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By H. W. Russell, Paul D. MILLER

IT is known that austenitic chromium-nickel steels that have free carbide in the grain boundaries are subject to intergranular corrosion. It is difficult to detect such a susceptible condition in a fabricated article because present test methods require a sample section for examination and in most cases this is difficult to obtain. The question of the nature and prevention of intergranular corrosion in austenitic stainless steels have been ably discussed by Bain and co-workers1-3 and by other investigators.4-10 The present methods of study subject samples to corrosive conditions in such reagents as the Strauss solution, a. mixture of copper sulphate and sulphuric acid. Such tests usually require at least 72 hr. to run. Various methods of measuring the degree of sensitization have been employed, such as the measurement of electrical resistivity, magnetic measurements, measurement of the degree of cracking produced on bending over a mandrel, and microscopic studies. The detection of carbides at the grain boundaries by metallographic polishing and etching methods is tedious and requires a skilled operator. A recent report on such methods of carbide detection is given by the American Society for Testing Materials Subcommittee VI of Committee A-10 11 and by Arness.12 The present investigation was undertaken to develop a simple test procedure for detecting carbide precipitation or susceptibility to intergranular corrosion. The test is designed for use in the plant and for the testing of fabricated structures. Carbide precipitation, the factor leading to susceptibility to corrosion, is produced by heating the alloy in the temperature range 800° to 1600°F., as in welding, in improper annealing or in service where such temperatures are met. The connection between such precipitation and susceptibility to corrosion has been thoroughly discussed, as has been the use of stabilizing addition elements to prevent precipitation. EXPERIMENTAL METHOD A small area of the steel under test is subjected to an anodic treatment in a cell that can be clamped onto a sample or an actual structure. The cell and electrical circuit used are illustrated in Fig. I. The cell C is lead, joined to the steel plate D and insulated from it by a short piece of rubber tubing E. The cell is forced tightly against the steel plate by a spring or clamping device. The seal formed by the rubber against the steel plate is sufficient to retain the liquid bath inside the cell. The spot treated can be made any shape desired, depending on the shape of the rubber gasket. The cell illustrated polishes a circular spot about 3/8-in. diameter. The bath consists of 60 per cent (by weight) sulphuric acid to which is added 5 ml. per liter of Glycyrrhiza extract (U.S.P.). The cell requires about 2 to 2.5

Jan 1, 1941

By Jack C. White

The purpose of this Bureau of Mines research was to determine the technical feasibility of direct sulfuric acid digestion of Florida land-pebble phosphate matrix. Preliminary tests in a continuous digestion circuit showed that 92 to 96 percent of the P2O5 contained in the matrix was extracted, while the P.05 concentration in the product acid ranged from 21 to 30 percent. The waste filter cake contained about 1 percent P205 and up to 18 percent water. These sandy compact filter cakes, comprised mostly of quartz and gypsum, appeared to be suitable for backfilling and reclamation of mined lands.

Jan 1, 1975

By Don W. Dotson

In 1962, Kondner prepared several papers dealing with hyperbolic stress-strain response of cohesive soils. The following year, Brinch Hansen proposed 80% and 90% failure criteria for stress-strain behavior of cohesive soils. Fellenius was instrumental in popularizing these failure criteria for pile load tests and offered a direct solution equation for the failure load according to the 80% failure criterion. Since the 90% Criterion has been incorporated into the International Building Code, equations for the direct solution of the failure load at the 90% Criterion would be useful to practicing engineers. This Technical Note supplies the derivation methodology for the 80% Criterion and provides expressions to determine the load and deflection at failure for the 90% Criterion.

