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By The Staff, Explosives Research Center

The principal activities of the Bureau of Mines Explosives Research Center from July 1, 1962, to June 30, 1963, are described briefly in part 1. Part 2 gives short abstracts of publications that appeared during fiscal year 1963; in general, the research reported in these publications antedates the report period.

Jun 24, 1964

By W. C. Labys

This chapter reports on recent modelling effects to analyze the US steam coal market with an econometric as well as a programming approach. The background to coal modelling is examined first. The particular aspects of the steam coal market to be modelled are then presented and the corresponding coal model described. Empirical results are presented and analyzed. Conclusions are then drawn regarding potential modelling applications in the policy area.

Jan 1, 1979

By Arthur Metcalfe, Edward Thomas, A. J. Barry

"Early in 1947 the Bureau of Mines became interested in adapting suspension roof support to coal mining 5/ as a possible means of reducing the high rate of accidents from falls of roof. For a time the program made little progress be¬cause of the shortage of steel products after the end of World War II, but during the past 8 months this restriction has eased, and as of May 1, 1949, 114 mines had either started experimental work or had ordered materials and equip¬ment in anticipation of trial installations. It is estimated that 30 linear miles of roof in underground passageways have been secured by this method in recent months, and no lost-time roof-fall accident has been reported in these areas up to that date.Many coal-mining companies in widely separated localities have cooperated in making experimental installations. In very few instances are these companies entirely satisfied that they have arrived at the best solution in determining the most efficient adaptation to suit their particular conditions. Moreover, new ideas and modifications of the basic principle are constantly being brought to light and are being tested. Available test data is far from complete, and it is conceivable that some new idea will be developed to alter the present concept of proper technique; therefore, this progress report does not attempt to answer all questions that might arise in connection with this method of roof support; it simply recounts the experience acquired to date. Consequently, few references to costs are made. Up-to-date quotations on material and equipment used in suspension roof-support installations may be obtained from numerous mine-supply companies.The authors gratefully acknowledge the cooperation of mining companies whose personnel made possible collection of the information contained in this circular: Bethlehem Collieries Corp., Barrackville, W. Va.; Berwind-White Coal Mining Co., Windber, Pa.; Consolidation Coal Co., (Ky.); Jenkins, Ky.; Consolidation Coal Co. (W. Va.), Fairmont, W.Va.; Clinchfield Coal Corp., Dante, Va.; Consolidated Coal Co., St. Louis, Mo.; Hanna Coal Co., St. Clairsville, Ohio; Missouri Portland Cement Co., Sugar Creek, Mo.; Pocahontas Fuel Corp., Pocahontas, Va.; Reppert Coal Co., Dola, W. Va.; St. Joseph Lead Co., Bonne Terre, Mo.; and Tennessee Coal, Iron, & Railroad Co., Birmingham, Ala.The fundamental theory of suspension roof supports is not new; in fact, its application in the construction of beams predates mining itself. The basic principle involved is the reinforcement of roof rock with steel rods inserted in the roof and anchored therein at points where the rock is least likely to be affected by stresses resulting from mining. Such roof supports have been used in mines for many years in widely separated localities. The St. Joseph Lead Co., operating in southeastern Missouri, apparently was the first large mining company to prove the practicability of the principle by applying it in a systematic manner for securing roof for more than 20 years (fig. 1)."

Sep 1, 1949

By John A. Owsiany

The effect of longwall mining on streams and shallow aquifers has been the subject of numerous research studies for more than twenty years. As a result of these studies, it has become common to consider an overburden thickness of 400 feet as the lower limit at which longwall mining methods may be used with little or no effect on hydrologic systems. This paper presents the results of a study documenting the response of a large high order stream to shallow cover undermining by longwall methods in the northern Appalachian coalfield. The field site is located in a narrow stream valley where the overburden, composed primarily of limestone and sandstone units interbedded with shales and siltstones, ranges in thickness from 340 to 285 feet above the main bench of the Pittsburgh coal seam. Streamflow monitoring and monitor well measurements indicate that no significant loss zones or water table lowering resulted from undermining the stream or the adjacent valley bottom area. Additionally, hydrographs for shallow near-stream wells exhibit fluctuations related to natural seasonal variations, which are nearly identical to those observed in a non-undermined control well in the same watershed. Environmental factors affecting streamflow were monitored through the use of a control stream in an adjacent non-undermined watershed to differentiate between natural and mining induced changes in flow.

