smelting industry have at one time or other sugge~ted the removal of all copper, arsenic and antimony from the lead blast-furnace charge as an aid to better metallurgy.

Jan 1, 1949

By A. A. Collins

OF widespread interest to all lead metal¬lurgists is a dross smelting process that will consistently give mattes and speiss of low lead and high copper contents. It is -a problem that has intrigued operators through the years. In the past few years, with increased amounts of copper and overcrowded metallurgical furnaces, it has been almost imperative to evolve some method. Experience at El Paso has shown that high copper-to-lead ratios can be consistently attained by use of the new soda process.* OLDER METHODS Three older methods; i.e., I. Dross plus siliceous ore and limestone, 2. Dross plus one fourth blast-furnace speiss and siliceous ore, 3. Dross plus sulphides and siliceous ore and scrap iron, do not give consistent results and the products are higher in lead and lower in copper than those produced with the soda process. Any radical changes in the blast-furnace drosses will throw any of these older methods into a tailspin. For almost ten years, El Paso used the third method, with varying results. It was noted that as the arsenic and antimony contents of the dross increased, the speiss and matte steadily increased in lead and decreased in copper. A dross containing four parts of copper to one part of arsenic was considered to be ideal. At times this balance of copper to arsenic was almost impossible to obtain, especially when handling copper Cottrell dusts, which vary so greatly in copper and arsenic. Custom smelters like El Paso, handling a great variety of dusts, concentrates and ores, are apt to have anywhere from 1 to 15 pct copper on charge, with a variable in arsenic of from 0.5 to 2 pct. With such conditions, and drosses varying from 12 to 40 pct copper, an operator using the older dross reverberatory practices would find it just about im¬possible to control the reverberatory operations and to produce a good product low in lead and high in copper. These conditions prevailed at El Paso from the year 1940 to the present. In May 1942 it, was decided to experiment with the soda process. THE SODA PROCESS After considerable work the soda method was finally evolved to the present state. It has never failed to produce a good product even under the most adverse conditions. It might be well to remember that many men of thought in the smelting industry have at one time or other suggested the removal of all copper, arsenic and antimony from the lead blast-furnace charge as an aid to better metallurgy.

Jan 1, 1947

The Virginia State Chamber of Commerce, Central National Bank bldg , Richmond, Va Clarence W. Newman, Director of Research. The State Chamber of Commerce has sponsored a book, entitled "Virginia-Economic and Civil," which is an industrial and technical survey of the state. It was prepared at Virginia Polytechnic Institute and contains a chapter by Roy J. Holden on "Minerals and Their Exploitation " A comprehensive view of the mineral resources of the state is presented The publisher is Whittet and Shepperson, 11 North Eighth St, Richmond, Va.; price, $4.

Jan 1, 1933

The American Association of Petroleum Geologists, P. 0. Box 1552, Tulsa, Okla. J. P. D. Hull, Business Manager. The official publication of this Association is the Bulletin of the American Association of Petroleum Geologists, issued monthly. It contains illustrated papers, maps, current notes, discussions, reviews and personals. Annual subscription is $15 ($15.40 outside the United States). Back numbers of the Bulletin, practically all of which are available, cost from $1.50 to $3 each; for several years back a uniform price of $1.50 each is charged.

Jan 1, 1933

By Roger Beckie, Leslie Smith, Craig Nichol

To study the hydrogeological processes that control the movement of water through unsaturated waste rock, an intermediate-scale (8m x 8m x 5m) waste rock pile has been constructed and instrumented. The constructed pile is monitored for moisture content, matric suction, temperature, matrix water chemistry, gas chemistry, gas pressure, rainfall, evaporation, discharge volume and discharge chemistry. The pile is built upon a grid of 16 contiguous lysimeters. The experiment is designed to investigate the mechanisms that create rapid water flow through a pile and its exchange with slower-moving matrix water.

Jan 1, 2000

By Laurence Neufville

Proper risk assessment and blast design are very desirable to the execution of a blast. Not only will this ensure that it achieves its desired outcome, but the probability of complaints and litigation will be reduced. Blasting engineers rely heavily on site-specific data for analysis and input to the blast design equations, and therefore data collection is critical to this process. The traditional approach to data collection is to carry out site-specific reconnaissance by visiting the site, but the time spent doing so can be reduced if a remote sensing approached is adopted.