Aug 1, 2013

By H. W. Kilau

The Bureau of Mines tested chromium-bearing waste slags from industrial stainless steel and other chrome alloy operations to determine their chromium leachability characteristics under acid precipitation conditions and to devise measures to prevent any pollution originating from this source. Two critical slag composition factors were found to control the chromium leachability: (1) CaO:Si02 ratio and (2) magnesium content. Above a 2.0 CaO:Si02 ratio, chromium exists in slag as CaO·Cr203, which can be vulnerable to leaching by acid precipitation especially if oxi-dized to CaCr04 when exposed to the environment over an extended period. Maximum chromium leachability from industrial slags occurred when the composition of the slag had about a 2.0 CaO:Si02 ratio. Between a 1.0 and 2.0 CaO:Si02 ratio, in the presence of sufficient magnesium, MgO ·Cr203 was formed, which is very resistant to oxidation and to dissolution by simulated acid precipitation. Addition of magnesium silicates to molten slag to fix the chromium in the MgO·Cr203 form was successful in preventing chromium leaching in simulated acid rain solutions. Experiments showed olivine and waste taconite tailings were suitable for this purpose. Olivine addition to a waste slag having a composition vulnerable to leaching (CaO:Si02 > 2) reduced the chromium leachability more than 80 pct.

Jan 1, 1984

By Andrew W. Jenike

The first significant studies of problems related to the handling and storage of bulk solids were reported at the end of the nineteenth century. Early work originated from the necessity to store large quantities of grain and was concerned mainly with pressures affecting the structural design of silos and bins. The Janssen formula (about 1898) and the work of Ketchum [1] form the highlights of that period. In more recent years, progress in mechanization, increasing plant capacities, and rising costs of labor have focused the attention of engineers on the problem of gravity flow of bulk solids. A great deal of work has been done with models, and flow patterns obtained in small scale bins have been described in several publications, for example [2, 3]. An attempt to develop a theory of flow of bulk solids was reported in 1954 [4, 5, 61 and presented to the in a paper [7] in the same year. AIME recommended the continuation of this work and, as a result, Engineering Foundation granted a sum of money to set up a Bulk Solids Flow Laboratory. Two and a half years ago the project gained the support of the University of Utah and a laboratory was set up on the campus of the University. This project is now in progress, it has received the support of the American Iron and Steel Institute and of Kaiser Engineers, Division of Henry J. Kaiser Company. The results obtained to date are summarized in this report.

Jan 1, 1959

By A Kobzev, C Robben

Sensor-based particle sorting of gold ores is the masterclass of preconcentration. The technical challenges of a grade in ppm scale makes a direct detection with currently available technology in milliseconds impossible. Consequently, the detection and classification of particles into ore and waste classes relies on detectable proxies which are the foundation for the classification. These must be reliable and repeatable across the ore bodies processed in future. A sensor-based particle ore sorting equipment must therefore be calibrated systematically by understanding the gold deportation in different lithological groups. Also, it must be in best operational state to minimise possible misplacement. The technical challenges are met by a stringent financial regime governing the business case. Many gold ore sorting projects require a stable grade of gold in the rejected waste significantly below 1gr/t. Two examples are introduced in this paper:  The pilot results and operational experience of X-ray transmission (XRT)-based particle ore sorting for pebble sorting of sulphide associated ore;  Laser-based particle ore sorting for pebble circuit of an orogenic, quartz associated gold ore. Usually, sensor-based particle sorters are installed in the crushing section of a plant. However, for large capacity plants, the number of equipment required, and the associated material handling costs result in significant capital and operating expenses for plants with 1200tph run-of-mine capacity. As a conclusion, it was decided to investigate sensor-based particle ore sorting applied to the pebble stream of two existing semi autogenous mills.

Nov 10, 2020

By B C. McLellan

The decline of ore grades on land, increasing demand and high prices for various minerals have led to an increased interest in mining the deep ocean sea floor. The potential deep ocean reserves are vast and in some circumstances the grades are high enough to consider mining. However, the consequences of such mining are as yet uncertain. This paper will present the results of a comparative assessment of life cycle impacts of deep ocean minerals. Two alternative extraction technologies from different deep ocean resource types were examined and key commodities are considered. Initial results indicate that the energy requirements will be higher than the average land-based resources, but may fall within the range of the deepest terrestrial mines.CITATION:McLellan, B C, 2015. Comparative life cycle impacts of deep ocean minerals and land-based counterparts, in Proceedings Third International Future Mining Conference, pp 253–260 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Nov 4, 2015

By İbrahim Gunes, ATILA GURHAN CELIK, Eren Komurlu

This study introduces a new apparatus designed to improve the load-bearing capacities and insertion efficiency of split set type friction bolts. Laboratory and site studies demonstrated the apparatus’s advantages in terms of practicality and prevention of buckling. The apparatus temporarily compresses the split tubes, reducing friction during insertion and increasing normal stresses and friction capacity at the bolt-rock contacts.

