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By T. Palangio

Most blasters wouldn’t think of initiating a shot without a seismograph to record vibration and air blast results. Some might even measure the velocity of detonation but few surprisingly record the event on video, photo document loading conditions or take pictures before and after the shot. This paper discusses digital imaging, the equipment, methods, techniques and information that can be learned from digital pictures taken in the field during blasting operations. The guy who said “a picture is worth a thousand words” probably understated it.

Jan 1, 2008

By Peter Duniam, Vivian Patz

History of the ExEx 1000 CAB system. l What we’ve learned using electronic timing. l Requirements for a second generation. EDD system. l The ExEx 2000 system - simple, versatile and cost effective

Jan 1, 1997

By F Diaz, G Hovestadt, B Friedrich, D Latacz, M Sommerfeld

The metallurgical sector significantly contributes to the global carbon footprint and encounters the challenge of developing more sustainable production methods. This study introduces novel approaches aimed at reducing CO2 emissions within the industrial sector, some of which have been developed up to the demonstration scale. In two case studies, urban waste from the agricultural sector (corn, olives, coconut etc) and waste electrical or electronic equipment (WEEE) recycling residues (shredder light fractions (SLF)) were subjected to thermal treatment. The resulting materials were then used as substitutes for conventional fossil-based reducing agents in both the copper and ferroalloy industries. Furthermore, hydrogen was employed at different scales to assess its efficacy as a reducing agent for recovering metal oxides from fayalitic copper slags. Our findings reveal promising prospects and defined specific challenges for the integration of these alternative reducing agents in the industry. The synergistic use of pyrolysed SLF, bio-coke, and hydrogen presents a viable pathway to significantly diminish CO2 emissions while simultaneously improving the sustainability of the metallurgical sector.

Jun 19, 2024

By M. A. Llavona

In Spain, as in many countries, the gold content of jewellery must be officially hallmarked. The official methods of assay are gravimetnc cupellation (a method which is highly accurate but both time and sample consuming), potentiometry, gravimetry and volumetry. In this paper, a procedure for measuring gold by flame atomic absorption in jewellery samples is described. The method is based on the acid digestion of a 40 mg sample. The quantity of aqua regia necessary for dissolving the gold, the ideal weight of a sample in order that the error may be minimal, the effect of the acids employed, the type of material used for its storage, and the necessity of employing a buffer to avoid the ionization of the solution are described. The method proposed is simple, highly accurate and causes little damage to the jewellery.

Jan 1, 1999

By M. Scaggs

"Respirable dust in underground coal mines has long been associated with lung diseases, and regular dust sampling is required for assessing occupational exposures. At present, respirable dust concentration and crystalline silica content are commonly determined, but considering recent and yet unexplained increases in the incidence of lung disease amongst miners in specific geographic regions, more information about specific dust characteristics is urgently needed. While particle-level dust analysis is ideal, it is impractical for large numbers of dust samples because it is both time and cost intensive. Thermogravimetric analysis (TGA), however, is an alternative option, which offers the ability to determine the total coal to mineral mass ratio in a dust sample – analogous to proximate analysis of bulk coal samples for determining ash content. Here, preliminary development of a TGA method for this purpose is presented. The method is being developed to evaluate dust collected on mixed cellulose ester (MCE) filters using approved permissible sampling equipment. INTRODUCTION Based on the particle size, airborne mine dust can be classified in three categories: inhalable dust (< 100 µm in size), thoracic dust (< 25 µm in size), and respirable dust (< 5 µm in size) (Ramani et al., 2003). The World Health Organization (WHO, 1999) defines inhalable dust particles as those which can be breathed into the nose and mouth, and thoracic dust particles as those which can penetrate airways of the head and enter the airways of the lung. On the other hand, respirable dust particles can penetrate beyond the terminal bronchioles into the gas-exchange regions (alveoli) of the lungs (WHO, 1999). Hlavay (1992) reported that the seriousness of the damage in the lungs and respiratory tract is based on amount of dust remaining in these organs, and the amount of dust depends on the extent of dust exposure, the size distribution of the dust particles, and the capability of the body for dust elimination. Inhalation of respirable coal dust by miners can cause a disabling and potentially fatal lung disease which is called coal worker’s pneumoconiosis (CWP). Silicosis is another fatal lung disease caused by inhalation of respirable silica dust. In CWP and silicosis, dust particles deposit in the lungs, damage the lung tissue, and ultimately cause scarring which cannot be reversed (Colinet, 2010). While overall incidence occupation-related lung disease amongst coal miners in the US has been declining for over 40 years, it appears that there has been a recent increase in specific locations in Central Appalachia (CDC, 2006; Pollock et al. 2010; Suarthana et al., 2011). Although this trend is yet unexplained, one theory is that particular dust characteristics in these locations may be a factor (Hassan and Lau; Page & Oraniscak 2002). For example, several studies have indicated that different coals may generate different amounts of respirable dust (e.g., see Page, 1993 and Litton and Page, 1994), and the surrounding geology may also play a role in terms of the types of dust particles generated. Although respirable dust concentration and crystalline silica content are commonly determined as part of regulatory compliance sampling, more information about specific dust characteristics (e.g., size, shape and composition) is urgently needed."