Jan 1, 2001

By AIME AIME

The name and address of the school are given first, followed by the length of the regular undergraduate curriculum, the degree granted, types of courses giben, and the name of the man in charge. This covers only work for the first or Bachelor degree in each case. The following abbreviations are used: B. Bachelor Cer. Ceramic. E. Engineer or Engineering Eng. Engineering or Engineer Geol. Geologist, Geological, or Geology M. Mines or Mining Met. Metallurgy or Metallurgical Mng. Mining Pet. Petroleum Ref. Refining S. Science Tech. Technology or Technical

Jan 1, 1939

By J. B. F. Champlin

The continuing development of the nuclear industry in the United States requires a program of waste disposal that insures against the release of large amounts of radioactivity to the environment. This paper describes research on one proposed means of disposal of this waste, that of injection into geologic formations at depth. Nuclear production plant wastes were simulated and injected into samples of sedimentary rock obtained from outcrops, quarries, and deep wells. Changes in the chemical and physical characteristics of the rocks caused by the interaction of ions and suspended particles in the waste solutions with the cementing material and claylike particles in the rock are discussed. Laboratory tests show that nuclear wastes can be injected into many natural porous, permeable geologic formations. Injectivity can be maintained over a longer period by monitoring the ionic balance and particle-size distribution of waste streams. The combination of permeability and porosity with low cation-retention capacity, as exhibited by most sandstones, would satisfy the engineering requirements for the subsurface disposal of nuclear waste. Shales and clays with their low permeability and high cation-retention capacity would make excellent confining formations. The amount of cation retained by sedimentary rocks increases with increasing valence or concentration of the cation or decreasing brine concentration. The use of rock cores as model reservoirs had proved successful in determining some of the parameters that need to be considered in full-scale field disposal of wastes.

Jan 1, 1967

By R. W. O. Kersten

"The aim was to investigate stable pillar design procedures currently in use on chrome and platinum mines, subject them to a critical appraisal, and review some of the alternatives proposed in the literature. It is concluded that these pillar design methodologies suffer from drawbacks that can be detrimental to the mining industry and that an improvement is essential.It was decided that the increased availability of analytical models and failure criteria could be exploited to update the empirical to an analytical/empirical method. The proposed methodology adopted FLAC2D simulations using the Hoek-Brown failure criterion to calculate full stress-deformation curves for typical pillars. The mine stiffness concept was introduced to determine the pillar load, integrating the influence of the pillar and strata stiffness and mining geometry.The proposed methodology was calibrated by comparing experimental and predicted deformations and failure depth of pillars in one hard-rock mine. The conclusion was that the methodology is an improvement over the one currently in use. An improved factor of safety is given by the intersection point of curves for the stiffness of the system and the pillar strength. IntroductionThe paper describes part of the findings of a PhD thesis (Kersten, 2016) on an alternative stable pillar design methodology. This publication contains sufficient information to implement the method for further interpretation and testing. A detailed comparison of measured and predicted data is dealt with in the thesis, and the results show that there is promise in the methodology.The design of stable pillars in mining is of fundamental importance, not only in the Bushveld Complex mines but throughout the mining industry. Wherever mining occurs, pillars are formed at some stage and it is essential to predict their behaviour, i.e. whether they will burst, yield, or remain stable. Although of crucial importance, pillar design still suffers from major shortcomings and weaknesses."

May 1, 2019

By M. Hayashi

The Bureau of Mines conducted laboratory studies on Idaho mudstones to examine techniques for extracting vanadium. Recovery of vanadium from low-grade sources could contribute to future vanadium production and reduce reliance on imports. An Idaho mudstone surface sample containing 0.30 pct V205 and an underground sample containing 0.21 pct V205 were used in the extraction tests. Leaching of the surface sample for 18 h at 800 C with the addition of up to 1,000 lb/ton H2S04 recovered 70 pct of the vanadium. How-ever, leaching of the underground sample under the same conditions re-covered only 47 pct. By adding 15 wt pct NaCl and roasting the samples at 7500 C for 2 h, followed by leaching with 800 lb/ton H2S04, vanadium extractions were increased to 78 pct from the surface sample and 83 pct from the underground sample. Water leaching of samples roasted at 7500 C for 4 h with a 25-wt-pct NaCI addition yielded about 60 pct of the vanadium from both surface and underground samples. Autoclave leaching at 2000 C for 3 h with 1,000 Ib/ton H2S04 extracted 97 pct of the vanadium from the surface sample and 86 pct from the underground sample. An exploratory solvent extraction investigation to purify and concentrate vanadium in the leach solution using several organic reagents was also conducted.