Jan 3, 2022

By Lung Cheng

The Bureau of Mines conducted laboratory tests to investigate the ease of frictional ingition with frozen (nonrotating) conical bits cutting into sandstone. The number of strikes with a new bit to obtain ignition of a combustible methane-air environment was measured. Tests were made with bits tipped with both tungsten carbide and steel at several bit attack angles (angle between bit axis and sandstone surface) and initial tip angles (included angle at the tip of the new bit). Carbide-tipped bits required more strikes for ingition than steel-tipped bits, by a factor of 7 to 10. With a carbide-tipped bit, the number of strikes for ingition increased by a factor of about 3 if the bit attack angle increased by 10° or if the initial tip angle decreased by 10°. During use, abrasive wear of the frozen bit caused a flat surface to form at the tip of the bit, thereby decreasing the tip angle. As the attack angle increased, however, the new bit involved a smaller wear-flat area whereby, abrasive wear was decreased.

Jan 1, 1987

By Katie Schumacher, Greg Roset, Dayle Flynn

The Columbus Processing Complex of the Stillwater Mining Company began operations at Columbus, Montana in 1990 based on electric furnace smelting treating a precious metals concentrate from the nearby Stillwater mine and mill. Since that time, the smelter plant has been expanded in stages in order to treat recycled materials in addition to the concentrate. This paper describes a number of changes made at the plant to effectively handle recycled materials.

Jan 1, 2014

By Ayumu Tokumaru, Shuji Owada, Gangfeng Liu

"Several million spent catalytic converters are disposed annually worldwideandeach containing about 0.5-1g ofplatinum and 1-2g of all the platinum group metals (PGMs), then,it is fairly significant to recover PGMs from the spent automobile catalyst. The PGMs’ recovery is a proven technology, including pyro-and hydrometallurgicalmethods, and the highestrecovery can achieve approx. 98 wt.% by acid-leaching method, but theserecyclingtechnology seems to be too highlyenergy-consuming. SincePGMs aredistributed only in coat layer in spent catalyst, it is of great significance to enrich the coat layerwith some physical methods as a pretreatment.In this paper, according to the double-deck structureof the catalyst andthe different properties of the two main compositions, alumina-ceria phase of coat layer and cordieritephase of substrate, the concentration of the coat layer was investigated by combiningthree kinds of physical separation technologies, heating-quenching, crushing and surface grinding. In the first stage, thermal stresscouldgeneratebetween the two phasesby thermal expansion difference,to producefracturesin the thinnest part of coat layerand micro-cracksin coat layerand at the interface of coat layerand cordierite substrate. The second stage of crushing, by jaw and roll crushers, could break dominantly the coat layer and the third stage of surface grinding, carried out by attritor, promoted further separation and concentration of coat layer fromthe substrate.We also improved the attritor grinding by adding a new lift-arm to the cell for achieving better mobility of sample particles in the selective surface grinding."