Jan 1, 2015

By A. E. Isaacson

The U.S. Bureau of Mines is studying the effect of supercritical water, at 400&apos; C and 3,500 psi, and subcritical water, at lower temperatures and pressures, on mixtures of minerals and metals to determine the possible applications of water at high temperature and pressure for processing these materials. This research was conducted using a flow-through bench-scale system. Copper-bearing minerals studied were chalcocite, chalcopyrite, covellite, and cuprite. In general, mixtures of copper minerals and pyrite reacted to form bornite. Intermediate phases formed were chalcopyrite and digenite. Similar reactions occurred between pyrite and metallic copper. A mixture of chalcopyrite and pyrite was inert in supercritical water&apos;. The reaction between cuprite and metallic zinc yielded metallic copper. The cuprite was reduced by hydrogen generated by the reaction between metallic zinc and water. None of the reactions occurred exclusively in supercritical water, but also occurred in water at high temperature and pressure below the critical point. &apos;Experimental results did show that a dual-reaction process, consisting of solid-state diffusion and fluid transport, was occurring.

Jan 1, 1989

By David J. Mack, A. H. Kasberg

The transformation characteristics are found to resemble a similar binary alloy. The differences are due to the alpha iron particles. While strength properties of the isothermally transformed alloys are high, ductility is low, resulting in high notch sensitivity. The elastic modulus can be varied widely and correlates with strength. Abnormal grain growth sometimes occurs. A CONSIDERABLE amount of work has been done on the isothermal transformation of high purity aluminum bronzes using the methods pioneered by Davenport and Bain.&apos; The first isothermal study of these alloys was made by Smith and Lind-lief,&apos; but more recently Mack", " and Klier and Grymko5 have continued the work. In commercial aluminum bronzes, one or more elements are always added to refine the ß grain size and to improve the mechanical properties. The effect of these elements on the isothermal transformation has not been reported in the literature. No systematic study of the properties of isother-mally transformed aluminum bronzes has apparently been reported, although adequate information is available on their properties after more conventional heat treatments. The fact that a eutectoid alloy will reject face-centered cubic a during isothermal transformation at appropriate temperatures2&apos;" warrants investigation of the properties of such structures. Another cogent reason for determination of properties is the fact that the modulus of elasticity of the eutectoid alloy varies widely with the nature of the heat treatment." Preliminary experiments7 indicated that a high purity eutectoid alloy would not give reproducible results in property determinations because of ex- cessive ß grain growth during heat treatment, a single ß grain frequently occupying the entire cross-section of a standard test bar. For this reason a commercial aluminum bronze containing iron as a grain growth inhibitor was used. The isothermal transformation diagram of the alloy was first determined. On this basis, the heat treatments necessary to produce representative structures were selected and the properties determined. Material A commercial alloy (Ampco Grade 20) of the following composition was used: Cu, 83.68 pct; Al, 12.31 pct; Fe, 3.68 pct; Ni, 0.28 pct; and Mn, 0.03 pct. This alloy proved to be very close to the eutectoid composition and may be compared with the accepted value of 11.8 pct A1 in the binary Cu-A1 system. Comparison is valid only because of the "negative replacement effect" of the iron? Since traces of excess y² are present, the alloy is slightly hyper-eutectoid. The material was received in the form of 3/4 in. round, hot extruded bars. Specimens of approximately ? in. thickness were cut from this stock and drilled to allow suspension in the salt bath. The structure of the as-received material varied from 5 to 40 pct a + y2* in a matrix of ß. The amount of a + y² present was dependent upon the ß grain size of the extruded material. The coarse grained portions did not form as much a + Y, as did