Jan 1, 1985

By J. W. Perez

A simple exponential model has been developed (Perez and Aplan. Process Mineralogy, VI, 1986) to describe the fractional yield of a given species out of a locked assemblage: Fractional Yield of Species A = a e X/U where 'X' is particle size and 'a' and 'U' are constants. In the present study, the general validity of this model has been further demonstrated. experimentally, for the liberation of coal and pyrite out of various raw coals and beneficiated fractions using a variety of crushing devices. Using data from the literature, the model is also shown to be applicable to the liberation of sulfide minerals out of ores.

Jan 1, 1987

By De-wen He

The distribution of persistent organic pollutants in the environment is studied using the multimedia environmental fugacity model, and environmental health risk assessment of POPs nearby a copper smelt enterprise is carried out. The result indicates that all are in an agreeable risk level without exception. The annual individual chronic risk index of HCB is 7.50×10-11. The annual individual risk index of 3,3',4,4'-TCB is 1.57×10-9, and the annual individual risk index of 2,3,7,8-TCDD is 6.57×10-9.

Jan 1, 2009

By R. L. Peyton

Risk analysis is used extensively in many engineering applications. Although its use in the field of dam safety has been limited in practice, it has received considerable attention in recent years in the dam safety literature. Thus far, it has been shown that risk analysis in the evaluation of existing dams has the potential for providing a more rational basis for decision- making because of its focus on the direct issues--likelihood of failure, likelihood of loss of life, and risk cost of damages. It provides for a logical balance between the risk a dam imposes and the degree to which rehabilitation is required, compared to traditional evaluations based on somewhat arbitrarily chosen design events applied to large classes of dams. Dam owners could benefit by optimizing the cost of remedial measures. Downstream landowners could benefit by minimizing the likelihood of flood damages. However, it is also clear that significant technical and policy issues remain to be resolved before risk analysis in dam safety is accepted and routinely implemented in engineering practice. An obvious and important potential application of risk analysis is its use by the state regulatory agency as an in-house evaluation tool, or even as part of regulatory policy, in the implementation of its state dam safety program. Adoption of such a policy would have an important impact on the mining industry. .Although no state dam safety programs are known by the writers to have officially incorporated risk analysis into their regulations, there appears to be considerable interest in the concept. In recent surveys 47 states agreed that the development and promotion of a risk assessment methodology for state dam safety programs should be encouraged (Tschantz, 1983; Tschantz, 1984). The issue has also received important attention within the Association of State Dam Safety Officials (1986). One state-Illinois-proposed regulations during 1986 to allow risk analysis to justify lower spillway requirements for existing dams (Illinois Department of Transportation, 1986). At the Federal level, the National Research Council has found risk analysis especially appropriate for assessing dam safety at high-hazard dams (National Research Council, 19851, the Bureau of Reclamation has published guidelines for incorporating risk analysis into their dam safety grogram (U.S. Department of the Interior, 1986), and the Federal Emergency Management Agency has recently sponsored workshops and supported research related to risk analysis in dam safety (Federal Emergency Management Agency, 1985a ; Federal Emergency Management Agency, 1985b; - - McCann, et. al., 1985a, 1985b).

Jan 1, 1986

By A. R. Mumford

During the course of an investigation conducted by the fuel section of the Bureau of Mines , on a hand- fired return- tubular boiler plant , it was found that the average cost of fuel to produce 1,000 lb. of steam was $ 0.5287 . Tests conducted after some simple changes had been made in the furnaces , and in the control of the boilers , showed the previous high cost of fuel per 1,000 lb. of steam could be reduced to the reasonable figure of $0.3540 , or the equivalent of over 30 per cent saving in fuel cost .

