Search Documents

By G. D. TRANT

HOT metal is commonly transported from the blast furnace to the open hearth by one or the other of two general methods: (1) by hot-metal ladles, usually in conjunction with a stationary mixer, or; (2) by means of mixer-type ladle cars, taking the place of both the hot-metal ladles and the stationary mixer. In both cases, the use of transfer ladles for charging the metal into the open-hearth furnaces is necessary. The American Rolling Mill Co. at its Middletown division, adopted hot metal practice on. June 2, 1928. The pig iron is produced' in a .blast furnace about 11 miles from the open-hearth furnaces, and is trans- ported in Pugh-type mixer cars having a capacity of 150 gross tons each. Three cars are in service and handle the delivery of hot metal to the pig machine and the open-hearth furnaces. The capacity of the blast furnace is 550 tons and casts are made every four hours.

Jan 1, 1929

By R. Poulin, R. Pakalnis, D. Peterson

Introduction A comprehensive project has been completed at the University of British Columbia that focused on the development of a commercially competitive composite cable bolt. Laboratory evaluation consisted of pull tests, preliminary shear tests, grout column testing and scanning electron microscope evaluation of the composite cable bolt. Field implementation at five underground mines throughout Canada were completed for technical and overall performance evaluation of the new product. The project began in 1989 under the sponsorship of HDRK Ltd., a consortium of mining companies including Inco, Noranda and Falconbridge Ltd. The objective was to develop a cuttable cable bolt that would serve as support for a continuous miner within a hardrock environment (Mah, 1994). The bolt was required to be cuttable by a continuous roadheader without adverse effects to equipment, personnel and the milling process. From the beginning, the focus was to employ existing cable bolt installation technology (Goris et al., 1994) whereby the cable bolts are grouted within a 4.8-cm-diam (1.08-in.diam) or larger employing a portland cement grout having a water: cement ratio between 0.35:1 to 0.4:1. The prototype, developed from Phase I, was technically comparable to that of conventional steel cable bolts. However, high cost and limited accessibility hindered its commercial acceptance. The second phase of the project was sponsored by the British Columbia Science Council and Pacific Pultrusions Ltd. of British Columbia to locally develop a glass fiber cable bolt. This phase of the project has resulted in the DAPPAM cable bolt (Pakalnis et al., 1994). DAPPAM Cable bolts are the second most used support method in Canadian underground mines after mechanical rock bolts. It is projected that 870,000 m (2.9 million ft) of cable bolts are installed annually in Canada (Poulin et al, 1994). The objective of the research program was to develop a glass fiber cable bolt with similar pullout strengths to the conventional steel cable bolts (267 kN - 60,000 lbf). More than 200 laboratory pull tests were conducted employing standard cable bolt test procedures, as outlined by the US Bureau of Mines (Goris, 1994), to assess optimum rod and surface composition, geometry, number required, pullout and shear characteristics, among others. This resulted in the DAPPAM cable bolt (Fig. 1). It consists of 10 individual 0.6cm-diam (0.25-in.-diam) rods enveloping a 2.2-cm (0.8-in.) outside diameter, high-density polyvinyl grout tube. The composite used in the construction of the rods is comprised of about 65% glass fiber within a 35% polyester resin matrix (by volume). Through pultrusion (a continuous fabrication technique), the fibers and resin are combined into a composite material. The strength of the overall composite is largely governed by the material properties, the alignment [ ] of the fibers relative to the applied load and the density and interaction of the overall components within the composite. A further modification to the composite was the addition of a sand grit to the surface of the individual rod. This increased the overall bond strength between the rod and the cement-based grout, used to solidify the cable bolt to the rock mass. The grout tube has an inside diameter of 1.9 cm (0.75 in.) and is rated at a pressure of 1.72 MPa (250 psi). During installation, the grout is pumped through the annulus of the grout tube thereby filling the hole from toe to collar. Laboratory and field trials concluded that a minimum drill hole diameter of 4.8 cm (1.08 in.) be used to ensure optimum grout coverage. Table 1 compares the design strengths (as tested) for DAPPAM vs. the ultimate strengths for a conventional 1.6cm (0.6-in.) steel cable bolt. The characteristics for the steel cable have been derived directly or indirectly by Goris et al. (1994). A design tensile strength of 289 kN (65,000 lbf) was proposed for the composite developed. However, recent tests have indicated maximum breaking strengths of more than 400 kN (90,000 lbf) (Fig. 2). Figure 2 shows the load vs. displacement pull out curves for steel and DAPPAM cable bolts. The methods of testing were standardized so as to be able to compare the results directly. The shear strength of the fiberglass cable is largely a function of the surface area sheared. Shear strengths of 89 kN (20,045 lbf) were obtained for the configuration shown in Fig. 1 when sheared normal to the axis of the cable. The testing procedure was similar to the shear tests performed on steel by Goris (1993). It is important to reinforce the implication that critical bond strength has on the success of an overall support system.