Jan 1, 1952

By Leandro de Arruda Santos, Lorena Isabela de Oliveira Ribeiro, Jéssica Dornelas Silva, Pedro Damas Resende, João Victor Lucas Amim, Suzanny Cristina Soares Martins, Vicente Tadeu Lopes Buono

O objetivo do presente estudo foi avaliar a resistência à fadiga de duas ligas de NiTi diferentes sob condições de teste controladas por deformação a 25°C por meio de testes de fadiga por flexão rotativa. Além disso, as propriedades mecânicas, térmicas e estruturais dos fios foram caracterizadas por ensaios de DSC, DRX, MEV/EDS e tração. Os resultados revelaram que ambos os materiais são superelásticos à temperatura ambiente e, portanto apresentaram composição basicamente austenítica de sua matriz. Os resultados de ensaio de tração são condizentes com a caracterização térmica e estrutural, pois os materiais apresentam recuperação total de forma após ciclos de carga e descarga em tração. Ambos os materiais são ricos em titânio, um deles apresenta camada de óxido superficial enquanto o outro apresenta acabamento superficial. Apesar das propriedades similares a amostra 1 apresentou média de 77 ciclos até a falha, enquanto a amostra 2 resistiu a 1827 ciclos..

Oct 25, 2019

By W. R. Clark, W. W. Cotter

Jan 1, 1946

By W. W. Cotter, W. R. Clark

Jan 1, 1946

By Judy Che, Steven Ceccio, Gretar Tryggvason

"A detailed understanding of drop deformation and solidification is essential for quantitative predictions of geometry and properties of parts made by ballistic particle manufacturing processes. Axisymmetric results of towers built by the deposition of multiple drops are presented. In these computations, fluid flow, heat transfer, and phase change are fully coupled throughout the drop deformation and solidification process. The solution method is based on a single set of conservation equations written for all phases simultaneously. The phase boundaries are treated as imbedded interfaces by adding the appropriate source terms to the conservation equations. A parameter study demonstrates the effect of Weber number, Peclet number, and drop deposition frequency on the final shape of the structure. Numerical results show that most successful method of building uniform towers is when two conditions are met. First, each drop solidifies at the same time in the deformation cycle. Second, the cooling rate is slow enough to allow for good adhesion between drops. The ability to predict the final shape of deposited drops will greatly reduce the amount of experimentation necessary to select the desired set parameters for any artifact.IntroductionMaterial deposition techniques based on layering small molten metal drops holds the promise to build small, coherent three-dimensional structures. In this process, numerous 20-100 µm diameter drops are deposited onto a substrate with a low impact velocity (on the order of 5 mis). Both the momentum and trajectory of each drop are controlled precisely to build up complex parts. This material layering technique differs from processes such as spray forming and splat quenching which involve high impact velocities (on the order of 100 mis) and high frequency deposition with little control over individual drop placement. This process of layering small drops can produce parts with near net shape accuracy, while spray forming produces slabs of material which must then be worked to make a usable part. The ability to computationally predict final drop shape and cooling rate has the advantage of allowing the user to select parameters to produce parts with desired shape and mechanical properties. However, the development of such predictive methods requires a thorough understanding of both drop deformation and solidification"

Jan 1, 1999

By J. M. B. Scarborough

This paper deals with measures taken to maintain effective operation of heavy-duty equipment in open-pit mining. at Pine Point, N.W.T., during periods of extreme cold weather. The points covered include equipment modifications designed to improve cold-weather performance, effective lubrication of machinery that is vulnerable to extreme cold and operating procedures designed to prevent equipment damage.