Jan 1, 2014

By W. Yang, R. Rajasingam, K. Mohanarangam

"Copper Electrowinning (EW) is a complex electrochemical process that involves the production of LME grade copper from copper rich electrolyte. The process involves the deposition of the copper ions onto the cathode from copper rich electrolyte with the production of oxygen bubbles at the anode. The process setups up a complex flow pattern within the cell as it is subjected to varying density gradients due to the deposition process along with oxygen bubble driven flow. It is a necessity to understand and quantify the flow behaviour within these cells in order to maintain the production of highest grade copper. In fact, the oxygen bubbles originating from the process is responsible for the generation of acid mist which is a designated as a carcinogen a major health hazard around EW tank houses. Hydrodynamic assessment of the process has so far been restricted to simple mass balances and some limited numerical modelling. All the models are based on assumed boundary conditions which has not so far been verified by any real-time physical measurement. This apparent gap has led to models which could not be directly used to track process changes or troubleshoot problems in EW tank houses. In order to address this gap, CSIRO has established a full size (width and height) transparent cell capable of simulating plant operating conditions (across the range currently used). With the use of sophisticated diagnostic analytical tools and measurement techniques it was possible to study all the operating variables (current density, flow rate, temperature, etc.) independently and their effect of bubble size, bubble velocity, gas hold-up as well as acid mist generation and its size. In order to address safety concerns in tank houses around acid mist early results outlining the factors contributing to its generation as well as the effect of various barriers to mitigate acid mist is outlined below.INTRODUCTIONA significant part of today’s copper production is through hydrometallurgical route which predominantly involves leaching, Solvent eXtraction (SX) followed by ElectroWinning (EW). Producing copper using this approach have shown to be environmentally friendly (Dresher, 2001) compared to the traditional smelting process. EW is the final step in the production of LME grade copper using the hydrometallurgy route. The electro-chemical process involves the use of a lead anode (Pb-Sn-Ca) and a stainless steel cathode to produce copper sheets using the copper rich electrolyte from the SX process and with the applications of direct current to the electrodes. This electro-chemical reaction results in the deposition of copper ions on the cathode with oxygen released from the anode as a by-product. Hydrodynamically, the oxygen bubbles create a bubble driven flow within the EW tanks with the surrounding electrolyte. A direct result of this could be seen from the quality of the copper deposited on the cathode. Most of the copper plates produced from the traditional tank houses have a rough texture at its bottom one-third while the top two-thirds have a smooth finish with a finer grain structure."

Jan 1, 2016

"THE PACIFIC CONTINENTAL MARGIN OF CANADA is de-fined, for the purposes of this paper, as the area sea-ward from the present mainland coast of British Columbia to the foot of the continental slope. It thus coincides with A. Sutherland Brown's Insular Tectonic Belt. The region is limited to the north and south by the political boundary with the U.S.A., the location of which is still in dispute.The region can be subdivided into: (1) an interior trough comprising the Queen Char-lotte, Comox and Nanaimo basins; (2) a medial uplift comprising Vancouver Island and the Queen Charlotte Islands; and (3) a marginal shelf which is extremely narrow (Jess than 5 km) west of the Queen Charlotte Islands, widens to 160 km in Queen Charlotte Sound and is about 35 km wide west of Vancouver Island, where it is underlain by the Tofino sedimentary basin, with its• extension, the Juan de Fuca Basin, at the southern end.The medial uplift consists of a highly disturbed anticlinorium of mainly Mesozoic rocks, with a core of Palaeozoic. The rocks include thick sequences of eugeosynclinal volcanics and sediments. There is strati-graphical evidence of repeated interruption in sedi-mentation. By late Jurassic, the main eugeosynclinal phase was over and a successor basin was initiated in the interior' trough. This became filled, during Cre-taceous and Tertiary time, with sediments ranging in environment from bathyal turbidites to terrestrial conglomerates and coals. West of the medial uplift, another successor basin developed in early Tertiary times and became filled with mainly deep-water marine sediments. A third effusive sequence marks the base of the Tertiary on Graham Island and over most of the Hecate Strait region and Tofino Basin."