Jan 1, 1995

By Pratama Mochamad Rizki, Andika Satya

High-risk area in open-pit mining should always be monitored by the operational supervisor because of its nature. One of this type is the soft soil dump area. Due to the unstable bearing capacity of the soil, it’s highly possible for us to find cracks in the area. This paper aims to build computer vision which able to detect truck’s distance from safe limit allowed during dumping activity. The system will warn the truck’s driver if the truck has crossed that predetermined safe limit.

Jun 25, 2023

By William Gleason

During the past five years, mining operations have had access to press technology for piping and joint fittings that can save owners a significant amount of time when installing or replacing pipes by eliminating the need for welding or threading. Viega, with North American headquarters in Wichita, KA, entered the mining sector in 2009, adding to its already expanding industrial sector. Since then, the company?s global engineering department has paid considerable attention to its industrial division, bringing its expertise in plumbing solutions for residential and commercial buildings to the mining and mineral extraction industry. ?We have a lot of applications in the mining industry.?We have a lot of applications in the mining industry throughout the United States, Canada and Mexico and continue to expand in the mining industry,? Tom Shields, Viega?s director for industrial accounts explained. ?Since we made the decision to increase our presence in the industrial markets, we have been aggressive and more than 240 applications have been approved by our engineering department in Germany.? Getting approval from Viega?s engineering department is no small feat. During a tour of the manufacturing facilities in Ennest and Großheringen, Germany, Mining Engineering, as well as a select few other publications and clients, were shown Viega?s manufacturing process. At the Ennest facility, hundreds of millions of fittings are produced, and each one is inspected mechanically and with a laser at the end of the production line. With four production facilities in Germany and one in the United States, Viega is able to ship to anywhere in the world. The company distributes everything from fittings to stainless steel pipe.

By Victor Kalcevic

A gas-flow retort for thermal processing of oil shale to recover shale oil was developed by the Bureau of Mines at its Oil-Shale Demonstration Plant, Rifle, Colo., from 1948 to 1952. The retort is a crossflow gas-to-broken-solids heat exchanger. The heating medium is the gas produced in the shale retorting process. The gas is heated in specially designed stoves outside the retort and recycled to the retort. Oil shale from the Mahogany ledge section of the Green River formation in northwestern Colorado was the material processed. Indicated maximum oil recoveries for 20-to 25-gallon-per-ton shale in a l2-inch-thick shale bed and a 20-inch bed are 96 and 91 weight-percent of Fischer assay, respectively. Heat requirements for maximum recovery are 600 to 750 B.t.u. per pound of shale. Properties of the recovered shale oil are affected slightly by shale-bed thickness and extent of retorting. Oil recovery from oil shales assaying over 30 gallons per ton is lower than that from leaner shales.