Jan 1, 1966

By S. T. Johansen, B. T. Løvfall, T. Rodriguez Duran, J. Zoric

A methodology for building pragmatic physics-based models is here adapted to predict the erosion of ladle linings in the steel industry, in order to support operators when deciding whether the lining can be used safely for another heat. A defective lining may allow 140 t of molten steel to spill, with disastrous consequences for workers and plant. The adopted work flow for the development, challenges faced, and some model results are presented. One key learning outcome is that model development should allow time for maturing the process understanding, as well as for many iterations by ‘questions-responses and actions’ at various stages in the model development. Good interaction between the development team and industry case owner is an important success factor. Combining or extending the model with the use of machine learning and cognition-related methods, such as knowledge graphs and self-adaptive algorithms, is discussed.

Apr 16, 2024

By G. Richards Gwinn

In modern warfare, mica is truly indispensable. Coordination of combatant units necessitates maintenance of intricate communications equipment, in the construction of which high-grade sheet mica is essential. Scrap, ground, and the poorer qualities of block mica, which are less essential to the military program, are not considered in this paper. Furthermore, as the paper is designed primarily to assist mica miners, mica derivatives, Such as splittings and films, also are excluded from discussion. The paper therefore relates solely to block mica of strategic quality. Understanding of t e many factor involved in marketing mica is definitely advantageous to mica, miners. The nature and detrimental effects

Jan 1, 1943

By H. J. McQueen

Pyro-reduction of ores to metal products developed markedly through the industrial revolution into the great depression. Nineteenth century resource and environmental sustainability were haphazardly improved by many process changes, although the motivation was primarily reduction in labor, feed stocks and fuel. Some notable achievements were coke and hot air for blast furnaces (later from waste heat stoves), puddling of wrought iron and steel ingot production with convertors advancing into oxygen use and continuous slab, billet and strip casting. Although advances in one sector were often counteracted by fall-backs in others, there was progress in that the resource consumption and pollution per unit of production was decreased. Improvements in the 2 decades following WW2 were mixed but popular notice of environmental hazards forced governments to legislate pollution controls and initiate steps in resource conservation. The energy crisis of the 1970’s saw an industrial energy-saving campaign and legislation of technology assessment procedures. Up until mid 18th Century, the training of iron masters depended on apprenticeship with some formalized knowledge from medieval books such as those of Biringuccio (1540) and Agricola (1556). The advances were very slow partly due to absence of scientific concepts of the smelting process. Nevertheless, some iron masters succeeded in improving the process and described procedures to instruct others. With the surge of steam power and the reverberatory puddling process for ductile wrought iron (WI), machinery changed from wood (iron strap reinforced) to WI machinery. With the clarification of the reduction and oxidation mechanisms by Cavendish and Lavoisier (~1780), productivity in iron production surged. The mechanical testing and microscopy of Kirkaldy (1862) spurred understanding of processing and properties of WI and steel. The various forms of C in steels were determined by chemists at the end of the 19th Century. It also became possible to control metal and slag chemistry in the open hearth furnace. But understanding of the transformations during heat treatment of steel only came in the first decades of the 20th Century.

Jan 1, 2012

By Robert E. Barieau

General expressions for evaluating practically all the thermodynamic properties of a fluid from a single equation of state are derived. Most of the formulas are expressed in terms of the compressibility factor, with this factor being an explicit function of the temperature and the molal density. Similar expressions are given using reduced variables.