Mar 1, 1923

By Juan Patricio Ibáñez

Separation of arsenic and copper from Cu-As-H2S04 electrolytes by electrodialysis has been investigated at room temperature. The effects of current density and pH were studied. An arsenic-free copper solution was obtained for all the tested conditions. The transport efficiency for copper ions was found to be higher than 98% after 3 hours' test. Transport of arsenic and copper through the ion exchange membranes was increased by increasing pH and current density. Solution pH was found to be a key parameter for the separation process, since it controls the speciation of the ions to be transported and the formation of unwanted precipitates which reduce the global efficiency of the electrodialysis process. The main conclusion is that electrodialysis is a promising technique to be used in separating and/or concentrating ions of interest in copper electrometallurgy.

Jan 1, 2003

By Kathleen M. Kowalski, Audrey Podlesny

The Maslach Burnout Inventory (MBI) was administered and scored for 154 Mine Safety and Health Administration (MSHA) employees kom the US Department of Labor. These employees serve as accident investigators for serious accidents and fatalities as part of their job duties. During a workshop on stress designed for them, subjects volunteered anonymous written anecdotes, confirming and illustrating the findings. The subjects represented locations across the USA and all mining commodities: coal, metal, non-metal, stone, and sand and gravel. The Maslach Burnout Inventory assesses three aspects of experienced burnout: emotional exhaustion, depersonalisation, and reduced personal accomplishments. The average results of the scores for each of the three subscales for the study group of MSHA accident investigators fell in the moderate range. These scores show that the subject population was at some risk for emotional exhaustion and depersonalisation, tending toward burnout. The group evidenced a lower sense of personal accomplishment in their jobs, indicating a higher risk for burnout. From this outcome accident investigators may be at moderate (note: this does not mean average) risk for burnout. The authors recommend follow-up with this population - specifically in training to work with grieving families; and greater organisational support for the accident investigators in this area would be appropriate. Keywords: Burnout; accident investigators; occupational safety and health; job stress.

By M. A. Elliott, F. W. Brown

"INTRODUCTION During the recent war the Bureau of Mines, at the request of one of the armed services, investigated the hazards that night be encountered 5n handling perchloric acid, particularly if spilled on certain materials. The hazardous nature of perchloric acid when mixed with reducing agents had been known qualitatively, but it was desired to obtain quantitative data on the explosion hazards of such materials. Accordingly, tests were made to determine the sensitivity of mixtures of perchloric acid and oxidizable materials to initiation by heat, impact, sparks, flame, and explosive impulses. This report summarizes the results of those tests.PROPERTIES OF PERCELORIC ACIDAnhydrous perchloric acid is a colorless,hygroscopic, volatile, mobile liquid that fumes in the air. The anhydrous acid is unstable at ordinary temperatures, and therefore the commercial acid is a water solution containing either 60 percent or 70 percent by weight of the anhydrous acid. The commercial acid is widely used in chemical analysis, frequently to oxidize organic material. If proper precautions are not observed, such an oxidixation may become exceedingly rapid and result in an explosion. Several such explosions involving the acid are mentioned in the literature. 4, 5, 6/"

Jan 1, 1948

By Melissa S. Beauregard, Randall A. Pietersen

This study focuses on quantifying the effects of water infiltration on a full-scale energy pile system’s ability to meet the thermal demand of an HVAC system. Theoretically, an energy pile system should increase its thermal capacity after a rain event due to increased moisture content creating an increase in thermal conductivity of the surrounding soil matrix. The United States Air Force Academy has an energy pile research site consisting of 8 full-scale energy piles located below a shower facility. The local colluvium surrounding the piles allows for relatively high water infiltration during rain events. This study uses an 11kW Precision Geothermal Geocube to apply a thermal load on two single-loop piles. A weather station located south of the structure records atmospheric conditions. Results indicate that moderate rain events can caused up to a 23% increase in the system’s thermal exchange capacity. This change is due to the increase in moisture content near the surface, which penetrates to deeper soil layers with time. The time required for moisture to penetrate to greater depths and then dissipate in the soil matrix, explains why increased system performance is seen for over a week following the passing of a singular rain event. 1 INTRODUCTION With a “future-forward” focus, there is an ever-pressing economic and environmental need to use sustainable sources to meet growing energy needs. HVAC is typically responsible for 34% of the overall energy required by commercial buildings and 48% of the energy required by residential buildings (USEIA, 2009; USEIA, 2012). Energy piles are a low cost, sustainable technology that have been used to offset this energy demand incurred by a building’s space heating and air conditioning requirements. An energy pile consists of heat exchanging elements in a closed loop system integrated into a building foundation and connected to a ground source heat pump (GSHP). It is most common for these heat- exchanging elements to be constructed within a drilled shaft foundation due to both construction practices and geometric considerations. This system operates based on the principle that at a certain depth below ground (typically 4 meters) subterranean temperature remains constant at a value equal to the mean annual air temperature at a given location (Kavanaugh et al., 1997). This allows the soil to function as a heat sink for cooling operations and a heat source for heating operations when exchanged within this zone of relatively constant temperature. For the past 25 years, the implementation of energy pile technology in public, residential, and even large-scale architectural complexes has slowly expanded which has created an increase in research into the topic as a result (Brandl, 2006; Hamada, 2007; Sekine et al., 2007; Gao, 2008; Bourne-Webb, 2009; Stewart and McCartney, 2013; Murphy et al., 2014). When pile construction takes place beneath the groundwater table, soil is under fully saturated conditions, maximizing thermal exchange for a GSHP system. Under unsaturated conditions, however, changing moisture contents change thermal conductivity values in a soil, which affect a GSHP system’s ability to meet a thermal demand. The observational data presented in this paper apply to GSHP systems in unsaturated soil conditions.