Jan 1, 2009

By Douglas Talley

This report describes a 4-inch diameter borehole probe which contains a low light level TV camera, magnetic compass, light illumination source, bottom/water detector sensor and a pointing angle sensor. The camera viewing angle is at a right angle to the probe's body. All data from the sensor is multiplexed into the closed circuit camera video for transmission on a single 50 ohm coaxial cable to a surface control unit. Likewise control of the probe's power, zoom lens, focus, panning and aperture is accomplished via a down-link multiplexed on the same cable.

Jan 9, 1984

By Jeffrey Shepherd, Scott R. Smith, Eduard Guerra

"Electrochemical and spectroscopic evidence for the dissolution of a Au electrode by meso-2,3- dimercaptosuccinic acid (DMSA) from an acidic LiCl04 electrolyte is presented. Near the potential of zero charge, DMSA was determined to form a stable layer on the metal surface but at more anodic polarizations, DMSA was displaced from the metal through an oxidative process. The anodic displacement of the layer from the electrode resulted in a small amount of Au that was detected in the electrolyte using atomic absorption analysis. The extent of Au dissolution, was monitored while holding the potential of the electrode for 24 hours at the thermodynamic Eo/H,O in LiCl04 electrolytes containing 10 mM DMSA. This routine resulted in detectable quantities of a soluble Au-DMSA complex in the electrolyte and the greatest leaching was observed at a pH = 2.0. At room temperature, the leaching rate was stable at 10.9 µg cm·2 hr·' however, upon increasing the temperature to 50.0°C, the rate of Au dissolution increased yielding an average rate of extraction of 40.1 µg cm·2 hr- 1. Interestingly, after the first 12 hours of leaching at 50.0°C, the leaching current decreased dramatically suggesting surface passivation which prevented further Au extraction. The implications of this process in the industrial leaching of Au will be discussed.IntroductionThe use of cyanide in the industrial process of leaching Au from ores has raised concerns regarding both operational safety and environmental issues surrounding the disposal of spent leaching eftluents in tailings ponds. Depending on the chemical nature of the processed ore, the spent solutions that are released into the tailings ponds can contain toxic cyanide, either dissolved or complexed with different metals and may pose serious risk to wildlife as well as freshwater contamination to nearby water systems. Because of these issues, some recent studies have focused on the exploration of more environmentally-friendly molecules to selectively leach Au with appropriate kinetics. However, to effectively leach Au into an aqueous solution, a suitable ligand that reacts to form a stable chemical bond with Au is needed to form soluble Au complexes that can be later recovered [I]. Recently several sulfur bearing alternatives have been shown to leach significant quantities of Au in aqueous solutions. These include thiourea [2], thiocyanate [3], and thiosulphate [4]. However, alkylthiols are also known to quickly form a stable covalent Au-S bond [5], but have been relatively understudied in term of their ability to leach Au in solution, even though some short chain thiols are water soluble and relatively nontoxic."

Jan 1, 2012

By C. Patrick

Annually, the US coal industry generates and must dispose of over 200 million st (180 million t) of coal refuse, expanding a major environmental problem. The purpose of this research was to investigate the feasibility of utilizing coal refuse as an aggregate in concrete. This paper reports on findings of the initial phases of a project to determine the viability of replacing traditional concrete blocks with refuse blocks for use in ventilation stoppings in underground mines. Refuse, collected from three active preparation plants in eastern Kentucky, was used as the primary as aggregate in the preparation of concrete cylinder. Stress-strain analyses on the refuse cylinders yielded compressive strengths of from 59% to 77 % of the control-group strengths. Low variability within the groups was found while significant differences between the groups existed. On-going determinations of the effects of weathering on the refuse cylinders is being conducted and will be completed in early 1995. The research results are favorable for the future direction of the overall project objectives.