Jan 1, 1970

By Hoberg H, Schneider FU

The stability of suspensions can frequently be controlled only by the use of supplementary polymeric agents. Such methods date back to the time of the ancient Egyptians, who used natural rubber as a deflocculant for carbon black in the manufacture of ink (Anon, EncyclopediaBritannica, 1968). Since the development of synthetic polymers in the 1950s they have been deployed in all manner of applications. Indeed the mining and paper industries as well as industrial or communal waste water treatment plants are largely dependent on flocculants which make a major contribution to the relief of the environment. As some of the polymers used are carried out from the process via purified water, problems can emanate from the application itself as long as no reliable data is available as to the exact whereabouts of the polymers and their impact on the biosphere. In order not to invade other systems, they would have to be biologically degradable which has not, until now, been confirmed (Blockhaus, Sequaris and Schwuger, 1991; Schumann, 1991). It has, however, previously been demonstrated (Hoberg et al, 1990) that when process water circulates in mineral processing operations, residual amounts of polymeric flocculants can have extremely adverse effects on the selectivity of flotation processes. The adsorption behaviour is consequently one of the most important considerations in the development of new polymers, the aim being to minimise the amount of non-absorbent matter. The objective of the investigations carried out on ampholitic synthetic polymers of high molecular weight to be reported on here was to permit the connection between settling index and adsorptivity to be characterised in greater detail. As the level of knowledge concerning flocculation and polymer adsorption in real systems is still limited in spite of numerous practical and theoretical studies in this field, the experiment was designed to be relatively broadly-based. As well as investigating various raw materials, an attempt was made to compile results on the influence exerted by different surface charges.

Jan 1, 1993

By Laura Bustemante, Bruce Vandenberg, Fred Huettig

Recent advances in solid-state, field portable, fast framing video camera systems and PC based frame capture hardware now allow blast imaging up to 1000 frames per second. Up to 8 seconds of data can be stored directly into the unit, downloaded to a PC or archived to a standard VCR without data compression. Since no film processing is involved, motion analysis can be performed instantly and on-site within a few minutes. This paper will describe the design features and applications of the KineView 1256P system and compare these with the analogous aspects of fii based cameras.

Jan 1, 1998

By Wolfgang Baum

Case studies from epithermal gold-silver deposits in the western United States and in Latin America show that the routine use of process-related mineralogical studies has become an important tool for the reduction of development, capital and operating costs. Bypassing the mineralogical characteristics of epithermal gold-silver ores, as a result of fast-track development approaches, has resulted in multimillion dollar metal losses and/or in considerable modification costs of existing operations.

Jan 1, 1988

By Atulya Verma, Samantha Espley, Nashel Kalaka

Numerical modelling simulations of proposed mining sequences are used to evaluate mining induced stress concentrations and their migration associated with the progress of mining. This analysis is a standard practice for most prospective mining projects at various levels of feasibility study. The studies are usually initiated at the beginning of the mining cycle, on a global scale, and are maintained and updated throughout the life of mine (LoM) to identify or address local issues and the required remedies as and when needed. Developments in numerical modeling techniques along with advancements in computing technology and data storage/management capacity have given rock engineers access to a huge volume of data that needs to be analyzed and assessed. The most common approach to numerically evaluate stress concentrations and migrations in underground mines is to select the points of interest in a given volume such as the back of an excavation or points within pillars around critical infrastructure, and plot the stresses or a derivative of stresses over time to represent life of mine concentrations and migrations of stresses. The problem with this approach is the sharp gradient of stresses close to excavation boundaries. Slight changes in the location of selected points can change the stress concentration and migration patterns substantially and all generalized statements about LoM risk can be challenged in one way or another. For global stresses, the most common current approach of data analysis is by viewing series of pictures representing stress contours. In this approach, it is easy to overlook some critical detail and/or be masked by personal preferences of contour/picture representation. To overcome the problem of representing and analyzing huge volume of stress simulation data, the authors, through their experience at different mining operations, developed a volume-based technique to reliably evaluate mining-induced stress concentrations and migrations. The volume-based approach is for risk-based assessments of adjacent regions in the rockmass, in and around planned stoping excavations. The volume of interest is the entire ore body that is planned to be mined, but it could be just a part of the ore body depending on the specific use case. The risk identifiers are the induced stresses as compared to the strength of the rockmass. Over the LoM, the risk identifiers are tracked versus the corresponding excavation ratio of the zone. This approach is very effective in identifying the stages of mining that are contributing the most to the mining induced stress risk and the results can be used for proactive planning and mitigations measures such as alternative mining sequences, or stope sizes, or extraction methods. The approach has also been very successful in application at mature mines, particularly in assessing the re-initiation of mining in zone that has been dormant for some time. The volume-based approach allows for an assessment of the current state of the rockmass and the identification of future risks when planning resumption of mining activities.