Jan 1, 1959

By Hamid Mazouz, Mohammed Hakkar, Rim Jouraiphy, Fatima Ezzahra Arhouni, Ahmed Mahrou, Aziz Boukhair, Mohammed Fahad

The wet process is the most commonly used worldwide for phosphoric acid (PA) production, in which phosphate rock (PR) is reacted with strong acid mainly sulfuric acid. This work aims on studying the rare earth elements (REEs) distribution during the production of phosphoric acid using different qualities of phosphate through various industrial technologies. At the onset of this work, the process started with 12 samples of PR, PA, and phosphogypsum (PG) being taken simultaneously from two different Moroccan basins (Ouled Abdoun mine represented by K09 and Gantour mine depicted by G10, G20, BG) and various production lines at two processing platforms (Jorf Lasfar and Safi). Afterward, collected samples were prepared and analyzed for REE characterization using an inductively coupled plasma mass spectrometry (ICP-MS). Based on the analysis results, a transfer factor ( TFX) was introduced with the aim of gauging the REE distribution between PA and PG. The results showed that the total concentration of REEs in different phosphate qualities ranged from 411 to 631 ppm; the major part of this concentration was attributed to the four elements: Y, La, Ce, and Nd which constitute more than 77%. The REE distribution between PA and PG depends on neither the phosphate quality nor the industrial technology used since that the distribution results showed that 55 up to 66% of the initial REEs in phosphate rock ended up in the PG. The behavior of each REE was common except for the element scandium, which transferred mainly to the phosphoric acid.

Nov 3, 2021

By J. C. White

"During the early development of the Mattabi Mine in 1970, discussions with the Ontario Government revealed their policy of prohibiting, as much as possible, the development of new, isolated, single-industry townsites. Subsequently, Mattabi located its first housing in the Township of Ignace, which is situated 50 miles from the site of the mine and plant. Over 200 employees now commute 100 miles daily to and from work.This paper describes the experience gained and discusses the advantages and disadvantages of a remote townsite."

Jan 1, 1976

By Bartho J. Admiraal, Antoine Feddema

Pneumatic sinking of caissons has been established from mid-19th century. The technique of pneumatic sinking has been applied on many projects for underground construction up to depths over 20m below groundwater level since that time. Volker Staal en Funderingen, a known deep foundation contractor in the Netherlands, was awarded two contracts in 2015 for sinking in total 2 caissons in Hamburg (Germany) to large depths (over 30 m (100 ft) and two projects near Amsterdam (the Netherlands). The latter concerned two gate chambers for the world’s largest sea-lock, one of them was 55x81 m2 (180x266 ft) to a depth of 25.5 m (84 ft), which would mean a world record for pneumatic sinking! But with depths and dimensions like these, the deployment of personnel is the main limiting factor for production, despite all developments to date. It was decided to develop a remote controlled process, including the necessary equipment and monitoring systems. Monitoring not only the kinematics of the equipment in the working chamber and the production parameters related to the excavation but also of the structural behaviour of the sea-lock gate chambers was essential for approval of this innovative execution method. The lay-out and the sizes of the largest caisson the structural integrity was extremely critical for torsion and bending moments. A displacement controlled execution by the observational method was therefore required. In engineering a new approach for modelling the semi-continuous failure mechanisms of the soil was needed to understand the sensitivity of the excavation process and to define limit values for the execution. In the paper these structural and geotechnical issues will be explained together with the experiences during the execution.

May 1, 2022

By J. R. Thoenen

This circular is the second of a series presenting methods employed in solving the technical problems encountered in the production of sand and gravel. The first paper3 discussed the methods use in prospecting and exploration. This one teals with the problems involved in bringing a raw prospect to the production stage and considers the various methods of development and the Factors affecting that development. Later publications are planned to present and discuss methods of recovery and treatment. The recovery of sand and ravel from natural deposits and their preparation for market involve a progressive sequence of operating steps or processes. Each step or process presents its own peculiar problems which require different angles of mental approach, methods, and tools, but all are more or less dependent on the step or process which precedes or follows.