Jan 1, 1997

By Lippe D. Sadwin

This report describes a high-speed streak camera technique for measuring the lateral shock pressure generated by a cylindrical explosive charge detonated from one end. Experimental data show that the magnitude of the lateral pressure is approximately 50 percent that of the pressure generated from the terminal end of the charge for three explosives studied.

Jan 1, 1965

By J. Groppo, W. Zhang, R. Honaker

"Rare earth elements (REEs) found in coal are in the form of minerals, ion-adsorbed onto clay surfaces or inner layers, or organically bound. Rare earth minerals such as monazite exist in coal and have grain sizes smaller than 5 µm. In this study, froth flotation was successful in concentrating rare earth minerals existing in a thickener underflow material derived from Fire Clay seam coal that contained around 431 ppm of total rare earth elements (TREE) on a dry ash basis. Conditioning with fatty acid followed by processing using multiple stages of conventional flotation produced a final concentrate containing 2,300 ppm TREE. Using a laboratory flotation column to limit hydraulic entrainment, the TREE content was further enriched to around 4,700 ppm, which equated to an enrichment ratio of 10:1.IntroductionRare earth elements (REEs) are becoming increasingly important and have been widely used as raw materials for the production of phosphor, metal catalysts, magnets and batteries (Binnemans et al., 2013; Zhang et al., 2015). REE recovery from alternative sources such as coal and coal byproducts has the potential to stabilize the economic viability of coal mining operations while providing a dependable supply of critical materials.The average REE content of the world’s coal resources is around 60 to 70 ppm (Zhang et al., 2015). There are many well-known coal beds with high contents of REEs such as those in the Far East coalfields in Russia with contents of 300 to 1,000 ppm, the Fire Clay coal seam in eastern Kentucky in the United States with contents around 500 ppm and the Sydney Basin in Nova Scotia, Canada, with contents of 72 to 483 ppm (Birk and White, 1991; Seredin, 1996; Hower, Ruppert and Eble, 1999; Blissett, Smalley and Rowson, 2014). The occurrence of REEs in coal and coal byproducts can be classified into three types: (1) rare earth minerals, such as monazite and xenotime, (2) ion-adsorbed REEs on clays and (3) REEs associated with organic matrices. The rare earth minerals in coal and coal byproducts are very small in particle size, generally on the micrometer and/or nanometer scales (Honaker et al., 2014). Froth flotation, which concentrates minerals based on surface chemistry differences, has been widely used to treat fine rare earth industrial minerals such as monazite, xenotime and bastnaesite (Abeidu, 1972; Cheng, Holtham and Tran, 1993; Pavez and Peres, 1994; Pavez, Brandao and Peres, 1996; Jordens et al., 2014). As such, flotation is a promising method for the concentration of rare earth minerals from coal and coal byproducts."

Jan 1, 2017

By J. O. CHESLEY

CURRENT widespread applications of aluminum in such industries as transportation, mining, and construction would have amazed the early proponents of its use, including Napoleon III, French Emperor Batik ill the middle nineteenth century, when aluminum was a precious metal, Napoleon had visions of making his army light and mobile through the use of aluminum for gun carriages, helmets, canteens, sabers, and similar articles. Whereas the emperor failed in his objectives, the modern Napoleons of industry have .been successful, and today aluminum finds its greatest applications wherever there is mass ill motion. Its lightness has made possible such modern marvels as the Union Pacific streamline trains, the Boeing and Douglas giant airships, and up-to-date mining equipment such as the new Calumet and Hecla mine skips.

Jan 1, 1938

By Charles L. Kimbell

The final tables of this chapter, tables 25-50, extend and expand the statistical series on production that was started in the 1963 edition of the Area Reports: International Volume of the Minerals Yearbook and that was subsequently updated and expanded in the 1965 and 1967-90 editions. Continuing the practice started in 1989, a column has been included in each of these tables providing a 5-year average for 1987-91, inclusive. This should provide a clearer picture more rapidly of the role of each major producer over the 5-year period. The listing order of major producers, however, continued to be, as in past years, in descending order of rank in the year of review, 1991. This group of tables now includes each of the crude minerals that ranked from? 1st to 19th in 1983 terms of value of their output (as well as four others of lesser rank). These 23 crude mineral commodities accounted for 93 % of the estimated value of world crude mineral production in 1983. In addition, world output of five key downstream products-aluminum, steel, cement, nitrogen in ammonia, and refined oil-is included because of their significance as products.