Jan 1, 2019

By E Beltran, S Ngunz, F Orrante, F van Zyl, M Westcott

"The primary control objective of the project is to achieve milling optimisation by ensuring that the energy available for rock breakage is used as efficiently as possible. This is achieved by increasing the level of mill filing until a process constraint is reached. Stable operation against this limiting constraint is then maintained to ensure long-term optimised operation.Semi-autogenous grinding (SAG) mill control optimisation presents a number of challenges. SAG mills have multiple inputs that are used to control multiple outputs (MIMO process). Secondly, the SAG mill loading process is a ‘high inertia’ process that can be approximated as an integrating process. This means that it is open-loop unstable. The hybrid control strategy presented implements an advanced ‘load stabiliser’, which transforms this integrator process into a more manageable first order process, which can be steered stably against the constraints. This SGS hybrid Expert control strategy implemented on both SAG mills at the Porgera concentrator therefore consists of two integrated parts responsible for:stabilising the mill load to a targetdriving the mill load target to the maximum determined by the process constraints (eg maximum power draw) to maximise efficiency and throughput. A comparative study is done between the operation of the plant for a period of a month before and a month after the implementation of this strategy. The results indicated a significant improvement in the SAG mills’ stability and operation as well as a reduction of overload situations leading to a loss of throughput.Citation:Ngunz, S, van Zyl, F, Orrante, F, Beltran, E, Westcott, M and Wilson, S, 2016. Simplified Hybrid Semi-autogenous Grinding Mill Control - Explanation and Practical Results at the Porgera Concentrator, in Proceedings 13th AusIMM Mill Operators’ Conference 2016, pp 313–320 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Oct 10, 2016

By R. W. Charles

The Los Alamos National Laboratory, under the sponsorship of the U.S. Department of Energy; is involved with laboratory and field experiments to assist in development of the Hot Dry Rock concept of geothermal energy. The field program consists of experiments in which hot rock of low permeability is hydraulically fractured between two wellbores. Water is circulated from one well to the other through the fractured hot rock. Our field experiments are designed to test reservoir engineering parameters such as heat-extraction rates, water-loss rates, flow characteristics including impedance and buoyancy, seismic activity, and fluid chemistry. Laboratory experiments were designed to provide information on the mineral-water reactivity encountered during the field program. Two experimental circulation systems tested the rates of dissolution and alteration during dynamic flow. SOlubil ity of rock in agitated systems was studied. Moreover, pure minerals, samples of the granodiorite from the actual reservoir, and Tijeras Canyon granite have been reacted with distilled water and various solutions of NaCl, NaOH, and Na.CO.. The results of these experimental systems are compared to the observations made in field experiments done within the hot dry rock reservoir at a depth of approxi-mately 3 km where the initial rock temperature was 150 to 200°C.