Jan 1, 1933

By Andreas Brandner

"At the beginning of 2007 the Austrian contractor PORR was awarded with remediation works for a 48-km long part of the railway line from Campina to Predeal – part of the Trans European main Corridors TEN-T priority line 22 Bucurest – Brasov, connecting the southeast European countries with the heart of Europe.Due to partly new realignment and change of regular sections as well as protection against rockfall and slope slide a huge bunch of slope stabilization works became necessary, which were awarded to the contractor PORR and their designer IB-Brandner.Following the studies of the tender documents for the planned protection measures responsible managers of PORR decided to propose an alternative protection design by IB- Brandner. Changing the original design a more flexible and environmentally compatible solution consisting of high performance net, soil nailing and rockfall protection systems (fences) was elaborated and adapted to local needs. During design process, several critical areas were identified and additionally taken into account.In the paper examples of the design and erection process show how difficulties in implementation starting with the presentation of the idea continuing to the realization on site were managed and a technically more sophisticated and commercially competitive solution could be delivered to the customer Romanian Railway – case study.The European Commission awarded – following an election process in which all citizens of the EU could join - the remediation project Railway line Campina – Predeal in Romania as the environmentally best EU co-financed infrastructure project. GENERAL PROJECT EVALUATIONDue to original design slope stabilization should be done by concrete slabs fixed with prestressed anchors and shotcrete cover.The area to be secured was limited to a 12-meter strip left and right from the railway track without reference to nature and local needs. Discussions with the client and his designer and rising awareness for the hazards to address took several months. Site visits in Austria to provide insight in the problems of dealing with natural hazards helped to convince the client of the needs and our alternative design."

Jan 1, 2017

By L. Hartsell Cash

INTRODUCTION Created in 1944 to help rebuild those economies, principally in Europe, which were seriously damaged or destroyed during the Second World War, the World Bank--or to use its correct name, the International Bank for Reconstruction and Development-began its operational phase by making a loan to the Government of France to accomplish two tasks: (i) to import coal for space heating purposes; and (ii) to buy new machinery and equipment to help rehabilitate its coal mines. Once the thrust of reconstruction in postwar Europe was largely accomplished, the World Bank Group (for today the World Bank has three separate lending windows) turned to mobilizing funds to improve living standards in developing countries, which remains its primary goal today. Over this period of time, the World Bank Group has continued to assist the world mining industry in various ways and, since 1955 the World Bank Group has financed mining or mineral processing projects with loans/credits totalling $1.5 billion. The World Bank Group consists of two institutions--the World Bank itself and the International Finance Corporation (IFC), which was founded as a separate institution in 1956 and three separate lending windows--the World Bank, the International Development Association (IDA), and IFC. The World Bank loans are provided at commercially-related interest rates but have grace periods usually of up to 3 to 5 years and repayment periods ranging from around 15 to 20 years. Since the World Bank raises its operating funds on the international capital markets in varying currencies and in varying interest rates, it relends a basket of currencies at floating interest rates which are fixed every six months to reflect the Bank's own borrowing cost. At the present time, the interest rate is just below 10% per year and in addition, a one-time front-end fee of 1/4 of 1% is charged. Also, a commitment fee of 3/4% per year is charged on the undisbursed amount of the loan itself. For loans to industrial and mining projects, it is normal to charge an additional guarantee fee of 1 to 1.5% in addition to the annual interest rate. This guarantee fee is payable to the government of the country in which the project is carried out since, by its charter, the World Bank is required to have the guarantee of the host government for each loan made in a specific country. By far the greatest source of lending funds within the World Bank Group is that of the World Bank itself and for the fiscal year ending June 30, 1984, the World Bank approved loans totalling $12 billion. The second lending window within the World Bank Group is IDA which performs the same functions as the Bank itself and has the same staff. Nevertheless, its loans (called credits) are made on much softer terms and are made to the poorest nations only. IDA funds are subscribed by the wealthier countries, usually as grants, and these are relent as credits to those countries with the lowest per capita income. IDA credits are made for 50 year periods, including 10 years of grace, to the government itself. The credits are interest free, but there is a service charge of 3/4% per year on the amount withdrawn and outstanding to defray the administrative costs of IDA. Credits approved during fiscal 1984 totalled $3.5 billion. The third lending window is IFC. While IFC is a separate corporation and operates quite separately from the World Bank and has its own staff and regulations, it works very closely with the World Bank on its overall approach to the mining sector and to a particular country. IFC's mission is essentially to supply venture capital and to stimulate development of the local private sector in capital markets as well as to promote the international flow of private capital to developing countries. Unlike the World Bank and IDA, the IFC does not lend directly to governments