Jan 1, 1993

By Gene Bryant, Wesley Schmutzler, Matteo Bertoni

The levees where the Mississippi River and the Lower Wood River meet near East Alton Illinois have been a problem area for years due to underseepage. The first phase of the deep cutoff wall was a 2,000-linear foot section that was completed in 2016 for the Illinois Flood Prevention District Council. This section was installed along the Wood River and the Mississippi river to depths of over 135’, The United States Army Corps of Engineers was tasked with continuing the cutoff wall along the Mississippi river. The wall was a continuation of phase I with depths up to 140’. The 1,000’ long cutoff wall was installed through fill, loose sands, cobbles, and sandy clay. The cutoff wall was terminated in either Glacial Till or sound rock. In order to provide wall permeability equal to or less than 1.0 X 10-6 cm/sec a self-hardening slurry (SHS) composed of ordinary Portland cement, slag cement, and water was utilized. The depths reached on this project using SHS is the deepest done to date in the United States. Along with the permeability requirements, a very narrow range for the unconfined compressive strength was specified at 50 – 180 PSI. In order to monitor the ground movement and water level fluctuations during the excavation of the panels with the Hydromill or Clamshell, 6 automated inclinometers were installed and monitored continuously during panel excavation in phase 1. Seven automated piezometers were monitored in phase 2. This paper will give an overview of the project with emphasis on the effect of the excavation on the instrumentation, specifically the reaction of the piezometers as the last panels were installed. INTRODUCTION The project is in Illinois, about 1000 feet downstream from where the Wood River Creek enters the Mississippi River between East Alton, IL and Wood River, IL adjacent to State Highway 143 (Fig. 1). The Wood River Lower Cutoff Wall Phase 2 Project (WR2) was awarded to TREVIICOS SOUTH (TIS) in September 2017. The Main Project features are: Construction of work platform, inclinometers installation and removal, cutoff wall construction by the Self-Hardening Slurry method (approx. 135,000 sf) up to 140' depth, clay cap installation, and site restoration. The levee system along this stretch of the Mississippi River has been plagued by under-seepage for several years. The phenomenon has worsened to varying degrees, depending on location, to the point that remediation was needed to ensure that Levee failure would not be an issue in the future.

Jan 1, 2019

By B. S. Butler

Apropos of metals low in the series illustrated by Dr. Butler's Table 11, it is interesting to note that Cress and Feldman29 reported traces of platinum metals in several samples of alunite. They found, chemically and spectrographically, several traces of platinum, palladium, and rhodium in alunite from Sugar Loaf Peak, near Quartzite, Ariz.; silver, platinum, and rhodium in alunite from Rio Grande County, Colorado; and traces of rubidium and gallium in various samples of alunite. These authors stated that the platinum metals appear to be present as Oxides and suggested deposition by hydrothermal solutions under near-surface conditions. AS described by Heineman,30 the wall rock of the Sugar Loaf alunite veins shows considerable alunitic alteration. Pyrite and hematite are relatively abundant in the wall rock but decrease progressively near the veins. Assays of samples of the Sugar Loaf alunite, run by J. B. Cunningham of the University of Arizona College of Mines, showed traces of silver and 0.002 to 0.004 oz of gold per ton, but the chemical form of the gold and silver in this occurrence remains undetermined.

Jan 1, 1957

By Wilfrid Comeau

Vibrograms, which last significantly longer than the actual blast (say 10 to 15 cycles or more), may be signalling an elastic response, which is not uniquely blast related. For example, geophones mounted on a part of a structure, which can elastically resonate at a frequency included in the seismogram, may not show the structure’s real reaction to the blast. This resonance usually amplifies the ground vibration. This contribution examines one particular case where blasting excited and amplified a resonant ground response, and the method used to significantly reduce or eliminate this undesirable condition.

Jan 1, 2007