Jan 1, 1981

By M. Hesham El Naggar, Mehdi Heidari

"Equivalent fixed-base cantilever model is a common approach for performance base seismic design of bridge structures supported by extended pile-shaft. In this method, global displacement ductility factor is related to local curvature ductility demand by assuming a concentrated plastic hinge at location of maximum bending moment. Equivalent plastic hinge length is one of the key parameters that should be assumed accurately in kinematic expression of the cantilever model. Although, some expressions have proposed to estimate the length of the in-ground plastic hinge; however, these relations yield differing results. In this paper, a general expression is derived based on the concept of distributed plasticity to predict the plastic region of yielded piles in clay and sand. A length modification factor is defined to relate the equivalent length of plastic hinge to the real plastic zone. Then, results from nonlinear pushover analyses are used to propose an equation for the modification factor as a function of displacement ductility factor.IntroductionDuring severe earthquake events, development of the plastic hinge in pile foundation below ground level is inevitable for bridge structures supported on extended pile-shafts. A common approach for seismic design of the yielding pile-shafts is to replace the pile-soil system by an equivalent fixed-base cantilever assuming the equivalent system has the same global response as that of the pile-shaft (Budek et al. 2000; Chai 2002). In this method, plastic curvature is concentrated at the center of the equivalent plastic hinge below ground surface. Prior knowledge of plastic-hinge length is essential for proper assessment of assess plastic displacement at the top of the pile-shaft. Unfortunately, existing recommendations for estimating plastichinge length are largely incomplete and/or inadequate.During the last two decades, several relationships have proposed for evaluating the equivalent plastic hinge length, Lp, based on experimental and numerical studies. Budek et al. (2000) conducted numerical modeling to calculate the plastic-hinge length of piles embedded in cohesionless soil. They found that the plastichinge length varies linearly with both soil stiffness and aboveground height, e. Chai and Hutchinson (2002) conducted full-scale experimental tests on reinforced concrete piles in sand. They reported that Lp depends primarily on the aboveground height of the pile, neither sensitive to the soil stiffness nor to the value of displacement ductility factor. They stated that the equivalent plastic hinge length is relatively independent of the displacement ductility factor and is not very sensitive to the change in soil density. On the contrary, Goel (2014) and Liu et al. (2016) conducted nonlinear numerical analyses which revealed that Lp changes with the displacement ductility factor and even suggested that using different values of Lp for different seismic design levels is essential for a reliable estimation of the ductility capacity."

Jan 1, 2017

Flinders Power, formerly NRG Flinders, is considering the possible use of low rank coal from Lake Phillipson, South Australia (SA) in its power stations at Port Augusta, SA. Typically, this coal contains about 35% moisture and 10% ash. Unfortunately, it also contains high levels of sodium (1% Na) and chloride (0.95% Cl) with a Na2O level in ash of 18.9%. Such levels cause serious problems during coal combustion, making the use of as-mined coal impractical for power generation. This paper describes the development of an aqueous leaching technique to remove 90% of the sodium and chloride and to yield a product with a Na2 O level in ash of less than 3%. Small-scale agitation leaching tests with good quality tap water at ambient temperatures showed that the coal needed to be crushed to minus 5.6 mm to obtain maximum removal of water-soluble sodium and chloride in 30 min. Leaching kinetics, but not the ultimate removal of salt, were enhanced by the use of higher temperatures (up to 150°C), but this was deemed uneconomic. Varying the pulp density between 20% and 50% had little effect on extractions and there was no benefit in multiple stage water washing. The best results by water leaching were 69%~74% extraction for sodium and 95%~97% for chloride, meaning that the sodium removal was well below the target level. From SEM examinations of the leached product it was concluded that the remaining sodium was organically bound to the carbon atoms in the coal. Further tests using aqueous solutions containing cation exchange additives such as calcium chloride (CaCl2) or ammonium chloride (NH4Cl) or sulphuric acid (H2SO4) showed that significantly enhanced sodium extractions were possible and target specifications were met. Two options, namely a single-stage and a two-stage leach, were then investigated. In a single-stage leach with additive, minus 5.6 mm coal was leached at 33%~50% solids for 30 min at ambient temperature and then filtered and washed with fresh water. This gave a sodium removal level of about 81% and a Na2O level in ash of about 5%. These levels do not quite meet tar-get specifications. In a two-stage leach, the coal was first leached with water alone without an additive as in the single stage leach, and the washed residue re-leached under similar conditions for about 5 min with an additive (CaCl2), and then filtered and washed. This gave a cumulative sodium removal of 96% and a Na2O level in ash of 1.4%~2.4%. These levels are well within target specifications.

Jan 1, 2014