Jan 1, 1967

By K. J. G Hedges

"Once a health based guidance limits for exposure to diesel exhaust have been established, and as part of a multi-disciplinary team, the program for exposure reduction should incorporate the plan-do-check-adjust cycle. Setting a suitably protective (health based) occupational exposure limit (OEL) for diesel particulate matter (DPM) and nitrogen dioxide is a key driver to reduce exposure. It is important to go beyond regulations and reduce exposure to diesel exhaust, DPM, as low as reasonably achievable (ALARA) such as that prescribed under the Australia, Queensland Mining and Quarrying Safety and Health Regulation 2017 where under section 135 Limiting workers exposure, the workers exposure must not exceed the exposure limit applying to the worker for the hazard; and is ALARA. It appears that previously acceptable OELs are no longer safe. Therefore it is important that the internal responsibility system be implemented and the precautionary principle approach be followed, especially as it may be some time before a suitably protective OEL specifically for DPM is in place. One leading multi-national mining company BHP Billiton has acknowledged a significant lag that exists between regulatory action and the level of science that informs health risk. This company is managing exposure to diesel exhaust to as low as technically feasible. This same company that has set an interim target for managing diesel exhaust to 0.03 mg/m3 is achieving these levels which paves the way for other mining companies and general industry including construction. The Occupational Cancer Research Centre 2017 recommends reducing personal exposure to within 0.02 mg/m3 (EC) for underground mining and 0.005 mg/m3 for other workplaces. Controlling DPM is important to prevent cancer however it is also important that that nitrogen dioxide (NO2) be reduced (ALARA) and that careful selection of control technology be considered such as the proper selection of a diesel oxidation catalyst so that the level of NO2 does not in fact increase. The example from BHP Billiton provides a leading practice including using a multi-disciplinary approach and the importance of controlling emission at source and having an auditable diesel emissions based monitoring program in place."

Jan 1, 2019

By J. B. Gayle

A half-ton experimental coke oven was installed at the Southern Experiment Station, Tuscaloosa, Ala., in 1948. Designated as the Tuscaloosa oven, this unit features a 17-inch carbonizing chamber, globar heating elements, and silica-brick walls designed to simulate as closely as possible the carbonizing conditions for commercial, slot-type ovens. The reasons for constructing an oven of this Size, the details of the design, and the operating characteristics of the oven have been given in previous publications.3/4 The present report deals with the reproducibility of test-oven data and the effects of variations in flue temperature on the physical properties of the cokes produced. Also included are the results of 2,400° carbonizing tests for several coals and coal blends not included in the earlier reports.

Jan 1, 1955

By D. Bienstock

The use of alkalized alumina in removing sulfur dioxide from a coal-combustion flue gas at 625° F was investigated on a pilot plant scale. The absorber was 26 feet long and 1.6 inches ED. Counter-current gas-solids flow at gas velocities of 8 to 15 ft/sec in the presence and absence of baffles, as well as solids entrainment at gas velocities of 20 to 23 ft/sec with solids recycle, were employed. The spent absorbent as regenerated as fixed bed with the reducing gases--reformed natural .7.7d hydrogen. Of absorption-regeneration were successful completed using the alkalized alumina rolled into spherical granules 10 to 16 mesh. There was no loss in activity of absorbent toward SO2 with a modest attrition equivalent to 0.l percent of the solids feed. Supporting studies were conducted on the effect of the sodium content in the absorbent, the composition of the reducing gas, thermal treatment to increase absorbent hardness, and removal of absorbed chlorine from the absorbent. A mathematical model was formulated to describe the removal of SO2 by alkalized aluminum from fixed and falling beds.

Jan 1, 1967

By B. O. Odera

The Pt-based alloys have a high potential for replacing some Ni-based superalloys (NBSAs) used in the highest temperature and most aggressive environments, and vanadium would be a beneficial alloying element. Six alloys of average compositions Pt-26.6Al-9.1V, Pt-23.1Al-17.8V, Pt-9.6Al-21.1V, Pt-17.4Al-6.4V, Pt-22.3Al-7.9V, and Pt-6.0Al-10.1V (all in at.%) were manufactured by arc-melting and examined in the as-cast condition using scanning electron microscopy and X-ray diffraction (XRD). Five samples were heat treated at 1 000°C for 1 500 hours and water quenched, then examined. The phases were identified using energy-dispersive X-ray spectroscopy and the identities were confirmed by XRD. In most of the samples, the phases existing in the as-cast condition were different from those at 1 000°C after ~1500 hours heat treatment. A solidification projection, an isothermal section and a liquidus surface projection were determined for the Pt-rich corner.

Jan 1, 2012