Jan 1, 1985

By J. W. Tsai

Both diamond crystals and diamond films were grown on silicon and copper substrates using a methane/hydrogen gas mixture as a precursor with thermal CVD techniques at low pressure environment. In addition to diamond particles, other crystalline phases including graphite and aluminum silicon carbide were observed on the substrate surface. ?The grown materials were analyzed with X-ray diffraction, electron microscopy, Auger electron spectroscopy and optical microscopy. Most synthesized diamond crystals were twinned. The flow rate of reactant gases, substrate nature, substrate temperature, decomposition temperature of the precursors, total pressure of reaction chamber, methane/hydrogen ratios and other possible parameters were varied during the growth processes, and the significant effects of these factors on nucleation and growth rate were evaluated.

Jan 1, 1989

By Olli Järvinen

The capacity of the Outokumpu Pori refinery is today about 125 000 mt in 1998. The anode slime amount is about 700-800 mt. The copper is removed with pressure leaching. Selenium roasting is done with the gas roasting. The doré smelting in the furnace is done with the tilting rotating converter with oxy-fuel burner (TROP). Doré anodes are treated in the silver electrolysis. Gold is recovered from the gold mud with the quick hydrochloric acid leaching process. The important point in the leaching is to get into contact the solid copper with the oxygen and liquid. Outokumpu has an efficient agitator for this purpose. The GLS-agitator (GLS=gas, liquid and solid) is powerful for mixing oxygen, liquid and solid together. The current production in Pori plant is 40000 kg of silver, 5000 kg gold, 40000 kg of selenium and one hundred kilograms of platinum-palladium concentrate.

Jan 1, 2000

By Stephen C. Tadolini

The anchorage capacity of four types of bolting systems was investigated in two mines with thick coal roofs. In conjunction with the in-mine tests, a simple axisymmetric finite element computer program was developed. Both the field and computer results indicated that thick coal roofs can be effectively supported entirely by the coal member.

Jan 1, 1986

By Yijun Caoa, Xiuxiang Taoc, Zhongbo Hub, Yinfei Liaoa

A new preparation scheme for a difficult-to-float coking coal from the Kailuan Mine, Tangshan, China was investigated. The results showed that grinding followed by column flotation was beneficial for obtaining products with low ash content. The positive effect of grinding on the coal floatability is attributed to the liberation of intergrowths and coal surface improvement. Tests indicated that 10 minutes was the optimum grinding time, and over grinding resulted in a deterioration in flotation performance. With a grinding time of 10 minutes, conventional flotation had potential to yield a product with around 12.42% ash content and 69.15% combustible recovery. Column flotation can reduce the product ash content to 11.15%and increase combustible recovery to 74.47%. Consistently better flotation results reveal that column flotation is more efficient than conventional flotation for such fines.

Jan 1, 2015

By Mark Sheppard

[Considerable research work hi been done on secondary crushing and coarse and fine grinding, and the literature on the general subject of Crushing contains many references to the work of investigators on the laws governing end the factors entering into the economical production of fine materials. However, little information on primary crushing in available The literature deals mainly with problems and practices in ore dressing, end in this field the engineer or investigator is concerned largely with the production of fine material and the unlocking of minerals in the ore. Under such conditions close control of screen sizes of primary-crusher products is a secondary consideration and has received very little attention.]