Jan 1, 2023

By P. Lopez, E. Wellman, N. Risso, A. Anani

Current machine learning models used for roof fall hazard prediction are mounted on expensive sensors, computationally expensive, or lack the robustness for accurate prediction in the underground mining environment. This research aims to provide a design methodology for a robust, low-cost, deep learning-based algorithm for underground mine roof fall hazard prediction. A data sampling plan is developed to ensure the replicability and robustness of the developed model. In addition, feature engineering and transformation methods are described to identify relevant features for hazard identification. The methodology described here will be used in model development, tested, and implemented as a real-time mobile device application. The new tool will be expected to detect roof fall hazards in real-time and contribute to a crowdsourcing approach for underground hazard detection.

Feb 1, 2023

By J. R. Andrews, R. P. Young, J. M. Reyes-Montes

"Microseismic monitoring provides insight into the location and extent of rock-mass fracturing induced by cave mining, enabling interpretation of the cave profile and validation of predictive numerical models. Source location uncertainties can lead to misinterpretation of the inferred characteristics of the fracture network. One principal source of uncertainty is the velocity model used to invert the location algorithm. Large-scale 3D numerical models of modulus changes across a caved mass can represent such complexities in the location algorithms, allowing more accurate interpretation of the microseismic activity. A Northparkes mine case study applies this advanced approach to microseismic data interpretation.RÉSUMÉ Le suivi microsismique fournit des renseignements sur la localisation et l’étendue des fractures de la masse rocheuse induites par l’exploitation par blocs foudroyés; cela permet d’interpréter le profil de la chambre foudroyée et de valider les modèles prédictifs numériques. Les incertitudes quant à la localisation de la source peuvent conduire à des mésinterprétations des caractéristiques inférés du réseau de fractures. Une des principales sources d’incertitudes est le modèle de vitesse utilisé pour inverser l’algorithme de localisation. Des modèles numériques tridimensionnels à grande échelle des changements du module d’élasticité à travers une masse foudroyée peuvent représenter de telles complexités dans les algorithmes de localisation, permettant ainsi une interprétation plus juste de l’activité microsismique. Une étude de cas à la mine Northparkes applique cette approche avancée à l’interprétation des données de microsismicité."

Jan 1, 2016

By X. Chi, J. W. Griffith, C. L. Schengrund, J. Sabol

"Experiments were carried out to determine the long-term effect of instillation of 500 mg of generic bituminous, anthracite, quartz, or titanium dioxide (Ti02) dust on the composition of pulmonary surfactant. Dust was instilled in the caudal lobe of the right lungs of female pigtailed macaque monkeys (Macaca nemestrina). The composition of surfactant isolated from cell-free bronchoalveolar lavage (CF-BAL) samples obtained from right lungs (dust exposed) at various times over the following year was compared with that of surfactant isolated from CF-BAL from left lungs (dust free) . Little change was seen in the amount of surfactant-associated lipid phosphorus as a result of exposure to dust. Exposure to quartz, anthracite, or Ti02 dust induced a significant increase in the total amount of protein in the surfactant-enriched fraction. The relative amount of specific proteins was also altered: surfactant-associated protein A decreased, and the amount of the heavy and light chains of immunoglobulin molecules (identified by NHiterminal amino acid sequence analysis) increased. These changes were visible more than a year after instillation of quartz and at least 3 months after instillation of anthracite dust. Despite variation in the responses of the individual animals, the changes observed might serve as an indicator of the severity of the effect of exposure of the lung to mineral dust and/or to pathogens. IntroductionSurfactant is essential for normal pulmonary function and gas exchange. It functions to reduce surface tension and may help to prevent pulmonary edema [19] and to protect against infection [13]. The importance of surfactant to normal Jung function is illustrated by the fact that neonates lacking appropriate surfactant undergo respiratory distress and do not survive without clinical support."

Dec 1, 1996