Jan 1, 1938

By D. L. Leach

This report covers laboratory experiments simulating in situ copper recovery from primary sulfide ores in sulfuric acid systems pressurized with oxygen. Copper extraction and acid consumption data are correlated with temperature in the range 50-150°C and quenched pH in the range 0.25-2. Adverse changes in the chemical composition of the leach solution and the formation of gangue-mineral alteration products and secondary sulfides can severely limit the extraction of copper above 90°C. Keeping the pH below the self-buffered value of about 2 and the temperature below about 110°C produces the maximum extraction rates. Forcing the pH too low not only results in excessively high acid consumption but may also limit the extraction of copper at temperatures above 100°C.

Jan 1, 1975

By Dale E. Hirschfeld

The clays in Eastern Washington occur in a variety of forms and are extracted for uses in Face Brick, paper coatings, and aggregates. Not in large volumes in comparison to other areas, not even from impressive large mines. However, mans utilization of these clays has progressed from historical clay tablets to the present technically oriented manufactured products of today. White Face Brick, perhaps the whitest produced anywhere is the unique product produced by INTERPACE CORPORATION's Mica Plant from these unusual clays. It is this basic characteristic feature of the clay's in the Mica area that differentiate them from the other clay's in this belt. ORIGIN The significant properties of clay's used in Face Brick are plasticity, fired color, fired strength, dry and fired shrinkage, the PCE or Pyrometeric Cone Equivalent, and extrudability. Testing clay's for these properties is standard laboratory procedure. No two clays are alike, and seldom can one clay be substituted for another. Mica White Clays respond favorable to all these properties, but more especially, the Mica Clays fire to a brilliant white color, from almost the natural state. The geologic history of Eastern Washington is largely conjectural because of the absence of rocks representing segments of geologic time. The oldest rocks in this area are the argillaceous and arenaceous sedimentary rocks which have been slightly metamorphosed. These rocks have been correlated with the Belt Series of the Pre-Cambrian age, although some may be older. These rocks were subsequently intruded by granadiorites and related rocks that are considered to

Jan 1, 1971

By Sebastian Fredes, Williams Calderon, Mauricio Toledo, Gonzalo Montes-Atenas

The influence of the temperature on leaching kinetics of copper-bearing minerals has been widely acknowledged: the leaching of copper oxide ores is generally described as exothermic reactions while copper sulfide ores are associated with endothermic reactions. Reports studying the influence of temperature on leaching kinetics at laboratory scale frequently involve the implementation of either fully flooded isothermal systems or jacketed column setups. Nevertheless, at industrial scale controlling or monitoring the temperature or temperature changes is almost impractical. In fact, leaching process is usually a large tonnage operation and changing the temperature of vast amounts of material would require an enormous amount of energy and highly specific heat transfer equipment. Preliminary computations on the amount of energy required to increase the temperature of a heap or dump in 1°C indicates that it would be impossible to find an energy source able to accomplish the task. In order to provide a solution to this matter it is suggested to create an energy managing protocol (EMP) that permits heat up or down the porous body locally taking advantage from the temperature gradients and from the reactivity of different regions within the material as a function of the leaching cycles. The aim of this study is to evaluate different heat transfer regimes in a 1 ton pilot column leach operation. It was found that best results of copper recovery are obtained when heating up the column in horizontal bands starting from the top of the column moving downwards as the leach cycle evolves. The system is expected to be suitable for industrial applications, but further development of the technique is required, particularly in the design of the heat transfer dispositive.

Jan 1, 2014

By Charles M. Packer, Oleg D. Sherby, Roy H. Johnson

Originally round tensile specimens of a eutectic Zn-A1 alloy develop elliptical cross sections during superplastic deformation. This observation, coupled with a detailed study of the microstructure and preferred orieniation, suggests that crystallographic slip and continuous grain boundary migration or re-crystallization are important processes during super-plastic deformation. In spite of the extensive activity in superplasticity1-15 and the numerous explanations proposed, no single model has had universal acceptance. It has been established, however, that the general requirements for superplastic extension of two-phase alloys include an extremely fine, stabilized grain size of the order of a few microns, a temperature about equal to or greater than one-half the melting point, a critical range of strain rate, and a similarity in the mechanical strength of the major phases. The proposed models can perhaps best be characterized in terms of the important phenomena associated with them. These phenomena include: phase instability,1 diffusional creep by volume diffusion3 or grain boundary diffusion4,5 slip and continuous grain boundary migration or recrystalliza-tion,= grain boundary Sliding,7-9,13,14 and dislocation glide.'5 In this paper, experimental observations will be reported which support a model involving slip and continuous grain boundary migration or recrystalliza-tion. Specifically, a correlation will be made between this model and the development of elliptical cross sections as originally round specimens are superplas-tically deformed. For the most part, superplasticity studies have been conducted with eutectic or eutectoid alloys. Probably the most thoroughly studied material has been the monotectoid Zn-A1 alloy.1,2,6,12,13,15 No attention to the eutectic Zn-A1 alloy has previously been reported, and the results discussed in this paper represent part of a general study of the superplastic properties of this alloy. MATERIALS The alloys used in this investigation were prepared by melting appropriate quantities of 99.99+ pct A1 and 99.999 pct Zn in air, mixing, and pouring into a water- cooled stainless-steel mold. Wet-chemical analysis was conducted with each heat of alloy prepared, using the procedure of Fish and smith.16 The composition of the eutectic alloy was 95.1 wt pct Zn. Ingots about 2 in. thick were rolled to 0.4-in. plate at about 300°C with a reduction of 5 to 10 pct per pass. Specimens were machined from the plate with the tensile axis parallel to the rolling direction. The specimens were round, with 0.150-in.-diam, 1.25-in.-long gage length, and 0.25-in.-diam threaded grip sections. EXPERIMENTAL PROCEDURE Specimens were mounted inside a uniform-temperature quartz tube which was surrounded by a double elliptical radiant furnace with a 12-in.-long uniform-temperature hot zone and a low thermal capacity. The tube extended through the top and bottom of the furnace and permitted rapid quenching of the loaded specimens when quickly filled with cold water at the conclusion of the test. The quench precluded any effects on specimen microstructure from a normal, slow cool. Constant stress was applied to test specimens by suspending a load on a constant stress cam of the type described by Hopkin.17 The design of this cam permitted application of a constant stress for elongations up to 200 pct. For greater elongation, approximately constant stress conditions were maintained by systematically reducing the load manually. RESULTS As part of an investigation of the superplastic properties of the eutectic Zn-A1 alloy, evidence was obtained for the development of elliptically shaped cross sections as originally round specimens were extended. For example, after an elongation of about 100 pct, a round specimen with an initial diameter of 0.150 in. became elliptical with major and minor axis of 0.128 and 0.88 in., respectively. Photographs are presented to illustrate the ellipticity developed during superplastic deformation, Fig. 1. The specimen shown was deformed at a stress of 500 psi, at a temperature of 285°C, and a strain rate of 2.28 x 10-2 min-1. The strain-rate sensitivity exponent* was measured at *The strain-rate sensitivity exponent, m, is defined as d In o/d In c where o is the steady-state flow stress and E is the strain rate. this temperature and in the strain rate range 10"3 to 10-1 min-1 was found to be about 0.5. This value is typical of those observed with superplastic materials. The material studied exhibited negligible strain hardening during superplastic deformation, the creep rate remaining constant under constant stress and temper-

Jan 1, 1969